ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-001
OLCC No. 1002158CD2E

Marijuana Potency Analysis by
High Performance Liquid Chromatography
Testing Accreditation #: 4091 Test Certificate #: 94625-001
Client Name, Sample Details

Doyle's Designs
Coburg, OR 97408
Sample: Gorilla Glue #4
Type: Flower
Method: FE04N-OR1 HPLC1100-OR1
***Water Activity: 0.447
***Moisture: 12.501%
Test Conditions

Prepsheet ID#: P-170608A
Scale: XS205-OR1
Temp: 19 °C
Baro Pressure: 993 hPa
Analyst: HRM
Technician: HRM
Sample ID#: 94625

Harvest/Process Date: 06/09/2017
Serving Size (g): 54088
Date Received: 06/09/2017
Test Date: 06/08/2017
Sample #94625
Sample #94625 Sample #94625
Test
Compounds		 CBDA CBD CBC CBG CBN THC THCA THCV   Calc. Max Act.
Amount N/D N/D 0.2 N/D N/D 9.7 16.8 0.5 CBD N/A N/A
LOQ 0.1% 0.1% 0.1% 0.1% 0.1% 0.1% 0.1% 0.1% THC 24.4336% 37%
Uncertainty† 14.29% RPD 16.00% RPD 10.17% RPD 13.86% RPD 15.09% RPD ±5% RPD 13.59% RPD 14.14% RPD Totals: 0.0% -

LOQ = Limit of Quantitation

RPD is relative percent difference between the LCS and LCS duplicate.

%RPD = Relative Percent Difference; Min. Value = Minimum Detectable Amount, CFU = Colony Forming Units, N/D = Not Detected

Calc. Max. is the calculated sum of CBD or THC and the amount of CBD or THC derived from CBDA or THCA; respectively .These values are calculated by applying a molar correction factor of 0.877 to the CBDA or THCA value.

*** Designated tests that use the method FE-45.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

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ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-001
OLCC No. 1002158CD2E

QC Report
Testing Accreditation #: 4091 Test Certificate #: 94625-001
Client Name, Sample Details

Doyle's Designs
Coburg, OR 97408
Sample: Gorilla Glue #4
Type: Flower
Method: FE04N-OR1 HPLC1100-OR1
***Water Activity: 0.447
***Moisture: 12.501%
Test Conditions

Prepsheet ID#: P-170608A
Scale: XS205-OR1
Temp: 19 °C
Baro Pressure: 993 hPa
Analyst: HRM
Technician: HRM
Sample ID#: 94625

Harvest/Process Date: 06/09/2017
Serving Size (g): 54088
Date Received: 06/09/2017
Test Date: 06/08/2017
Sample #94625
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Cannabidivarin (CBDV) N.D. 5 5.4 108.00 4.6 92.00 16.00%
Cannabidiolic Acid (CBDA) N.D. 5 6 120.00 5.2 104.00 14.29%
Cannabigerol (CBG) N.D. 5 5.4 108.00 4.7 94.00 13.86%
Cannabidiol (CBD) N.D. 5 5.4 108.00 4.6 92.00 16.00%
Δ9-Tetrahydrocannabivarin (THCV) N.D. 5 5.3 106.00 4.6 92.00 14.14%
Cannabinol (CBN) N.D. 5 5.7 114.00 4.9 98.00 15.09%
Δ9-Tetrahydrocannabinol (THC) N.D. 5 5.5 110.00 4.8 96.00 13.59%
Cannabichromene (CBC) N.D. 5 6.2 124.00 5.6 112.00 10.17%
Tetrahydrocannabinolic acid (THCA) N.D. 5 5.5 110.00 4.8 96.00 13.59%

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

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