IRON Laboratories

Marihuana Potency Analysis by
Gas Chromatography
Test Certificate #: 92602-001
Client Name, Sample Details

313 Bud Maker
Shelby Township, MI 48317
Sample: Holy Grail
Type: Flower
Method: FE03 GC6890-1
Test Conditions

Scale: XS205-MI1
Temp: 21.9 °C
Baro Pressure: 991.3 hPa
Analyst: JCM
Technician: JCM
Sample ID#: 92602

Harvest/Process Date: 04/13/2017
Serving Size (g): 0.97
Date Received: 04/12/2017
Test Date: 04/12/2017
Valid Through: 04/12/2018
Report Issued: 04/11/2017
Sample #92602
Sample #92602 Sample #92602
Test
Compounds		 CBDV THCV CBC CBD Δ8 THC Δ9 THC CBG CBN TOTAL
Amount N/D 0.1 0.2 N/D N/D 15.6 3.4 N/D 19.3%
Min. Value 0.1% 0.1% 0.1% 0.1% 0.1% 0.1% 0.1% 0.1% -
Uncertainty† ±5% RSD ±5% RSD ±5% RSD ±5% RSD ±5% RSD ±5% RSD ±5% RSD ±5% RSD -

†Uncertainty measurement is for the test procedure and the instrument used; and is calculated in accordance with the ISO "Guide of Uncertainty in Measurement" (GUM) Test Results and uncertainty are only representative of the sample submit to our laboratory. Uncertainty does not account for any uncertainty in the sampling. The measurement of uncertainty is the expanded uncertainty and is an estimate of uncertainty calculated with normal distribution and a coverage factor of 2 (K=2) to approximate a 95% confidence level. 

%RSD = Relative Standard Deviation; Min. Value = Minimum Detectable Amount, CFU = Colony Forming Units

N/D designates a value that is not detected above the methods Limit of quantitation (min. value)

Values are not adjusted for moisture content.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Makenzie Hyman Iron laboratories Makenzie Hyman

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

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IRON Laboratories

Terpene Report
Test Certificate #: 92602-001
Client Name, Sample Details

313 Bud Maker
Shelby Township, MI 48317
Sample: Holy Grail
Type: Flower
Test Conditions

Sample ID#: 92602

Harvest/Process Date: 04/13/2017
Serving Size (g): 0.97
Date Received: 04/12/2017
Sample #92602

Mono Terpenes

Weight Percentage Dry Matter (wt/wt%)

α-Pinene:

 N/D

β-Ocimene:

 N/D

Camphene:

 N/D

Eucalyptol (1,8-Cineol):

 N/D

Sabinene:

 N/D

γ-Terpinene:

 N/D

Myrcene:

 N/D

α-Terpinolene:

 N/D

β-Pinene:

 N/D

Linalool:

 N/D

∆3-Carene:

 N/D

Fenchone:

 N/D

α-Terpinene:

 N/D

Fenchol:

 N/D

Ocimene:

 N/D

Isopulegol:

 N/D

Limonene:

 N/D

Geraniol:

 N/D

4-Cymene:

 N/D

Sequi Terpenes

Weight Percentage Dry Matter (wt/wt%)

β-Caryophyllene:

 N/D

α-Humulene:

 N/D

Nerolidol 1:

 N/D

Nerolidol 2:

 N/D

Guaiol:

 N/D

Caryophyllene Oxide:

 N/D

α-Bisabolol:

 N/D

Other Terpenes

Total: 0.000%
N/D

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Tested by Iron Laboratories

Page 2 of 5
IRON Laboratories

Terpene Report
Test Certificate #: 92602-001
Client Name, Sample Details

313 Bud Maker
Shelby Township, MI 48317
Sample: Holy Grail
Type: Flower
Test Conditions

Sample ID#: 92602

Harvest/Process Date: 04/13/2017
Serving Size (g): 0.97
Date Received: 04/12/2017
Sample #92602

Mono Terpenes

Weight Percentage Dry Matter (wt/wt%)

α-Pinene:

 N/D

β-Ocimene:

 N/D

Camphene:

 N/D

Eucalyptol (1,8-Cineol):

 N/D

Sabinene:

 N/D

γ-Terpinene:

 N/D

Myrcene:

 N/D

α-Terpinolene:

 N/D

β-Pinene:

 N/D

Linalool:

 N/D

∆3-Carene:

 N/D

Fenchone:

 N/D

α-Terpinene:

 N/D

Fenchol:

 N/D

Ocimene:

 N/D

Isopulegol:

 N/D

Limonene:

 N/D

Geraniol:

 N/D

4-Cymene:

 N/D

Sequi Terpenes

Weight Percentage Dry Matter (wt/wt%)

β-Caryophyllene:

 N/D

α-Humulene:

 N/D

Nerolidol 1:

 N/D

Nerolidol 2:

 N/D

Guaiol:

 N/D

Caryophyllene Oxide:

 N/D

α-Bisabolol:

 N/D

Other Terpenes

Total: 0.000%
N/D

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Tested by Iron Laboratories

Page 3 of 5
IRON Laboratories

Terpene Report
Test Certificate #: 92602-001
Client Name, Sample Details

313 Bud Maker
Shelby Township, MI 48317
Sample: Holy Grail
Type: Flower
Test Conditions

Sample ID#: 92602

Harvest/Process Date: 04/13/2017
Serving Size (g): 0.97
Date Received: 04/12/2017
Sample #92602

Mono Terpenes

Weight Percentage Dry Matter (wt/wt%)

α-Pinene:

 N/D

β-Ocimene:

 N/D

Camphene:

 N/D

Eucalyptol (1,8-Cineol):

 N/D

Sabinene:

 N/D

γ-Terpinene:

 N/D

Myrcene:

 N/D

α-Terpinolene:

 N/D

β-Pinene:

 N/D

Linalool:

 N/D

∆3-Carene:

 N/D

Fenchone:

 N/D

α-Terpinene:

 N/D

Fenchol:

 N/D

Ocimene:

 N/D

Isopulegol:

 N/D

Limonene:

 N/D

Geraniol:

 N/D

4-Cymene:

 N/D

Sequi Terpenes

Weight Percentage Dry Matter (wt/wt%)

β-Caryophyllene:

 N/D

α-Humulene:

 N/D

Nerolidol 1:

 N/D

Nerolidol 2:

 N/D

Guaiol:

 N/D

Caryophyllene Oxide:

 N/D

α-Bisabolol:

 N/D

Other Terpenes

Total: 0.000%
N/D

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Tested by Iron Laboratories

Page 4 of 5
IRON Laboratories

Bio Analysis by
Gas Chromatography
Test Certificate #: 92602-001
Client Name, Sample Details

313 Bud Maker
Shelby Township, MI 48317
Sample: Holy Grail
Type: Flower
Method: FE03 GC6890-1
Test Conditions

Scale: XS205-MI1
Temp: 21.9 °C
Baro Pressure: 991.3 hPa
Analyst: JCM
Technician: JCM
Sample ID#: 92602

Harvest/Process Date: 04/13/2017
Serving Size (g): 0.97
Date Received: 04/12/2017
Test Date: 04/12/2017
Valid Through: 04/12/2018
Report Issued: 04/11/2017
Sample #92602
Sample #92602 Sample #92602
Impurities: Not Detected
Molds: No Types: N/A
Pests: No Types: N/A
Anthers: No
Detritus: No
Fibers: No
Hair: No
Mature Seeds: No
Premature Seeds: No
Unidentified Foliar Spray: No
Other Impurities: No
*Moisture 8

*Moisture is not part of the accredited scope of Iron Laboratories.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 5 of 5