IRON Laboratories

Marijuana Potency Analysis by
High Performance Liquid Chromatography
Test Certificate #: 92141-001
Client Name, Sample Details

Doyle's Designs
Coburg, OR 97408
Sample: LSD
Type: Flower
Method: FE04N-OR1 HPLC1100-OR1
Test Conditions

Scale: XS205-OR1
Temp: 21 °C
Baro Pressure: 1012 hPa
Analyst: HRA
Technician: HRA
Sample ID#: 92141

Harvest/Process Date: 01/01/2017
Serving Size (g): 51741
Date Received: 03/28/2017
Test Date: 04/10/2017
Sample #92141
Sample #92141 Sample #92141
Test
Compounds		 CBDA CBD CBC CBG CBN THC THCA THCV   Calc. Max Act.
Amount 0.2 N/D 0.1 0.2 0.6 6.4 16.0 0.3 CBD N/A 0%
LOQ 0.1% 0.1% 0.1% 0.1% 0.1% 0.1% 0.1% 0.1% THC 20.432% 29%
Uncertainty† ±5% RPD ±5% RPD ±5% RPD ±5% RPD ±5% RPD ±5% RPD ±5% RPD ±5% RPD Totals: 0.0% -

LOQ = Limit of Quantitation

RPD is relative percent difference between the LCS and LCS duplicate.

%RPD = Relative Percent Difference; Min. Value = Minimum Detectable Amount, CFU = Colony Forming Units, N/D = Not Detected

Calc. Max. is the calculated sum of CBD or THC and the amount of CBD or THC derived from CBDA or THCA; respectively .These values are calculated by applying a molar correction factor of 0.877 to the CBDA or THCA value.

*** Designated tests that use the method FE-45.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 1 of 8
IRON Laboratories

Pesticide Analysis by
Mass Spectrometer
Test Certificate #: 92141-001
Client Name, Sample Details

Doyle's Designs
Coburg, OR 97408
Sample: LSD
Type: Flower
Method: AOAC 2007.01
Test Conditions

Sample ID#: 92141

Harvest/Process Date: 01/01/2017
Serving Size (g): 51741
Date Received: 03/28/2017
Test Date: 04/12/2017
Sample #92141
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
Aldicarb 0.400 0.054 Pass/<LOD Abamectin**** 0.500 0.217 Pass/<LOD
Acephate 0.400 0.407 Pass/<LOD Acequinocyl 2.000 0.407 Pass/<LOD
Acetamiprid 0.200 0.054 Pass/<LOD Azoxystrobin 0.200 0.054 Pass/<LOD
Bifenazate 0.200 0.027 Pass/<LOD Bifenthrin 0.200 0.136 Pass/<LOD
Boscalid 0.400 0.271 Pass/<LOD Carbaryl 0.200 0.054 Pass/<LOD
Carbofuran 0.200 0.054 Pass/<LOD Chlorantraniliprole 0.200 0.163 Pass/<LOD
Chlorfenapyr 1.000 0.054 Pass/<LOD Chlorpyrifos 0.200 0.054 Pass/<LOD
Clofentezine 0.200 0.163 Pass/<LOD Cyfluthrin** 1.000 0.054 Pass/<LOD
Cypermethrin*** 1.000 0.054 Pass/<LOD Daminozide 1.000 0.950 Pass/<LOD
DDVP (Dichlorvos) 0.100 0.136 Pass/<LOD Diazinon 0.200 0.054 Pass/<LOD
Dimethoate 0.200 0.054 Pass/<LOD Ethoprophos 0.200 0.054 Pass/<LOD
Etofenprox 0.400 0.054 Pass/<LOD Etoxazole 0.200 0.027 Pass/<LOD
Fenoxycarb 0.200 0.054 Pass/<LOD Fenpyroximate 0.400 0.027 Pass/<LOD
Fipronil 0.400 0.054 Pass/<LOD Flonicamid 1.000 0.054 Pass/<LOD
Fludioxonil 0.400 0.027 Pass/<LOD Hexythiazox 1.000 0.136 Pass/<LOD
Imazalil 0.200 0.054 Pass/<LOD Imidacloprid 0.400 0.054 Pass/<LOD
Kresoxim Methyl 0.400 0.054 Pass/<LOD Malathion 0.200 0.027 Pass/<LOD
Metalaxyl 0.200 0.027 Pass/<LOD Methiocarb 0.200 0.027 Pass/<LOD
Methomyl 0.400 0.136 Pass/<LOD Methyl Parathion 0.200 0.054 Pass/<LOD
MGK-264‡ 0.200 0.054 Pass/<LOD Myclobutanil 0.200 0.136 Pass/<LOD
Naled 0.500 0.136 Pass/<LOD Oxamyl 1.000 0.054 Pass/<LOD
Paclobutrazol 0.400 0.081 Pass/<LOD Permethrins† 0.200 0.190 Pass/<LOD
Phosmet 0.200 0.054 Pass/<LOD Piperonyl Butoxide 2.000 0.054 Pass/<LOD
Prallethrin 0.200 0.190 Pass/<LOD Propiconazole 0.400 0.271 Pass/<LOD
Propoxur 0.200 0.027 Pass/<LOD Pyrethrins* 1.000 0.407 Pass/<LOD
Pyridaben 0.200 0.054 Pass/<LOD Spinosad***** 0.200 0.054 Pass/<LOD
Spiromesifen 0.200 0.054 Pass/<LOD Spirotetramat 0.200 0.054 Pass/<LOD
Spiroxamine‡ 0.400 0.054 Pass/<LOD Tebuconazole 0.400 0.054 Pass/<LOD
Thiacloprid 0.200 0.054 Pass/<LOD Thiamethoxam 0.200 0.054 Pass/<LOD
Trifloxystrobin 0.200 0.054 Pass/<LOD

Pesticide testing outsourced to OG analytical

* Pyrethrins are reported as the sum of Jasmolin I, Cinerin I, and Pyrethrin I
** Cyfluthrins are reported as the sum of isomers Cyfluthrin I, II, III, and IV
*** Cypermethrins are reported as the sum of isomers Cypermethrin I, II, III, and IV
**** Abamectin is reported as the sum of Avermectin B1a and Avermectin B1b
***** Spinosad is reported as the sum of Spinosyn A and Spinosyn D
† Permethrin and Prallethrin are reported as the sum of cis and trans isomers
‡ MGK-264 and Spiroximine are reported as the sum of isomers I and II
MRL - Maximum Residue Limit; LOD - Limit of Detection

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 2 of 8
IRON Laboratories

Terpene Report
Test Certificate #: 92141-001
Client Name, Sample Details

Doyle's Designs
Coburg, OR 97408
Sample: LSD
Type: Flower
Test Conditions

Sample ID#: 92141

Harvest/Process Date: 01/01/2017
Serving Size (g): 51741
Date Received: 03/28/2017
Sample #92141

Mono Terpenes

Weight Percentage Dry Matter (wt/wt%)

α-Pinene:

 N/D

β-Ocimene:

 N/D

Camphene:

 N/D

Eucalyptol (1,8-Cineol):

 N/D

Sabinene:

 N/D

γ-Terpinene:

 N/D

Myrcene:

 N/D

α-Terpinolene:

 N/D

β-Pinene:

 N/D

Linalool:

 N/D

∆3-Carene:

 N/D

Fenchone:

 N/D

α-Terpinene:

 N/D

Fenchol:

 N/D

Ocimene:

 N/D

Isopulegol:

 N/D

Limonene:

 N/D

Geraniol:

 N/D

4-Cymene:

 N/D

Sequi Terpenes

Weight Percentage Dry Matter (wt/wt%)

β-Caryophyllene:

 N/D

α-Humulene:

 N/D

Nerolidol 1:

 N/D

Nerolidol 2:

 N/D

Guaiol:

 N/D

Caryophyllene Oxide:

 N/D

α-Bisabolol:

 N/D

Other Terpenes

Total: 0.000%
N/D

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Tested by Iron Laboratories

Page 3 of 8
IRON Laboratories

Terpene Report
Test Certificate #: 92141-001
Client Name, Sample Details

Doyle's Designs
Coburg, OR 97408
Sample: LSD
Type: Flower
Test Conditions

Sample ID#: 92141

Harvest/Process Date: 01/01/2017
Serving Size (g): 51741
Date Received: 03/28/2017
Sample #92141

Mono Terpenes

Weight Percentage Dry Matter (wt/wt%)

α-Pinene:

 N/D

β-Ocimene:

 N/D

Camphene:

 N/D

Eucalyptol (1,8-Cineol):

 N/D

Sabinene:

 N/D

γ-Terpinene:

 N/D

Myrcene:

 N/D

α-Terpinolene:

 N/D

β-Pinene:

 N/D

Linalool:

 N/D

∆3-Carene:

 N/D

Fenchone:

 N/D

α-Terpinene:

 N/D

Fenchol:

 N/D

Ocimene:

 N/D

Isopulegol:

 N/D

Limonene:

 N/D

Geraniol:

 N/D

4-Cymene:

 N/D

Sequi Terpenes

Weight Percentage Dry Matter (wt/wt%)

β-Caryophyllene:

 N/D

α-Humulene:

 N/D

Nerolidol 1:

 N/D

Nerolidol 2:

 N/D

Guaiol:

 N/D

Caryophyllene Oxide:

 N/D

α-Bisabolol:

 N/D

Other Terpenes

Total: 0.000%
N/D

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Tested by Iron Laboratories

Page 4 of 8
IRON Laboratories

Terpene Report
Test Certificate #: 92141-001
Client Name, Sample Details

Doyle's Designs
Coburg, OR 97408
Sample: LSD
Type: Flower
Test Conditions

Sample ID#: 92141

Harvest/Process Date: 01/01/2017
Serving Size (g): 51741
Date Received: 03/28/2017
Sample #92141

Mono Terpenes

Weight Percentage Dry Matter (wt/wt%)

α-Pinene:

 N/D

β-Ocimene:

 N/D

Camphene:

 N/D

Eucalyptol (1,8-Cineol):

 N/D

Sabinene:

 N/D

γ-Terpinene:

 N/D

Myrcene:

 N/D

α-Terpinolene:

 N/D

β-Pinene:

 N/D

Linalool:

 N/D

∆3-Carene:

 N/D

Fenchone:

 N/D

α-Terpinene:

 N/D

Fenchol:

 N/D

Ocimene:

 N/D

Isopulegol:

 N/D

Limonene:

 N/D

Geraniol:

 N/D

4-Cymene:

 N/D

Sequi Terpenes

Weight Percentage Dry Matter (wt/wt%)

β-Caryophyllene:

 N/D

α-Humulene:

 N/D

Nerolidol 1:

 N/D

Nerolidol 2:

 N/D

Guaiol:

 N/D

Caryophyllene Oxide:

 N/D

α-Bisabolol:

 N/D

Other Terpenes

Total: 0.000%
N/D

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Tested by Iron Laboratories

Page 5 of 8
IRON Laboratories

Terpene Report
Test Certificate #: 92141-001
Client Name, Sample Details

Doyle's Designs
Coburg, OR 97408
Sample: LSD
Type: Flower
Test Conditions

Sample ID#: 92141

Harvest/Process Date: 01/01/2017
Serving Size (g): 51741
Date Received: 03/28/2017
Sample #92141

Mono Terpenes

Weight Percentage Dry Matter (wt/wt%)

α-Pinene:

 N/D

β-Ocimene:

 N/D

Camphene:

 N/D

Eucalyptol (1,8-Cineol):

 N/D

Sabinene:

 N/D

γ-Terpinene:

 N/D

Myrcene:

 N/D

α-Terpinolene:

 N/D

β-Pinene:

 N/D

Linalool:

 N/D

∆3-Carene:

 N/D

Fenchone:

 N/D

α-Terpinene:

 N/D

Fenchol:

 N/D

Ocimene:

 N/D

Isopulegol:

 N/D

Limonene:

 N/D

Geraniol:

 N/D

4-Cymene:

 N/D

Sequi Terpenes

Weight Percentage Dry Matter (wt/wt%)

β-Caryophyllene:

 N/D

α-Humulene:

 N/D

Nerolidol 1:

 N/D

Nerolidol 2:

 N/D

Guaiol:

 N/D

Caryophyllene Oxide:

 N/D

α-Bisabolol:

 N/D

Other Terpenes

Total: 0.000%
N/D

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Tested by Iron Laboratories

Page 6 of 8
IRON Laboratories

Terpene Report
Test Certificate #: 92141-001
Client Name, Sample Details

Doyle's Designs
Coburg, OR 97408
Sample: LSD
Type: Flower
Test Conditions

Sample ID#: 92141

Harvest/Process Date: 01/01/2017
Serving Size (g): 51741
Date Received: 03/28/2017
Sample #92141

Mono Terpenes

Weight Percentage Dry Matter (wt/wt%)

α-Pinene:

 N/D

β-Ocimene:

 N/D

Camphene:

 N/D

Eucalyptol (1,8-Cineol):

 N/D

Sabinene:

 N/D

γ-Terpinene:

 N/D

Myrcene:

 N/D

α-Terpinolene:

 N/D

β-Pinene:

 N/D

Linalool:

 N/D

∆3-Carene:

 N/D

Fenchone:

 N/D

α-Terpinene:

 N/D

Fenchol:

 N/D

Ocimene:

 N/D

Isopulegol:

 N/D

Limonene:

 N/D

Geraniol:

 N/D

4-Cymene:

 N/D

Sequi Terpenes

Weight Percentage Dry Matter (wt/wt%)

β-Caryophyllene:

 N/D

α-Humulene:

 N/D

Nerolidol 1:

 N/D

Nerolidol 2:

 N/D

Guaiol:

 N/D

Caryophyllene Oxide:

 N/D

α-Bisabolol:

 N/D

Other Terpenes

Total: 0.000%
N/D

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Tested by Iron Laboratories

Page 7 of 8
IRON Laboratories

Bio Analysis by
High Performance Liquid Chromatography
Test Certificate #: 92141-001
Client Name, Sample Details

Doyle's Designs
Coburg, OR 97408
Sample: LSD
Type: Flower
Method: FE04N-OR1 HPLC1100-OR1
***Water Activity:

Test Conditions

Scale: XS205-OR1
Temp: 21 °C
Baro Pressure: 1012 hPa
Analyst: HRA
Technician: HRA
Sample ID#: 92141

Harvest/Process Date: 01/01/2017
Serving Size (g): 51741
Date Received: 03/28/2017
Test Date: 04/10/2017
Sample #92141
Sample #92141 Sample #92141
Impurities: Detected
Molds: No Types: N/A
Pests: No Types: N/A
Anthers: No
Detritus: No
Fibers: No
Hair: No
Mature Seeds: No
Premature Seeds: No
Unidentified Foliar Spray: No
Other Impurities: No
*Moisture 12.53

*Moisture is not part of the accredited scope of Iron Laboratories.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 8 of 8