IRON Laboratories

Marihuana Potency Analysis by
High Performance Liquid Chromatography
Test Certificate #: 91148-001
Client Name, Sample Details

Superior Extracts
Ironwood, MI 49938
Sample: Marshallo
Type: Infused Product
Method: FE04 HPLC1100-1
Test Conditions

Scale: XS205-MI2
Temp: 21.5 °C
Baro Pressure: 978.3 hPa
Analyst: MEH
Technician: MEH
Sample ID#: 91148

Harvest/Process Date: 02/28/2017
Serving Size (g): 26.1
Date Received: 02/28/2017
Test Date: 02/28/2017
Valid Through: 02/28/2018
Report Issued: 02/27/2017
Sample #91148
Sample #91148 Sample #91148
Test
Compounds		 CBDA CBD CBN THC THCA TOTAL CBD Act. THC Act.
Amount N/D N/D N/D 1.7 0.1 1.8 N/A 94%
Min. Value 0.1 mg/g 0.1 mg/g 0.1 mg/g 0.1 mg/g 0.1 mg/g - - -
Amount per Serving~ N/D N/D N/D 44.4 mg/srv 2.6 mg/srv 47.0 mg/srv Serving Size~ (g): 26.10 g
Uncertainty† ±5% RSD ±5% RSD ±5% RSD ±5% RSD ±5% RSD - - -

†Uncertainty measurement is for the test procedure and the instrument used; and is calculated in accordance with the ISO "Guide of Uncertainty in Measurement" (GUM) Test Results and uncertainty are only representative of the sample submit to our laboratory. Uncertainty does not account for any uncertainty in the sampling. The measurement of uncertainty is the expanded uncertainty and is an estimate of uncertainty calculated with normal distribution and a coverage factor of 2 (K=2) to approximate a 95% confidence level. 

%RSD = Relative Standard Deviation; Min. Value = Minimum Detectable Amount, CFU = Colony Forming Units

N/D designates a value that is not detected above the methods Limit of quantitation (min. value)

Values are not adjusted for moisture content.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Makenzie Hyman Iron laboratories Makenzie Hyman

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

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IRON Laboratories

Terpene Report
Test Certificate #: 91148-001
Client Name, Sample Details

Superior Extracts
Ironwood, MI 49938
Sample: Marshallo
Type: Infused Product
Test Conditions

Sample ID#: 91148

Harvest/Process Date: 02/28/2017
Serving Size (g): 26.1
Date Received: 02/28/2017
Sample #91148

Mono Terpenes

Weight Percentage Dry Matter (wt/wt%)

α-Pinene:

 N/D

β-Ocimene:

 N/D

Camphene:

 N/D

Eucalyptol (1,8-Cineol):

 N/D

Sabinene:

 N/D

γ-Terpinene:

 N/D

Myrcene:

 N/D

α-Terpinolene:

 N/D

β-Pinene:

 N/D

Linalool:

 N/D

∆3-Carene:

 N/D

Fenchone:

 N/D

α-Terpinene:

 N/D

Fenchol:

 N/D

Ocimene:

 N/D

Isopulegol:

 N/D

Limonene:

 N/D

Geraniol:

 N/D

4-Cymene:

 N/D

Sequi Terpenes

Weight Percentage Dry Matter (wt/wt%)

β-Caryophyllene:

 N/D

α-Humulene:

 N/D

Nerolidol 1:

 N/D

Nerolidol 2:

 N/D

Guaiol:

 N/D

Caryophyllene Oxide:

 N/D

α-Bisabolol:

 N/D

Other Terpenes

Total: 0.000%
N/D

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Tested by Iron Laboratories

Page 2 of 5
IRON Laboratories

Terpene Report
Test Certificate #: 91148-001
Client Name, Sample Details

Superior Extracts
Ironwood, MI 49938
Sample: Marshallo
Type: Infused Product
Test Conditions

Sample ID#: 91148

Harvest/Process Date: 02/28/2017
Serving Size (g): 26.1
Date Received: 02/28/2017
Sample #91148

Mono Terpenes

Weight Percentage Dry Matter (wt/wt%)

α-Pinene:

 N/D

β-Ocimene:

 N/D

Camphene:

 N/D

Eucalyptol (1,8-Cineol):

 N/D

Sabinene:

 N/D

γ-Terpinene:

 N/D

Myrcene:

 N/D

α-Terpinolene:

 N/D

β-Pinene:

 N/D

Linalool:

 N/D

∆3-Carene:

 N/D

Fenchone:

 N/D

α-Terpinene:

 N/D

Fenchol:

 N/D

Ocimene:

 N/D

Isopulegol:

 N/D

Limonene:

 N/D

Geraniol:

 N/D

4-Cymene:

 N/D

Sequi Terpenes

Weight Percentage Dry Matter (wt/wt%)

β-Caryophyllene:

 N/D

α-Humulene:

 N/D

Nerolidol 1:

 N/D

Nerolidol 2:

 N/D

Guaiol:

 N/D

Caryophyllene Oxide:

 N/D

α-Bisabolol:

 N/D

Other Terpenes

Total: 0.000%
N/D

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Tested by Iron Laboratories

Page 3 of 5
IRON Laboratories

Terpene Report
Test Certificate #: 91148-001
Client Name, Sample Details

Superior Extracts
Ironwood, MI 49938
Sample: Marshallo
Type: Infused Product
Test Conditions

Sample ID#: 91148

Harvest/Process Date: 02/28/2017
Serving Size (g): 26.1
Date Received: 02/28/2017
Sample #91148

Mono Terpenes

Weight Percentage Dry Matter (wt/wt%)

α-Pinene:

 N/D

β-Ocimene:

 N/D

Camphene:

 N/D

Eucalyptol (1,8-Cineol):

 N/D

Sabinene:

 N/D

γ-Terpinene:

 N/D

Myrcene:

 N/D

α-Terpinolene:

 N/D

β-Pinene:

 N/D

Linalool:

 N/D

∆3-Carene:

 N/D

Fenchone:

 N/D

α-Terpinene:

 N/D

Fenchol:

 N/D

Ocimene:

 N/D

Isopulegol:

 N/D

Limonene:

 N/D

Geraniol:

 N/D

4-Cymene:

 N/D

Sequi Terpenes

Weight Percentage Dry Matter (wt/wt%)

β-Caryophyllene:

 N/D

α-Humulene:

 N/D

Nerolidol 1:

 N/D

Nerolidol 2:

 N/D

Guaiol:

 N/D

Caryophyllene Oxide:

 N/D

α-Bisabolol:

 N/D

Other Terpenes

Total: 0.000%
N/D

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Tested by Iron Laboratories

Page 4 of 5
IRON Laboratories

Bio Analysis by
High Performance Liquid Chromatography
Test Certificate #: 91148-001
Client Name, Sample Details

Superior Extracts
Ironwood, MI 49938
Sample: Marshallo
Type: Infused Product
Method: FE04 HPLC1100-1
Test Conditions

Scale: XS205-MI2
Temp: 21.5 °C
Baro Pressure: 978.3 hPa
Analyst: MEH
Technician: MEH
Sample ID#: 91148

Harvest/Process Date: 02/28/2017
Serving Size (g): 26.1
Date Received: 02/28/2017
Test Date: 02/28/2017
Valid Through: 02/28/2018
Report Issued: 02/27/2017
Sample #91148
Sample #91148 Sample #91148
Impurities: Not Detected
Molds: No Types: N/A
Pests: No Types: N/A
Anthers: No
Detritus: No
Fibers: No
Hair: No
Mature Seeds: No
Premature Seeds: No
Unidentified Foliar Spray: No
Other Impurities: No
*Moisture -

*Moisture is not part of the accredited scope of Iron Laboratories.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 5 of 5