IRON Laboratories

Marihuana Potency Analysis by
Gas Chromatography
Test Certificate #: 90816-001
Client Name, Sample Details

Kenneth Rogers
Novi, MI 48377
Sample: Pennywise Wax
Type: Medical Compliant Flower
Method: FE03 GC6890-1
Test Conditions

Scale: XS205-MI1
Temp: 21.2 °C
Baro Pressure: 989 hPa
Analyst: JCM
Technician: JCM
Sample ID#: 90816

Harvest/Process Date: 02/21/2017
Serving Size (g): 50465
Date Received: 02/17/2017
Test Date: 02/20/2017
Valid Through: 02/20/2018
Report Issued: 02/17/2017
Sample #90816
Sample #90816 Sample #90816
Test
Compounds		 CBDV THCV CBC CBD Δ8 THC Δ9 THC CBG CBN TOTAL
Amount 0.1 0.2 1.9 33.1 0.5 32.4 1.8 0.7 70.7%
Min. Value 0.1% 0.1% 0.1% 0.1% 0.1% 0.1% 0.1% 0.1% -
Uncertainty† ±5% RSD ±5% RSD ±5% RSD ±5% RSD ±5% RSD ±5% RSD ±5% RSD ±5% RSD -

†Uncertainty measurement is for the test procedure and the instrument used; and is calculated in accordance with the ISO "Guide of Uncertainty in Measurement" (GUM) Test Results and uncertainty are only representative of the sample submit to our laboratory. Uncertainty does not account for any uncertainty in the sampling. The measurement of uncertainty is the expanded uncertainty and is an estimate of uncertainty calculated with normal distribution and a coverage factor of 2 (K=2) to approximate a 95% confidence level. 

%RSD = Relative Standard Deviation; Min. Value = Minimum Detectable Amount, CFU = Colony Forming Units

N/D designates a value that is not detected above the methods Limit of quantitation (min. value)

Values are not adjusted for moisture content.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Makenzie Hyman Iron laboratories Makenzie Hyman

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 1 of 4
IRON Laboratories

Residual Solvents Analysis by
Mass Spectrometer
Test Certificate #: 90816-001
Client Name, Sample Details

Kenneth Rogers
Novi, MI 48377
Sample: Pennywise Wax
Type: Medical Compliant Flower
Method: SOP FE-44-OR3
Test Conditions

Scale: XS205-MI1
Temp: 22.5 °C
Baro Pressure: 986.2 hPa
Analyst: JER
Technician: MEH
Sample ID#: 90816

Harvest/Process Date: 02/21/2017
Serving Size (g): 50465
Date Received: 02/17/2017
Report Issued: 03/20/2017
Sample #90816
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
1,2-Dichloroethane 2 1 Pass/<LOD 1,2-Dimethoxyethane 100 5 Pass/<LOD
1,4-dioxane 380 200 Pass/<LOD 1-Butanol 5,000 100 Pass/<LOD
1-Pentanol 5,000 100 Pass/<LOD 1-Propanol 5,000 100 Pass/<LOD
2,2-Dimethylpropane (Neopentane) 5,000 100 Pass/<LOD 2,2-Dimethylbutane (Hexanes) 0 0 Not Tested
2,3-Dimethylbutane (Hexanes) 0 0 Not Tested 2-Butanol 5,000 100 Pass/<LOD
2-Butanone (MEK) 5,000 50 Pass/<LOD 2-Ethoxyethanol 160 40 Pass/<LOD
2-Methylbutane (Isopentane) 5,000 50 Pass/801 2-Methylpentane (Hexanes) 290 50 Pass/25
2-Methylpropane (Isobutane) 5,000 100 Pass/99 2-propanol (Isopropyl Alcohol) 5,000 50 Pass/<LOD
2-Propanone (Acetone) 5,000 50 Pass/231 3-Methylpentane (Hexanes) 290 50 Pass/19
Acetonitrile 410 100 Pass/<LOD Benzene 2 1 Pass/<LOD
Butane 5,000 100 Pass/1,156 Chloroform 2 1 Pass/<LOD
Cumene 70 35 Pass/<LOD Cyclohexane 3,880 1,000 Pass/100
Dichloromethane 600 150 Pass/<LOD Dimethylsulfoxide (DMSO) 5,000 500 Pass/<LOD
Ethanol 5,000 500 Pass/<LOD Ethyl acetate 5,000 50 Pass/<LOD
Ethyl ether 5,000 500 Pass/<LOD Ethylene glycol 620 310 Pass/<LOD
Ethylene oxide 50 50 Pass/<LOD Heptane 5,000 50 Pass/<LOD
Hexane 290 50 Pass/<LOD Isopropyl acetate 5,000 50 Pass/<LOD
Methanol 3,000 500 Pass/<LOD Naptha 400 100 Pass/<LOD
N,N-Dimethylacetamide 1,090 273 Pass/<LOD N,N-Dimethylformamide (DMF) 880 500 Pass/<LOD
Pentane 5,000 50 Pass/232 Petroleum Ether 400 5 Pass/<LOD
Propane 5,000 100 Pass/<LOD Pyridine 200 10 Pass/<LOD
Sulfolane 160 200 Pass/<LOD Tetrahydrofuran (THF) 720 200 Pass/<LOD
Toluene 890 50 Pass/<LOD Trichloroethylene 5,000 100 Pass/<LOD
Xylenes* 2,170 50 Pass/<LOD

Total PPM: 2,663.00
* Xylenes are reported as the sum of o-xylene, m-xylene, p-xylene, and ethylbenzene
MRL - Maximum Residue Limit; LOD - Limit of Detection

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Makenzie Hyman Iron laboratories Makenzie Hyman

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 2 of 4
IRON Laboratories

Terpene Report
Test Certificate #: 90816-001
Client Name, Sample Details

Kenneth Rogers
Novi, MI 48377
Sample: Pennywise Wax
Type: Medical Compliant Flower
Test Conditions

Sample ID#: 90816

Harvest/Process Date: 02/21/2017
Serving Size (g): 50465
Date Received: 02/17/2017
Sample #90816

Mono Terpenes

Weight Percentage Dry Matter (wt/wt%)

α-Pinene:

 N/D

β-Ocimene:

 N/D

Camphene:

 N/D

Eucalyptol (1,8-Cineol):

 N/D

Sabinene:

 N/D

γ-Terpinene:

 N/D

Myrcene:

 N/D

α-Terpinolene:

 N/D

β-Pinene:

 N/D

Linalool:

 N/D

∆3-Carene:

 N/D

Fenchone:

 N/D

α-Terpinene:

 N/D

Fenchol:

 N/D

Ocimene:

 N/D

Isopulegol:

 N/D

Limonene:

 N/D

Geraniol:

 N/D

4-Cymene:

 N/D

Sequi Terpenes

Weight Percentage Dry Matter (wt/wt%)

β-Caryophyllene:

 N/D

α-Humulene:

 N/D

Nerolidol 1:

 N/D

Nerolidol 2:

 N/D

Guaiol:

 N/D

Caryophyllene Oxide:

 N/D

α-Bisabolol:

 N/D

Other Terpenes

Total: 0.000%
N/D

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Tested by Iron Laboratories

Page 3 of 4
IRON Laboratories

Bio Analysis by
Gas Chromatography
Test Certificate #: 90816-001
Client Name, Sample Details

Kenneth Rogers
Novi, MI 48377
Sample: Pennywise Wax
Type: Medical Compliant Flower
Method: FE03 GC6890-1
Test Conditions

Scale: XS205-MI1
Temp: 21.2 °C
Baro Pressure: 989 hPa
Analyst: JCM
Technician: JCM
Sample ID#: 90816

Harvest/Process Date: 02/21/2017
Serving Size (g): 50465
Date Received: 02/17/2017
Test Date: 02/20/2017
Valid Through: 02/20/2018
Report Issued: 02/17/2017
Sample #90816
Sample #90816 Sample #90816
Impurities: Not Detected
Molds: No Types: N/A
Pests: No Types: N/A
Anthers: No
Detritus: No
Fibers: No
Hair: No
Mature Seeds: No
Premature Seeds: No
Unidentified Foliar Spray: No
Other Impurities: No
*Moisture -

*Moisture is not part of the accredited scope of Iron Laboratories.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 4 of 4