Full Report - 90571

Marihuana Potency Analysis by
High Performance Liquid Chromatography

Test Certificate #: 90571-001

Client Name, Sample Details
ADA East Detroit, MI 48224 Sample: Macberry Cookie Type: Infused Product Method: FE04 HPLC1100-1

Test Conditions
Scale: XS205-MI2 Temp: 21.3 °C Baro Pressure: 987.7 hPa Analyst: MEH Technician: MEH

Sample ID#: 90571
Harvest/Process Date: 02/13/2017 Serving Size (g): 57.2 Date Received: 02/13/2017 Test Date: 02/13/2017 Valid Through: 02/13/2018 Report Issued: 02/10/2017

Test Compounds	CBDA	CBD	CBN	THC	THCA	TOTAL	CBD Act.	THC Act.
Amount	N/D	N/D	0.1	0.9	N/D	1.0	N/A	100%
Min. Value	0.1 mg/g	0.1 mg/g	0.1 mg/g	0.1 mg/g	0.1 mg/g	-	-	-
Amount per Serving~	N/D	N/D	5.7 mg/srv	51.5 mg/srv	N/D	57.2 mg/srv	Serving Size~ (g):	57.20 g
Uncertainty†	±5% RSD	±5% RSD	±5% RSD	±5% RSD	±5% RSD	-	-	-

†Uncertainty measurement is for the test procedure and the instrument used; and is calculated in accordance with the ISO "Guide of Uncertainty in Measurement" (GUM) Test Results and uncertainty are only representative of the sample submit to our laboratory. Uncertainty does not account for any uncertainty in the sampling. The measurement of uncertainty is the expanded uncertainty and is an estimate of uncertainty calculated with normal distribution and a coverage factor of 2 (K=2) to approximate a 95% confidence level.

%RSD = Relative Standard Deviation; Min. Value = Minimum Detectable Amount, CFU = Colony Forming Units

N/D designates a value that is not detected above the methods Limit of quantitation (min. value)

Values are not adjusted for moisture content.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390
Page 1 of 4

Terpene Report

Test Certificate #: 90571-001

Client Name, Sample Details
ADA East Detroit, MI 48224 Sample: Macberry Cookie Type: Infused Product

Test Conditions

Sample ID#: 90571
Harvest/Process Date: 02/13/2017 Serving Size (g): 57.2 Date Received: 02/13/2017

Mono Terpenes

Weight Percentage Dry Matter (wt/wt%)

α-Pinene:	N/D	β-Ocimene:	N/D
Camphene:	N/D	Eucalyptol (1,8-Cineol):	N/D
Sabinene:	N/D	γ-Terpinene:	N/D
Myrcene:	N/D	α-Terpinolene:	N/D
β-Pinene:	N/D	Linalool:	N/D
∆3-Carene:	N/D	Fenchone:	N/D
α-Terpinene:	N/D	Fenchol:	N/D
Ocimene:	N/D	Isopulegol:	N/D
Limonene:	N/D	Geraniol:	N/D
4-Cymene:	N/D

Sequi Terpenes

Weight Percentage Dry Matter (wt/wt%)

β-Caryophyllene:	N/D
α-Humulene:	N/D
Nerolidol 1:	N/D
Nerolidol 2:	N/D
Guaiol:	N/D
Caryophyllene Oxide:	N/D
α-Bisabolol:	N/D

Other Terpenes Total: 0.000%
N/D

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Tested by Iron Laboratories
Page 2 of 4

Terpene Report

Test Certificate #: 90571-001

Client Name, Sample Details
ADA East Detroit, MI 48224 Sample: Macberry Cookie Type: Infused Product

Test Conditions

Sample ID#: 90571
Harvest/Process Date: 02/13/2017 Serving Size (g): 57.2 Date Received: 02/13/2017

Mono Terpenes

Weight Percentage Dry Matter (wt/wt%)

α-Pinene:	N/D	β-Ocimene:	N/D
Camphene:	N/D	Eucalyptol (1,8-Cineol):	N/D
Sabinene:	N/D	γ-Terpinene:	N/D
Myrcene:	N/D	α-Terpinolene:	N/D
β-Pinene:	N/D	Linalool:	N/D
∆3-Carene:	N/D	Fenchone:	N/D
α-Terpinene:	N/D	Fenchol:	N/D
Ocimene:	N/D	Isopulegol:	N/D
Limonene:	N/D	Geraniol:	N/D
4-Cymene:	N/D

Sequi Terpenes

Weight Percentage Dry Matter (wt/wt%)

β-Caryophyllene:	N/D
α-Humulene:	N/D
Nerolidol 1:	N/D
Nerolidol 2:	N/D
Guaiol:	N/D
Caryophyllene Oxide:	N/D
α-Bisabolol:	N/D

Other Terpenes Total: 0.000%
N/D

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Tested by Iron Laboratories
Page 3 of 4

Bio Analysis by
High Performance Liquid Chromatography

Test Certificate #: 90571-001

Client Name, Sample Details
ADA East Detroit, MI 48224 Sample: Macberry Cookie Type: Infused Product Method: FE04 HPLC1100-1

Test Conditions
Scale: XS205-MI2 Temp: 21.3 °C Baro Pressure: 987.7 hPa Analyst: MEH Technician: MEH

Sample ID#: 90571
Harvest/Process Date: 02/13/2017 Serving Size (g): 57.2 Date Received: 02/13/2017 Test Date: 02/13/2017 Valid Through: 02/13/2018 Report Issued: 02/10/2017

Impurities:	Not Detected
Molds:	No	Types: N/A
Pests:	No	Types: N/A
Anthers:	No
Detritus:	No
Fibers:	No
Hair:	No
Mature Seeds:	No
Premature Seeds:	No
Unidentified Foliar Spray:	No
Other Impurities:	No
*Moisture	-

*Moisture is not part of the accredited scope of Iron Laboratories.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390
Page 4 of 4

Marihuana Potency Analysis byHigh Performance Liquid Chromatography

Client Name, Sample Details

Test Conditions

Sample ID#: 90571

Terpene Report

Client Name, Sample Details

Test Conditions

Sample ID#: 90571

Mono Terpenes

α-Pinene:

β-Ocimene:

Camphene:

Eucalyptol (1,8-Cineol):

Sabinene:

γ-Terpinene:

Myrcene:

α-Terpinolene:

β-Pinene:

Linalool:

∆3-Carene:

Fenchone:

α-Terpinene:

Fenchol:

Ocimene:

Isopulegol:

Limonene:

Geraniol:

4-Cymene:

Sequi Terpenes

β-Caryophyllene:

α-Humulene:

Nerolidol 1:

Nerolidol 2:

Guaiol:

Caryophyllene Oxide:

α-Bisabolol:

Other Terpenes

Terpene Report

Client Name, Sample Details

Test Conditions

Sample ID#: 90571

Mono Terpenes

α-Pinene:

β-Ocimene:

Camphene:

Eucalyptol (1,8-Cineol):

Sabinene:

γ-Terpinene:

Myrcene:

α-Terpinolene:

β-Pinene:

Linalool:

∆3-Carene:

Fenchone:

α-Terpinene:

Fenchol:

Ocimene:

Isopulegol:

Limonene:

Geraniol:

4-Cymene:

Sequi Terpenes

β-Caryophyllene:

α-Humulene:

Nerolidol 1:

Nerolidol 2:

Guaiol:

Caryophyllene Oxide:

α-Bisabolol:

Other Terpenes

Bio Analysis byHigh Performance Liquid Chromatography

Client Name, Sample Details

Test Conditions

Sample ID#: 90571

Marihuana Potency Analysis by
High Performance Liquid Chromatography

Bio Analysis by
High Performance Liquid Chromatography