Full Report - 89933

Marijuana Potency Analysis by
High Performance Liquid Chromatography

Test Certificate #: 89933-001

Client Name, Sample Details
45th Parallel Farms LLC Dallas, OR 97338 Sample: Northern Wreck Shake License: 010-100164183CE Type: Flower Method: FE04N-OR1 HPLC1100-OR1

Test Conditions
Scale: XS205-OR1 Temp: 21.3 °C Baro Pressure: 1004 hPa Analyst: PHJ Technician: PHJ

Sample ID#: 89933
Harvest/Process Date: 10/17/2017 Serving Size (g): 49598 Date Received: 01/24/2017 Test Date: 01/24/2017

Test Compounds	CBDA	CBD	CBC	CBG	CBN	THC	THCA	THCV		Calc. Max	Act.
Amount	N/D	N/D	N/D	0.1	N/D	1.5	17.4	N/D	CBD	N/A	N/A
LOQ	0.1%	0.1%	0.1%	0.1%	0.1%	0.1%	0.1%	0.1%	THC	16.7598%	8%
Uncertainty†	±5% RPD	±5% RPD	±5% RPD	±5% RPD	±5% RPD	±5% RPD	±5% RPD	±5% RPD	Totals:	0.0%	-

LOQ = Limit of Quantitation

RPD is relative percent difference between the LCS and LCS duplicate.

%RPD = Relative Percent Difference; Min. Value = Minimum Detectable Amount, CFU = Colony Forming Units, N/D = Not Detected

Calc. Max. is the calculated sum of CBD or THC and the amount of CBD or THC derived from CBDA or THCA; respectively .These values are calculated by applying a molar correction factor of 0.877 to the CBDA or THCA value.

*** Designated tests that use the method FE-45.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401
Page 1 of 6

Terpene Report

Test Certificate #: 89933-001

Client Name, Sample Details
45th Parallel Farms LLC Dallas, OR 97338 Sample: Northern Wreck Shake License: 010-100164183CE Type: Flower

Test Conditions

Sample ID#: 89933
Harvest/Process Date: 10/17/2017 Serving Size (g): 49598 Date Received: 01/24/2017

Mono Terpenes

Weight Percentage Dry Matter (wt/wt%)

α-Pinene:	N/D	β-Ocimene:	N/D
Camphene:	N/D	Eucalyptol (1,8-Cineol):	N/D
Sabinene:	N/D	γ-Terpinene:	N/D
Myrcene:	N/D	α-Terpinolene:	N/D
β-Pinene:	N/D	Linalool:	N/D
∆3-Carene:	N/D	Fenchone:	N/D
α-Terpinene:	N/D	Fenchol:	N/D
Ocimene:	N/D	Isopulegol:	N/D
Limonene:	N/D	Geraniol:	N/D
4-Cymene:	N/D

Sequi Terpenes

Weight Percentage Dry Matter (wt/wt%)

β-Caryophyllene:	N/D
α-Humulene:	N/D
Nerolidol 1:	N/D
Nerolidol 2:	N/D
Guaiol:	N/D
Caryophyllene Oxide:	N/D
α-Bisabolol:	N/D

Other Terpenes Total: 0.000%
N/D

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Tested by Iron Laboratories
Page 2 of 6

Terpene Report

Test Certificate #: 89933-001

Client Name, Sample Details
45th Parallel Farms LLC Dallas, OR 97338 Sample: Northern Wreck Shake License: 010-100164183CE Type: Flower

Test Conditions

Sample ID#: 89933
Harvest/Process Date: 10/17/2017 Serving Size (g): 49598 Date Received: 01/24/2017

Mono Terpenes

Weight Percentage Dry Matter (wt/wt%)

α-Pinene:	N/D	β-Ocimene:	N/D
Camphene:	N/D	Eucalyptol (1,8-Cineol):	N/D
Sabinene:	N/D	γ-Terpinene:	N/D
Myrcene:	N/D	α-Terpinolene:	N/D
β-Pinene:	N/D	Linalool:	N/D
∆3-Carene:	N/D	Fenchone:	N/D
α-Terpinene:	N/D	Fenchol:	N/D
Ocimene:	N/D	Isopulegol:	N/D
Limonene:	N/D	Geraniol:	N/D
4-Cymene:	N/D

Sequi Terpenes

Weight Percentage Dry Matter (wt/wt%)

β-Caryophyllene:	N/D
α-Humulene:	N/D
Nerolidol 1:	N/D
Nerolidol 2:	N/D
Guaiol:	N/D
Caryophyllene Oxide:	N/D
α-Bisabolol:	N/D

Other Terpenes Total: 0.000%
N/D

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Tested by Iron Laboratories
Page 3 of 6

Terpene Report

Test Certificate #: 89933-001

Client Name, Sample Details
45th Parallel Farms LLC Dallas, OR 97338 Sample: Northern Wreck Shake License: 010-100164183CE Type: Flower

Test Conditions

Sample ID#: 89933
Harvest/Process Date: 10/17/2017 Serving Size (g): 49598 Date Received: 01/24/2017

Mono Terpenes

Weight Percentage Dry Matter (wt/wt%)

α-Pinene:	N/D	β-Ocimene:	N/D
Camphene:	N/D	Eucalyptol (1,8-Cineol):	N/D
Sabinene:	N/D	γ-Terpinene:	N/D
Myrcene:	N/D	α-Terpinolene:	N/D
β-Pinene:	N/D	Linalool:	N/D
∆3-Carene:	N/D	Fenchone:	N/D
α-Terpinene:	N/D	Fenchol:	N/D
Ocimene:	N/D	Isopulegol:	N/D
Limonene:	N/D	Geraniol:	N/D
4-Cymene:	N/D

Sequi Terpenes

Weight Percentage Dry Matter (wt/wt%)

β-Caryophyllene:	N/D
α-Humulene:	N/D
Nerolidol 1:	N/D
Nerolidol 2:	N/D
Guaiol:	N/D
Caryophyllene Oxide:	N/D
α-Bisabolol:	N/D

Other Terpenes Total: 0.000%
N/D

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Tested by Iron Laboratories
Page 4 of 6

Terpene Report

Test Certificate #: 89933-001

Client Name, Sample Details
45th Parallel Farms LLC Dallas, OR 97338 Sample: Northern Wreck Shake License: 010-100164183CE Type: Flower

Test Conditions

Sample ID#: 89933
Harvest/Process Date: 10/17/2017 Serving Size (g): 49598 Date Received: 01/24/2017

Mono Terpenes

Weight Percentage Dry Matter (wt/wt%)

α-Pinene:	N/D	β-Ocimene:	N/D
Camphene:	N/D	Eucalyptol (1,8-Cineol):	N/D
Sabinene:	N/D	γ-Terpinene:	N/D
Myrcene:	N/D	α-Terpinolene:	N/D
β-Pinene:	N/D	Linalool:	N/D
∆3-Carene:	N/D	Fenchone:	N/D
α-Terpinene:	N/D	Fenchol:	N/D
Ocimene:	N/D	Isopulegol:	N/D
Limonene:	N/D	Geraniol:	N/D
4-Cymene:	N/D

Sequi Terpenes

Weight Percentage Dry Matter (wt/wt%)

β-Caryophyllene:	N/D
α-Humulene:	N/D
Nerolidol 1:	N/D
Nerolidol 2:	N/D
Guaiol:	N/D
Caryophyllene Oxide:	N/D
α-Bisabolol:	N/D

Other Terpenes Total: 0.000%
N/D

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Tested by Iron Laboratories
Page 5 of 6

Bio Analysis by
High Performance Liquid Chromatography

Test Certificate #: 89933-001

Client Name, Sample Details
45th Parallel Farms LLC Dallas, OR 97338 Sample: Northern Wreck Shake License: 010-100164183CE Type: Flower Method: FE04N-OR1 HPLC1100-OR1

Test Conditions
Scale: XS205-OR1 Temp: 21.3 °C Baro Pressure: 1004 hPa Analyst: PHJ Technician: PHJ

Sample ID#: 89933
Harvest/Process Date: 10/17/2017 Serving Size (g): 49598 Date Received: 01/24/2017 Test Date: 01/24/2017

Impurities:	Detected
Molds:	No	Types: N/A
Pests:	No	Types: N/A
Anthers:	No
Detritus:	No
Fibers:	No
Hair:	No
Mature Seeds:	No
Premature Seeds:	No
Unidentified Foliar Spray:	No
Other Impurities:	No
*Moisture	9.4

*Moisture is not part of the accredited scope of Iron Laboratories.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401
Page 6 of 6

Marijuana Potency Analysis byHigh Performance Liquid Chromatography

Client Name, Sample Details

Test Conditions

Sample ID#: 89933

Terpene Report

Client Name, Sample Details

Test Conditions

Sample ID#: 89933

Mono Terpenes

α-Pinene:

β-Ocimene:

Camphene:

Eucalyptol (1,8-Cineol):

Sabinene:

γ-Terpinene:

Myrcene:

α-Terpinolene:

β-Pinene:

Linalool:

∆3-Carene:

Fenchone:

α-Terpinene:

Fenchol:

Ocimene:

Isopulegol:

Limonene:

Geraniol:

4-Cymene:

Sequi Terpenes

β-Caryophyllene:

α-Humulene:

Nerolidol 1:

Nerolidol 2:

Guaiol:

Caryophyllene Oxide:

α-Bisabolol:

Other Terpenes

Terpene Report

Client Name, Sample Details

Test Conditions

Sample ID#: 89933

Mono Terpenes

α-Pinene:

β-Ocimene:

Camphene:

Eucalyptol (1,8-Cineol):

Sabinene:

γ-Terpinene:

Myrcene:

α-Terpinolene:

β-Pinene:

Linalool:

∆3-Carene:

Fenchone:

α-Terpinene:

Fenchol:

Ocimene:

Isopulegol:

Limonene:

Geraniol:

4-Cymene:

Sequi Terpenes

β-Caryophyllene:

α-Humulene:

Nerolidol 1:

Nerolidol 2:

Guaiol:

Caryophyllene Oxide:

α-Bisabolol:

Other Terpenes

Terpene Report

Client Name, Sample Details

Test Conditions

Sample ID#: 89933

Mono Terpenes

α-Pinene:

β-Ocimene:

Camphene:

Eucalyptol (1,8-Cineol):

Sabinene:

Marijuana Potency Analysis by
High Performance Liquid Chromatography

Bio Analysis by
High Performance Liquid Chromatography