IRON Laboratories

Marijuana Potency Analysis by
High Performance Liquid Chromatography
Test Certificate #: 89929-001
Client Name, Sample Details

45th Parallel Farms LLC
Dallas, OR 97338
Sample: Jakes Grape
License: 010-100164183CE
Type: Flower
Method: FE04N-OR1 HPLC1100-OR1
Test Conditions

Scale: XS205-OR1
Temp: 21.3 °C
Baro Pressure: 1004 hPa
Analyst: PHJ
Technician: PHJ
Sample ID#: 89929

Harvest/Process Date: 01/24/2017
Serving Size (g): 49594
Date Received: 01/24/2017
Test Date: 01/24/2017
Sample #89929
Sample #89929 Sample #89929
Test
Compounds		 CBDA CBD CBC CBG CBN THC THCA THCV   Calc. Max Act.
Amount N/D N/D 0.1 0.3 0.6 2.4 17.2 N/D CBD N/A N/A
LOQ 0.1% 0.1% 0.1% 0.1% 0.1% 0.1% 0.1% 0.1% THC 17.4844% 12%
Uncertainty† ±5% RPD ±5% RPD ±5% RPD ±5% RPD ±5% RPD ±5% RPD ±5% RPD ±5% RPD Totals: 0.0% -

LOQ = Limit of Quantitation

RPD is relative percent difference between the LCS and LCS duplicate.

%RPD = Relative Percent Difference; Min. Value = Minimum Detectable Amount, CFU = Colony Forming Units, N/D = Not Detected

Calc. Max. is the calculated sum of CBD or THC and the amount of CBD or THC derived from CBDA or THCA; respectively .These values are calculated by applying a molar correction factor of 0.877 to the CBDA or THCA value.

*** Designated tests that use the method FE-45.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

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IRON Laboratories

Terpene Report
Test Certificate #: 89929-001
Client Name, Sample Details

45th Parallel Farms LLC
Dallas, OR 97338
Sample: Jakes Grape
License: 010-100164183CE
Type: Flower
Test Conditions

Sample ID#: 89929

Harvest/Process Date: 01/24/2017
Serving Size (g): 49594
Date Received: 01/24/2017
Sample #89929

Mono Terpenes

Weight Percentage Dry Matter (wt/wt%)

α-Pinene:

 N/D

β-Ocimene:

 N/D

Camphene:

 N/D

Eucalyptol (1,8-Cineol):

 N/D

Sabinene:

 N/D

γ-Terpinene:

 N/D

Myrcene:

 N/D

α-Terpinolene:

 N/D

β-Pinene:

 N/D

Linalool:

 N/D

∆3-Carene:

 N/D

Fenchone:

 N/D

α-Terpinene:

 N/D

Fenchol:

 N/D

Ocimene:

 N/D

Isopulegol:

 N/D

Limonene:

 N/D

Geraniol:

 N/D

4-Cymene:

 N/D

Sequi Terpenes

Weight Percentage Dry Matter (wt/wt%)

β-Caryophyllene:

 N/D

α-Humulene:

 N/D

Nerolidol 1:

 N/D

Nerolidol 2:

 N/D

Guaiol:

 N/D

Caryophyllene Oxide:

 N/D

α-Bisabolol:

 N/D

Other Terpenes

Total: 0.000%
N/D

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Tested by Iron Laboratories

Page 2 of 5
IRON Laboratories

Terpene Report
Test Certificate #: 89929-001
Client Name, Sample Details

45th Parallel Farms LLC
Dallas, OR 97338
Sample: Jakes Grape
License: 010-100164183CE
Type: Flower
Test Conditions

Sample ID#: 89929

Harvest/Process Date: 01/24/2017
Serving Size (g): 49594
Date Received: 01/24/2017
Sample #89929

Mono Terpenes

Weight Percentage Dry Matter (wt/wt%)

α-Pinene:

 N/D

β-Ocimene:

 N/D

Camphene:

 N/D

Eucalyptol (1,8-Cineol):

 N/D

Sabinene:

 N/D

γ-Terpinene:

 N/D

Myrcene:

 N/D

α-Terpinolene:

 N/D

β-Pinene:

 N/D

Linalool:

 N/D

∆3-Carene:

 N/D

Fenchone:

 N/D

α-Terpinene:

 N/D

Fenchol:

 N/D

Ocimene:

 N/D

Isopulegol:

 N/D

Limonene:

 N/D

Geraniol:

 N/D

4-Cymene:

 N/D

Sequi Terpenes

Weight Percentage Dry Matter (wt/wt%)

β-Caryophyllene:

 N/D

α-Humulene:

 N/D

Nerolidol 1:

 N/D

Nerolidol 2:

 N/D

Guaiol:

 N/D

Caryophyllene Oxide:

 N/D

α-Bisabolol:

 N/D

Other Terpenes

Total: 0.000%
N/D

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Tested by Iron Laboratories

Page 3 of 5
IRON Laboratories

Terpene Report
Test Certificate #: 89929-001
Client Name, Sample Details

45th Parallel Farms LLC
Dallas, OR 97338
Sample: Jakes Grape
License: 010-100164183CE
Type: Flower
Test Conditions

Sample ID#: 89929

Harvest/Process Date: 01/24/2017
Serving Size (g): 49594
Date Received: 01/24/2017
Sample #89929

Mono Terpenes

Weight Percentage Dry Matter (wt/wt%)

α-Pinene:

 N/D

β-Ocimene:

 N/D

Camphene:

 N/D

Eucalyptol (1,8-Cineol):

 N/D

Sabinene:

 N/D

γ-Terpinene:

 N/D

Myrcene:

 N/D

α-Terpinolene:

 N/D

β-Pinene:

 N/D

Linalool:

 N/D

∆3-Carene:

 N/D

Fenchone:

 N/D

α-Terpinene:

 N/D

Fenchol:

 N/D

Ocimene:

 N/D

Isopulegol:

 N/D

Limonene:

 N/D

Geraniol:

 N/D

4-Cymene:

 N/D

Sequi Terpenes

Weight Percentage Dry Matter (wt/wt%)

β-Caryophyllene:

 N/D

α-Humulene:

 N/D

Nerolidol 1:

 N/D

Nerolidol 2:

 N/D

Guaiol:

 N/D

Caryophyllene Oxide:

 N/D

α-Bisabolol:

 N/D

Other Terpenes

Total: 0.000%
N/D

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Tested by Iron Laboratories

Page 4 of 5
IRON Laboratories

Bio Analysis by
High Performance Liquid Chromatography
Test Certificate #: 89929-001
Client Name, Sample Details

45th Parallel Farms LLC
Dallas, OR 97338
Sample: Jakes Grape
License: 010-100164183CE
Type: Flower
Method: FE04N-OR1 HPLC1100-OR1
Test Conditions

Scale: XS205-OR1
Temp: 21.3 °C
Baro Pressure: 1004 hPa
Analyst: PHJ
Technician: PHJ
Sample ID#: 89929

Harvest/Process Date: 01/24/2017
Serving Size (g): 49594
Date Received: 01/24/2017
Test Date: 01/24/2017
Sample #89929
Sample #89929 Sample #89929
Impurities: Detected
Molds: No Types: N/A
Pests: No Types: N/A
Anthers: No
Detritus: No
Fibers: No
Hair: No
Mature Seeds: No
Premature Seeds: No
Unidentified Foliar Spray: No
Other Impurities: No
*Moisture 10.94

*Moisture is not part of the accredited scope of Iron Laboratories.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

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