Full Report - 89078

Marijuana Potency Analysis by
High Performance Liquid Chromatography

Test Certificate #: 89078-001

Client Name, Sample Details
3 Little Birds, LLC Grants Pass, OR 97526 Sample: Old Man Gary Type: Flower Method: FE04N-OR1 HPLC1100-OR1 Metrc Test Pkg#: 1A4010300001132000000016

Test Conditions
Scale: XS205-OR1 Temp: 21.7 °C Baro Pressure: 991.4 hPa Analyst: PHJ Technician: PHJ

Sample ID#: 89078
Harvest/Process Date: 11/23/2016 Serving Size (g): 48765 Date Received: 12/22/2016 Test Date: 01/10/2017

Test Compounds	CBDA	CBD	CBC	CBG	CBN	THC	THCA	THCV		Calc. Max	Act.
Amount	4.0	N/D	N/D	0.2	N/D	1.0	26.6	N/D	CBD	N/A	0%
LOQ	0.1%	0.1%	0.1%	0.1%	0.1%	0.1%	0.1%	0.1%	THC	24.3282%	4%
Uncertainty†	±5% RPD	±5% RPD	±5% RPD	±5% RPD	±5% RPD	±5% RPD	±5% RPD	±5% RPD	Totals:	0.0%	-

LOQ = Limit of Quantitation

RPD is relative percent difference between the LCS and LCS duplicate.

%RPD = Relative Percent Difference; Min. Value = Minimum Detectable Amount, CFU = Colony Forming Units, N/D = Not Detected

Calc. Max. is the calculated sum of CBD or THC and the amount of CBD or THC derived from CBDA or THCA; respectively .These values are calculated by applying a molar correction factor of 0.877 to the CBDA or THCA value.

*** Designated tests that use the method FE-45.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401
Page 1 of 4

Pesticide Analysis by
Mass Spectrometer

Test Certificate #: 89078-001

Client Name, Sample Details
3 Little Birds, LLC Grants Pass, OR 97526 Sample: Old Man Gary Type: Flower Method: AOAC 2007.01 Metrc Test Pkg#: 1A4010300001132000000016

Test Conditions

Sample ID#: 89078
Harvest/Process Date: 11/23/2016 Serving Size (g): 48765 Date Received: 12/22/2016 Test Date: 03/22/2017

Compound	MRL (µg/g)	LOD (µg/g)	Status (µg/g)	Compound	MRL (µg/g)	LOD (µg/g)	Status (µg/g)
Aldicarb	0.400	0.054	Pass/<LOD	Abamectin****	0.500	0.217	Pass/<LOD
Acephate	0.400	0.408	Pass/<LOD	Acequinocyl	2.000	0.408	Pass/<LOD
Acetamiprid	0.200	0.054	Pass/<LOD	Azoxystrobin	0.200	0.054	Pass/<LOD
Bifenazate	0.200	0.136	Pass/<LOD	Bifenthrin	0.200	0.136	Pass/<LOD
Boscalid	0.400	0.272	Pass/<LOD	Carbaryl	0.200	0.054	Pass/<LOD
Carbofuran	0.200	0.054	Pass/<LOD	Chlorantraniliprole	0.200	0.163	Pass/<LOD
Chlorfenapyr	1.000	0.054	Pass/<LOD	Chlorpyrifos	0.200	0.054	Pass/<LOD
Clofentezine	0.200	0.163	Pass/<LOD	Cyfluthrin**	1.000	0.054	Pass/<LOD
Cypermethrin***	1.000	0.054	Pass/<LOD	Daminozide	1.000	0.951	Pass/<LOD
DDVP (Dichlorvos)	0.100	0.136	Pass/<LOD	Diazinon	0.200	0.054	Pass/<LOD
Dimethoate	0.200	0.054	Pass/<LOD	Ethoprophos	0.200	0.054	Pass/<LOD
Etofenprox	0.400	0.054	Pass/<LOD	Etoxazole	0.200	0.027	Pass/<LOD
Fenoxycarb	0.200	0.054	Pass/<LOD	Fenpyroximate	0.400	0.027	Pass/<LOD
Fipronil	0.400	0.054	Pass/<LOD	Flonicamid	1.000	0.054	Pass/<LOD
Fludioxonil	0.400	0.027	Pass/<LOD	Hexythiazox	1.000	0.136	Pass/<LOD
Imazalil	0.200	0.054	Pass/<LOD	Imidacloprid	0.400	0.054	Pass/<LOD
Kresoxim Methyl	0.400	0.054	Pass/<LOD	Malathion	0.200	0.027	Pass/<LOD
Metalaxyl	0.200	0.027	Pass/<LOD	Methiocarb	0.200	0.027	Pass/<LOD
Methomyl	0.400	0.136	Pass/<LOD	Methyl Parathion	0.200	0.054	Pass/<LOD
MGK-264‡	0.200	0.054	Pass/<LOD	Myclobutanil	0.200	0.136	Pass/<LOD
Naled	0.500	0.136	Pass/<LOD	Oxamyl	1.000	0.054	Pass/<LOD
Paclobutrazol	0.400	0.082	Pass/<LOD	Permethrins†	0.200	0.190	Pass/<LOD
Phosmet	0.200	0.054	Pass/<LOD	Piperonyl Butoxide	2.000	0.054	Pass/<LOD
Prallethrin	0.200	0.190	Pass/<LOD	Propiconazole	0.400	0.272	Pass/<LOD
Propoxur	0.200	0.027	Pass/<LOD	Pyrethrins*	1.000	0.408	Pass/<LOD
Pyridaben	0.200	0.054	Pass/<LOD	Spinosad*****	0.200	0.054	Pass/<LOD
Spiromesifen	0.200	0.054	Pass/<LOD	Spirotetramat	0.200	0.054	Pass/<LOD
Spiroxamine‡	0.400	0.054	Pass/<LOD	Tebuconazole	0.400	0.054	Pass/<LOD
Thiacloprid	0.200	0.054	Pass/<LOD	Thiamethoxam	0.200	0.054	Pass/<LOD
Trifloxystrobin	0.200	0.054	Pass/<LOD

* Pyrethrins are reported as the sum of Jasmolin I, Cinerin I, and Pyrethrin I
** Cyfluthrins are reported as the sum of isomers Cyfluthrin I, II, III, and IV
*** Cypermethrins are reported as the sum of isomers Cypermethrin I, II, III, and IV
**** Abamectin is reported as the sum of Avermectin B1a and Avermectin B1b
***** Spinosad is reported as the sum of Spinosyn A and Spinosyn D
† Permethrin and Prallethrin are reported as the sum of cis and trans isomers
‡ MGK-264 and Spiroximine are reported as the sum of isomers I and II
MRL - Maximum Residue Limit; LOD - Limit of Detection

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401
Page 2 of 4

Terpene Report

Test Certificate #: 89078-001

Client Name, Sample Details
3 Little Birds, LLC Grants Pass, OR 97526 Sample: Old Man Gary Type: Flower Metrc Test Pkg#: 1A4010300001132000000016

Test Conditions

Sample ID#: 89078
Harvest/Process Date: 11/23/2016 Serving Size (g): 48765 Date Received: 12/22/2016

Mono Terpenes

Weight Percentage Dry Matter (wt/wt%)

α-Pinene:	N/D	β-Ocimene:	N/D
Camphene:	N/D	Eucalyptol (1,8-Cineol):	N/D
Sabinene:	N/D	γ-Terpinene:	N/D
Myrcene:	N/D	α-Terpinolene:	N/D
β-Pinene:	N/D	Linalool:	N/D
∆3-Carene:	N/D	Fenchone:	N/D
α-Terpinene:	N/D	Fenchol:	N/D
Ocimene:	N/D	Isopulegol:	N/D
Limonene:	N/D	Geraniol:	N/D
4-Cymene:	N/D

Sequi Terpenes

Weight Percentage Dry Matter (wt/wt%)

β-Caryophyllene:	N/D
α-Humulene:	N/D
Nerolidol 1:	N/D
Nerolidol 2:	N/D
Guaiol:	N/D
Caryophyllene Oxide:	N/D
α-Bisabolol:	N/D

Other Terpenes Total: 0.000%
N/D

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Tested by Iron Laboratories
Page 3 of 4

Bio Analysis by
High Performance Liquid Chromatography

Test Certificate #: 89078-001

Client Name, Sample Details
3 Little Birds, LLC Grants Pass, OR 97526 Sample: Old Man Gary Type: Flower Method: FE04N-OR1 HPLC1100-OR1 Metrc Test Pkg#: 1A4010300001132000000016

Test Conditions
Scale: XS205-OR1 Temp: 21.7 °C Baro Pressure: 991.4 hPa Analyst: PHJ Technician: PHJ

Sample ID#: 89078
Harvest/Process Date: 11/23/2016 Serving Size (g): 48765 Date Received: 12/22/2016 Test Date: 01/10/2017

Impurities:	Detected
Molds:	No	Types: N/A
Pests:	No	Types: N/A
Anthers:	No
Detritus:	No
Fibers:	No
Hair:	No
Mature Seeds:	No
Premature Seeds:	No
Unidentified Foliar Spray:	No
Other Impurities:	No
*Moisture	10.9

*Moisture is not part of the accredited scope of Iron Laboratories.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401
Page 4 of 4

Marijuana Potency Analysis byHigh Performance Liquid Chromatography

Client Name, Sample Details

Test Conditions

Sample ID#: 89078

Pesticide Analysis byMass Spectrometer

Client Name, Sample Details

Test Conditions

Sample ID#: 89078

Terpene Report

Client Name, Sample Details

Test Conditions

Sample ID#: 89078

Mono Terpenes

α-Pinene:

β-Ocimene:

Camphene:

Eucalyptol (1,8-Cineol):

Sabinene:

γ-Terpinene:

Myrcene:

α-Terpinolene:

β-Pinene:

Linalool:

∆3-Carene:

Fenchone:

α-Terpinene:

Fenchol:

Ocimene:

Isopulegol:

Limonene:

Geraniol:

4-Cymene:

Sequi Terpenes

β-Caryophyllene:

α-Humulene:

Nerolidol 1:

Nerolidol 2:

Guaiol:

Caryophyllene Oxide:

α-Bisabolol:

Other Terpenes

Bio Analysis byHigh Performance Liquid Chromatography

Client Name, Sample Details

Test Conditions

Sample ID#: 89078

Marijuana Potency Analysis by
High Performance Liquid Chromatography

Pesticide Analysis by
Mass Spectrometer

Bio Analysis by
High Performance Liquid Chromatography