Full Report - 87332

Marijuana Potency Analysis by
High Performance Liquid Chromatography

Test Certificate #: 87332-001

Client Name, Sample Details
Phoenix Pharms Dallas , OR 97338 Sample: Double OG #3 Type: Flower Method: FE04N-OR1 HPLC1100-OR1 Metrc Test Pkg#: 1A40103000023F4000000004

Test Conditions
Scale: XS205-OR1 Temp: 20.6 °C Baro Pressure: 1009 hPa Analyst: HRM Technician: HRM

Sample ID#: 87332
Harvest/Process Date: 11/17/2016 Serving Size (g): 47033 Date Received: 11/17/2016 Test Date: 11/17/2016

Test Compounds	CBDA	CBD	CBC	CBG	CBN	THC	THCA	THCV		Calc. Max	Act.
Amount	N/D	N/D	N/D	0.1	N/D	0.9	23.6	N/D	CBD	N/A	N/A
LOQ	0.1%	0.1%	0.1%	0.1%	0.1%	0.1%	0.1%	0.1%	THC	21.5972%	4%
Uncertainty†	±5% RPD	±5% RPD	±5% RPD	±5% RPD	±5% RPD	±5% RPD	±5% RPD	±5% RPD	Totals:	0.0%	-

LOQ = Limit of Quantitation

RPD is relative percent difference between the LCS and LCS duplicate.

%RPD = Relative Percent Difference; Min. Value = Minimum Detectable Amount, CFU = Colony Forming Units, N/D = Not Detected

Calc. Max. is the calculated sum of CBD or THC and the amount of CBD or THC derived from CBDA or THCA; respectively .These values are calculated by applying a molar correction factor of 0.877 to the CBDA or THCA value.

*** Designated tests that use the method FE-45.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401
Page 1 of 7

Pesticide Analysis by
Mass Spectrometer

Test Certificate #: 87332-001

Client Name, Sample Details
Phoenix Pharms Dallas , OR 97338 Sample: Double OG #3 Type: Flower Method: AOAC 2007.01 Metrc Test Pkg#: 1A40103000023F4000000004

Test Conditions

Sample ID#: 87332
Harvest/Process Date: 11/17/2016 Serving Size (g): 47033 Date Received: 11/17/2016 Test Date: 04/14/2017

Compound	MRL (µg/g)	LOD (µg/g)	Status (µg/g)	Compound	MRL (µg/g)	LOD (µg/g)	Status (µg/g)
Aldicarb	0.400	0.055	Not Tested	Abamectin****	0.500	0.220	Not Tested
Acephate	0.400	0.413	Not Tested	Acequinocyl	2.000	0.413	Not Tested
Acetamiprid	0.200	0.055	Not Tested	Azoxystrobin	0.200	0.055	Not Tested
Bifenazate	0.200	0.028	Not Tested	Bifenthrin	0.200	0.138	Not Tested
Boscalid	0.400	0.275	Not Tested	Carbaryl	0.200	0.055	Not Tested
Carbofuran	0.200	0.055	Not Tested	Chlorantraniliprole	0.200	0.165	Not Tested
Chlorfenapyr	1.000	0.055	Not Tested	Chlorpyrifos	0.200	0.055	Not Tested
Clofentezine	0.200	0.165	Not Tested	Cyfluthrin**	1.000	0.055	Not Tested
Cypermethrin***	1.000	0.055	Not Tested	Daminozide	1.000	1.376	Not Tested
DDVP (Dichlorvos)	0.100	0.138	Not Tested	Diazinon	0.200	0.055	Not Tested
Dimethoate	0.200	0.055	Not Tested	Ethoprophos	0.200	0.055	Not Tested
Etofenprox	0.400	0.055	Not Tested	Etoxazole	0.200	0.028	Not Tested
Fenoxycarb	0.200	0.055	Not Tested	Fenpyroximate	0.400	0.028	Not Tested
Fipronil	0.400	0.055	Not Tested	Flonicamid	1.000	0.055	Not Tested
Fludioxonil	0.400	0.028	Not Tested	Hexythiazox	1.000	0.138	Not Tested
Imazalil	0.200	0.055	Not Tested	Imidacloprid	0.400	0.055	Not Tested
Kresoxim Methyl	0.400	0.055	Not Tested	Malathion	0.200	0.028	Not Tested
Metalaxyl	0.200	0.028	Not Tested	Methiocarb	0.200	0.028	Not Tested
Methomyl	0.400	0.138	Not Tested	Methyl Parathion	0.200	0.055	Not Tested
MGK-264‡	0.200	0.055	Not Tested	Myclobutanil	0.200	0.138	Not Tested
Naled	0.500	0.138	Not Tested	Oxamyl	1.000	0.055	Not Tested
Paclobutrazol	0.400	0.083	Not Tested	Permethrins†	0.200	0.193	Not Tested
Phosmet	0.200	0.055	Not Tested	Piperonyl Butoxide	2.000	0.055	Not Tested
Prallethrin	0.200	0.193	Not Tested	Propiconazole	0.400	0.275	Not Tested
Propoxur	0.200	0.028	Not Tested	Pyrethrins*	1.000	0.413	Not Tested
Pyridaben	0.200	0.055	Not Tested	Spinosad*****	0.200	0.055	Not Tested
Spiromesifen	0.200	0.055	Not Tested	Spirotetramat	0.200	0.055	Not Tested
Spiroxamine‡	0.400	0.055	Not Tested	Tebuconazole	0.400	0.055	Not Tested
Thiacloprid	0.200	0.055	Not Tested	Thiamethoxam	0.200	0.055	Not Tested
Trifloxystrobin	0.200	0.055	Not Tested

Pesticide testing outsourced to OG Analytical Pesticide testing applicable to samples 87330 & 87331 METRC IDs

* Pyrethrins are reported as the sum of Jasmolin I, Cinerin I, and Pyrethrin I
** Cyfluthrins are reported as the sum of isomers Cyfluthrin I, II, III, and IV
*** Cypermethrins are reported as the sum of isomers Cypermethrin I, II, III, and IV
**** Abamectin is reported as the sum of Avermectin B1a and Avermectin B1b
***** Spinosad is reported as the sum of Spinosyn A and Spinosyn D
† Permethrin and Prallethrin are reported as the sum of cis and trans isomers
‡ MGK-264 and Spiroximine are reported as the sum of isomers I and II
MRL - Maximum Residue Limit; LOD - Limit of Detection

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401
Page 2 of 7

Terpene Report

Test Certificate #: 87332-001

Client Name, Sample Details
Phoenix Pharms Dallas , OR 97338 Sample: Double OG #3 Type: Flower Metrc Test Pkg#: 1A40103000023F4000000004

Test Conditions

Sample ID#: 87332
Harvest/Process Date: 11/17/2016 Serving Size (g): 47033 Date Received: 11/17/2016

Mono Terpenes

Weight Percentage Dry Matter (wt/wt%)

α-Pinene:	N/D	β-Ocimene:	N/D
Camphene:	N/D	Eucalyptol (1,8-Cineol):	N/D
Sabinene:	N/D	γ-Terpinene:	N/D
Myrcene:	N/D	α-Terpinolene:	N/D
β-Pinene:	N/D	Linalool:	N/D
∆3-Carene:	N/D	Fenchone:	N/D
α-Terpinene:	N/D	Fenchol:	N/D
Ocimene:	N/D	Isopulegol:	N/D
Limonene:	N/D	Geraniol:	N/D
4-Cymene:	N/D

Sequi Terpenes

Weight Percentage Dry Matter (wt/wt%)

β-Caryophyllene:	N/D
α-Humulene:	N/D
Nerolidol 1:	N/D
Nerolidol 2:	N/D
Guaiol:	N/D
Caryophyllene Oxide:	N/D
α-Bisabolol:	N/D

Other Terpenes Total: 0.000%
N/D

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Tested by Iron Laboratories
Page 3 of 7

Terpene Report

Test Certificate #: 87332-001

Client Name, Sample Details
Phoenix Pharms Dallas , OR 97338 Sample: Double OG #3 Type: Flower Metrc Test Pkg#: 1A40103000023F4000000004

Test Conditions

Sample ID#: 87332
Harvest/Process Date: 11/17/2016 Serving Size (g): 47033 Date Received: 11/17/2016

Mono Terpenes

Weight Percentage Dry Matter (wt/wt%)

α-Pinene:	N/D	β-Ocimene:	N/D
Camphene:	N/D	Eucalyptol (1,8-Cineol):	N/D
Sabinene:	N/D	γ-Terpinene:	N/D
Myrcene:	N/D	α-Terpinolene:	N/D
β-Pinene:	N/D	Linalool:	N/D
∆3-Carene:	N/D	Fenchone:	N/D
α-Terpinene:	N/D	Fenchol:	N/D
Ocimene:	N/D	Isopulegol:	N/D
Limonene:	N/D	Geraniol:	N/D
4-Cymene:	N/D

Sequi Terpenes

Weight Percentage Dry Matter (wt/wt%)

β-Caryophyllene:	N/D
α-Humulene:	N/D
Nerolidol 1:	N/D
Nerolidol 2:	N/D
Guaiol:	N/D
Caryophyllene Oxide:	N/D
α-Bisabolol:	N/D

Other Terpenes Total: 0.000%
N/D

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Tested by Iron Laboratories
Page 4 of 7

Terpene Report

Test Certificate #: 87332-001

Client Name, Sample Details
Phoenix Pharms Dallas , OR 97338 Sample: Double OG #3 Type: Flower Metrc Test Pkg#: 1A40103000023F4000000004

Test Conditions

Sample ID#: 87332
Harvest/Process Date: 11/17/2016 Serving Size (g): 47033 Date Received: 11/17/2016

Mono Terpenes

Weight Percentage Dry Matter (wt/wt%)

α-Pinene:	N/D	β-Ocimene:	N/D
Camphene:	N/D	Eucalyptol (1,8-Cineol):	N/D
Sabinene:	N/D	γ-Terpinene:	N/D
Myrcene:	N/D	α-Terpinolene:	N/D
β-Pinene:	N/D	Linalool:	N/D
∆3-Carene:	N/D	Fenchone:	N/D
α-Terpinene:	N/D	Fenchol:	N/D
Ocimene:	N/D	Isopulegol:	N/D
Limonene:	N/D	Geraniol:	N/D
4-Cymene:	N/D

Sequi Terpenes

Weight Percentage Dry Matter (wt/wt%)

β-Caryophyllene:	N/D
α-Humulene:	N/D
Nerolidol 1:	N/D
Nerolidol 2:	N/D
Guaiol:	N/D
Caryophyllene Oxide:	N/D
α-Bisabolol:	N/D

Other Terpenes Total: 0.000%
N/D

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Tested by Iron Laboratories
Page 5 of 7

Terpene Report

Test Certificate #: 87332-001

Client Name, Sample Details
Phoenix Pharms Dallas , OR 97338 Sample: Double OG #3 Type: Flower Metrc Test Pkg#: 1A40103000023F4000000004

Test Conditions

Sample ID#: 87332
Harvest/Process Date: 11/17/2016 Serving Size (g): 47033 Date Received: 11/17/2016

Mono Terpenes

Weight Percentage Dry Matter (wt/wt%)

α-Pinene:	N/D	β-Ocimene:	N/D
Camphene:	N/D	Eucalyptol (1,8-Cineol):	N/D
Sabinene:	N/D	γ-Terpinene:	N/D
Myrcene:	N/D	α-Terpinolene:	N/D
β-Pinene:	N/D	Linalool:	N/D
∆3-Carene:	N/D	Fenchone:	N/D
α-Terpinene:	N/D	Fenchol:	N/D
Ocimene:	N/D	Isopulegol:	N/D
Limonene:	N/D	Geraniol:	N/D
4-Cymene:	N/D

Sequi Terpenes

Weight Percentage Dry Matter (wt/wt%)

β-Caryophyllene:	N/D
α-Humulene:	N/D
Nerolidol 1:	N/D
Nerolidol 2:	N/D
Guaiol:	N/D
Caryophyllene Oxide:	N/D
α-Bisabolol:	N/D

Other Terpenes Total: 0.000%
N/D

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Tested by Iron Laboratories
Page 6 of 7

Bio Analysis by
High Performance Liquid Chromatography

Test Certificate #: 87332-001

Client Name, Sample Details
Phoenix Pharms Dallas , OR 97338 Sample: Double OG #3 Type: Flower Method: FE04N-OR1 HPLC1100-OR1 Metrc Test Pkg#: 1A40103000023F4000000004

Test Conditions
Scale: XS205-OR1 Temp: 20.6 °C Baro Pressure: 1009 hPa Analyst: HRM Technician: HRM

Sample ID#: 87332
Harvest/Process Date: 11/17/2016 Serving Size (g): 47033 Date Received: 11/17/2016 Test Date: 11/17/2016

Impurities:	Detected
Molds:	No	Types: N/A
Pests:	No	Types: N/A
Anthers:	No
Detritus:	No
Fibers:	No
Hair:	No
Mature Seeds:	No
Premature Seeds:	No
Unidentified Foliar Spray:	No
Other Impurities:	No
*Moisture	9.88

*Moisture is not part of the accredited scope of Iron Laboratories.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401
Page 7 of 7

Marijuana Potency Analysis byHigh Performance Liquid Chromatography

Client Name, Sample Details

Test Conditions

Sample ID#: 87332

Pesticide Analysis byMass Spectrometer

Client Name, Sample Details

Test Conditions

Sample ID#: 87332

Terpene Report

Client Name, Sample Details

Test Conditions

Sample ID#: 87332

Mono Terpenes

α-Pinene:

β-Ocimene:

Camphene:

Eucalyptol (1,8-Cineol):

Sabinene:

γ-Terpinene:

Myrcene:

α-Terpinolene:

β-Pinene:

Linalool:

∆3-Carene:

Fenchone:

α-Terpinene:

Fenchol:

Ocimene:

Isopulegol:

Limonene:

Geraniol:

4-Cymene:

Sequi Terpenes

β-Caryophyllene:

α-Humulene:

Nerolidol 1:

Nerolidol 2:

Guaiol:

Caryophyllene Oxide:

α-Bisabolol:

Other Terpenes

Terpene Report

Client Name, Sample Details

Test Conditions

Sample ID#: 87332

Mono Terpenes

α-Pinene:

β-Ocimene:

Camphene:

Eucalyptol (1,8-Cineol):

Sabinene:

γ-Terpinene:

Myrcene:

α-Terpinolene:

β-Pinene:

Linalool:

∆3-Carene:

Fenchone:

α-Terpinene:

Fenchol:

Ocimene:

Isopulegol:

Limonene:

Geraniol:

4-Cymene:

Sequi Terpenes

β-Caryophyllene:

α-Humulene:

Nerolidol 1:

Nerolidol 2:

Guaiol:

Caryophyllene Oxide:

α-Bisabolol:

Other Terpenes

Terpene Report

Client Name, Sample Details

Test Conditions

Sample ID#: 87332

Mono Terpenes

α-Pinene:

Marijuana Potency Analysis by
High Performance Liquid Chromatography

Pesticide Analysis by
Mass Spectrometer

Bio Analysis by
High Performance Liquid Chromatography