IRON Laboratories

Marijuana Potency Analysis by
High Performance Liquid Chromatography
Test Certificate #: 86057-001
Client Name, Sample Details

Da Kine Extracts
Eugene, OR 97404
Sample: GSC
Type: Medical Flower
Method: FE04N-OR1 HPLC1100-OR1
Test Conditions

Scale: XS205-OR1
Temp: 20.9 °C
Baro Pressure: 1003 hPa
Analyst: PHJ
Technician: PHJ
Sample ID#: 86057

Harvest/Process Date: 10/08/2016
Serving Size (g): 45765
Date Received: 10/05/2016
Test Date: 10/07/2016
Sample #86057
Sample #86057 Sample #86057
Test
Compounds		 CBDA CBD CBC CBG CBN THC THCA THCV   Calc. Max Act.
Amount 0.1 N/D N/D 0.3 0.1 12.3 58.0 N/D CBD N/A 0%
LOQ 0.1% 0.1% 0.1% 0.1% 0.1% 0.1% 0.1% 0.1% THC 63.166% 17%
Uncertainty† ±5% RPD ±5% RPD ±5% RPD ±5% RPD ±5% RPD ±5% RPD ±5% RPD ±5% RPD Totals: 0.0% -

LOQ = Limit of Quantitation

RPD is relative percent difference between the LCS and LCS duplicate.

%RPD = Relative Percent Difference; Min. Value = Minimum Detectable Amount, CFU = Colony Forming Units, N/D = Not Detected

Calc. Max. is the calculated sum of CBD or THC and the amount of CBD or THC derived from CBDA or THCA; respectively .These values are calculated by applying a molar correction factor of 0.877 to the CBDA or THCA value.

*** Designated tests that use the method FE-45.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 1 of 5
IRON Laboratories

Pesticide Analysis by
Mass Spectrometer
Test Certificate #: 86057-001
Client Name, Sample Details

Da Kine Extracts
Eugene, OR 97404
Sample: GSC
Type: Medical Flower
Method: FE-52 (EN 15662 & AOAC 2007.01)
Test Conditions

Analyst: JER
Technician: PHJ
Sample ID#: 86057

Harvest/Process Date: 10/08/2016
Serving Size (g): 45765
Date Received: 10/05/2016
Test Date: 12/29/2016
Sample #86057
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
Aldicarb 0.400 0.100 Pass/<LOD Abamectin**** 0.500 0.100 Pass/<LOD
Acephate 0.400 0.100 Pass/<LOD Acequinocyl 2.000 0.100 Pass/<LOD
Acetamiprid 0.200 0.100 Pass/<LOD Azoxystrobin 0.200 0.100 Pass/<LOD
Bifenazate 0.200 0.100 Pass/<LOD Bifenthrin 0.200 0.100 Pass/<LOD
Boscalid 0.400 0.100 Pass/<LOD Carbaryl 0.200 0.100 Pass/<LOD
Carbofuran 0.200 0.100 Pass/<LOD Chlorantraniliprole 0.200 0.100 Pass/<LOD
Chlorfenapyr 1.000 1.000 Pass/<LOD Chlorpyrifos 0.200 0.100 Pass/<LOD
Clofentezine 0.200 0.100 Pass/<LOD Cyfluthrin** 1.000 1.000 Pass/<LOD
Cypermethrin*** 1.000 1.000 Pass/<LOD Daminozide 1.000 0.100 Pass/<LOD
DDVP (Dichlorvos) 0.100 0.100 Pass/<LOD Diazinon 0.200 0.100 Pass/<LOD
Dimethoate 0.200 0.100 Pass/<LOD Ethoprophos 0.200 0.100 Pass/<LOD
Etofenprox 0.400 0.100 Pass/<LOD Etoxazole 0.200 0.100 Pass/<LOD
Fenoxycarb 0.200 0.100 Pass/<LOD Fenpyroximate 0.400 0.100 Pass/<LOD
Fipronil 0.400 0.100 Pass/<LOD Flonicamid 1.000 0.100 Pass/<LOD
Fludioxonil 0.400 0.100 Pass/<LOD Hexythiazox 1.000 0.100 Pass/<LOD
Imazalil 0.200 0.100 Pass/<LOD Imidacloprid 0.400 0.100 Pass/<LOD
Kresoxim Methyl 0.400 0.100 Pass/<LOD Malathion 0.200 0.100 Pass/<LOD
Metalaxyl 0.200 0.100 Pass/<LOD Methiocarb 0.200 0.100 Pass/<LOD
Methomyl 0.400 0.100 Pass/<LOD Methyl Parathion 0.200 1.000 Pass/<LOD
MGK-264‡ 0.200 1.000 Pass/<LOD Myclobutanil 0.200 0.100 Failed/0.347
Naled 0.500 0.000 Not Tested Oxamyl 1.000 0.100 Pass/<LOD
Paclobutrazol 0.400 0.100 Pass/<LOD Permethrins† 0.200 1.000 Pass/<LOD
Phosmet 0.200 0.100 Pass/<LOD Piperonyl Butoxide 2.000 0.100 Pass/<LOD
Prallethrin 0.200 0.100 Pass/<LOD Propiconazole 0.400 0.100 Pass/<LOD
Propoxur 0.200 0.100 Pass/<LOD Pyrethrins* 1.000 1.000 Pass/<LOD
Pyridaben 0.200 0.100 Pass/<LOD Spinosad***** 0.200 0.100 Pass/<LOD
Spiromesifen 0.200 0.000 Not Tested Spirotetramat 0.200 0.100 Pass/<LOD
Spiroxamine‡ 0.400 0.100 Pass/<LOD Tebuconazole 0.400 0.100 Pass/<LOD
Thiacloprid 0.200 0.100 Pass/<LOD Thiamethoxam 0.200 0.100 Pass/<LOD
Trifloxystrobin 0.200 0.100 Pass/<LOD

* Pyrethrins are reported as the sum of Jasmolin I, Cinerin I, and Pyrethrin I
** Cyfluthrins are reported as the sum of isomers Cyfluthrin I, II, III, and IV
*** Cypermethrins are reported as the sum of isomers Cypermethrin I, II, III, and IV
**** Abamectin is reported as the sum of Avermectin B1a and Avermectin B1b
***** Spinosad is reported as the sum of Spinosyn A and Spinosyn D
† Permethrin and Prallethrin are reported as the sum of cis and trans isomers
‡ MGK-264 and Spiroximine are reported as the sum of isomers I and II
MRL - Maximum Residue Limit; LOD - Limit of Detection

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Tested by Iron Laboratories

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IRON LaboratoriesPJLA

ISO/IEC 17025:2005 Accredited

Residual Solvents Analysis by
Mass Spectrometer
Testing Accreditation #: 77802 Test Certificate #: 86057-001
Client Name, Sample Details

Da Kine Extracts
Eugene, OR 97404
Sample: GSC
Type: Medical Flower
Method: FE03 HP5890-1
Test Conditions

Scale: XS205-OR1
Temp: 20.9 °C
Baro Pressure: 1003 hPa
Analyst: JCM
Technician: JCM
Sample ID#: 86057

Harvest/Process Date: 10/08/2016
Serving Size (g): 45765
Date Received: 10/05/2016
Report Issued: 10/05/2016
Sample #86057
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
1,2-Dichloroethane 2 1 Pass/<LOD 1,2-Dimethoxyethane 100 5 Pass/<LOD
1,4-dioxane 380 200 Pass/<LOD 1-Butanol 5,000 100 Pass/<LOD
1-Pentanol 5,000 100 Pass/<LOD 1-Propanol 5,000 100 Pass/<LOD
2,2-Dimethylpropane (Neopentane) 290 100 Pass/<LOD 2,2-Dimethylbutane (Hexanes) 0 0 Not Tested
2,3-Dimethylbutane (Hexanes) 0 0 Not Tested 2-Butanol 5,000 100 Pass/<LOD
2-Butanone (MEK) 5,000 50 Pass/<LOD 2-Ethoxyethanol 160 40 Pass/<LOD
2-Methylbutane (Isopentane) 5,000 50 Pass/<LOD 2-Methylpentane (Hexanes) 5,000 50 Pass/<LOD
2-Methylpropane (Isobutane) 5,000 100 Pass/<LOD 2-propanol (Isopropyl Alcohol) 5,000 50 Pass/<LOD
2-Propanone (Acetone) 50 50 Pass/<LOD 3-Methylpentane (Hexanes) 50 50 Pass/<LOD
Acetonitrile 410 100 Pass/<LOD Benzene 2 1 Pass/<LOD
Butane 5,000 100 Pass/<LOD Chloroform 2 1 Pass/<LOD
Cumene 70 35 Pass/<LOD Cyclohexane 3,880 1,000 Pass/<LOD
Dichloromethane 600 50 Pass/<LOD Dimethylsulfoxide (DMSO) 5,000 500 Pass/<LOD
Ethanol 5,000 500 Pass/<LOD Ethyl acetate 5,000 50 Pass/<LOD
Ethyl ether 5,000 500 Pass/<LOD Ethylene glycol 620 310 Pass/<LOD
Ethylene oxide 50 50 Pass/<LOD Heptane 5,000 50 Pass/<LOD
Hexane 290 50 Pass/<LOD Isopropyl acetate 5,000 50 Pass/<LOD
Methanol 3,000 500 Pass/<LOD Naptha 400 100 Pass/<LOD
N,N-Dimethylacetamide 1,090 273 Pass/<LOD N,N-Dimethylformamide (DMF) 880 500 Pass/<LOD
Pentane 5,000 50 Pass/<LOD Petroleum Ether 400 5 Pass/<LOD
Propane 5,000 100 Pass/<LOD Pyridine 200 10 Pass/<LOD
Sulfolane 160 200 Pass/<LOD Tetrahydrofuran (THF) 720 200 Pass/<LOD
Toluene 890 50 Pass/<LOD Trichloroethylene 5,000 100 Pass/<LOD
Xylenes* 2,170 50 Pass/<LOD

* Xylenes are reported as the sum of o-xylene, m-xylene, p-xylene, and ethylbenzene
MRL - Maximum Residue Limit; LOD - Limit of Detection

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Makenzie Hyman Iron laboratories Makenzie Hyman

Iron Laboratories, LLC is an ISO/IEC 17025:2005 Testing Laboratory laboratory, accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 3 of 5
IRON Laboratories

Terpene Report
Test Certificate #: 86057-001
Client Name, Sample Details

Da Kine Extracts
Eugene, OR 97404
Sample: GSC
Type: Medical Flower
Test Conditions

Sample ID#: 86057

Harvest/Process Date: 10/08/2016
Serving Size (g): 45765
Date Received: 10/05/2016
Sample #86057

Mono Terpenes

Weight Percentage Dry Matter (wt/wt%)

α-Pinene:

0.050 %

β-Ocimene:

 N/D

Camphene:

 N/D

Eucalyptol (1,8-Cineol):

 N/D

Sabinene:

 N/D

γ-Terpinene:

 N/D

Myrcene:

0.050 %

α-Terpinolene:

0.040 %

β-Pinene:

0.070 %

Linalool:

0.220 %

∆3-Carene:

 N/D

Fenchone:

 N/D

α-Terpinene:

 N/D

Fenchol:

0.270 %

Ocimene:

 N/D

Isopulegol:

 N/D

Limonene:

0.150 %

Geraniol:

 N/D

4-Cymene:

 N/D

Sequi Terpenes

Weight Percentage Dry Matter (wt/wt%)

β-Caryophyllene:

4.410 %

α-Humulene:

1.600 %

Nerolidol 1:

0.210 %

Nerolidol 2:

 N/D

Guaiol:

 N/D

Caryophyllene Oxide:

0.060 %

α-Bisabolol:

0.280 %

Other Terpenes

Total: 7.410%
N/D

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Tested by Iron Laboratories

Page 4 of 5
IRON Laboratories

Bio Analysis by
High Performance Liquid Chromatography
Test Certificate #: 86057-001
Client Name, Sample Details

Da Kine Extracts
Eugene, OR 97404
Sample: GSC
Type: Medical Flower
Method: FE04N-OR1 HPLC1100-OR1
Test Conditions

Scale: XS205-OR1
Temp: 20.9 °C
Baro Pressure: 1003 hPa
Analyst: PHJ
Technician: PHJ
Sample ID#: 86057

Harvest/Process Date: 10/08/2016
Serving Size (g): 45765
Date Received: 10/05/2016
Test Date: 10/07/2016
Sample #86057
Sample #86057 Sample #86057
Impurities: Not Detected
Molds: No Types: N/A
Pests: No Types: N/A
Anthers: No
Detritus: No
Fibers: No
Hair: No
Mature Seeds: No
Premature Seeds: No
Unidentified Foliar Spray: No
Other Impurities: No
*Moisture -

*Moisture is not part of the accredited scope of Iron Laboratories.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 5 of 5