IRON Laboratories

Marijuana Potency Analysis by
High Performance Liquid Chromatography
Test Certificate #: 85262-001
Client Name, Sample Details

Da Kine Extracts
Eugene, OR 97404
Sample: GSC
Type: Medical Compliant Flower
Method: FE04N-OR1 HPLC1100-OR1
Test Conditions

Scale: XS205-OR1
Temp: 19.2 °C
Baro Pressure: 1003 hPa
Analyst: PHJ
Technician: PHJ
Sample ID#: 85262

Harvest/Process Date: 09/13/2016
Serving Size (g): 44973
Date Received: 09/12/2016
Test Date: 09/12/2016
Sample #85262
Sample #85262 Sample #85262
Test
Compounds		 CBDA CBD CBC CBG CBN THC THCA THCV   Calc. Max Act.
Amount 1.0 N/D 0.7 0.2 0.4 10.1 65.6 0.1 CBD N/A 0%
LOQ 0.1% 0.1% 0.1% 0.1% 0.1% 0.1% 0.1% 0.1% THC 67.61751% 13%
Uncertainty† ±5% RPD ±5% RPD ±5% RPD ±5% RPD ±5% RPD ±5% RPD ±5% RPD ±5% RPD Totals: 0.0% -

LOQ = Limit of Quantitation

RPD is relative percent difference between the LCS and LCS duplicate.

%RPD = Relative Percent Difference; Min. Value = Minimum Detectable Amount, CFU = Colony Forming Units, N/D = Not Detected

Calc. Max. is the calculated sum of CBD or THC and the amount of CBD or THC derived from CBDA or THCA; respectively .These values are calculated by applying a molar correction factor of 0.877 to the CBDA or THCA value.

*** Designated tests that use the method FE-45.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

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IRON LaboratoriesPJLA

ISO/IEC 17025:2005 Accredited

Residual Solvents Analysis by
Mass Spectrometer
Testing Accreditation #: 77802 Test Certificate #: 85262-001
Client Name, Sample Details

Da Kine Extracts
Eugene, OR 97404
Sample: GSC
Type: Medical Compliant Flower
Method: FE03 HP5890-1
Test Conditions

Scale: XS205-OR1
Temp: 19.2 °C
Baro Pressure: 1003 hPa
Analyst: JCM
Technician: JCM
Sample ID#: 85262

Harvest/Process Date: 09/13/2016
Serving Size (g): 44973
Date Received: 09/12/2016
Report Issued: 09/10/2016
Sample #85262
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
1,2-Dichloroethane 2 1 Pass/<LOD 1,2-Dimethoxyethane 100 5 Pass/<LOD
1,4-dioxane 380 200 Pass/<LOD 1-Butanol 5,000 100 Pass/<LOD
1-Pentanol 5,000 100 Pass/<LOD 1-Propanol 5,000 100 Pass/<LOD
2,2-Dimethylpropane (Neopentane) 290 100 Pass/<LOD 2,2-Dimethylbutane (Hexanes) 0 0 Not Tested
2,3-Dimethylbutane (Hexanes) 0 0 Not Tested 2-Butanol 5,000 100 Pass/<LOD
2-Butanone (MEK) 5,000 50 Pass/<LOD 2-Ethoxyethanol 160 40 Pass/<LOD
2-Methylbutane (Isopentane) 5,000 50 Pass/<LOD 2-Methylpentane (Hexanes) 5,000 50 Pass/<LOD
2-Methylpropane (Isobutane) 5,000 100 Pass/<LOD 2-propanol (Isopropyl Alcohol) 5,000 50 Pass/<LOD
2-Propanone (Acetone) 50 50 Pass/<LOD 3-Methylpentane (Hexanes) 50 50 Pass/<LOD
Acetonitrile 410 100 Pass/<LOD Benzene 2 1 Pass/<LOD
Butane 5,000 100 Pass/<LOD Chloroform 2 1 Pass/<LOD
Cumene 70 35 Pass/<LOD Cyclohexane 3,880 1,000 Pass/<LOD
Dichloromethane 600 50 Pass/<LOD Dimethylsulfoxide (DMSO) 5,000 500 Pass/<LOD
Ethanol 5,000 500 Pass/<LOD Ethyl acetate 5,000 50 Pass/<LOD
Ethyl ether 5,000 500 Pass/<LOD Ethylene glycol 620 310 Pass/<LOD
Ethylene oxide 50 50 Pass/<LOD Heptane 5,000 50 Pass/<LOD
Hexane 290 50 Pass/<LOD Isopropyl acetate 5,000 50 Pass/<LOD
Methanol 3,000 500 Pass/<LOD Naptha 400 100 Pass/<LOD
N,N-Dimethylacetamide 1,090 273 Pass/<LOD N,N-Dimethylformamide (DMF) 880 500 Pass/<LOD
Pentane 5,000 50 Pass/<LOD Petroleum Ether 400 5 Pass/<LOD
Propane 5,000 100 Pass/<LOD Pyridine 200 10 Pass/<LOD
Sulfolane 160 200 Pass/<LOD Tetrahydrofuran (THF) 720 200 Pass/<LOD
Toluene 890 50 Pass/<LOD Trichloroethylene 5,000 100 Pass/<LOD
Xylenes* 2,170 50 Pass/<LOD

* Xylenes are reported as the sum of o-xylene, m-xylene, p-xylene, and ethylbenzene
MRL - Maximum Residue Limit; LOD - Limit of Detection

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Makenzie Hyman Iron laboratories Makenzie Hyman

Iron Laboratories, LLC is an ISO/IEC 17025:2005 Testing Laboratory laboratory, accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

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IRON Laboratories

Terpene Report
Test Certificate #: 85262-001
Client Name, Sample Details

Da Kine Extracts
Eugene, OR 97404
Sample: GSC
Type: Medical Compliant Flower
Test Conditions

Sample ID#: 85262

Harvest/Process Date: 09/13/2016
Serving Size (g): 44973
Date Received: 09/12/2016
Sample #85262

Mono Terpenes

Weight Percentage Dry Matter (wt/wt%)

α-Pinene:

0.068 %

β-Ocimene:

 N/D

Camphene:

0.054 %

Eucalyptol (1,8-Cineol):

 N/D

Sabinene:

0.004 %

γ-Terpinene:

0.035 %

Myrcene:

0.060 %

α-Terpinolene:

0.049 %

β-Pinene:

0.087 %

Linalool:

0.322 %

∆3-Carene:

 N/D

Fenchone:

0.025 %

α-Terpinene:

0.039 %

Fenchol:

0.343 %

Ocimene:

 N/D

Isopulegol:

 N/D

Limonene:

0.120 %

Geraniol:

0.016 %

4-Cymene:

0.040 %

Sequi Terpenes

Weight Percentage Dry Matter (wt/wt%)

β-Caryophyllene:

0.536 %

α-Humulene:

0.174 %

Nerolidol 1:

0.026 %

Nerolidol 2:

 N/D

Guaiol:

 N/D

Caryophyllene Oxide:

0.176 %

α-Bisabolol:

0.019 %

Other Terpenes

Total: 2.193%
N/D

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Tested by Iron Laboratories

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IRON Laboratories

Bio Analysis by
High Performance Liquid Chromatography
Test Certificate #: 85262-001
Client Name, Sample Details

Da Kine Extracts
Eugene, OR 97404
Sample: GSC
Type: Medical Compliant Flower
Method: FE04N-OR1 HPLC1100-OR1
Test Conditions

Scale: XS205-OR1
Temp: 19.2 °C
Baro Pressure: 1003 hPa
Analyst: PHJ
Technician: PHJ
Sample ID#: 85262

Harvest/Process Date: 09/13/2016
Serving Size (g): 44973
Date Received: 09/12/2016
Test Date: 09/12/2016
Sample #85262
Sample #85262 Sample #85262
Impurities: Not Detected
Molds: No Types: N/A
Pests: No Types: N/A
Anthers: No
Detritus: No
Fibers: No
Hair: No
Mature Seeds: No
Premature Seeds: No
Unidentified Foliar Spray: No
Other Impurities: No
*Moisture -

*Moisture is not part of the accredited scope of Iron Laboratories.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

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