IRON Laboratories

Marijuana Potency Analysis by
High Performance Liquid Chromatography
Test Certificate #: 73998-001
Client Name, Sample Details

David Cole
, MI
Sample: Dave's Test #20
License: 1234567890ABCDEFG
Type: Infused Product
Method: FE04U HPLC-UV
Test Conditions

Prepsheet ID#: HS-170213a
Scale: XS205-MI1
Temp: 23.6 °C
Baro Pressure: 982.4 hPa
Analyst: Dave
Technician: Dave
Sample ID#: 73998

Harvest/Process Date: 06/17/2016
Serving Size (g): 10
Date Received: 11/17/2015
Test Date: 11/17/2019
Sample #73998
Sample #73998 Sample #73998
Test
Compounds		 THC THCA CBD CBDA CBN CBG CBC THCV* CBDV Total
Cannabinoids*		 Total THC Total CBD Calc Max Total
Cannabinoids*
Amount (%) 0.1 15.8 N/D 1.2 0.1 0.2 0.1 3.4 N/D 20.8 13.9 1.0 18.6
Amount (mg/g) 1.0 157.5 N/D 11.6 0.6 1.9 0.8 34.1 N/D 207.5 138.6 10.2 186.5
Amount per Serving (mg) 10.0 1,575.0 N\D 116.0 6.0 19.0 8.0 341.0 N\D 2,075.0 Serving Size~ (g): 10.0
LOQ (mg/g) 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1   %Decarb. THC CBD
±%RPD 0.19 0.30 20.21 0.23 0.27 0.24 0.30 0.23 0.21 1 0

LOQ = Limit of Quantitation; %RPD = Relative Percent Deviation; %RSD = Relative Standard Deviation; N/D = Not Detected

*Designates values that are not currently included in the accredited scope of Iron Laboratories.

*** Designates tests that use the method FE-45. FE-45 is performed using AOAC 966.02 and 32.004-32.009. FE-45 has relative expanded (k=2) uncertainties of 1.098% for moisture, 1.754% for water activity for unprocessed plant materials, and 13.102% for water activity for infused products. Vitamin E acetate analysis has a relative expanded (k=2) uncertainty of 18.614%.

Total THC and CBD is the calculated sum of THC or CBD and the amount of THC or CBD derived from THCA or CBDA, respectively. These values are calculated by applying a molar correction factor of 0.877 to the THCA or the CBDA value. Calc Max Total Cannabinoids is the sum of Total THC, Total CBD, CBN, CBG, CBC, THCV, and CBDV.

%Decarb. THC and CBD refer to the percentage of THC or CBD relative to THCA or CBDA, respectively.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 1 of 11
IRON Laboratories

QC Report
Test Certificate #: 73998-001
Client Name, Sample Details

David Cole
, MI
Sample: Dave's Test #20
License: 1234567890ABCDEFG
Type: Infused Product
Method: FE04U HPLC-UV
Test Conditions

Prepsheet ID#: HS-170213a
Scale: XS205-MI1
Temp: 23.6 °C
Baro Pressure: 982.4 hPa
Analyst: Dave
Technician: Dave
Sample ID#: 73998

Harvest/Process Date: 06/17/2016
Serving Size (g): 10
Date Received: 11/17/2015
Test Date: 11/17/2019
Sample #73998
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Cannabidivarin (CBDV) N.D. 5 4.82 96.40 4.83 96.60 0.21
Cannabidiolic Acid (CBDA) N.D. 5 4.32 86.40 4.33 86.60 0.23
Cannabigerol (CBG) N.D. 5 4.25 85.00 4.26 85.20 0.24
Cannabidiol (CBD) N.D. 5 5.23 104.60 4.27 85.40 20.21
Δ9-Tetrahydrocannabivarin (THCV) N.D. 5 4.27 85.40 4.28 85.60 0.23
Cannabinol (CBN) N.D. 5 3.65 73.00 3.66 73.20 0.27
Δ9-Tetrahydrocannabinol (THC) N.D. 5 5.33 106.60 5.34 106.80 0.19
Cannabichromene (CBC) N.D. 5 3.34 66.80 3.35 67.00 0.30
Tetrahydrocannabinolic acid (THCA) N.D. 5 3.33 66.60 3.34 66.80 0.30

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 2 of 11

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-001
OLCC No. 1002158CD2E

Pesticide Analysis by
Gas Chromatography
Testing Accreditation #: 4091 Test Certificate #: 73998-001
Client Name, Sample Details

David Cole
, MI
Sample: Dave's Test #20
License: 1234567890ABCDEFG
Type: Infused Product
Method: FE03 HP5890-2
Test Conditions

Prepsheet ID#: P-170927D
Scale: XS205-MI2
Temp: 19.8 °C
Baro PE: 999.3 hPa
Analyst: DMC
Technician: HRM
Sample ID#: 73998

Harvest/Process Date: 06/17/2016
Serving Size (g): 10
Date Received: 11/17/2015
Test Date: 04/25/2018
Sample #73998
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
Aldicarb 0.400 0.100 Failed/<LOD Abamectin**** 0.500 0.100 Pass/<LOD
Acephate 0.400 0.100 Pass/<LOD Acequinocyl 2.000 0.200 Pass/<LOD
Acetamiprid 0.200 0.100 Pass/<LOD Azoxystrobin 0.200 0.100 Pass/<LOD
Bifenazate 0.200 0.100 Pass/<LOD Bifenthrin 0.200 0.100 Pass/<LOD
Boscalid 0.400 0.100 Pass/<LOD Carbaryl 0.200 0.100 Pass/<LOD
Carbofuran 0.200 0.100 Pass/<LOD Chlorantraniliprole 0.200 0.100 Pass/<LOD
Chlorfenapyr 1.000 1.000 Pass/<LOD Chlorpyrifos 0.200 0.100 Pass/<LOD
Clofentezine 0.200 0.100 Pass/<LOD Cyfluthrin** 1.000 0.500 Pass/<LOD
Cypermethrin*** 1.000 0.500 Pass/<LOD Daminozide 1.000 0.100 Pass/<LOD
DDVP (Dichlorvos) 0.100 0.100 Pass/<LOD Diazinon 0.200 0.100 Pass/<LOD
Dimethoate 0.200 0.100 Pass/<LOD Ethoprophos 0.200 0.100 Pass/<LOD
Etofenprox 0.400 0.100 Pass/<LOD Etoxazole 0.200 0.100 Pass/<LOD
Fenoxycarb 0.200 0.100 Pass/<LOD Fenpyroximate 0.400 0.100 Pass/<LOD
Fipronil 0.400 0.100 Pass/<LOD Flonicamid 1.000 0.100 Pass/<LOD
Fludioxonil 0.400 0.100 Pass/<LOD Hexythiazox 1.000 0.100 Pass/<LOD
Imazalil 0.200 0.100 Pass/<LOD Imidacloprid 0.400 0.100 Pass/<LOD
Kresoxim Methyl 0.400 0.100 Pass/<LOD Malathion 0.200 0.100 Pass/<LOD
Metalaxyl 0.200 0.100 Pass/<LOD Methiocarb 0.200 0.100 Pass/<LOD
Methomyl 0.400 0.100 Pass/<LOD Methyl Parathion 0.200 0.500 Pass/<LOD
MGK-264‡ 0.200 0.100 Pass/<LOD Myclobutanil 0.200 0.100 Pass/<LOD
Naled 0.500 0.100 Pass/<LOD Oxamyl 1.000 0.100 Pass/<LOD
Paclobutrazol 0.400 0.100 Pass/<LOD Permethrins† 0.200 0.100 Pass/<LOD
Phosmet 0.200 0.100 Pass/<LOD Piperonyl Butoxide 2.000 0.100 Pass/<LOD
Prallethrin 0.200 0.100 Pass/<LOD Propiconazole 0.400 0.100 Pass/<LOD
Propoxur 0.200 0.100 Pass/<LOD Pyrethrins* 1.000 0.100 Pass/<LOD
Pyridaben 0.200 0.100 Pass/<LOD Spinosad***** 0.200 0.100 Pass/<LOD
Spiromesifen 0.200 0.100 Pass/<LOD Spirotetramat 0.200 0.100 Pass/<LOD
Spiroxamine‡ 0.400 0.100 Pass/<LOD Tebuconazole 0.400 0.100 Pass/<LOD
Thiacloprid 0.200 0.100 Pass/<LOD Thiamethoxam 0.200 0.100 Pass/<LOD
Trifloxystrobin 0.200 0.100 Pass/<LOD

* Pyrethrins are reported as the sum of Jasmolin I, Cinerin I, and Pyrethrin I
** Cyfluthrins are reported as the sum of isomers Cyfluthrin I, II, III, and IV
*** Cypermethrins are reported as the sum of isomers Cypermethrin I, II, III, and IV
**** Abamectin is reported as the sum of Avermectin B1a and Avermectin B1b
***** Spinosad is reported as the sum of Spinosyn A and Spinosyn D
† Permethrin and Prallethrin are reported as the sum of cis and trans isomers
‡ MGK-264 and Spiroximine are reported as the sum of isomers I and II
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 2 of 11

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-001
OLCC No. 1002158CD2E

Pesticide QC Report
Testing Accreditation #: 4091 Test Certificate #: 73998-001
Client Name, Sample Details

David Cole
, MI
Sample: Dave's Test #20
License: 1234567890ABCDEFG
Type: Infused Product
Method: FE03 HP5890-2
Test Conditions

Prepsheet ID#: P-170927D
Scale: XS205-MI2
Temp: 19.8 °C
Baro PE: 999.3 hPa
Analyst: DMC
Technician: HRM
Sample ID#: 73998

Harvest/Process Date: 06/17/2016
Serving Size (g): 10
Date Received: 11/17/2015
Test Date: 04/25/2018
Sample #73998
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS recovery% MSD recovery% Relative Percent Difference (%) QC Flag
Acephate nan nan
Acequinocyl nan nan
Acetamiprid nan nan
Aldicarb nan nan
Avermectin B1a nan nan
Azoxystrobin nan nan
Bifenazate nan nan
Bifenthrin nan nan
Boscalid nan nan
Carbaryl nan nan
Carbofuran nan nan
Chlorantraniliprole nan nan
Chlorfenapyr nan nan
Chlorpyriphos nan nan
Clofentezine nan nan
Cyfluthrin nan nan
Cypermethrin nan nan
Daminoside nan nan
Diazanon nan nan
Dichlorvos nan nan
Dimethoate nan nan
Ethoprophos nan nan
Etofenprox nan nan
Etoxazole nan nan
Fenoxycarb nan nan
Fenpyroximate nan nan
Fipronil nan nan
Flonicamid nan nan
Fludioxonil nan nan
Hexythiazox nan nan
Imazalil nan nan
Imidacloprid nan nan
Kresoxim-methyl nan nan
Malathion nan nan
Metalaxyl nan nan
Methiocarb nan nan
Methomyl nan nan
MGK-264 nan nan
Myclobutanil nan nan
Naled (dibrom) nan nan
Oxamyl nan nan
Paclobutrazol nan nan
Parathion-methyl nan nan
Permethrins nan nan
Phosmet nan nan
Piperonyl butoxide nan nan
Prallethrin nan nan
Propiconazole nan nan
Propoxur nan nan
Pyrethrin nan nan
Pyridaben nan nan
SpinosynA nan nan
SpinosynD nan nan
Spiromesifen nan nan
Spirotetramat nan nan
Spiroxamine nan nan
Tebuconazole nan nan
Thiacloprid nan nan
Thiamethoxam nan nan
Trifloxystrobin nan nan

N.D. = Not Detected

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 30%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (60-120%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 3 of 11

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-001
OLCC No. 1002158CD2E

Residual Solvents Analysis by
Gas Chromatography
Testing Accreditation #: 4091 Test Certificate #: 73998-001
Client Name, Sample Details

David Cole
, MI
Sample: Dave's Test #20
License: 1234567890ABCDEFG
Type: Infused Product
Method: FE04U12 HPLC-UV
Test Conditions

Prepsheet ID#: PS170922b
Scale: XS205-MI2
Temp: 21.1 °C
Baro PE: 1002 hPa
Analyst: DMC
Technician: JER
Sample ID#: 73998

Harvest/Process Date: 06/17/2016
Serving Size (g): 10
Date Received: 11/17/2015
Test Date: 04/25/2018
Sample #73998
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
1,2-Dichloroethane 2 1 Pass/<LOD 1,2-Dimethoxyethane 100 5 Pass/<LOD
1,4-dioxane 380 200 Pass/<LOD 1-Butanol 5,000 100 Pass/<LOD
1-Pentanol 5,000 100 Pass/<LOD 1-Propanol 5,000 100 Pass/<LOD
2,2-Dimethylpropane (Neopentane) 5,000 100 Pass/<LOD 2,2-Dimethylbutane (Hexanes) 290 100 Pass/<LOD
2,3-Dimethylbutane (Hexanes) 290 100 Pass/<LOD 2-Butanol 5,000 100 Pass/<LOD
2-Butanone (MEK) 5,000 50 Pass/<LOD 2-Ethoxyethanol 160 40 Pass/<LOD
2-Methylbutane (Isopentane) 5,000 50 Pass/<LOD 2-Methylpentane (Hexanes) 290 50 Pass/<LOD
2-Methylpropane (Isobutane) 5,000 100 Pass/<LOD 2-propanol (Isopropyl Alcohol) 5,000 50 Pass/<LOD
2-Propanone (Acetone) 5,000 50 Pass/<LOD 3-Methylpentane (Hexanes) 290 50 Pass/<LOD
Acetonitrile 410 100 Pass/<LOD Benzene 2 1 Pass/<LOD
Butane 5,000 100 Pass/<LOD Chloroform 2 1 Pass/<LOD
Cumene 70 35 Pass/<LOD Cyclohexane 3,880 1,000 Pass/<LOD
Dichloromethane 600 150 Pass/<LOD Dimethylsulfoxide (DMSO) 5,000 500 Pass/<LOD
Ethanol 5,000 500 Pass/<LOD Ethyl acetate 5,000 50 Pass/<LOD
Ethyl ether 5,000 500 Pass/<LOD Ethylene glycol 620 310 Pass/<LOD
Ethylene oxide 50 50 Pass/<LOD Heptane 5,000 50 Pass/<LOD
Hexane 290 50 Pass/<LOD Isopropyl acetate 5,000 50 Pass/<LOD
Methanol 3,000 500 Pass/<LOD Naptha 400 100 Pass/<LOD
N,N-Dimethylacetamide 1,090 273 Pass/<LOD N,N-Dimethylformamide (DMF) 880 500 Pass/<LOD
Pentane 5,000 50 Pass/<LOD Petroleum Ether 400 5 Pass/<LOD
Propane 5,000 100 Pass/<LOD Pyridine 200 10 Pass/<LOD
Sulfolane 160 200 Pass/<LOD Tetrahydrofuran (THF) 720 200 Pass/<LOD
Toluene 890 50 Pass/<LOD Trichloroethylene 5,000 100 Pass/<LOD
Xylenes* 2,170 50 Pass/<LOD

* Xylenes are reported as the sum of o-xylene, m-xylene, p-xylene, and ethylbenzene
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 4 of 11

ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-001
OLCC No. 1002158CD2E

Residual Solvents QC Report
Testing Accreditation #: 4091 Test Certificate #: 73998-001
Client Name, Sample Details

David Cole
, MI
Sample: Dave's Test #20
License: 1234567890ABCDEFG
Type: Infused Product
Method: FE04U12 HPLC-UV
Test Conditions

Prepsheet ID#: PS170922b
Scale: XS205-MI2
Temp: 21.1 °C
Baro PE: 1002 hPa
Analyst: DMC
Technician: JER
Sample ID#: 73998

Harvest/Process Date: 06/17/2016
Serving Size (g): 10
Date Received: 11/17/2015
Test Date: 04/25/2018
Sample #73998
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS Recovery (%) MSD Recovery (%) Relative Percent Difference (%) QC Flag
1,2-Dichloroethane nan nan
n-Propane nan nan
Isobutane nan nan
Methanol nan nan
n-Butane nan nan
2,2-Dimethylpropane nan nan
Ethanol nan nan
Isopentane nan nan
Acetonitrile nan nan
Diethyl ether nan nan
2-propanone nan nan
2-propanol nan nan
n-Pentane nan nan
2,2-Dimethylbutane nan nan
2,3-Dimethylbutane nan nan
Methylene chloride nan nan
2-Methylpentane nan nan
3-Methylpentane nan nan
2-Butanol 0.00 0.00 0.00
n-Hexane nan nan
Ethyl acetate nan nan
Tetrahydrofuran 0.00 0.00 0.00
Trichloroethylene nan nan
Isopropyl acetate 0.00 0.00 0.00
Benzene nan nan
Chloroform nan nan
Cyclohexane 0.00 0.00 0.00
Ethylene glycol 0.00 0.00 0.00
Heptane 0.00 0.00 0.00
2-Ethoxyethanol 0.00 0.00 0.00
1,4-Dioxane 0.00 0.00 0.00
Pyridine 0.00 0.00 0.00
Toluene 0.00 0.00 0.00
Chlorobenzene 0.00 0.00 0.00
Ethylbenzene 0.00 0.00 0.00
m-Xylene/p-Xylene 0.00 0.00 0.00
o-Xylene 0.00 0.00 0.00
Cumene 0.00 0.00 0.00
Ethylene oxide 0.00 0.00 0.00

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

N.D. = Not Detected

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 5 of 11
IRON Laboratories

Homogeneity Report by
Gas Chromatography
Test Certificate #: 73998-001
Client Name, Sample Details

David Cole
, MI
Sample: Dave's Test #20
License: 1234567890ABCDEFG
Type: Infused Product
Sample ID#: 73998

Harvest/Process Date: 06/17/2016
Serving Size (g): 10
Date Received: 11/17/2015
Sample #73998
Increments Tested (mg/g) TOTAL THC TOTAL CBD THC THCA THCV CBD CBC CBDA CBDV CBG CBN
Increment 1 2.0 2.0 2.0 N.D. 1.0 2.0 2.0 N.D. N.D. 1.0 12.0
Average Value 1.00 1.00 1.00 N.D. 0.50 1.00 1.00 N.D. N.D. 0.50 6.00
Max Value 2.00 2.00 2.00 N.D. 1.00 2.00 2.00 N.D. N.D. 1.00 12.00
Min Value 2.00 2.00 2.00 N.D. 1.00 2.00 2.00 N.D. N.D. 1.00 12.00
Relative Percent Difference (RPD) ±200.00 ±200.00 ±200.00 N.D. ±200.00 ±200.00 ±200.00 N.D. N.D. ±200.00 ±200.00
Average Cannabinoids Per Package N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D.
Average Cannabinoids Per Serving 10.00 10.00 10.00 N.D. 5.00 10.00 10.00 N.D. N.D. 5.00 60.00
Max Concentration Per Serving (THC)   Fail
Max Concentration Per Package (THC)   Fail
Relative Percent Difference (RPD)   Fail
Control Study   Yes, ABCDEFG
Field Duplicate   Fail

N.D. = Not Detected, Min = Minimum, Max = Maximum

RPD is the relative percent difference between increment 1 and increment 2.

RSD is the relative standard deviation between all increments tested.

Total THC and CBD is the calculated sum of CBD or THC and the amount of CBD or THC derived from CBDA or THCA, respectively. These values are calculated by adding a molar correction factor of 0.877 to the CBDA or THCA value.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Tested by Iron Laboratories

Page 6 of 11
IRON Laboratories

Terpene Report
Test Certificate #: 73998-001
Client Name, Sample Details

David Cole
, MI
Sample: Dave's Test #20
License: 1234567890ABCDEFG
Type: Infused Product
Test Conditions

Sample ID#: 73998

Harvest/Process Date: 06/17/2016
Serving Size (g): 10
Date Received: 11/17/2015
Sample #73998

Mono Terpenes

Weight Percentage Dry Matter (wt/wt%)

α-Pinene:

5.000 %

β-Ocimene:

 N/D

Camphene:

 N/D

Eucalyptol (1,8-Cineol):

 N/D

Sabinene:

 N/D

γ-Terpinene:

 N/D

Myrcene:

 N/D

α-Terpinolene:

 N/D

β-Pinene:

 N/D

Linalool:

 N/D

∆3-Carene:

 N/D

Fenchone:

 N/D

α-Terpinene:

 N/D

Fenchol:

 N/D

Ocimene:

 N/D

Isopulegol:

 N/D

Limonene:

 N/D

Geraniol:

 N/D

4-Cymene:

 N/D

Sequi Terpenes

Weight Percentage Dry Matter (wt/wt%)

β-Caryophyllene:

 N/D

α-Humulene:

 N/D

Nerolidol 1:

 N/D

Nerolidol 2:

 N/D

Guaiol:

 N/D

Caryophyllene Oxide:

 N/D

α-Bisabolol:

 N/D

Other Terpenes

Total: 5.000%
N/D

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Tested by Iron Laboratories

Page 7 of 11
IRON Laboratories

Terpene Report
Test Certificate #: 73998-001
Client Name, Sample Details

David Cole
, MI
Sample: Dave's Test #20
License: 1234567890ABCDEFG
Type: Infused Product

Test Conditions

Sample ID#: 73998

Harvest/Process Date: 06/17/2016
Serving Size (g): 10
Date Received: 11/17/2015

Sample #73998
Sample #73998
  • α-Pinene (5.00%)
  • β-Ocimene (9.00%)
  • Camphene (4.00%)
  • Eucalyptol (1,8-Cineol) (7.00%)
  • Sabinene (3.00%)
  • γ-Terpinene (5.00%)
  • Myrcene (2.00%)
  • α-Terpinolene (4.00%)
  • β-Pinene (1.00%)
  • Linalool (0.00%)
  • ∆3-Carene (1.00%)
  • Fenchone (0.00%)
  • α-Terpinene (2.00%)
  • endo-Fenchol (0.00%)
  • α-Ocimene (5.00%)
  • Isopulegol (0.00%)
  • Limonene (7.00%)
  • Geraniol (0.00%)
  • p-Cymene (8.00%)
  • β-Caryophyllene (0.00%)
  • α-Humulene (0.00%)
  • Nerolidol 1 (cis) (0.00%)
  • Nerolidol 2 (trans) (0.00%)
  • Guaiol (0.00%)
  • Caryophyllene Oxide (0.00%)
  • α-Bisabolol (0.00%)
  • α-Phellandrene (0.00%)
  • α-Terpineol (0.00%)
  • Valenence (0.00%)

Total: 63.000%

Predominant Terpenes

9.00%   β-Ocimene Citrus, tropical, woody, green 8.00%   p-Cymene Fresh, citrus, woody, spicy
7.00%   Eucalyptol (1,8-Cineol) Eucalyptus, herbal, camphor 7.00%   Limonene Citrus, orange, sweet
5.00%   α-Pinene Fresh camphor, sweet, pine, earthy, woody 5.00%   α-Ocimene Fruity, floral, laundered cloth

Value in parenthesis indicates percentage of terpene present in the total sample (weight percentage, wt/wt%).
Value in doughnut slice indicates individual terpene abundance with respect to the total terpenes detected.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Tested by Iron Laboratories

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ORELAPIRON LaboratoriesNELAP Accredited Laboratory

ORELAP Cert No. 4092-001
OLCC No. 1002158CD2E

Microbiology Analysis
Testing Accreditation #: 4091 Test Certificate #: 73998-001
Client Name, Sample Details

David Cole
, MI
Sample: Dave's Test #20
License: 1234567890ABCDEFG
Type: Infused Product
***Water Activity:
***Moisture: %
Test Conditions

Scale: XS205-MI2
Temp: 21.3 °C
Baro Pressure: 987.9 hPa
Analyst: DMC
Technician: DMC
Sample ID#: 73998

Harvest/Process Date: 06/17/2016
Serving Size (g): 10
Date Received: 11/17/2015
Test Date: 04/25/2018
Sample #73998
Test Method MCFU (CFU/g) LOD (CFU/g) Status (CFU/g)
Total Aerobic FE-45 2.8 1.3 Pass/4.0
Yeast & Mold FE-52 2.3 0.2 Pass/2.0
E. Coli FE-37 1.0 0.3 Failed/1.0
Salmonella FE-37 1.2 0.5 Pass/3.0
Aspergillus spp. Not Tested N/A 0.0 Not Tested

Test Method MRL (µg/g) LOD (µg/g) Status (µg/g)
Total Aflatoxin (B1, B2, G1, and G2) Not Tested 0.02 0.02 Pass/<0.02µg/g
REFERENCE AHPA NSF/ANSI USP
Material Dried, unprocessed herbs Botanical ingredient, non-extract Dried botanicals
Total combined yeast and mold count (limits) in colony forming units / gram (cfu/g) 100000 cfu/g 100000 cfu/g 1000 cfu/g

AHPA - American Herbal Products Association, Guidance on Microbiology & Mycotoxins, 2012
NSF/ANSI - NSF International Standard / American National Standard NSF/ANSI 173-2012
USP - United States Pharmacopeial Convention, USP-NF 37-32, 2014

TNTC = Too Numerous To Count. Maximum Colony Forming Units (MCFU) represents the minimum value that a test would need to achieve in order to be considered a failed result (if applicable). LOD is the Limit of Detection for the method. CFU/g = Colony Forming Units per gram. Aspergillus spp. consists of A. flavus, A. fumigatus, A. niger, and A. terreus.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

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IRON Laboratories

Bio Analysis by
High Performance Liquid Chromatography
Test Certificate #: 73998-001
Client Name, Sample Details

David Cole
, MI
Sample: Dave's Test #20
License: 1234567890ABCDEFG
Type: Infused Product
Method: FE04 HPLC1100-1
Test Conditions

Scale: AB-200
Temp: 20 °C
Baro Pressure: 990 hPa
Analyst: Dave
Technician: Dave
Sample ID#: 73998

Harvest/Process Date: 06/17/2016
Serving Size (g): 10
Date Received: 11/17/2015
Test Date: 11/17/2015
Sample #73998
Sample #73998 Sample #73998
Severity Rating
Mold and Mildew 3 Pass
Mites (not Russet) 1 Pass
Russet Mites ≤1% Pass
Thrips 3 Pass
Aphids 3 Pass
Other Pests ≤5% Pass
Other Organic Matter 1 Pass
Inorganic Matter 7 Pass
Total Organic Foreign Matter ≤5% Pass
Inorganic Foreign Matter ≤5% Fail
Stem Material ≤5% Pass
Severity Rating Key
Correlating %FM ≤2% FM >2% FM
Severity Rating 0 None 1 Mild 2 Moderate 3 Severe Units
Mold and Mildew <2 2 3 4+ Locations/g
Mites (not russet) <1 1-5 6-10 11+ Amount/g
Russet Mites <1 1-10 11-50 51+ Amount/g
Thrips <1 1-3 4-5 6+ Amount/g
Aphids <1 1 2-4 5+ Amount/g
Other Pests <1 1-5 6-10 11+ Amount/g
Other Organic Matter <1 1-5 6-10 11+ Amount/g
Inorganic Matter 0 — — >0 Amount/g

In compliance with the MMFLA regulation, the action limits for foreign matter are as follows; no more that 2% organic matter, 5% stem material, and no presence of inorganic matter. Percent foreign contamination is based off of total surface area.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

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IRON LaboratoriesPJLA

ISO/IEC 17025:2005 Accredited

Heavy Metals Analysis
Testing Accreditation #: 77802 Test Certificate #: 73998-001
Client Name, Sample Details

David Cole
, MI
Sample: Dave's Test #20
License: 1234567890ABCDEFG
Type: Infused Product
Method: FE03 HP5890-1
Test Conditions

Analyst: Dave
Technician: Dave
Sample ID#: 73998

Harvest/Process Date: 06/17/2016
Serving Size (g): 10
Date Received: 11/17/2015
Test Date: 02/19/2020
Valid Through: 02/19/2021
Report Issued: 02/19/2020
Sample #73998
Sample #73998 Sample #73998
Test Compound MRL (PPM) LOD (PPM) Status (PPM)
Arsenic 0.24 0.5 Pass/<LOD
Copper 0.26 0.5 Pass/<LOD
Cadmium 0.33 0.5 Pass/<LOD
Chromium 0.26 0.5 Pass/<LOD
Lead 0.12 0.5 Pass/<LOD
Mercury 0.27 0.5 Pass/<LOD
Nickel 0.33 0.5 Pass/<LOD

MRL - Maximum Residue Limit; LOD - Limit of Detection

Tested in accordance with the information provided in the Medical Marihuana Facilities Licensing Act (MMFLA) and the Emergency Rules published December 4, 2017

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Iron Laboratories, LLC is an ISO/IEC 17025:2005 Testing Laboratory laboratory, accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

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