IRON Laboratories

Marihuana Potency Analysis by
Mass Spectrometer
Test Certificate #: 70999-001
Client Name, Sample Details

Superior Extracts
Ironwood, MI 49938
Sample: Ultra Sour Shatter RSA
Type: Medical Compliant Flower
Method: FE03 HP5890-2
Test Conditions

Scale: Balance AB-200
Temp: 24.7 °C
Baro Pressure: 979 hPa
Analyst: JER
Technician: JER
Sample ID#: 70999

Harvest/Process Date: 08/28/2015
Serving Size (g): 31460
Date Received: 08/28/2015
Test Date: 08/28/2015
Valid Through: 08/28/2016
Report Issued: 08/28/2015
Sample #70999
Sample #70999 Sample #70999
Test
Compounds		 CBDV THCV CBC CBD Δ8 THC Δ9 THC CBG CBN TOTAL
Amount N/D N/D N/D N/D N/D N/D N/D N/D 0.0%
Min. Value 0.1% 0.1% 0.1% 0.1% 0.1% 0.1% 0.1% 0.1% -
Uncertainty† ±5% RSD ±5% RSD ±5% RSD ±5% RSD ±5% RSD ±5% RSD ±5% RSD ±5% RSD -

RPD is relative percent difference between the LCS and LCS duplicate.

%RPD = Relative Percent Difference; N/D = Not Detected

*** Designated tests that use the method FE-45.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Makenzie Hyman Iron laboratories Makenzie Hyman

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

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IRON LaboratoriesPJLA

ISO/IEC 17025:2005 Accredited

Residual Solvents Analysis by
Mass Spectrometer
Testing Accreditation #: 77802 Test Certificate #: 70999-001
Client Name, Sample Details

Superior Extracts
Ironwood, MI 49938
Sample: Ultra Sour Shatter RSA
Type: Medical Compliant Flower
Method: FE03 HP5890-1
Test Conditions

Scale: Balance AB-200
Temp: 24.7 °C
Baro Pressure: 979 hPa
Analyst: JCM
Technician: JCM
Sample ID#: 70999

Harvest/Process Date: 08/28/2015
Serving Size (g): 31460
Date Received: 08/28/2015
Report Issued: 08/28/2015
Sample #70999
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
1,2-Dichloroethane 2 1 Pass/<LOD 1,2-Dimethoxyethane 100 5 Pass/<LOD
1,4-dioxane 380 200 Pass/<LOD 1-Butanol 5,000 100 Pass/<LOD
1-Pentanol 5,000 100 Pass/<LOD 1-Propanol 5,000 100 Pass/<LOD
2,2-Dimethylpropane (Neopentane) 290 100 Pass/<LOD 2,2-Dimethylbutane (Hexanes) 0 0 Not Tested
2,3-Dimethylbutane (Hexanes) 0 0 Not Tested 2-Butanol 5,000 100 Pass/<LOD
2-Butanone (MEK) 5,000 50 Pass/<LOD 2-Ethoxyethanol 160 40 Pass/<LOD
2-Methylbutane (Isopentane) 5,000 50 Pass/<LOD 2-Methylpentane (Hexanes) 5,000 50 Pass/<LOD
2-Methylpropane (Isobutane) 5,000 100 Pass/<LOD 2-propanol (Isopropyl Alcohol) 5,000 50 Pass/<LOD
2-Propanone (Acetone) 50 50 Pass/<LOD 3-Methylpentane (Hexanes) 50 50 Pass/<LOD
Acetonitrile 410 100 Pass/<LOD Benzene 2 1 Pass/<LOD
Butane 5,000 100 Pass/<LOD Chloroform 2 1 Pass/<LOD
Cumene 70 35 Pass/<LOD Cyclohexane 3,880 1,000 Pass/<LOD
Dichloromethane 600 50 Pass/<LOD Dimethylsulfoxide (DMSO) 5,000 500 Pass/<LOD
Ethanol 5,000 500 Pass/<LOD Ethyl acetate 5,000 50 Pass/<LOD
Ethyl ether 5,000 500 Pass/<LOD Ethylene glycol 620 310 Pass/<LOD
Ethylene oxide 50 50 Pass/<LOD Heptane 5,000 50 Pass/<LOD
Hexane 290 50 Pass/<LOD Isopropyl acetate 5,000 50 Pass/<LOD
Methanol 3,000 500 Pass/<LOD Naptha 400 100 Pass/<LOD
N,N-Dimethylacetamide 1,090 273 Pass/<LOD N,N-Dimethylformamide (DMF) 880 500 Pass/<LOD
Pentane 5,000 50 Pass/<LOD Petroleum Ether 400 5 Pass/<LOD
Propane 5,000 100 Pass/<LOD Pyridine 200 10 Pass/<LOD
Sulfolane 160 200 Pass/<LOD Tetrahydrofuran (THF) 720 200 Pass/<LOD
Toluene 890 50 Pass/<LOD Trichloroethylene 5,000 100 Pass/<LOD
Xylenes* 2,170 50 Pass/<LOD

* Xylenes are reported as the sum of o-xylene, m-xylene, p-xylene, and ethylbenzene
MRL - Maximum Residue Limit; LOD - Limit of Detection

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Makenzie Hyman Iron laboratories Makenzie Hyman

Iron Laboratories, LLC is an ISO/IEC 17025:2005 Testing Laboratory laboratory, accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

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IRON Laboratories

Bio Analysis by
Mass Spectrometer
Test Certificate #: 70999-001
Client Name, Sample Details

Superior Extracts
Ironwood, MI 49938
Sample: Ultra Sour Shatter RSA
Type: Medical Compliant Flower
Method: FE03 HP5890-2
Test Conditions

Scale: Balance AB-200
Temp: 24.7 °C
Baro Pressure: 979 hPa
Analyst: JER
Technician: JER
Sample ID#: 70999

Harvest/Process Date: 08/28/2015
Serving Size (g): 31460
Date Received: 08/28/2015
Test Date: 08/28/2015
Valid Through: 08/28/2016
Report Issued: 08/28/2015
Sample #70999
Sample #70999 Sample #70999
Impurities: Not Detected
Molds: No Types: N/A
Pests: No Types: N/A
Anthers: No
Detritus: No
Fibers: No
Hair: No
Mature Seeds: No
Premature Seeds: No
Unidentified Foliar Spray: No
Other Impurities: No
*Moisture -

*Moisture is not part of the accredited scope of Iron Laboratories.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

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