IRON Laboratories

Marihuana Potency Analysis by
Gas Chromatography
Test Certificate #: 22-001
Client Name, Sample Details

Ann Arbor Health Collective
Ann Arbor, MI 48108
Sample: Skunk
Type: Flower
Method: FE03 HP5890-1
Test Conditions

Sample ID#: 22

Harvest/Process Date: 03/14/2012
Date Received: 03/14/2012
Test Date: 03/14/2012
Valid Through: 03/14/2013
Report Issued: 03/14/2012
Sample #22
Test
Compounds		 CBDV THCV CBC CBD Δ8 THC Δ9 THC CBG CBN TOTAL
Amount N/D N/D 0.3 0.3 0.1 20.4 2.4 0.2 23.6%
Min. Value 0.1% 0.1% 0.1% 0.1% 0.1% 0.1% 0.1% 0.1% -
Uncertainty† ±5% RSD ±5% RSD ±5% RSD ±5% RSD ±5% RSD ±5% RSD ±5% RSD ±5% RSD -

RPD is relative percent difference between the LCS and LCS duplicate.

%RPD = Relative Percent Difference; N/D = Not Detected

*** Designated tests that use the method FE-45.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Makenzie Hyman Iron laboratories Makenzie Hyman

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 1 of 8
IRON Laboratories

Residual Solvents Analysis by
Mass Spectrometer
Test Certificate #: 22-001
Client Name, Sample Details

Ann Arbor Health Collective
Ann Arbor, MI 48108
Sample: Skunk
Type: Flower
Method: SOP FE-44-OR3
Test Conditions

Prepsheet ID#: MIHS190709b
Scale: XS205-MI2
Temp: 23.7 °C
Baro PE: 982 hPa
Analyst: JRT
Technician: JRT
Sample ID#: 22

Harvest/Process Date: 03/14/2012
Date Received: 03/14/2012
Test Date: 07/09/2019
Valid Through: 07/08/2020
Report Issued: 07/11/2019
Sample #22
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
1,2-Dichloroethane 5 1 Pass/<LOD 1,2-Dimethoxyethane 5,000 200 Pass/<LOD
1,4-dioxane 5,000 200 Pass/<LOD 1-Butanol 5,000 200 Pass/<LOD
1-Pentanol 5,000 200 Pass/<LOD 1-Propanol 5,000 100 Pass/<LOD
2,2-Dimethylpropane (Neopentane) 5,000 50 Pass/<LOD 2,2-Dimethylbutane (Hexanes) 290 50 Pass/<LOD
2,3-Dimethylbutane (Hexanes) 290 50 Pass/<LOD 2-Butanol 5,000 200 Pass/<LOD
2-Butanone (MEK) 5,000 200 Pass/<LOD 2-Ethoxyethanol 5,000 200 Pass/<LOD
2-Methylbutane (Isopentane) 5,000 50 Pass/<LOD 2-Methylpentane (Hexanes) 290 50 Pass/<LOD
2-Methylpropane (Isobutane) 5,000 50 Pass/<LOD 2-propanol (Isopropyl Alcohol) 5,000 50 Pass/<LOD
2-Propanone (Acetone) 5,000 50 Pass/<LOD 3-Methylpentane (Hexanes) 290 50 Pass/<LOD
Acetonitrile 410 50 Pass/<LOD Benzene 2 2 Pass/<LOD
Butane 5,000 50 Pass/<LOD Chloroform 60 50 Pass/<LOD
Cumene 5,000 1,000 Pass/<LOD Cyclohexane 290 50 Pass/<LOD
Dichloromethane 600 50 Pass/<LOD Dimethylsulfoxide (DMSO) 5,000 500 Pass/<LOD
Ethanol 5,000 500 Pass/<LOD Ethyl acetate 5,000 50 Pass/<LOD
Ethyl ether 5,000 100 Pass/<LOD Ethylene glycol 5,000 500 Pass/<LOD
Ethylene oxide 50 50 Pass/<LOD Heptane 5,000 50 Pass/<LOD
Hexane 290 50 Pass/<LOD Isopropyl acetate 5,000 200 Pass/<LOD
Methanol 3,000 200 Pass/<LOD Naptha 400 100 Pass/<LOD
N,N-Dimethylacetamide 5,000 500 Pass/<LOD N,N-Dimethylformamide (DMF) 5,000 500 Pass/<LOD
Pentane 5,000 50 Pass/<LOD Petroleum Ether 400 100 Pass/<LOD
Propane 5,000 50 Pass/<LOD Pyridine 5,000 200 Pass/<LOD
Sulfolane 5,000 200 Pass/<LOD Tetrahydrofuran (THF) 5,000 200 Pass/<LOD
Toluene 890 50 Pass/<LOD Trichloroethylene 80 5 Pass/<LOD
Xylenes* 2,170 50 Pass/<LOD

Total Butanes = 0 ug/g (PASS); Total Pentanes = 0 ug/g (PASS); Total Hexanes = 0 ug/g (PASS)

* Xylenes are reported as the sum of o-xylene, m-xylene, p-xylene, and ethylbenzene
MRL - Maximum Residue Limit; LOD - Limit of Detection

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
MEH QM Iron laboratories MEH QM

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 2 of 8
IRON Laboratories

Residual Solvents QC Report
Test Certificate #: 22-001
Client Name, Sample Details

Ann Arbor Health Collective
Ann Arbor, MI 48108
Sample: Skunk
Type: Flower
Method: SOP FE-44-OR3
Test Conditions

Prepsheet ID#: MIHS190709b
Scale: XS205-MI2
Temp: 23.7 °C
Baro PE: 982 hPa
Analyst: JRT
Technician: JRT
Sample ID#: 22

Harvest/Process Date: 03/14/2012
Date Received: 03/14/2012
Test Date: 07/09/2019
Valid Through: 07/08/2020
Report Issued: 07/11/2019
Sample #22
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS Recovery (%) MSD Recovery (%) Relative Percent Difference (%) QC Flag
1,2-Dichloroethane N.D. 250 226 228 90.40 91.20 0.88
n-Propane N.D. 250 317 219 126.80 87.60 36.57 Q
Isobutane N.D. 250 236 242 94.40 96.80 2.51
Methanol N.D. 250 179 175 71.60 70.00 2.26 LR
n-Butane N.D. 250 359 242 143.60 96.80 38.94 HRQ
2,2-Dimethylpropane N.D. 250 230 235 92.00 94.00 2.15
Ethanol N.D. 250 232 222 92.80 88.80 4.41
Isopentane N.D. 250 237 243 94.80 97.20 2.50
Acetonitrile N.D. 250 219 222 87.60 88.80 1.36
Diethyl ether N.D. 250 227 236 90.80 94.40 3.89
2-propanone N.D. 250 206 239 82.40 95.60 14.83
2-propanol N.D. 250 229 241 91.60 96.40 5.11
n-Pentane N.D. 250 948 236 379.20 94.40 120.27 HRQ
2,2-Dimethylbutane N.D. 250 235 236 94.00 94.40 0.42
2,3-Dimethylbutane N.D. 250 231 224 92.40 89.60 3.08
Methylene chloride N.D. 250 229 225 91.60 90.00 1.76
2-Methylpentane N.D. 250 242 248 96.80 99.20 2.45
3-Methylpentane N.D. 250 245 246 98.00 98.40 0.41
2-Butanol N.D. 0 0 0 0.00 0.00 0.00
n-Hexane N.D. 250 394 246 157.60 98.40 46.25 HRQ
Ethyl acetate N.D. 250 262 237 104.80 94.80 10.02
Tetrahydrofuran N.D. 0 0 0 0.00 0.00 0.00
Trichloroethylene N.D. 25 25 25 100.00 100.00 0.00
Isopropyl acetate N.D. 0 0 0 0.00 0.00 0.00
Benzene N.D. 25 25 25 100.00 100.00 0.00
Chloroform N.D. 25 24 23 96.00 92.00 4.26
Cyclohexane N.D. 0 0 0 0.00 0.00 0.00
Ethylene glycol N.D. 0 0 0 0.00 0.00 0.00
Heptane N.D. 250 1472 254 588.80 101.60 141.14 HRQ
2-Ethoxyethanol N.D. 0 0 0 0.00 0.00 0.00
1,4-Dioxane N.D. 0 0 0 0.00 0.00 0.00
Pyridine N.D. 0 0 0 0.00 0.00 0.00
Toluene N.D. 250 258 259 103.20 103.60 0.39
Chlorobenzene 250 226 228 90.40 91.20 0.88
Ethylbenzene N.D. 0 0 0 0.00 0.00 0.00
m-Xylene/p-Xylene N.D. 125 141 138 112.80 110.40 2.15
o-Xylene N.D. 125 140 138 112.00 110.40 1.44
Cumene N.D. 0 0 0 0.00 0.00 0.00
Ethylene oxide N.D. 0 0 0 0.00 0.00 0.00

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

N.D. = Not Detected

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
MEH QM Iron laboratories MEH QM

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 3 of 8

IRON Laboratories     PJLA

ISO/IEC 17025:2017 Accredited

Residual Solvents Analysis by
Mass Spectrometer
Testing Accreditation #: 77802 Test Certificate #: 22-001
Client Name, Sample Details

Ann Arbor Health Collective
Ann Arbor, MI 48108
Sample: Skunk
Type: Flower
Method: SOP FE-44-MI
Test Conditions

Prepsheet ID#: MIHS210211a
Scale: XS205-MI2
Temp: 21.2 °C
Baro PE: 986 hPa
Analyst: KEB
Technician: ANJ
Sample ID#: 22

Harvest/Process Date: 03/14/2012
Date Received: 03/14/2012
Test Date: 02/11/2021
Valid Through: 02/11/2022
Report Issued: 02/12/2021
Sample #22
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
1,2-Dichloroethane 2 1 Pass/<LOD 1,2-Dimethoxyethane 5,000 250 Not Tested
1,4-dioxane 5,000 25 Not Tested 1-Butanol 5,000 250 Not Tested
1-Pentanol 5,000 250 Not Tested 1-Propanol 5,000 250 Not Tested
2,2-Dimethylpropane (Neopentane) 750 25 Pass/<LOD 2,2-Dimethylbutane (Hexanes) 50 25 Pass/<LOD
2,3-Dimethylbutane (Hexanes) 50 25 Pass/<LOD 2-Butanol 5,000 25 Not Tested
2-Butanone (MEK) 5,000 250 Not Tested 2-Ethoxyethanol 5,000 25 Not Tested
2-Methylbutane (Isopentane) 750 25 Pass/<LOD 2-Methylpentane (Hexanes) 50 25 Pass/<LOD
2-Methylpropane (Isobutane) 800 25 Pass/<LOD 2-propanol (Isopropyl Alcohol) 500 25 Pass/<LOD
2-Propanone (Acetone) 750 25 Pass/<LOD 3-Methylpentane (Hexanes) 50 25 Pass/<LOD
Acetonitrile 60 30 Pass/<LOD Benzene 1 1 Pass/<LOD
Butane 800 25 Pass/<LOD Chloroform 2 1 Pass/<LOD
Cumene 5,000 25 Not Tested Cyclohexane 50 25 Not Tested
Dichloromethane 125 25 Pass/<LOD Dimethylsulfoxide (DMSO) 5,000 250 Not Tested
Ethanol 1,000 50 Pass/<LOD Ethyl acetate 400 25 Pass/<LOD
Ethyl ether 500 25 Pass/<LOD Ethylene glycol 5,000 25 Not Tested
Ethylene oxide 5 3 Pass/<LOD Heptane 500 25 Pass/<LOD
Hexane 50 25 Pass/<LOD Isopropyl acetate 5,000 25 Not Tested
Methanol 250 125 Pass/<LOD Naptha 400 100 Not Tested
N,N-Dimethylacetamide 5,000 250 Not Tested N,N-Dimethylformamide (DMF) 5,000 250 Not Tested
Pentane 750 25 Pass/<LOD Petroleum Ether 400 100 Not Tested
Propane 2,100 25 Pass/<LOD Pyridine 5,000 250 Not Tested
Sulfolane 5,000 25 Not Tested Tetrahydrofuran (THF) 5,000 25 Not Tested
Toluene 150 25 Pass/<LOD Trichloroethylene 25 25 Pass/<LOD
Xylenes* 150 25 Pass/<LOD

Total Butanes = 0 ug/g (PASS); Total Pentanes = 0 ug/g (PASS); Total Hexanes = 0 ug/g (PASS)

* Xylenes are reported as the sum of o-xylene, m-xylene, p-xylene, and ethylbenzene
MRL - Maximum Residue Limit; LOD - Limit of Detection

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
KEB - LM Iron laboratories KEB - LM

Iron Laboratories, LLC is an ISO/IEC 17025:2017 Testing Laboratory laboratory accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 4 of 8

IRON Laboratories     PJLA

ISO/IEC 17025:2017 Accredited

Residual Solvents QC Report
Testing Accreditation #: 77802 Test Certificate #: 22-001
Client Name, Sample Details

Ann Arbor Health Collective
Ann Arbor, MI 48108
Sample: Skunk
Type: Flower
Method: SOP FE-44-MI
Test Conditions

Prepsheet ID#: MIHS210211a
Scale: XS205-MI2
Temp: 21.2 °C
Baro PE: 986 hPa
Analyst: KEB
Technician: ANJ
Sample ID#: 22

Harvest/Process Date: 03/14/2012
Date Received: 03/14/2012
Test Date: 02/11/2021
Valid Through: 02/11/2022
Report Issued: 02/12/2021
Sample #22
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS Recovery (%) MSD Recovery (%) Relative Percent Difference (%) QC Flag
1,2-Dichloroethane N.D. 250 229 228 91.60 91.20 0.44
n-Propane N.D. 250 60 55 24.00 22.00 8.70 LR
Isobutane N.D. 250 89 89 35.60 35.60 0.00 LR
Methanol N.D. 250 195 209 78.00 83.60 6.93
n-Butane N.D. 250 110 111 44.00 44.40 0.90 LR
2,2-Dimethylpropane N.D. 250 121 124 48.40 49.60 2.45 LR
Ethanol N.D. 250 212 219 84.80 87.60 3.25
Isopentane N.D. 250 153 153 61.20 61.20 0.00 LR
Acetonitrile N.D. 250 197 199 78.80 79.60 1.01
Diethyl ether N.D. 250 197 200 78.80 80.00 1.51
2-propanone N.D. 250 222 215 88.80 86.00 3.20
2-propanol N.D. 250 225 230 90.00 92.00 2.20
n-Pentane N.D. 250 188 191 75.20 76.40 1.58
2,2-Dimethylbutane N.D. 250 188 190 75.20 76.00 1.06
2,3-Dimethylbutane N.D. 250 181 177 72.40 70.80 2.23
Methylene chloride N.D. 250 226 223 90.40 89.20 1.34
2-Methylpentane N.D. 250 178 184 71.20 73.60 3.31
3-Methylpentane N.D. 250 190 187 76.00 74.80 1.59
2-Butanol N.D. 0 0 0 0.00 0.00 0.00
n-Hexane N.D. 250 189 190 75.60 76.00 0.53
Ethyl acetate N.D. 250 222 222 88.80 88.80 0.00
Tetrahydrofuran N.D. 0 0 0 0.00 0.00 0.00
Trichloroethylene N.D. 250 224 222 89.60 88.80 0.90
Isopropyl acetate N.D. 0 0 0 0.00 0.00 0.00
Benzene N.D. 250 221 214 88.40 85.60 3.22
Chloroform N.D. 250 226 221 90.40 88.40 2.24
Cyclohexane N.D. 0 0 0 0.00 0.00 0.00
Ethylene glycol N.D. 0 0 0 0.00 0.00 0.00
Heptane N.D. 250 207 203 82.80 81.20 1.95
2-Ethoxyethanol N.D. 0 0 0 0.00 0.00 0.00
1,4-Dioxane N.D. 0 0 0 0.00 0.00 0.00
Pyridine N.D. 0 0 0 0.00 0.00 0.00
Toluene N.D. 250 225 221 90.00 88.40 1.79
Chlorobenzene N.D. 0 0 0 0.00 0.00 0.00
Ethylbenzene N.D. 0 0 0 0.00 0.00 0.00
m-Xylene/p-Xylene N.D. 500 457 407 91.40 81.40 11.57
o-Xylene N.D. 250 225 202 90.00 80.80 10.77
Cumene N.D. 0 0 0 0.00 0.00 0.00
Ethylene oxide N.D. 250 221 235 88.40 94.00 6.14

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

N.D. = Not Detected

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
KEB - LM Iron laboratories KEB - LM

Iron Laboratories, LLC is an ISO/IEC 17025:2017 Testing Laboratory laboratory accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 5 of 8

IRON Laboratories     PJLA

ISO/IEC 17025:2017 Accredited

Residual Solvents Analysis by
Mass Spectrometer
Testing Accreditation #: 77802 Test Certificate #: 22-001
Client Name, Sample Details

Ann Arbor Health Collective
Ann Arbor, MI 48108
Sample: Skunk
Type: Flower
Method: SOP FE-44-MI
Test Conditions

Prepsheet ID#: MIHS210211a
Scale: XS205-MI2
Temp: 21.2 °C
Baro PE: 986 hPa
Analyst: KEB
Technician: ANJ
Sample ID#: 22

Harvest/Process Date: 03/14/2012
Date Received: 03/14/2012
Test Date: 02/11/2021
Valid Through: 02/11/2022
Report Issued: 02/12/2021
Sample #22
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
1,2-Dichloroethane 2 1 Pass/<LOD 1,2-Dimethoxyethane 5,000 250 Not Tested
1,4-dioxane 5,000 25 Not Tested 1-Butanol 5,000 250 Not Tested
1-Pentanol 5,000 250 Not Tested 1-Propanol 5,000 250 Not Tested
2,2-Dimethylpropane (Neopentane) 750 25 Pass/<LOD 2,2-Dimethylbutane (Hexanes) 50 25 Pass/<LOD
2,3-Dimethylbutane (Hexanes) 50 25 Pass/<LOD 2-Butanol 5,000 25 Not Tested
2-Butanone (MEK) 5,000 250 Not Tested 2-Ethoxyethanol 5,000 25 Not Tested
2-Methylbutane (Isopentane) 750 25 Pass/<LOD 2-Methylpentane (Hexanes) 50 25 Pass/<LOD
2-Methylpropane (Isobutane) 800 25 Pass/<LOD 2-propanol (Isopropyl Alcohol) 500 25 Pass/<LOD
2-Propanone (Acetone) 750 25 Pass/<LOD 3-Methylpentane (Hexanes) 50 25 Pass/<LOD
Acetonitrile 60 30 Pass/<LOD Benzene 1 1 Pass/<LOD
Butane 800 25 Pass/<LOD Chloroform 2 1 Pass/<LOD
Cumene 5,000 25 Not Tested Cyclohexane 50 25 Not Tested
Dichloromethane 125 25 Pass/<LOD Dimethylsulfoxide (DMSO) 5,000 250 Not Tested
Ethanol 1,000 50 Pass/<LOD Ethyl acetate 400 25 Pass/<LOD
Ethyl ether 500 25 Pass/<LOD Ethylene glycol 5,000 25 Not Tested
Ethylene oxide 5 3 Pass/<LOD Heptane 500 25 Pass/<LOD
Hexane 50 25 Pass/<LOD Isopropyl acetate 5,000 25 Not Tested
Methanol 250 125 Pass/<LOD Naptha 400 100 Not Tested
N,N-Dimethylacetamide 5,000 250 Not Tested N,N-Dimethylformamide (DMF) 5,000 250 Not Tested
Pentane 750 25 Pass/<LOD Petroleum Ether 400 100 Not Tested
Propane 2,100 25 Pass/<LOD Pyridine 5,000 250 Not Tested
Sulfolane 5,000 25 Not Tested Tetrahydrofuran (THF) 5,000 25 Not Tested
Toluene 150 25 Pass/<LOD Trichloroethylene 25 25 Pass/<LOD
Xylenes* 150 25 Pass/<LOD

Total Butanes = 0 ug/g (PASS); Total Pentanes = 0 ug/g (PASS); Total Hexanes = 0 ug/g (PASS)

* Xylenes are reported as the sum of o-xylene, m-xylene, p-xylene, and ethylbenzene
MRL - Maximum Residue Limit; LOD - Limit of Detection

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
KEB - LM Iron laboratories KEB - LM

Iron Laboratories, LLC is an ISO/IEC 17025:2017 Testing Laboratory laboratory accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 6 of 8

IRON Laboratories     PJLA

ISO/IEC 17025:2017 Accredited

Residual Solvents QC Report
Testing Accreditation #: 77802 Test Certificate #: 22-001
Client Name, Sample Details

Ann Arbor Health Collective
Ann Arbor, MI 48108
Sample: Skunk
Type: Flower
Method: SOP FE-44-MI
Test Conditions

Prepsheet ID#: MIHS210211a
Scale: XS205-MI2
Temp: 21.2 °C
Baro PE: 986 hPa
Analyst: KEB
Technician: ANJ
Sample ID#: 22

Harvest/Process Date: 03/14/2012
Date Received: 03/14/2012
Test Date: 02/11/2021
Valid Through: 02/11/2022
Report Issued: 02/12/2021
Sample #22
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS Recovery (%) MSD Recovery (%) Relative Percent Difference (%) QC Flag
1,2-Dichloroethane N.D. 250 229 228 91.60 91.20 0.44
n-Propane N.D. 250 60 55 24.00 22.00 8.70 LR
Isobutane N.D. 250 89 89 35.60 35.60 0.00 LR
Methanol N.D. 250 195 209 78.00 83.60 6.93
n-Butane N.D. 250 110 111 44.00 44.40 0.90 LR
2,2-Dimethylpropane N.D. 250 121 124 48.40 49.60 2.45 LR
Ethanol N.D. 250 212 219 84.80 87.60 3.25
Isopentane N.D. 250 153 153 61.20 61.20 0.00 LR
Acetonitrile N.D. 250 197 199 78.80 79.60 1.01
Diethyl ether N.D. 250 197 200 78.80 80.00 1.51
2-propanone N.D. 250 222 215 88.80 86.00 3.20
2-propanol N.D. 250 225 230 90.00 92.00 2.20
n-Pentane N.D. 250 188 191 75.20 76.40 1.58
2,2-Dimethylbutane N.D. 250 188 190 75.20 76.00 1.06
2,3-Dimethylbutane N.D. 250 181 177 72.40 70.80 2.23
Methylene chloride N.D. 250 226 223 90.40 89.20 1.34
2-Methylpentane N.D. 250 178 184 71.20 73.60 3.31
3-Methylpentane N.D. 250 190 187 76.00 74.80 1.59
2-Butanol N.D. 0 0 0 0.00 0.00 0.00
n-Hexane N.D. 250 189 190 75.60 76.00 0.53
Ethyl acetate N.D. 250 222 222 88.80 88.80 0.00
Tetrahydrofuran N.D. 0 0 0 0.00 0.00 0.00
Trichloroethylene N.D. 250 224 222 89.60 88.80 0.90
Isopropyl acetate N.D. 0 0 0 0.00 0.00 0.00
Benzene N.D. 250 221 214 88.40 85.60 3.22
Chloroform N.D. 250 226 221 90.40 88.40 2.24
Cyclohexane N.D. 0 0 0 0.00 0.00 0.00
Ethylene glycol N.D. 0 0 0 0.00 0.00 0.00
Heptane N.D. 250 207 203 82.80 81.20 1.95
2-Ethoxyethanol N.D. 0 0 0 0.00 0.00 0.00
1,4-Dioxane N.D. 0 0 0 0.00 0.00 0.00
Pyridine N.D. 0 0 0 0.00 0.00 0.00
Toluene N.D. 250 225 221 90.00 88.40 1.79
Chlorobenzene N.D. 0 0 0 0.00 0.00 0.00
Ethylbenzene N.D. 0 0 0 0.00 0.00 0.00
m-Xylene/p-Xylene N.D. 500 457 407 91.40 81.40 11.57
o-Xylene N.D. 250 225 202 90.00 80.80 10.77
Cumene N.D. 0 0 0 0.00 0.00 0.00
Ethylene oxide N.D. 250 221 235 88.40 94.00 6.14

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

N.D. = Not Detected

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
KEB - LM Iron laboratories KEB - LM

Iron Laboratories, LLC is an ISO/IEC 17025:2017 Testing Laboratory laboratory accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 7 of 8
IRON Laboratories

Bio Analysis by
Gas Chromatography
Test Certificate #: 22-001
Client Name, Sample Details

Ann Arbor Health Collective
Ann Arbor, MI 48108
Sample: Skunk
Type: Flower
Method: FE03 HP5890-1
Test Conditions

Sample ID#: 22

Harvest/Process Date: 03/14/2012
Date Received: 03/14/2012
Test Date: 03/14/2012
Valid Through: 03/14/2013
Report Issued: 03/14/2012
Sample #22
Impurities: Not Detected
Molds: No Types: N/A
Pests: No Types: N/A
Anthers: No
Detritus: No
Fibers: No
Hair: No
Mature Seeds: No
Premature Seeds: No
Unidentified Foliar Spray: No
Other Impurities: No
*Moisture 10

*Moisture is not part of the accredited scope of Iron Laboratories.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

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