IRON Laboratories     PJLA

ISO/IEC 17025:2017 Accredited

Marihuana Potency Analysis by
High Performance Liquid Chromatography
Testing Accreditation #: 77802 Test Certificate #: 152843-001
Client Name, Sample Details

@caregiverpharms
Westland, MI 48185
Sample: insulin Shock
Type: Flower
Method: FE04U12 HPLC-UV
Test Conditions

Prepsheet ID#: MIP250115a
Scale: XS205-MI1
Temp: 22 °C
Baro Pressure: 980.1 hPa
Analyst: MEH
Technician: ARH
Sample ID#: 152843

Harvest/Process Date: 01/13/2025
Serving Size (g): 1
Date Received: 01/13/2025
Test Date: 01/15/2025
Valid Through: 01/16/2026
Report Issued: 01/17/2025
Sample #152843
Sample #152843 Sample #152843
Test
Compounds		 Δ9-THC THCA Δ8-THC CBD CBDA CBG CBGA CBN CBC CBL THCV CBDV Total
Cannabinoids*		 Total THC Total CBD Calc Max Total
Cannabinoids*
Amount (%) 0.3 16.0 N/D N/D N/D N/D 1.8 N/D N/D 0.1 N/D N/D 18.3 14.4 0.0 16.1
Amount (mg/g) 3.4 160.4 N/D N/D N/D N/D 18.02 N/D N/D 1.0 N/D N/D 182.82 144.1 0.0 160.9
Amount per Serving (mg) 3.4 160.4 N/D N/D N/D N/D 18.02 N/D N/D 1 N/D N/D 182.8 Serving Size~ (g): 1.0
LOQ (mg/g) 0.78 0.78 0.78 0.78 0.78 0.78 0.78 0.78 0.78 0.78 0.78 0.78   %Decarb. THC CBD
±%RPD 1.95% 0.14% 2.18% 0.13% 1.35% 1.06% 0.47% 1.13% 0.37% 3.10% 0.26% 0.02% 2 N/A

LOQ = Limit of Quantitation; %RPD = Relative Percent Deviation; %RSD = Relative Standard Deviation; N/D = Not Detected

*Designates values that are not currently included in the accredited scope of Iron Laboratories.

*** Designates tests that use the method FE-45. FE-45 is performed using AOAC 966.02 and 32.004-32.009.

FE-45 has relative expanded (k=2) uncertainties of 1.098% for moisture, 1.754% for water activity for unprocessed plant materials, and 13.102% for water activity for infused products.

Vitamin E acetate analysis has a relative expanded (k=2) uncertainty of 18.614%.

Total THC and CBD is the calculated sum of Δ9-THC and Δ8-THC or CBD plus the amount of THC or CBD derived from THCA or CBDA, respectively.

These values are calculated by applying a molar correction factor of 0.877 to the THCA or the CBDA value.

Calc Max Total Cannabinoids is the sum of Total THC, Total CBD, CBN, Total CBG, CBC, THCV, CBDV, and CBL.

Total CBG is calculated as CBG plus CBGA*0.878 (the molar correction factor for CBGA to CBG conversion).

%Decarb. THC and CBD refer to the percentage of Δ9-THC or CBD relative to THCA or CBDA, respectively.

This sample has not undergone random sampling and has not been tested for compliant state, batch representative testing. These results should therefore be used for research and development or quality control purposes only. Results apply to the sample as received.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
ARH - LM Iron laboratories ARH - LM

Iron Laboratories, LLC is an ISO/IEC 17025:2017 Testing Laboratory laboratory accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

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IRON Laboratories     PJLA

ISO/IEC 17025:2017 Accredited

QC Report
Testing Accreditation #: 77802 Test Certificate #: 152843-001
Client Name, Sample Details

@caregiverpharms
Westland, MI 48185
Sample: insulin Shock
Type: Flower
Method: FE04U12 HPLC-UV
Test Conditions

Prepsheet ID#: MIP250115a
Scale: XS205-MI1
Temp: 22 °C
Baro Pressure: 980.1 hPa
Analyst: MEH
Technician: ARH
Sample ID#: 152843

Harvest/Process Date: 01/13/2025
Serving Size (g): 1
Date Received: 01/13/2025
Test Date: 01/15/2025
Valid Through: 01/16/2026
Report Issued: 01/17/2025
Sample #152843
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Δ9-THC 0 5.4348 5.22287 96.10 5.32582 97.99 1.95%
THCA 0 5.37081 5.39578 100.46 5.38849 100.33 0.14%
Δ8-THC 0 5.40902 5.26566 97.35 5.38162 99.49 2.18%
CBD 0 5.8448 5.1696 88.45 5.16281 88.33 0.13% LR
CBDA 0 5.14684 5.21883 101.40 5.14888 100.04 1.35%
CBG 0 5.64127 5.19514 92.09 5.14019 91.12 1.06%
CBGA 0 5.17969 5.1661 99.74 5.1419 99.27 0.47%
CBN 0 5.1279 5.17505 100.92 5.23364 102.06 1.13%
CBC 0 5.04213 5.16479 102.43 5.18388 102.81 0.37%
CBCA N/A 0 0 0.00 0 0.00 0% N/A
CBL 0 4.96951 4.9761 100.13 5.13285 103.29 3.10%
THCV 0 5.11818 5.11141 99.87 5.12457 100.12 0.26%
CBDV 0 5.07351 5.06675 99.87 5.06569 99.85 0.02%

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

This sample has not undergone random sampling and has not been tested for compliant state, batch representative testing. These results should therefore be used for research and development or quality control purposes only. Results apply to the sample as received.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
ARH - LM Iron laboratories ARH - LM

Iron Laboratories, LLC is an ISO/IEC 17025:2017 Testing Laboratory laboratory accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

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