IRON Laboratories     PJLA

ISO/IEC 17025:2017 Accredited

Marihuana Potency Analysis by
High Performance Liquid Chromatography

Testing Accreditation #: 77802 Test Certificate #: 147342-001
Client Name, Sample Details

Greenroom Gardens LLC AU-G-C-000910
Muskegon, MI 49441
Sample: Glueberry OG
License: AU-G-C-000910
Type: Adult Use Flower
Method: FE04U12 HPLC-UV
Metrc Test Pkg#: 1A4050300032E11000000858
Metrc Source Pkg#: 1A4050300032E11000000857
***Water Activity: 0.56

Test Conditions

Prepsheet ID#: MIP240531A
Scale: XS205-MI2
Temp: 22.9 °C
Baro Pressure: 976.9 hPa
Analyst: MEH
Technician: ARH

Sample ID#: 147342

Harvest/Process Date: 05/30/2024
Serving Size (g): 1
Date Received: 05/30/2024
Test Date: 05/31/2024
Valid Through: 06/01/2025
Report Issued: 06/04/2024

Sample #147342
Sample #147342 Sample #147342
Test
Compounds
Δ9-THC THCA Δ8-THC CBD CBDA CBG CBGA CBN CBC CBL THCV CBDV Total
Cannabinoids*
Total THC Total CBD Calc Max Total
Cannabinoids*
Amount (%) 0.9 23.0 N/D N/D N/D N/D 1.0 N/D N/D N/D N/D N/D 24.9 21.1 0.0 22.0
Amount (mg/g) 9.3 230.1 N/D N/D N/D N/D 10.04 N/D N/D N/D N/D N/D 249.44 211.1 0.0 219.9
Amount per Serving (mg) 9.3 230.1 N/D N/D N/D N/D 10.04 N/D N/D N/D N/D N/D 249.4 Serving Size~ (g): 1.0
LOQ (mg/g) 0.75 0.75 0.75 0.75 0.75 0.75 0.75 0.75 0.75 0.75 0.75 0.75   %Decarb. THC CBD
±%RPD 1.05% 0.53% 1.18% 0.66% 0.12% 2.37% 0.59% 0.07% 0.54% 6.85% 0.19% 0.71% 4 N/A

Sample passes for water activity (sample fails if Aw>0.65). Water activity is measured utilizing SOP FE-45 (water activity meter).

LOQ = Limit of Quantitation; %RPD = Relative Percent Deviation; %RSD = Relative Standard Deviation; N/D = Not Detected

*Designates values that are not currently included in the accredited scope of Iron Laboratories.

*** Designates tests that use the method FE-45. FE-45 is performed using AOAC 966.02 and 32.004-32.009.

FE-45 has relative expanded (k=2) uncertainties of 1.098% for moisture, 1.754% for water activity for unprocessed plant materials, and 13.102% for water activity for infused products.

Vitamin E acetate analysis has a relative expanded (k=2) uncertainty of 18.614%.

Total THC and CBD is the calculated sum of Δ9-THC and Δ8-THC or CBD plus the amount of THC or CBD derived from THCA or CBDA, respectively.

These values are calculated by applying a molar correction factor of 0.877 to the THCA or the CBDA value.

Calc Max Total Cannabinoids is the sum of Total THC, Total CBD, CBN, Total CBG, CBC, THCV, CBDV, and CBL.

Total CBG is calculated as CBG plus CBGA*0.878 (the molar correction factor for CBGA to CBG conversion).

%Decarb. THC and CBD refer to the percentage of Δ9-THC or CBD relative to THCA or CBDA, respectively.

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

ARH - LM Iron laboratories ARH - LM

Iron Laboratories, LLC is an ISO/IEC 17025:2017 Testing Laboratory laboratory accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 1 of 7

IRON Laboratories     PJLA

ISO/IEC 17025:2017 Accredited

QC Report

Testing Accreditation #: 77802 Test Certificate #: 147342-001
Client Name, Sample Details

Greenroom Gardens LLC AU-G-C-000910
Muskegon, MI 49441
Sample: Glueberry OG
License: AU-G-C-000910
Type: Adult Use Flower
Method: FE04U12 HPLC-UV
Metrc Test Pkg#: 1A4050300032E11000000858
Metrc Source Pkg#: 1A4050300032E11000000857
***Water Activity: 0.56

Test Conditions

Prepsheet ID#: MIP240531A
Scale: XS205-MI2
Temp: 22.9 °C
Baro Pressure: 976.9 hPa
Analyst: MEH
Technician: ARH

Sample ID#: 147342

Harvest/Process Date: 05/30/2024
Serving Size (g): 1
Date Received: 05/30/2024
Test Date: 05/31/2024
Valid Through: 06/01/2025
Report Issued: 06/04/2024

Sample #147342
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Δ9-THC 0 5.13804 5.05837 98.45 5.11188 99.49 1.05%
THCA 0 4.86405 4.85769 99.87 4.88374 100.40 0.53%
Δ8-THC 0 5.12574 5.0297 98.13 5.08964 99.30 1.18%
CBD 0 5.08622 5.13214 100.90 5.09841 100.24 0.66%
CBDA 0 5.05663 5.06799 100.22 5.06175 100.10 0.12%
CBG 0 5.20812 5.26202 101.03 5.13852 98.66 2.37%
CBGA 0 5.02033 5.02259 100.05 4.99305 99.46 0.59%
CBN 0 5.02818 5.04149 100.26 5.04523 100.34 0.07%
CBC 0 5.075 5.07778 100.05 5.10525 100.60 0.54%
CBCA N/A 0 0 0.00 0 0.00 0% N/A
CBL 0 5.73599 5.22722 91.13 5.59773 97.59 6.85%
THCV 0 5.0303 5.1797 102.97 5.18944 103.16 0.19%
CBDV 0 5.01326 4.9982 99.70 5.03392 100.41 0.71%

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

ARH - LM Iron laboratories ARH - LM

Iron Laboratories, LLC is an ISO/IEC 17025:2017 Testing Laboratory laboratory accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 2 of 7

IRON Laboratories     PJLA

ISO/IEC 17025:2017 Accredited

Pesticide Analysis by
Mass Spectrometer

Testing Accreditation #: 77802 Test Certificate #: 147342-001
Client Name, Sample Details

Greenroom Gardens LLC AU-G-C-000910
Muskegon, MI 49441
Sample: Glueberry OG
License: AU-G-C-000910
Type: Adult Use Flower
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A4050300032E11000000858
Metrc Source Pkg#: 1A4050300032E11000000857

Test Conditions

Prepsheet ID#: MIPS240531b
Scale: XS205-MI1
Temp: 22.1 °C
Baro PE: 970.8 hPa
Analyst: OSB
Technician: OSB

Sample ID#: 147342

Harvest/Process Date: 05/30/2024
Serving Size (g): 1
Date Received: 05/30/2024
Test Date: 05/31/2024
Valid Through: 05/31/2025
Report Issued: 06/04/2024

Sample #147342
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
Aldicarb 0.400 0.200 Pass/<LOD Abamectin**** 0.500 0.250 Pass/<LOD
Acephate 0.400 0.200 Pass/<LOD Acequinocyl 2.000 1.000 Pass/<LOD
Acetamiprid 0.200 0.100 Pass/<LOD Azoxystrobin 0.200 0.100 Pass/<LOD
Bifenazate 0.200 0.100 Pass/<LOD Bifenthrin 0.200 0.100 Pass/<LOD
Boscalid 0.400 0.200 Pass/<LOD Carbaryl 0.200 0.100 Pass/<LOD
Carbofuran 0.200 0.100 Pass/<LOD Chlorantraniliprole 0.200 0.100 Pass/<LOD
Chlorfenapyr 1.000 0.500 Pass/<LOD Chlorpyrifos 0.200 0.100 Pass/<LOD
Clofentezine 0.200 0.100 Pass/<LOD Cyfluthrin** 1.000 0.500 Pass/<LOD
Cypermethrin*** 1.000 0.500 Pass/<LOD Daminozide 1.000 0.500 Pass/<LOD
DDVP (Dichlorvos) 1.000 0.500 Pass/<LOD Diazinon 0.200 0.100 Pass/<LOD
Dimethoate 0.200 0.100 Pass/<LOD Ethoprophos 0.200 0.100 Pass/<LOD
Etofenprox 0.400 0.200 Pass/<LOD Etoxazole 0.200 0.100 Pass/<LOD
Fenoxycarb 0.200 0.100 Pass/<LOD Fenpyroximate 0.400 0.200 Pass/<LOD
Fipronil 0.400 0.200 Pass/<LOD Flonicamid 1.000 0.500 Pass/<LOD
Fludioxonil 0.400 0.200 Pass/<LOD Hexythiazox 1.000 0.500 Pass/<LOD
Imazalil 0.200 0.100 Pass/<LOD Imidacloprid 0.400 0.200 Pass/<LOD
Kresoxim Methyl 0.400 0.200 Pass/<LOD Malathion 0.200 0.100 Pass/<LOD
Metalaxyl 0.200 0.100 Pass/<LOD Methiocarb 0.200 0.100 Pass/<LOD
Methomyl 0.400 0.200 Pass/<LOD Methyl Parathion 0.200 0.100 Pass/<LOD
MGK-264‡ 0.200 0.100 Pass/<LOD Myclobutanil 0.200 0.100 Pass/<LOD
Naled 0.500 0.250 Pass/<LOD Oxamyl 1.000 0.500 Pass/<LOD
Paclobutrazol 0.400 0.200 Pass/<LOD Permethrins† 0.200 0.100 Pass/<LOD
Phosmet 0.200 0.100 Pass/<LOD Piperonyl Butoxide 100.000 1.900 Not Tested
Prallethrin 0.200 0.100 Pass/<LOD Propiconazole 0.400 0.200 Pass/<LOD
Propoxur 0.200 0.100 Pass/<LOD Pyrethrins* 1.000 0.500 Pass/<LOD
Pyridaben 0.200 0.100 Pass/<LOD Spinosad***** 0.200 0.100 Pass/<LOD
Spiromesifen 0.200 0.100 Pass/<LOD Spirotetramat 0.200 0.100 Pass/<LOD
Spiroxamine‡ 0.400 0.200 Pass/<LOD Tebuconazole 0.400 0.200 Pass/<LOD
Thiacloprid 0.200 0.100 Pass/<LOD Thiamethoxam 0.200 0.100 Pass/<LOD
Trifloxystrobin 0.200 0.100 Pass/<LOD

* Pyrethrins are reported as the sum of Jasmolin I, Cinerin I, and Pyrethrin I
** Cyfluthrins are reported as the sum of isomers Cyfluthrin I, II, III, and IV
*** Cypermethrins are reported as the sum of isomers Cypermethrin I, II, III, and IV
**** Abamectin is reported as the sum of Avermectin B1a and Avermectin B1b
***** Spinosad is reported as the sum of Spinosyn A and Spinosyn D
† Permethrin and Prallethrin are reported as the sum of cis and trans isomers
‡ MGK-264 and Spiroximine are reported as the sum of isomers I and II
MRL - Maximum Residue Limit; LOD - Limit of Detection

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

ARH - LM Iron laboratories ARH - LM

Iron Laboratories, LLC is an ISO/IEC 17025:2017 Testing Laboratory laboratory accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 2 of 7

IRON Laboratories     PJLA

ISO/IEC 17025:2017 Accredited

Pesticide QC Report

Testing Accreditation #: 77802 Test Certificate #: 147342-001
Client Name, Sample Details

Greenroom Gardens LLC AU-G-C-000910
Muskegon, MI 49441
Sample: Glueberry OG
License: AU-G-C-000910
Type: Adult Use Flower
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A4050300032E11000000858
Metrc Source Pkg#: 1A4050300032E11000000857

Test Conditions

Prepsheet ID#: MIPS240531b
Scale: XS205-MI1
Temp: 22.1 °C
Baro PE: 970.8 hPa
Analyst: OSB
Technician: OSB

Sample ID#: 147342

Harvest/Process Date: 05/30/2024
Serving Size (g): 1
Date Received: 05/30/2024
Test Date: 05/31/2024
Valid Through: 05/31/2025
Report Issued: 06/04/2024

Sample #147342
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS recovery% MSD recovery% Relative Percent Difference (%) QC Flag
Acephate N.D. 1 0.981 0.952 98.10 95.20 3.00
Acequinocyl N.D. 1 1.01 1.04 101.00 104.00 2.93
Acetamiprid N.D. 1 1.04 1.08 104.00 108.00 3.77
Aldicarb N.D. 1 1.12 1.11 112.00 111.00 0.90
Avermectin B1a N.D. 1 0.904 0.851 90.40 85.10 6.04
Azoxystrobin N.D. 1 1.01 0.962 101.00 96.20 4.87
Bifenazate N.D. 1 0.0428 0.0424 4.28 4.24 0.94 LR
Bifenthrin N.D. 1 1.07 1.07 107.00 107.00 0.00
Boscalid N.D. 1 1.05 1.09 105.00 109.00 3.74
Carbaryl N.D. 1 0.977 1 97.70 100.00 2.33
Carbofuran N.D. 1 1.04 1.08 104.00 108.00 3.77
Chlorantraniliprole N.D. 1 1.01 1 101.00 100.00 1.00
Chlorfenapyr N.D. 1 1.1 1.14 110.00 114.00 3.57
Chlorpyriphos N.D. 1 0.975 1 97.50 100.00 2.53
Clofentezine N.D. 1 0.906 0.92 90.60 92.00 1.53
Cyfluthrin N.D. 1 0.927 0.964 92.70 96.40 3.91
Cypermethrin N.D. 1 0.917 0.905 91.70 90.50 1.32
Daminoside N.D. 1 0.678 0.647 67.80 64.70 4.68
Diazanon N.D. 1 10.4 10.4 1,040.00 1,040.00 0.00 HR
Dichlorvos N.D. 1 0.949 0.993 94.90 99.30 4.53
Dimethoate N.D. 1 0.962 0.979 96.20 97.90 1.75
Ethoprophos N.D. 1 0.987 1.03 98.70 103.00 4.26
Etofenprox N.D. 1 1.03 1.03 103.00 103.00 0.00
Etoxazole N.D. 1 1.08 1.09 108.00 109.00 0.92
Fenoxycarb N.D. 1 1.03 1.03 103.00 103.00 0.00
Fenpyroximate N.D. 1 1.05 1.04 105.00 104.00 0.96
Fipronil N.D. 1 1.17 1.26 117.00 126.00 7.41 HR
Flonicamid N.D. 1 0.985 1.03 98.50 103.00 4.47
Fludioxonil N.D. 1 0.957 0.984 95.70 98.40 2.78
Hexythiazox N.D. 1 1.04 1.04 104.00 104.00 0.00
Imazalil N.D. 1 0.705 0.617 70.50 61.70 13.31
Imidacloprid N.D. 1 0.93 0.978 93.00 97.80 5.03
Kresoxim-methyl N.D. 1 0.913 0.983 91.30 98.30 7.38
Malathion N.D. 1 0.995 1.02 99.50 102.00 2.48
Metalaxyl N.D. 1 0.981 0.963 98.10 96.30 1.85
Methiocarb N.D. 1 1.02 1.03 102.00 103.00 0.98
Methomyl N.D. 1 0.896 0.903 89.60 90.30 0.78
MGK-264 N.D. 1 0.983 0.929 98.30 92.90 5.65
Myclobutanil N.D. 1 1.06 1.06 106.00 106.00 0.00
Naled (dibrom) N.D. 1 0.469 0.484 46.90 48.40 3.15 LR
Oxamyl N.D. 1 1.01 1.01 101.00 101.00 0.00
Paclobutrazol N.D. 1 1.02 0.986 102.00 98.60 3.39
Parathion-methyl N.D. 1 0.784 0.743 78.40 74.30 5.37
Permethrins N.D. 1 1.083 1.073 108.30 107.30 0.93
Phosmet N.D. 1 1.03 1.02 103.00 102.00 0.98
Piperonyl butoxide N/A N/A N/A N/A nan nan N/A
Prallethrin N.D. 1 1.01 1 101.00 100.00 1.00
Propiconazole N.D. 1 1.01 1 101.00 100.00 1.00
Propoxur N.D. 1 1 1.04 100.00 104.00 3.92
Pyrethrin N.D. 1 1.35 1.34 135.00 134.00 0.74 HR
Pyridaben N.D. 1 1.06 1.06 106.00 106.00 0.00
SpinosynA N.D. 0.82 0.712 0.72 86.83 87.80 1.12
SpinosynD N.D. 0.18 0.224 0.221 124.44 122.78 1.35 HR
Spiromesifen N.D. 1 0.965 0.91 96.50 91.00 5.87
Spirotetramat N.D. 1 1.02 1.06 102.00 106.00 3.85
Spiroxamine N.D. 1 0.928 0.96 92.80 96.00 3.39
Tebuconazole N.D. 1 1.06 1.04 106.00 104.00 1.90
Thiacloprid N.D. 1 1.02 1.04 102.00 104.00 1.94
Thiamethoxam N.D. 1 0.929 0.916 92.90 91.60 1.41
Trifloxystrobin N.D. 1 0.947 0.943 94.70 94.30 0.42

N.D. = Not Detected

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 30%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (60-120%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

ARH - LM Iron laboratories ARH - LM

Iron Laboratories, LLC is an ISO/IEC 17025:2017 Testing Laboratory laboratory accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 3 of 7

IRON Laboratories     PJLA

ISO/IEC 17025:2017 Accredited

Terpene Report by
Mass Spectrometer

Testing Accreditation #: 77802 Test Certificate #: 147342-001
Client Name, Sample Details

Greenroom Gardens LLC AU-G-C-000910
Muskegon, MI 49441
Sample: Glueberry OG
License: AU-G-C-000910
Type: Adult Use Flower
Method: SOP FE-44-MI
Metrc Test Pkg#: 1A4050300032E11000000858
Metrc Source Pkg#: 1A4050300032E11000000857

Test Conditions

Scale: XS205-MI1
Temp: 22.9 °C
Baro Pressure: 976.9 hPa
Analyst: OSB
Technician: MEH

Sample ID#: 147342

Harvest/Process Date: 05/30/2024
Serving Size (g): 1
Date Received: 05/30/2024

Sample #147342
Sample #147342
  • α-Pinene (0.36%)
  • β-Ocimene (0.07%)
  • Camphene (0.01%)
  • Eucalyptol (1,8-Cineol) (0.00%)
  • Sabinene (0.00%)
  • γ-Terpinene (0.00%)
  • Myrcene (0.21%)
  • α-Terpinolene (0.00%)
  • β-Pinene (0.98%)
  • Linalool (0.18%)
  • ∆3-Carene (0.00%)
  • Fenchone (0.00%)
  • α-Terpinene (0.00%)
  • endo-Fenchol (0.00%)
  • α-Ocimene (0.00%)
  • Isopulegol (0.00%)
  • Limonene (0.08%)
  • Geraniol (0.00%)
  • p-Cymene (0.00%)
  • β-Caryophyllene (0.83%)
  • α-Humulene (0.27%)
  • Nerolidol 1 (cis) (0.00%)
  • Nerolidol 2 (trans) (0.09%)
  • Guaiol (0.00%)
  • Caryophyllene Oxide (0.00%)
  • α-Bisabolol (0.26%)
  • α-Phellandrene (0.00%)
  • α-Terpineol (0.00%)
  • Valenence (0.00%)

Total: 3.340%

Predominant Terpenes

0.98%   β-Pinene Woody, fresh pine, hay 0.83%   β-Caryophyllene Sweet, woody, spicy, clove
0.36%   α-Pinene Fresh camphor, sweet, pine, earthy, woody 0.27%   α-Humulene Woody, oceanic-watery, spicy clove
0.26%   α-Bisabolol Fruity, nutty, coconut 0.21%   Myrcene Peppery, spicy balsam

Results should be interpreted as qualitative only (present/absent). Quantitative values are only estimations for the purpose of research and development, and are not included in Iron Laboratories accredited scope. Eucalyptol, Sabinene, Fenchone, endo-Fenchol, Caryophyllene Oxide, a-Phellandrene, a-Terpineol, and Valencene are not currently tested for by Iron Laboratories Michigan. LOQ = 0.01%. Expanded uncertainty (k=2) for terpene analysis is 25.92%.

Value in parenthesis indicates percentage of terpene present in the total sample (weight percentage, wt/wt%).
Value in doughnut slice indicates individual terpene abundance with respect to the total terpenes detected.

These results should be used for research and development or quality control purposes only. If applicable, results for caregivers apply to the sample as received.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

ARH - LM Iron laboratories ARH - LM

Iron Laboratories, LLC is an ISO/IEC 17025:2017 Testing Laboratory laboratory accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 4 of 7

IRON Laboratories     PJLA

ISO/IEC 17025:2017 Accredited

Microbiology Analysis

Testing Accreditation #: 77802 Test Certificate #: 147342-001
Client Name, Sample Details

Greenroom Gardens LLC AU-G-C-000910
Muskegon, MI 49441
Sample: Glueberry OG
License: AU-G-C-000910
Type: Adult Use Flower
Metrc Test Pkg#: 1A4050300032E11000000858
Metrc Source Pkg#: 1A4050300032E11000000857

Test Conditions

Scale: Pioneer-MI1
Temp: 23.4 °C
Baro Pressure: 987.4 hPa
Analyst: EDB
Technician: EDB

Sample ID#: 147342

Harvest/Process Date: 05/30/2024
Serving Size (g): 1
Date Received: 05/30/2024
Test Date: 05/31/2024
Valid Through: 05/31/2025
Report Issued: 06/04/2024

Sample #147342
Test Method MCFU (CFU/g) LOD (CFU/g) Status (CFU/g)
Total Aerobic Not Tested N/A 0 Not Tested
Yeast & Mold FE-66 (MPN) 100,001 100 Pass/<LOD
Bile-tolerant gram-negative bacteria Not Tested N/A 0 Not Tested
Total Coliforms FE-66 (MPN) 1,001 100 Pass/<LOD
E. Coli FE-65 (PCR) 1 1 Pass/Not Present
Salmonella FE-65 (PCR) 1 1 Pass/Not Present
Aspergillus spp. FE-65 (PCR) 1 1 Pass/Not Present

E. coli test screens exclusively for Shiga toxin-producing E. coli. TNTC values for yeast and mold are >150,000 CFU/g. TNTC values for total coliforms are >15,000 CFU/g. The maximum relative uncertainty is 6% for PCR and 40% for MPN.

TNTC = Too Numerous To Count. Maximum Colony Forming Units (MCFU) represents the minimum value that a test would need to achieve in order to be considered a failed result (if applicable). LOD is the Limit of Detection for the method. CFU/g = Colony Forming Units per gram. Aspergillus spp. consists of A. flavus, A. fumigatus, A. niger, and A. terreus.

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

MEH QM Iron laboratories MEH QM

Iron Laboratories, LLC is an ISO/IEC 17025:2017 Testing Laboratory laboratory accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 5 of 7

IRON Laboratories     PJLA

ISO/IEC 17025:2017 Accredited

Bio Analysis by
Microscopic Visual Inspection

Testing Accreditation #: 77802 Test Certificate #: 147342-001
Client Name, Sample Details

Greenroom Gardens LLC AU-G-C-000910
Muskegon, MI 49441
Sample: Glueberry OG
License: AU-G-C-000910
Type: Adult Use Flower
Method: FE02 Microscope Dissection
Metrc Test Pkg#: 1A4050300032E11000000858
Metrc Source Pkg#: 1A4050300032E11000000857

Test Conditions

Analyst: ARH
Technician: ARH

Sample ID#: 147342

Harvest/Process Date: 05/30/2024
Serving Size (g): 1
Date Received: 05/30/2024
Test Date: 05/31/2024
Valid Through: 05/31/2025
Report Issued: 06/04/2024

Sample #147342
Sample #147342 Sample #147342
Severity Rating
Mold and Mildew 0 Pass
Mites (not Russet) 0 Pass
Russet Mites 0 Pass
Thrips 0 Pass
Aphids 0 Pass
Other Pests 0 Pass
Other Organic Matter 0 Pass
Inorganic Matter 0 Pass
Total Organic Foreign Matter <2% Pass
Inorganic Foreign Matter 0% Pass
Stem Material <5% Pass
Severity Rating Key
Correlating %FM ≤2% FM >2% FM
Severity Rating 0 None 1 Mild 2 Moderate 3 Severe Units
Mold and Mildew <2 2 3 4+ Locations/g
Mites (not russet) <1 1-5 6-10 11+ Amount/g
Russet Mites <1 1-10 11-50 51+ Amount/g
Thrips <1 1-3 4-5 6+ Amount/g
Aphids <1 1 2-4 5+ Amount/g
Other Pests <1 1-5 6-10 11+ Amount/g
Other Organic Matter <1 1-5 6-10 11+ Amount/g
Inorganic Matter 0 >0 Amount/g

In compliance with the MMFLA regulation, the action limits for foreign matter are as follows; no more that 2% organic matter, 5% stem material, and no presence of inorganic matter. Percent foreign contamination is based off of total surface area.

Scale: PIONEER-MI1.

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

MEH QM Iron laboratories MEH QM

Iron Laboratories, LLC is an ISO/IEC 17025:2017 Testing Laboratory laboratory accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 6 of 7

IRON Laboratories     PJLA

ISO/IEC 17025:2017 Accredited

Heavy Metals Analysis

Testing Accreditation #: 77802 Test Certificate #: 147342-001
Client Name, Sample Details

Greenroom Gardens LLC AU-G-C-000910
Muskegon, MI 49441
Sample: Glueberry OG
License: AU-G-C-000910
Type: Adult Use Flower
Method: FE60 ICPMS-MI
Metrc Test Pkg#: 1A4050300032E11000000858
Metrc Source Pkg#: 1A4050300032E11000000857

Test Conditions

Prepsheet ID#: HMMIICP240603fMK
Temp: 23.0 °C
Baro PE: 978.4 hPa
Analyst: MK
Technician: MK

Sample ID#: 147342

Harvest/Process Date: 05/30/2024
Serving Size (g): 1
Date Received: 05/30/2024
Test Date: 06/03/2024
Valid Through: 06/03/2025
Report Issued: 06/05/2024

Sample #147342
Sample #147342 Sample #147342
Test Compound MRL (PPM) LOD (PPM) Status (PPM)
Arsenic 0.4 0.1 Pass/<LOD
Copper 0 1.5 Not Tested
Cadmium 0.4 0.1 Pass/<LOD
Chromium 1.2 0.3 Pass/<LOD
Lead 1 0.25 Pass/<LOD
Mercury 0.2 0.05 Pass/<LOD
Nickel 1 0.25 Pass/<LOD

MRL - Maximum Residue Limit; LOD - Limit of Detection

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

MEH QM Iron laboratories MEH QM

Iron Laboratories, LLC is an ISO/IEC 17025:2017 Testing Laboratory laboratory accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 7 of 7

IRON Laboratories     PJLA

ISO/IEC 17025:2017 Accredited

QC Report

Testing Accreditation #: 77802 Test Certificate #: 147342-001
Client Name, Sample Details

Greenroom Gardens LLC AU-G-C-000910
Muskegon, MI 49441
Sample: Glueberry OG
License: AU-G-C-000910
Type: Adult Use Flower
Method: FE60 ICPMS-MI
Metrc Test Pkg#: 1A4050300032E11000000858
Metrc Source Pkg#: 1A4050300032E11000000857

Test Conditions

Prepsheet ID#: HMMIICP240603fMK
Temp: 23.0 °C
Baro PE: 978.4 hPa
Analyst: MK
Technician: MK

Sample ID#: 147342

Harvest/Process Date: 05/30/2024
Serving Size (g): 1
Date Received: 05/30/2024
Test Date: 06/03/2024
Valid Through: 06/03/2025
Report Issued: 06/05/2024

Sample #147342
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD QC Flag
Arsenic N/D 0.160 0.177 110.63 0.181 113.13
Cadmium N/D 0.160 0.199 124.38 0.212 132.50
Chromium N/D 0.480 0.503 104.79 0.518 107.92
Copper N/D 2.400 3.163 131.79 3.232 134.67
Lead N/D 0.400 0.436 109.00 0.444 111.00
Mercury N/D 0.080 0.093 116.25 0.096 120.00
Nickel N/D 0.400 0.346 86.50 0.351 87.75

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

MEH QM Iron laboratories MEH QM

Iron Laboratories, LLC is an ISO/IEC 17025:2017 Testing Laboratory laboratory accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 8 of 7