IRON Laboratories     PJLA

ISO/IEC 17025:2017 Accredited

Marihuana Potency Analysis by
High Performance Liquid Chromatography
Testing Accreditation #: 77802 Test Certificate #: 142620-001
Client Name, Sample Details

Holistic Healing Tim/RoseAnn
Troy, MI 48083
Sample: 3KBS Tincture
Type: Generic Concentrate
Method: FE04U12 HPLC-UV
Test Conditions

Prepsheet ID#: MIP231023A
Scale: XS205-MI2
Temp: 22.5 °C
Baro Pressure: 978.3 hPa
Analyst: ARH
Technician: ARH
Sample ID#: 142620

Harvest/Process Date: 10/25/2023
Serving Size (g): 28
Date Received: 10/25/2023
Test Date: 10/23/2023
Valid Through: 10/23/2024
Report Issued: 10/27/2023
Sample #142620
Sample #142620 Sample #142620
Test
Compounds		 Δ9-THC THCA Δ8-THC CBD CBDA CBG CBGA CBN CBC CBL THCV CBDV Total
Cannabinoids*		 Total THC Total CBD Calc Max Total
Cannabinoids*
Amount (%) N/D N/D N/D 13.1 N/D 0.1 N/D 0.1 0.1 N/D N/D 0.1 13.5 0.0 13.1 13.5
Amount (mg/g) 0.2 N/D N/D 130.7 N/D 0.9 N/D 0.7 1.2 0.1 N/D 1.2 135 0.2 130.7 135.0
Amount per Serving (mg) 5.6 N/D N/D 3659.6 N/D 25.2 N/D 19.6 33.6 2.8 N/D 33.6 3,780.0  
LOQ (mg/g) 0.08 0.08 0.08 0.08 0.08 0.08 0.08 0.08 0.08 0.08 0.08 0.08   %Decarb. THC CBD
±%RPD 0.99% 4.46% 0.61% 1.12% 3.22% 5.34% 8.78% 0.01% 0.84% 1.18% 0.18% 0.83% 100% 100%

Serving Size = 1 bottle = 1 oz.

LOQ = Limit of Quantitation; %RPD = Relative Percent Deviation; %RSD = Relative Standard Deviation; N/D = Not Detected. *Designates values that are not currently included in the accredited scope of Iron Laboratories. *** Designates tests that use the SOP FE-45 (water activity meter) method. FE-45 is performed using AOAC 966.02 and 32.004-32.009.

FE-45 has relative expanded (k=2) uncertainties of 1.098% for moisture, 1.754% for water activity for unprocessed plant materials, and 13.102% for water activity for infused products.

Vitamin E acetate analysis has a relative expanded (k=2) uncertainty of 18.614%. Sample fails vitamin E acetate if VEA>100 ug/g.

Total THC and CBD is the calculated sum of Δ9-THC and Δ8-THC or CBD plus the amount of THC or CBD derived from THCA or CBDA, respectively.

These values are calculated by applying a molar correction factor of 0.877 to the THCA or the CBDA value. Calc Max Total Cannabinoids is the sum of Total THC, Total CBD, CBN, Total CBG, CBC, THCV, CBDV, and CBL. Total CBG is calculated as CBG plus CBGA*0.878 (the molar correction factor for CBGA to CBG conversion). %Decarb. THC and CBD refer to the percentage of Δ9-THC or CBD relative to THCA or CBDA, respectively.

Potency Action Limits
Product Type Action Limit
Concentrates & Vapes Delta-8 concentration cannot exceed 10%
Infused Products

Delta-8 cannot exceed 10% of the maximum THC limits;

Homogeneity must be ≤15% RSD; Variance must be ≤10%
Maximum THC (Sum of Delta-8 and Delta-9) Concentrations for Infused Products (in mg)

 Category

Medical

(Per Dose)

Medical

(Per Container)

Adult-Use

(Per Dose)

Adult-Use

(Per Container)
Infused edibles (gummies, baked goods, drink enhancers, syrup) 50 200 10 200
Medicinal products (capsules, tinctures, oil-based drops) 100 2000 10 200
Medicinal Products not consumed orally (suppositories, tampons, transdermal patches) 100 2000 100 2000
Beverages 10 100 10 100

This sample has not undergone random sampling and has not been tested for compliant state, batch representative testing. These results should therefore be used for research and development or quality control purposes only. Results apply to the sample as received.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
ARH - LM Iron laboratories ARH - LM

Iron Laboratories, LLC is an ISO/IEC 17025:2017 Testing Laboratory laboratory accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

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IRON Laboratories     PJLA

ISO/IEC 17025:2017 Accredited

QC Report
Testing Accreditation #: 77802 Test Certificate #: 142620-001
Client Name, Sample Details

Holistic Healing Tim/RoseAnn
Troy, MI 48083
Sample: 3KBS Tincture
Type: Generic Concentrate
Method: FE04U12 HPLC-UV
Test Conditions

Prepsheet ID#: MIP231023A
Scale: XS205-MI2
Temp: 22.5 °C
Baro Pressure: 978.3 hPa
Analyst: ARH
Technician: ARH
Sample ID#: 142620

Harvest/Process Date: 10/25/2023
Serving Size (g): 28
Date Received: 10/25/2023
Test Date: 10/23/2023
Valid Through: 10/23/2024
Report Issued: 10/27/2023
Sample #142620
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Δ9-THC 0 6.16325 6.24956 101.40 6.18776 100.40 0.99%
THCA 0 4.92926 5.17288 104.94 4.9471 100.36 4.46%
Δ8-THC 0 5.49674 5.61131 102.08 5.57733 101.47 0.61%
CBD 0 6.32702 6.03182 95.33 5.96454 94.27 1.12%
CBDA 0 4.94839 4.88574 98.73 4.73078 95.60 3.22%
CBG 0 7.15938 6.89373 96.29 6.535 91.28 5.34%
CBGA 0 5.47674 5.45068 99.52 4.992 91.15 8.78%
CBN 0 5.65738 5.60935 99.15 5.61014 99.16 0.01%
CBC 0 5.48346 5.44452 99.29 5.49065 100.13 0.84%
CBCA 0 0 0.00 0 0.00 0%
CBL 0 5.31562 5.40653 101.71 5.47084 102.92 1.18%
THCV 0 5.52776 5.54338 100.28 5.55364 100.47 0.18%
CBDV 0 5.55056 5.29597 95.41 5.34 96.21 0.83%

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

This sample has not undergone random sampling and has not been tested for compliant state, batch representative testing. These results should therefore be used for research and development or quality control purposes only. Results apply to the sample as received.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
ARH - LM Iron laboratories ARH - LM

Iron Laboratories, LLC is an ISO/IEC 17025:2017 Testing Laboratory laboratory accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

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