IRON Laboratories     PJLA

ISO/IEC 17025:2017 Accredited

Marihuana Potency Analysis by
High Performance Liquid Chromatography
Testing Accreditation #: 77802 Test Certificate #: 142544-001
Client Name, Sample Details

Holistic Healing Tim/RoseAnn
Troy, MI 48083
Sample: Tincture 1 1oz
Type: Generic Concentrate
Method: FE04U12 HPLC-UV
Test Conditions

Prepsheet ID#: MIP230927C
Scale: XS205-MI2
Temp: 22.9 °C
Baro Pressure: 982.9 hPa
Analyst: ARH
Technician: ARH
Sample ID#: 142544

Harvest/Process Date: 09/28/2023
Serving Size (g): 0.92
Date Received: 09/28/2023
Test Date: 09/27/2023
Valid Through: 09/27/2024
Report Issued: 10/03/2023
Sample #142544
Sample #142544 Sample #142544
Test
Compounds		 Δ9-THC THCA Δ8-THC CBD CBDA CBG CBGA CBN CBC CBL THCV CBDV Total
Cannabinoids*		 Total THC Total CBD Calc Max Total
Cannabinoids*
Amount (%) 0.1 N/D N/D 5.8 N/D 5.0 N/D N/D 0.3 N/D N/D 0.1 11.4 0.1 5.8 11.4
Amount (mg/g) 1.4 N/D N/D 58.0 N/D 50.4 N/D N/D 3.4 N/D N/D 0.6 113.8 1.4 58.0 113.8
Amount per Serving (mg) 1.288 N/D N/D 53.36 N/D 46.368 N/D N/D 3.128 N/D N/D 0.552 104.7 Serving Size~ (g): 0.9
LOQ (mg/g) 0.2 0.2 0.2 0.2 0.2 0.2 0.2 0.2 0.2 0.2 0.2 0.2   %Decarb. THC CBD
±%RPD 2.78% 2.63% 5.08% 2.96% 2.70% 3.28% 2.69% 3.03% 2.96% 2.74% 2.18% 2.99% 100% 100%

serving size = 1ml = 0.92g.

LOQ = Limit of Quantitation; %RPD = Relative Percent Deviation; %RSD = Relative Standard Deviation; N/D = Not Detected

*Designates values that are not currently included in the accredited scope of Iron Laboratories.

*** Designates tests that use the method FE-45. FE-45 is performed using AOAC 966.02 and 32.004-32.009.

FE-45 has relative expanded (k=2) uncertainties of 1.098% for moisture, 1.754% for water activity for unprocessed plant materials, and 13.102% for water activity for infused products.

Vitamin E acetate analysis has a relative expanded (k=2) uncertainty of 18.614%.

Total THC and CBD is the calculated sum of Δ9-THC and Δ8-THC or CBD plus the amount of THC or CBD derived from THCA or CBDA, respectively.

These values are calculated by applying a molar correction factor of 0.877 to the THCA or the CBDA value.

Calc Max Total Cannabinoids is the sum of Total THC, Total CBD, CBN, Total CBG, CBC, THCV, CBDV, and CBL.

Total CBG is calculated as CBG plus CBGA*0.878 (the molar correction factor for CBGA to CBG conversion).

%Decarb. THC and CBD refer to the percentage of Δ9-THC or CBD relative to THCA or CBDA, respectively.

This sample has not undergone random sampling and has not been tested for compliant state, batch representative testing. These results should therefore be used for research and development or quality control purposes only. Results apply to the sample as received.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
ARH - LM Iron laboratories ARH - LM

Iron Laboratories, LLC is an ISO/IEC 17025:2017 Testing Laboratory laboratory accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

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IRON Laboratories     PJLA

ISO/IEC 17025:2017 Accredited

QC Report
Testing Accreditation #: 77802 Test Certificate #: 142544-001
Client Name, Sample Details

Holistic Healing Tim/RoseAnn
Troy, MI 48083
Sample: Tincture 1 1oz
Type: Generic Concentrate
Method: FE04U12 HPLC-UV
Test Conditions

Prepsheet ID#: MIP230927C
Scale: XS205-MI2
Temp: 22.9 °C
Baro Pressure: 982.9 hPa
Analyst: ARH
Technician: ARH
Sample ID#: 142544

Harvest/Process Date: 09/28/2023
Serving Size (g): 0.92
Date Received: 09/28/2023
Test Date: 09/27/2023
Valid Through: 09/27/2024
Report Issued: 10/03/2023
Sample #142544
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Δ9-THC 0 5.80095 5.80867 100.13 5.64943 97.39 2.78%
THCA 0 5.76525 5.6873 98.65 5.53975 96.09 2.63%
Δ8-THC 0 5.81406 5.78946 99.58 5.5025 94.64 5.08%
CBD 0 5.85636 5.88993 100.57 5.71824 97.64 2.96%
CBDA 0 5.76815 5.75904 99.84 5.60542 97.18 2.70%
CBG 0 5.83374 5.87654 100.73 5.68695 97.48 3.28%
CBGA 0 5.6515 5.66031 100.16 5.50996 97.50 2.69%
CBN 0 5.79766 5.85022 100.91 5.67549 97.89 3.03%
CBC 0 5.75163 5.69039 98.94 5.52418 96.05 2.96%
CBCA 0 0 0.00 0 0.00 0%
CBL 0 5.67173 5.54694 97.80 5.39692 95.15 2.74%
THCV 0 5.75308 5.72757 99.56 5.6043 97.41 2.18%
CBDV 0 5.77703 5.91059 102.31 5.73647 99.30 2.99%

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

This sample has not undergone random sampling and has not been tested for compliant state, batch representative testing. These results should therefore be used for research and development or quality control purposes only. Results apply to the sample as received.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
ARH - LM Iron laboratories ARH - LM

Iron Laboratories, LLC is an ISO/IEC 17025:2017 Testing Laboratory laboratory accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

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