IRON Laboratories     PJLA

ISO/IEC 17025:2017 Accredited

Marihuana Potency Analysis by
High Performance Liquid Chromatography
Testing Accreditation #: 77802 Test Certificate #: 140143-001
Client Name, Sample Details

Greenroom Gardens LLC AU-G-C-000910
Muskegon, MI 49441
Sample: Sticky Zkittle
License: AU-G-C-000910
Type: Flower
Method: FE04U12 HPLC-UV
Metrc Test Pkg#: 1A4050300032E11000000370
Metrc Source Pkg#: 1A4050300032E11000000366
***Water Activity: 0.55
Test Conditions

Prepsheet ID#: MIP230403A
Scale: XS205-MI2
Temp: 21.7 °C
Baro Pressure: 972.6 hPa
Analyst: KEB
Technician: KEB
Sample ID#: 140143

Harvest/Process Date: 03/30/2023
Serving Size (g): 1
Date Received: 03/30/2023
Test Date: 04/03/2023
Valid Through: 04/03/2024
Report Issued: 04/04/2023
Sample #140143
Sample #140143 Sample #140143
Test
Compounds		 Δ9-THC THCA Δ8-THC CBD CBDA CBG CBGA CBN CBC CBL THCV CBDV Total
Cannabinoids*		 Total THC Total CBD Calc Max Total
Cannabinoids*
Amount (%) 0.9 21.1 N/D N/D 0.1 0.2 0.3 N/D N/D N/D N/D N/D 22.5 19.3 0.1 19.9
Amount (mg/g) 8.7 210.5 N/D N/D 0.8 2.2 2.85 N/D N/D N/D N/D N/D 225.05 193.3 0.7 198.7
Amount per Serving (mg) 8.7 210.5 N/D N/D 0.8 2.2 2.85 N/D N/D N/D N/D N/D 225.1 Serving Size~ (g): 1.0
LOQ (mg/g) 0.72 0.72 0.72 0.72 0.72 0.72 0.72 0.72 0.72 0.72 0.72 0.72   %Decarb. THC CBD
±%RPD 1.91% 3.35% 1.70% 1.64% 1.34% 1.74% 1.77% 1.10% 1.88% 4.58% 1.53% 1.58% 4 0%

Sample passes for water activity (sample fails if Aw>0.65).

LOQ = Limit of Quantitation; %RPD = Relative Percent Deviation; %RSD = Relative Standard Deviation; N/D = Not Detected

*Designates values that are not currently included in the accredited scope of Iron Laboratories.

*** Designates tests that use the method FE-45. FE-45 is performed using AOAC 966.02 and 32.004-32.009.

FE-45 has relative expanded (k=2) uncertainties of 1.098% for moisture, 1.754% for water activity for unprocessed plant materials, and 13.102% for water activity for infused products.

Vitamin E acetate analysis has a relative expanded (k=2) uncertainty of 18.614%.

Total THC and CBD is the calculated sum of Δ9-THC and Δ8-THC or CBD plus the amount of THC or CBD derived from THCA or CBDA, respectively.

These values are calculated by applying a molar correction factor of 0.877 to the THCA or the CBDA value.

Calc Max Total Cannabinoids is the sum of Total THC, Total CBD, CBN, Total CBG, CBC, THCV, CBDV, and CBL.

Total CBG is calculated as CBG plus CBGA*0.878 (the molar correction factor for CBGA to CBG conversion).

%Decarb. THC and CBD refer to the percentage of Δ9-THC or CBD relative to THCA or CBDA, respectively.

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
KEB - LM Iron laboratories KEB - LM

Iron Laboratories, LLC is an ISO/IEC 17025:2017 Testing Laboratory laboratory accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 1 of 7

IRON Laboratories     PJLA

ISO/IEC 17025:2017 Accredited

QC Report
Testing Accreditation #: 77802 Test Certificate #: 140143-001
Client Name, Sample Details

Greenroom Gardens LLC AU-G-C-000910
Muskegon, MI 49441
Sample: Sticky Zkittle
License: AU-G-C-000910
Type: Flower
Method: FE04U12 HPLC-UV
Metrc Test Pkg#: 1A4050300032E11000000370
Metrc Source Pkg#: 1A4050300032E11000000366
***Water Activity: 0.55
Test Conditions

Prepsheet ID#: MIP230403A
Scale: XS205-MI2
Temp: 21.7 °C
Baro Pressure: 972.6 hPa
Analyst: KEB
Technician: KEB
Sample ID#: 140143

Harvest/Process Date: 03/30/2023
Serving Size (g): 1
Date Received: 03/30/2023
Test Date: 04/03/2023
Valid Through: 04/03/2024
Report Issued: 04/04/2023
Sample #140143
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Δ9-THC 0 5.3982 5.39561 99.95 5.29371 98.06 1.91%
THCA 0 5.03854 4.93031 97.85 5.09817 101.18 3.35%
Δ8-THC 0 5.47999 5.17737 94.48 5.26605 96.10 1.70%
CBD 0 5.21168 5.17947 99.38 5.2652 101.03 1.64%
CBDA 0 5.09738 5.06736 99.41 5.13568 100.75 1.34%
CBG 0 5.18057 5.14418 99.30 5.23463 101.04 1.74%
CBGA 0 5.14986 5.08239 98.69 5.17301 100.45 1.77%
CBN 0 5.05864 5.00854 99.01 5.06398 100.11 1.10%
CBC 0 5.03445 4.98064 98.93 5.0754 100.81 1.88%
CBCA N/A 0 0 0.00 0 0.00 0%
CBL 0 5.20261 5.13755 98.75 5.37836 103.38 4.58%
THCV 0 5.17243 5.14468 99.46 5.22421 101.00 1.53%
CBDV 0 5.10595 5.1455 100.77 5.22722 102.38 1.58%

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
KEB - LM Iron laboratories KEB - LM

Iron Laboratories, LLC is an ISO/IEC 17025:2017 Testing Laboratory laboratory accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 2 of 7

IRON Laboratories     PJLA

ISO/IEC 17025:2017 Accredited

Pesticide Analysis by
Mass Spectrometer
Testing Accreditation #: 77802 Test Certificate #: 140143-001
Client Name, Sample Details

Greenroom Gardens LLC AU-G-C-000910
Muskegon, MI 49441
Sample: Sticky Zkittle
License: AU-G-C-000910
Type: Flower
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A4050300032E11000000370
Metrc Source Pkg#: 1A4050300032E11000000366
Test Conditions

Prepsheet ID#: MIPS230331a
Scale: XS205-MI1
Temp: 22.4 °C
Baro PE: 969.2 hPa
Analyst: MEH
Technician: MK
Sample ID#: 140143

Harvest/Process Date: 03/30/2023
Serving Size (g): 1
Date Received: 03/30/2023
Test Date: 03/31/2023
Valid Through: 03/30/2024
Report Issued: 04/03/2023
Sample #140143
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
Aldicarb 0.400 0.125 Pass/<LOD Abamectin**** 0.500 0.125 Pass/<LOD
Acephate 0.400 0.125 Pass/<LOD Acequinocyl 2.000 0.250 Pass/<LOD
Acetamiprid 0.200 0.125 Pass/<LOD Azoxystrobin 0.200 0.125 Pass/<LOD
Bifenazate 0.200 0.125 Pass/<LOD Bifenthrin 0.200 0.125 Pass/<LOD
Boscalid 0.400 0.125 Pass/<LOD Carbaryl 0.200 0.125 Pass/<LOD
Carbofuran 0.200 0.125 Pass/<LOD Chlorantraniliprole 0.200 0.125 Pass/<LOD
Chlorfenapyr 1.000 0.500 Pass/<LOD Chlorpyrifos 0.200 0.125 Pass/<LOD
Clofentezine 0.200 0.125 Pass/<LOD Cyfluthrin** 1.000 0.500 Pass/<LOD
Cypermethrin*** 1.000 0.500 Pass/<LOD Daminozide 1.000 0.500 Pass/<LOD
DDVP (Dichlorvos) 1.000 0.250 Pass/<LOD Diazinon 0.200 0.125 Pass/<LOD
Dimethoate 0.200 0.125 Pass/<LOD Ethoprophos 0.200 0.125 Pass/<LOD
Etofenprox 0.400 0.125 Pass/<LOD Etoxazole 0.200 0.125 Pass/<LOD
Fenoxycarb 0.200 0.125 Pass/<LOD Fenpyroximate 0.400 0.125 Pass/<LOD
Fipronil 0.400 0.125 Pass/<LOD Flonicamid 1.000 0.125 Pass/<LOD
Fludioxonil 0.400 0.125 Pass/<LOD Hexythiazox 1.000 0.125 Pass/<LOD
Imazalil 0.200 0.125 Pass/<LOD Imidacloprid 0.400 0.125 Pass/<LOD
Kresoxim Methyl 0.400 0.125 Pass/<LOD Malathion 0.200 0.125 Pass/<LOD
Metalaxyl 0.200 0.125 Pass/<LOD Methiocarb 0.200 0.125 Pass/<LOD
Methomyl 0.400 0.125 Pass/<LOD Methyl Parathion 0.200 0.125 Pass/<LOD
MGK-264‡ 0.200 0.125 Pass/<LOD Myclobutanil 0.200 0.125 Pass/<LOD
Naled 0.500 0.125 Pass/<LOD Oxamyl 1.000 0.125 Pass/<LOD
Paclobutrazol 0.400 0.125 Pass/<LOD Permethrins† 0.200 0.125 Pass/<LOD
Phosmet 0.200 0.125 Pass/<LOD Piperonyl Butoxide 100.000 1.900 Not Tested
Prallethrin 0.200 0.125 Pass/<LOD Propiconazole 0.400 0.125 Pass/<LOD
Propoxur 0.200 0.125 Pass/<LOD Pyrethrins* 1.000 0.125 Pass/0.232
Pyridaben 0.200 0.125 Pass/<LOD Spinosad***** 0.200 0.125 Pass/<LOD
Spiromesifen 0.200 0.125 Pass/<LOD Spirotetramat 0.200 0.125 Pass/<LOD
Spiroxamine‡ 0.400 0.125 Pass/<LOD Tebuconazole 0.400 0.125 Pass/<LOD
Thiacloprid 0.200 0.125 Pass/<LOD Thiamethoxam 0.200 0.125 Pass/<LOD
Trifloxystrobin 0.200 0.125 Pass/<LOD

* Pyrethrins are reported as the sum of Jasmolin I, Cinerin I, and Pyrethrin I
** Cyfluthrins are reported as the sum of isomers Cyfluthrin I, II, III, and IV
*** Cypermethrins are reported as the sum of isomers Cypermethrin I, II, III, and IV
**** Abamectin is reported as the sum of Avermectin B1a and Avermectin B1b
***** Spinosad is reported as the sum of Spinosyn A and Spinosyn D
† Permethrin and Prallethrin are reported as the sum of cis and trans isomers
‡ MGK-264 and Spiroximine are reported as the sum of isomers I and II
MRL - Maximum Residue Limit; LOD - Limit of Detection

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
KEB - LM Iron laboratories KEB - LM

Iron Laboratories, LLC is an ISO/IEC 17025:2017 Testing Laboratory laboratory accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 2 of 7

IRON Laboratories     PJLA

ISO/IEC 17025:2017 Accredited

Pesticide QC Report
Testing Accreditation #: 77802 Test Certificate #: 140143-001
Client Name, Sample Details

Greenroom Gardens LLC AU-G-C-000910
Muskegon, MI 49441
Sample: Sticky Zkittle
License: AU-G-C-000910
Type: Flower
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A4050300032E11000000370
Metrc Source Pkg#: 1A4050300032E11000000366
Test Conditions

Prepsheet ID#: MIPS230331a
Scale: XS205-MI1
Temp: 22.4 °C
Baro PE: 969.2 hPa
Analyst: MEH
Technician: MK
Sample ID#: 140143

Harvest/Process Date: 03/30/2023
Serving Size (g): 1
Date Received: 03/30/2023
Test Date: 03/31/2023
Valid Through: 03/30/2024
Report Issued: 04/03/2023
Sample #140143
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS recovery% MSD recovery% Relative Percent Difference (%) QC Flag
Acephate N.D. 1 0.834 0.601 83.40 60.10 32.47 Q
Acequinocyl N.D. 1 0.122 0.204 12.20 20.40 50.31 LRQ
Acetamiprid N.D. 1 0.816 1.03 81.60 103.00 23.19
Aldicarb N.D. 1 0.88 1.07 88.00 107.00 19.49
Avermectin B1a N.D. 1 0.738 1.06 73.80 106.00 35.82 Q
Azoxystrobin N.D. 1 0.673 0.882 67.30 88.20 26.88
Bifenazate N.D. 1 0.645 0.88 64.50 88.00 30.82 Q
Bifenthrin N.D. 1 0.696 1.01 69.60 101.00 36.81 Q
Boscalid N.D. 1 0.78 1.08 78.00 108.00 32.26 Q
Carbaryl N.D. 1 0.732 0.828 73.20 82.80 12.31
Carbofuran N.D. 1 0.821 0.949 82.10 94.90 14.46
Chlorantraniliprole N.D. 1 0.73 1.07 73.00 107.00 37.78 Q
Chlorfenapyr N.D. 1 1.14 1.17 114.00 117.00 2.60
Chlorpyriphos N.D. 1 0.703 1.01 70.30 101.00 35.84 Q
Clofentezine N.D. 1 1.21 1.96 121.00 196.00 47.32 HRQ
Cyfluthrin N.D. 1 0.76 1.16 76.00 116.00 41.67 Q
Cypermethrin N.D. 1 0.606 0.984 60.60 98.40 47.55 Q
Daminoside N.D. 1 0.191 0.253 19.10 25.30 27.93 LR
Diazanon N.D. 1 1.08 1.46 108.00 146.00 29.92 HR
Dichlorvos N.D. 1 0.81 1.01 81.00 101.00 21.98
Dimethoate N.D. 1 0.851 1.02 85.10 102.00 18.07
Ethoprophos N.D. 1 0.704 0.943 70.40 94.30 29.02
Etofenprox N.D. 1 0.00738 0.458 0.74 45.80 193.66 LRQ
Etoxazole N.D. 1 0.805 1.11 80.50 111.00 31.85 Q
Fenoxycarb N.D. 1 0.841 1.16 84.10 116.00 31.88 Q
Fenpyroximate N.D. 1 0.729 1.09 72.90 109.00 39.69 Q
Fipronil N.D. 1 1.37 1.15 137.00 115.00 17.46 HR
Flonicamid N.D. 1 0.97 1.5 97.00 150.00 42.91 HRQ
Fludioxonil N.D. 1 1.46 1.14 146.00 114.00 24.62 HR
Hexythiazox N.D. 1 0.752 1.04 75.20 104.00 32.14 Q
Imazalil N.D. 1 0.716 0.905 71.60 90.50 23.32
Imidacloprid N.D. 1 0.709 0.926 70.90 92.60 26.54
Kresoxim-methyl N.D. 1 0.846 1.08 84.60 108.00 24.30
Malathion N.D. 1 0.767 1.04 76.70 104.00 30.22 Q
Metalaxyl N.D. 1 0.877 1.12 87.70 112.00 24.34
Methiocarb N.D. 1 0.787 1.36 78.70 136.00 53.38 HRQ
Methomyl N.D. 1 0.968 1.47 96.80 147.00 41.18 HRQ
MGK-264 N.D. 1 0.67 0.906 67.00 90.60 29.95
Myclobutanil N.D. 1 0.779 0.942 77.90 94.20 18.94
Naled (dibrom) N.D. 1 0.435 0.579 43.50 57.90 28.40 LR
Oxamyl N.D. 1 0.906 1.23 90.60 123.00 30.34 HRQ
Paclobutrazol N.D. 1 0.788 0.904 78.80 90.40 13.71
Parathion-methyl N.D. 1 1.03 1.06 103.00 106.00 2.87
Permethrins N.D. 1 0.783 1.136 78.30 113.60 36.79 Q
Phosmet N.D. 1 0.866 1.38 86.60 138.00 45.77 HRQ
Piperonyl butoxide N/A N/A N/A N/A nan nan N/A
Prallethrin N.D. 1 0.645 0.993 64.50 99.30 42.49 Q
Propiconazole N.D. 1 0.775 1.07 77.50 107.00 31.98 Q
Propoxur N.D. 1 0.805 0.997 80.50 99.70 21.31
Pyrethrin N.D. 1 0.736 1.02 73.60 102.00 32.35 Q
Pyridaben N.D. 1 0.714 1.06 71.40 106.00 39.01 Q
SpinosynA N.D. 0.82 0.377 0.568 45.98 69.27 40.42 LRQ
SpinosynD N.D. 0.18 0.114 0.159 63.33 88.33 32.97 Q
Spiromesifen N.D. 1 0.399 0.568 39.90 56.80 34.95 LRQ
Spirotetramat N.D. 1 0.635 0.897 63.50 89.70 34.20 Q
Spiroxamine N.D. 1 0.901 1.1 90.10 110.00 19.89
Tebuconazole N.D. 1 0.817 1.03 81.70 103.00 23.06
Thiacloprid N.D. 1 0.819 1.01 81.90 101.00 20.89
Thiamethoxam N.D. 1 0.819 0.919 81.90 91.90 11.51
Trifloxystrobin N.D. 1 0.74 1.08 74.00 108.00 37.36 Q

N.D. = Not Detected

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 30%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (60-120%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
KEB - LM Iron laboratories KEB - LM

Iron Laboratories, LLC is an ISO/IEC 17025:2017 Testing Laboratory laboratory accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 3 of 7

IRON Laboratories     PJLA

ISO/IEC 17025:2017 Accredited

Terpene Report by
Mass Spectrometer
Testing Accreditation #: 77802 Test Certificate #: 140143-001
Client Name, Sample Details

Greenroom Gardens LLC AU-G-C-000910
Muskegon, MI 49441
Sample: Sticky Zkittle
License: AU-G-C-000910
Type: Flower
Method: SOP FE-44-MI
Metrc Test Pkg#: 1A4050300032E11000000370
Metrc Source Pkg#: 1A4050300032E11000000366

Test Conditions

Scale: XS205-MI1
Temp: 21.8 °C
Baro Pressure: 974.5 hPa
Analyst: MEH
Technician: MEH

Sample ID#: 140143

Harvest/Process Date: 03/30/2023
Serving Size (g): 1
Date Received: 03/30/2023

Sample #140143
Sample #140143
  • α-Pinene (0.02%)
  • β-Ocimene (0.00%)
  • Camphene (0.01%)
  • Eucalyptol (1,8-Cineol) (0.00%)
  • Sabinene (0.00%)
  • γ-Terpinene (0.00%)
  • Myrcene (0.73%)
  • α-Terpinolene (0.00%)
  • β-Pinene (0.04%)
  • Linalool (0.10%)
  • ∆3-Carene (0.00%)
  • Fenchone (0.00%)
  • α-Terpinene (0.00%)
  • endo-Fenchol (0.00%)
  • α-Ocimene (0.00%)
  • Isopulegol (0.00%)
  • Limonene (0.17%)
  • Geraniol (0.01%)
  • p-Cymene (0.00%)
  • β-Caryophyllene (0.14%)
  • α-Humulene (0.03%)
  • Nerolidol 1 (cis) (0.00%)
  • Nerolidol 2 (trans) (0.01%)
  • Guaiol (0.00%)
  • Caryophyllene Oxide (0.00%)
  • α-Bisabolol (0.01%)
  • α-Phellandrene (0.00%)
  • α-Terpineol (0.00%)
  • Valenence (0.00%)

Total: 1.270%

Predominant Terpenes

0.73%   Myrcene Peppery, spicy balsam 0.17%   Limonene Citrus, orange, sweet
0.14%   β-Caryophyllene Sweet, woody, spicy, clove 0.10%   Linalool Citrus, floral, sweet, bois de rose, woody, green, blueberry
0.04%   β-Pinene Woody, fresh pine, hay 0.03%   α-Humulene Woody, oceanic-watery, spicy clove

Results should be interpreted as qualitative only (present/absent). Quantitative values are only estimations for the purpose of research and development, and are not included in Iron Laboratories accredited scope. Eucalyptol, Sabinene, Fenchone, endo-Fenchol, Caryophyllene Oxide, a-Phellandrene, a-Terpineol, and Valencene are not currently tested for by Iron Laboratories Michigan. LOQ = 0.01%. Expanded uncertainty (k=2) for terpene analysis is 25.92%.

Value in parenthesis indicates percentage of terpene present in the total sample (weight percentage, wt/wt%).
Value in doughnut slice indicates individual terpene abundance with respect to the total terpenes detected.

These results should be used for research and development or quality control purposes only. If applicable, results for caregivers apply to the sample as received.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
KEB - LM Iron laboratories KEB - LM

Iron Laboratories, LLC is an ISO/IEC 17025:2017 Testing Laboratory laboratory accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 4 of 7

IRON Laboratories     PJLA

ISO/IEC 17025:2017 Accredited

Microbiology Analysis
Testing Accreditation #: 77802 Test Certificate #: 140143-001
Client Name, Sample Details

Greenroom Gardens LLC AU-G-C-000910
Muskegon, MI 49441
Sample: Sticky Zkittle
License: AU-G-C-000910
Type: Flower
Metrc Test Pkg#: 1A4050300032E11000000370
Metrc Source Pkg#: 1A4050300032E11000000366
Test Conditions

Scale: XS205-MI1
Temp: 20.1 °C
Baro Pressure: 971.2 hPa
Analyst: SKM
Technician: SKM
Sample ID#: 140143

Harvest/Process Date: 03/30/2023
Serving Size (g): 1
Date Received: 03/30/2023
Test Date: 03/31/2023
Valid Through: 03/30/2024
Report Issued: 04/04/2023
Sample #140143
Test Method MCFU (CFU/g) LOD (CFU/g) Status (CFU/g)
Total Aerobic Not Tested N/A 0 Not Tested
Yeast & Mold FE-66 (MPN) 100,001 100 Pass/<LOD
Bile-tolerant gram-negative bacteria Not Tested N/A 0 Not Tested
Total Coliforms FE-66 (MPN) 1,001 100 Pass/<LOD
E. Coli FE-65 (PCR) 1 1 Pass/Not Present
Salmonella FE-65 (PCR) 1 1 Pass/Not Present
Aspergillus spp. FE-65 (PCR) 1 1 Pass/Not Present

E. coli test screens exclusively for Shiga toxin-producing E. coli. TNTC values for yeast and mold are >150,000 CFU/g. TNTC values for total coliforms are >15,000 CFU/g. The maximum relative uncertainty is 6% for PCR and 40% for MPN.

TNTC = Too Numerous To Count. Maximum Colony Forming Units (MCFU) represents the minimum value that a test would need to achieve in order to be considered a failed result (if applicable). LOD is the Limit of Detection for the method. CFU/g = Colony Forming Units per gram. Aspergillus spp. consists of A. flavus, A. fumigatus, A. niger, and A. terreus.

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
MEH QM Iron laboratories MEH QM

Iron Laboratories, LLC is an ISO/IEC 17025:2017 Testing Laboratory laboratory accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 5 of 7

IRON Laboratories     PJLA

ISO/IEC 17025:2017 Accredited

Bio Analysis by
Microscopic Visual Inspection
Testing Accreditation #: 77802 Test Certificate #: 140143-001
Client Name, Sample Details

Greenroom Gardens LLC AU-G-C-000910
Muskegon, MI 49441
Sample: Sticky Zkittle
License: AU-G-C-000910
Type: Flower
Method: FE02 Microscope Dissection
Metrc Test Pkg#: 1A4050300032E11000000370
Metrc Source Pkg#: 1A4050300032E11000000366
Test Conditions

Analyst: ARH
Technician: ARH
Sample ID#: 140143

Harvest/Process Date: 03/30/2023
Serving Size (g): 1
Date Received: 03/30/2023
Test Date: 03/30/2023
Valid Through: 03/29/2024
Report Issued: 03/31/2023
Sample #140143
Sample #140143 Sample #140143
Severity Rating
Mold and Mildew 0 Pass
Mites (not Russet) 0 Pass
Russet Mites 0 Pass
Thrips 0 Pass
Aphids 0 Pass
Other Pests 0 Pass
Other Organic Matter 0 Pass
Inorganic Matter 0 Pass
Total Organic Foreign Matter <2% Pass
Inorganic Foreign Matter 0% Pass
Stem Material <5% Pass
Severity Rating Key
Correlating %FM ≤2% FM >2% FM
Severity Rating 0 None 1 Mild 2 Moderate 3 Severe Units
Mold and Mildew <2 2 3 4+ Locations/g
Mites (not russet) <1 1-5 6-10 11+ Amount/g
Russet Mites <1 1-10 11-50 51+ Amount/g
Thrips <1 1-3 4-5 6+ Amount/g
Aphids <1 1 2-4 5+ Amount/g
Other Pests <1 1-5 6-10 11+ Amount/g
Other Organic Matter <1 1-5 6-10 11+ Amount/g
Inorganic Matter 0 — — >0 Amount/g

In compliance with the MMFLA regulation, the action limits for foreign matter are as follows; no more that 2% organic matter, 5% stem material, and no presence of inorganic matter. Percent foreign contamination is based off of total surface area.

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
MEH QM Iron laboratories MEH QM

Iron Laboratories, LLC is an ISO/IEC 17025:2017 Testing Laboratory laboratory accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 6 of 7

IRON Laboratories     PJLA

ISO/IEC 17025:2017 Accredited

Heavy Metals Analysis
Testing Accreditation #: 77802 Test Certificate #: 140143-001
Client Name, Sample Details

Greenroom Gardens LLC AU-G-C-000910
Muskegon, MI 49441
Sample: Sticky Zkittle
License: AU-G-C-000910
Type: Flower
Method: FE60 ICPMS-MI
Metrc Test Pkg#: 1A4050300032E11000000370
Metrc Source Pkg#: 1A4050300032E11000000366
Test Conditions

Prepsheet ID#: MIICP 230331fMK
Temp: 22.4 °C
Baro PE: 969.3 hPa
Analyst: MK
Technician: MK
Sample ID#: 140143

Harvest/Process Date: 03/30/2023
Serving Size (g): 1
Date Received: 03/30/2023
Test Date: 03/31/2023
Valid Through: 03/30/2024
Report Issued: 03/31/2023
Sample #140143
Sample #140143 Sample #140143
Test Compound MRL (PPM) LOD (PPM) Status (PPM)
Arsenic 0.4 0.1 Pass/<LOD
Copper 0 1.5 Not Tested
Cadmium 0.4 0.1 Pass/<LOD
Chromium 1.2 0.3 Pass/<LOD
Lead 1 0.25 Pass/<LOD
Mercury 0.2 0.05 Pass/<LOD
Nickel 1 0.25 Pass/<LOD

MRL - Maximum Residue Limit; LOD - Limit of Detection

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
MEH QM Iron laboratories MEH QM

Iron Laboratories, LLC is an ISO/IEC 17025:2017 Testing Laboratory laboratory accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 7 of 7

IRON Laboratories     PJLA

ISO/IEC 17025:2017 Accredited

QC Report
Testing Accreditation #: 77802 Test Certificate #: 140143-001
Client Name, Sample Details

Greenroom Gardens LLC AU-G-C-000910
Muskegon, MI 49441
Sample: Sticky Zkittle
License: AU-G-C-000910
Type: Flower
Method: FE60 ICPMS-MI
Metrc Test Pkg#: 1A4050300032E11000000370
Metrc Source Pkg#: 1A4050300032E11000000366
Test Conditions

Prepsheet ID#: MIICP 230331fMK
Temp: 22.4 °C
Baro PE: 969.3 hPa
Analyst: MK
Technician: MK
Sample ID#: 140143

Harvest/Process Date: 03/30/2023
Serving Size (g): 1
Date Received: 03/30/2023
Test Date: 03/31/2023
Valid Through: 03/30/2024
Report Issued: 03/31/2023
Sample #140143
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD QC Flag
Arsenic N/D 0.160 0.177 110.63 0.176 110.00
Cadmium N/D 0.160 0.175 109.38 0.174 108.75
Chromium N/D 0.480 0.477 99.38 0.487 101.46
Copper N/D 2.400 1.869 77.88 1.890 78.75
Lead N/D 0.400 0.433 108.25 0.432 108.00
Mercury N/D 0.080 0.093 116.25 0.088 110.00
Nickel N/D 0.400 0.531 132.75 0.537 134.25

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
MEH QM Iron laboratories MEH QM

Iron Laboratories, LLC is an ISO/IEC 17025:2017 Testing Laboratory laboratory accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 8 of 7