IRON Laboratories     PJLA

ISO/IEC 17025:2017 Accredited

Marihuana Potency Analysis by
High Performance Liquid Chromatography
Testing Accreditation #: 77802 Test Certificate #: 137090-001
Client Name, Sample Details

4432 Ace LLC AU-P-000233
Bay City, MI 48706
Sample: Covert Cups - S'mores Retest 1
License: AU-P-000233
Type: Edible
Method: FE04U12 HPLC-UV
Metrc Test Pkg#: 1A4050300029235000000395
Metrc Source Pkg#: 1A4050300009AB1000019300
Test Conditions

Prepsheet ID#: MIP220617B
Scale: XS205-MI2
Temp: 20.8 °C
Baro Pressure: 977.4 hPa
Technician: SKM
Sample ID#: 137090

Harvest/Process Date: 06/15/2022
Serving Size (g): 3.65
Date Received: 06/15/2022
Test Date: 06/17/2022
Valid Through: 06/18/2023
Report Issued: 06/20/2022
Sample #137090
Sample #137090 Sample #137090
Test
Compounds		 Δ9-THC THCA Δ8-THC CBD CBDA CBG CBGA CBN CBC CBL THCV CBDV Total
Cannabinoids*		 Total THC Total CBD Calc Max Total
Cannabinoids*
Amount (%) 0.2 N/D N/D N/D N/D N/D N/D N/D N/D N/D N/D N/D 0.3 0.3 0.0 0.3
Amount (mg/g) 2.4 N/D 0.4 N/D N/D 0.1 N/D N/D N/D N/D N/D N/D 2.9 2.8 0.0 2.9
Amount per Serving (mg) 8.76 N/D 1.46 N/D N/D 0.365 N/D N/D N/D N/D N/D N/D 10.6 Serving Size~ (g): 3.65 3.7
LOQ (mg/g) 0.04 0.04 0.04 0.04 0.04 0.04 0.04 0.04 0.04 0.04 0.04 0.04   %Decarb. THC CBD
±%RPD 0.15% 2.38% 2.37% 2.90% 0.04% 1.26% 0.54% 2.38% 0.26% 0.92% 0.70% 0.76% 100% N/A

Serving size = 1/5 cup, 10 servings per package.

LOQ = Limit of Quantitation; %RPD = Relative Percent Deviation; %RSD = Relative Standard Deviation; N/D = Not Detected

*Designates values that are not currently included in the accredited scope of Iron Laboratories.

*** Designates tests that use the method FE-45. FE-45 is performed using AOAC 966.02 and 32.004-32.009.

FE-45 has relative expanded (k=2) uncertainties of 1.098% for moisture, 1.754% for water activity for unprocessed plant materials, and 13.102% for water activity for infused products.

Vitamin E acetate analysis has a relative expanded (k=2) uncertainty of 18.614%.

Total THC and CBD is the calculated sum of Δ9-THC and Δ8-THC or CBD plus the amount of THC or CBD derived from THCA or CBDA, respectively.

These values are calculated by applying a molar correction factor of 0.877 to the THCA or the CBDA value.

Calc Max Total Cannabinoids is the sum of Total THC, Total CBD, CBN, Total CBG, CBC, THCV, CBDV, and CBL.

Total CBG is calculated as CBG plus CBGA*0.878 (the molar correction factor for CBGA to CBG conversion).

%Decarb. THC and CBD refer to the percentage of Δ9-THC or CBD relative to THCA or CBDA, respectively.

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
KEB - LM Iron laboratories KEB - LM

Iron Laboratories, LLC is an ISO/IEC 17025:2017 Testing Laboratory laboratory accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

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IRON Laboratories     PJLA

ISO/IEC 17025:2017 Accredited

QC Report
Testing Accreditation #: 77802 Test Certificate #: 137090-001
Client Name, Sample Details

4432 Ace LLC AU-P-000233
Bay City, MI 48706
Sample: Covert Cups - S'mores Retest 1
License: AU-P-000233
Type: Edible
Method: FE04U12 HPLC-UV
Metrc Test Pkg#: 1A4050300029235000000395
Metrc Source Pkg#: 1A4050300009AB1000019300
Test Conditions

Prepsheet ID#: MIP220617B
Scale: XS205-MI2
Temp: 20.8 °C
Baro Pressure: 977.4 hPa
Technician: SKM
Sample ID#: 137090

Harvest/Process Date: 06/15/2022
Serving Size (g): 3.65
Date Received: 06/15/2022
Test Date: 06/17/2022
Valid Through: 06/18/2023
Report Issued: 06/20/2022
Sample #137090
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Δ9-THC 0 5.53414 5.63546 101.83 5.6269 101.68 0.15%
THCA 0 5.57309 5.66359 101.62 5.53027 99.23 2.38%
Δ8-THC 0 6.10044 6.1923 101.51 6.34099 103.94 2.37%
CBD 0 5.81849 5.92121 101.77 5.7517 98.85 2.90%
CBDA 0 5.53523 5.51827 99.69 5.52025 99.73 0.04%
CBG 0 6.27721 6.33522 100.92 6.25567 99.66 1.26%
CBGA 0 5.88897 5.90808 100.32 5.87615 99.78 0.54%
CBN 0 5.66758 5.65815 99.83 5.79448 102.24 2.38%
CBC 0 6.05216 6.07728 100.42 6.09333 100.68 0.26%
CBCA 0 0 0.00 0 0.00 0%
CBL 0 6.13622 6.08132 99.11 6.02537 98.19 0.92%
THCV 0 6.06149 6.12664 101.07 6.08383 100.37 0.70%
CBDV 0 6.31653 6.01251 95.19 6.05842 95.91 0.76%

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
KEB - LM Iron laboratories KEB - LM

Iron Laboratories, LLC is an ISO/IEC 17025:2017 Testing Laboratory laboratory accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

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