IRON Laboratories     PJLA

ISO/IEC 17025:2017 Accredited

Marihuana Potency Analysis by
High Performance Liquid Chromatography
Testing Accreditation #: 77802 Test Certificate #: 136345-001
Client Name, Sample Details

Kenneth Rogers
Novi, MI 48377
Sample: Monkey Breath
Type: Flower
Method: FE04U12 HPLC-UV
Test Conditions

Prepsheet ID#: MIP220405A
Scale: XS205-MI2
Temp: 21.2 °C
Baro Pressure: 969.6 hPa
Analyst: SKM
Technician: SKM
Sample ID#: 136345

Harvest/Process Date: 04/06/2022
Serving Size (g): 1
Date Received: 04/06/2022
Test Date: 04/05/2022
Valid Through: 04/06/2023
Report Issued: 04/06/2022
Sample #136345
Sample #136345 Sample #136345
Test
Compounds		 Δ9-THC THCA Δ8-THC CBD CBDA CBG CBGA CBN CBC CBL THCV CBDV Total
Cannabinoids*		 Total THC Total CBD Calc Max Total
Cannabinoids*
Amount (%) 0.6 18.2 N/D N/D N/D 0.1 0.4 N/D N/D N/D N/D N/D 19.3 16.6 0.0 17.0
Amount (mg/g) 5.9 182.1 N/D N/D N/D 1.3 3.56 N/D N/D N/D N/D N/D 192.86 165.6 0.0 170.0
Amount per Serving (mg) 5.9 182.1 N/D N/D N/D 1.3 3.56 N/D N/D N/D N/D N/D 192.9 Serving Size~ (g): 1.0
LOQ (mg/g) 0.74 0.74 0.74 0.74 0.74 0.74 0.74 0.74 0.74 0.74 0.74 0.74   %Decarb. THC CBD
±%RPD 0.72% 0.56% 1.66% 0.89% 0.37% 0.82% +/-5% 0.52% 0.46% 2.41% 0.74% 0.60% 3 N/A

LOQ = Limit of Quantitation; %RPD = Relative Percent Deviation; %RSD = Relative Standard Deviation; N/D = Not Detected

*Designates values that are not currently included in the accredited scope of Iron Laboratories.

*** Designates tests that use the method FE-45. FE-45 is performed using AOAC 966.02 and 32.004-32.009.

FE-45 has relative expanded (k=2) uncertainties of 1.098% for moisture, 1.754% for water activity for unprocessed plant materials, and 13.102% for water activity for infused products.

Vitamin E acetate analysis has a relative expanded (k=2) uncertainty of 18.614%.

Total THC and CBD is the calculated sum of Δ9-THC and Δ8-THC or CBD plus the amount of THC or CBD derived from THCA or CBDA, respectively.

These values are calculated by applying a molar correction factor of 0.877 to the THCA or the CBDA value.

Calc Max Total Cannabinoids is the sum of Total THC, Total CBD, CBN, Total CBG, CBC, THCV, CBDV, and CBL.

Total CBG is calculated as CBG plus CBGA*0.878 (the molar correction factor for CBGA to CBG conversion).

%Decarb. THC and CBD refer to the percentage of Δ9-THC or CBD relative to THCA or CBDA, respectively.

This sample has not undergone random sampling and has not been tested for compliant state, batch representative testing. These results should therefore be used for research and development or quality control purposes only. Results apply to the sample as received.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
KEB - LM Iron laboratories KEB - LM

Iron Laboratories, LLC is an ISO/IEC 17025:2017 Testing Laboratory laboratory accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 1 of 2

IRON Laboratories     PJLA

ISO/IEC 17025:2017 Accredited

QC Report
Testing Accreditation #: 77802 Test Certificate #: 136345-001
Client Name, Sample Details

Kenneth Rogers
Novi, MI 48377
Sample: Monkey Breath
Type: Flower
Method: FE04U12 HPLC-UV
Test Conditions

Prepsheet ID#: MIP220405A
Scale: XS205-MI2
Temp: 21.2 °C
Baro Pressure: 969.6 hPa
Analyst: SKM
Technician: SKM
Sample ID#: 136345

Harvest/Process Date: 04/06/2022
Serving Size (g): 1
Date Received: 04/06/2022
Test Date: 04/05/2022
Valid Through: 04/06/2023
Report Issued: 04/06/2022
Sample #136345
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Δ9-THC 0 5.58485 5.57603 99.84 5.61617 100.56 0.72%
THCA 0 5.15914 5.00198 96.95 4.97417 96.41 0.56%
Δ8-THC 0 5.69956 5.75157 100.91 5.65664 99.25 1.66%
CBD 0 5.27989 5.2762 99.93 5.22969 99.05 0.89%
CBDA 0 4.91506 4.89865 99.67 4.91687 100.04 0.37%
CBG 0 6.09092 6.06209 99.53 6.01263 98.71 0.82%
CBGA 0 5.04707 5.01479 99.36 5.01488 99.36 0.00%
CBN 0 5.22827 5.25196 100.45 5.22446 99.93 0.52%
CBC 0 5.82618 5.80784 99.69 5.7813 99.23 0.46%
CBCA N/A 0 0 0.00 0 0.00 0%
CBL 0 5.81787 5.74302 98.71 5.60626 96.36 2.41%
THCV 0 5.81853 5.81401 99.92 5.77138 99.19 0.74%
CBDV 0 5.7516 5.72788 99.59 5.76227 100.19 0.60%

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

This sample has not undergone random sampling and has not been tested for compliant state, batch representative testing. These results should therefore be used for research and development or quality control purposes only. Results apply to the sample as received.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
KEB - LM Iron laboratories KEB - LM

Iron Laboratories, LLC is an ISO/IEC 17025:2017 Testing Laboratory laboratory accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

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IRON Laboratories     PJLA

ISO/IEC 17025:2017 Accredited

Terpene Report by
Mass Spectrometer
Testing Accreditation #: 77802 Test Certificate #: 136345-001
Client Name, Sample Details

Kenneth Rogers
Novi, MI 48377
Sample: Monkey Breath
Type: Flower
Method: SOP FE-44-MI

Test Conditions

Scale: XS205-MI2
Temp: 20.9 °C
Baro Pressure: 975.6 hPa
Analyst: SKM
Technician: SKM

Sample ID#: 136345

Harvest/Process Date: 04/06/2022
Serving Size (g): 1
Date Received: 04/06/2022

Sample #136345
Sample #136345
  • α-Pinene (0.02%)
  • β-Ocimene (0.00%)
  • Camphene (0.01%)
  • Eucalyptol (1,8-Cineol) (0.00%)
  • Sabinene (0.00%)
  • γ-Terpinene (0.00%)
  • Myrcene (0.06%)
  • α-Terpinolene (0.00%)
  • β-Pinene (0.05%)
  • Linalool (0.05%)
  • ∆3-Carene (0.00%)
  • Fenchone (0.00%)
  • α-Terpinene (0.00%)
  • endo-Fenchol (0.00%)
  • α-Ocimene (0.00%)
  • Isopulegol (0.00%)
  • Limonene (0.10%)
  • Geraniol (0.00%)
  • p-Cymene (0.00%)
  • β-Caryophyllene (0.62%)
  • α-Humulene (0.19%)
  • Nerolidol 1 (cis) (0.03%)
  • Nerolidol 2 (trans) (0.00%)
  • Guaiol (0.00%)
  • Caryophyllene Oxide (0.00%)
  • α-Bisabolol (0.13%)
  • α-Phellandrene (0.00%)
  • α-Terpineol (0.00%)
  • Valenence (0.00%)

Total: 1.260%

Predominant Terpenes

0.62%   β-Caryophyllene Sweet, woody, spicy, clove 0.19%   α-Humulene Woody, oceanic-watery, spicy clove
0.13%   α-Bisabolol Fruity, nutty, coconut 0.10%   Limonene Citrus, orange, sweet
0.06%   Myrcene Peppery, spicy balsam 0.05%   β-Pinene Woody, fresh pine, hay

Results should be interpreted as qualitative only (present/absent). Quantitative values are only estimations for the purpose of research and development, and are not included in Iron Laboratories accredited scope. Eucalyptol, Sabinene, Fenchone, endo-Fenchol, Caryophyllene Oxide, a-Phellandrene, a-Terpineol, and Valencene are not currently tested for by Iron Laboratories Michigan. LOQ = 0.01%. Expanded uncertainty (k=2) for terpene analysis is 25.92%.

Value in parenthesis indicates percentage of terpene present in the total sample (weight percentage, wt/wt%).
Value in doughnut slice indicates individual terpene abundance with respect to the total terpenes detected.

These results should be used for research and development or quality control purposes only. If applicable, results for caregivers apply to the sample as received.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
KEB - LM Iron laboratories KEB - LM

Iron Laboratories, LLC is an ISO/IEC 17025:2017 Testing Laboratory laboratory accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 2 of 2