Harvest/Process Date: 04/06/2022 Serving Size (g): 1 Date Received: 04/06/2022 Test Date: 04/05/2022 Valid Through: 04/06/2023 Report Issued: 04/06/2022
Test Compounds
Δ9-THC
THCA
Δ8-THC
CBD
CBDA
CBG
CBGA
CBN
CBC
CBL
THCV
CBDV
Total Cannabinoids*
Total THC
Total CBD
Calc Max Total Cannabinoids*
Amount (%)
0.6
18.2
N/D
N/D
N/D
0.1
0.4
N/D
N/D
N/D
N/D
N/D
19.3
16.6
0.0
17.0
Amount (mg/g)
5.9
182.1
N/D
N/D
N/D
1.3
3.56
N/D
N/D
N/D
N/D
N/D
192.86
165.6
0.0
170.0
Amount per Serving (mg)
5.9
182.1
N/D
N/D
N/D
1.3
3.56
N/D
N/D
N/D
N/D
N/D
192.9
Serving Size~ (g):
1.0
LOQ (mg/g)
0.74
0.74
0.74
0.74
0.74
0.74
0.74
0.74
0.74
0.74
0.74
0.74
%Decarb.
THC
CBD
±%RPD
0.72%
0.56%
1.66%
0.89%
0.37%
0.82%
+/-5%
0.52%
0.46%
2.41%
0.74%
0.60%
3
N/A
LOQ = Limit of Quantitation; %RPD = Relative Percent Deviation; %RSD = Relative Standard Deviation; N/D = Not Detected
*Designates values that are not currently included in the accredited scope of Iron Laboratories.
*** Designates tests that use the method FE-45. FE-45 is performed using AOAC 966.02 and 32.004-32.009.
FE-45 has relative expanded (k=2) uncertainties of 1.098% for moisture, 1.754% for water activity for unprocessed plant materials, and 13.102% for water activity for infused products.
Vitamin E acetate analysis has a relative expanded (k=2) uncertainty of 18.614%.
Total THC and CBD is the calculated sum of Δ9-THC and Δ8-THC or CBD plus the amount of THC or CBD derived from THCA or CBDA, respectively.
These values are calculated by applying a molar correction factor of 0.877 to the THCA or the CBDA value.
Calc Max Total Cannabinoids is the sum of Total THC, Total CBD, CBN, Total CBG, CBC, THCV, CBDV, and CBL.
Total CBG is calculated as CBG plus CBGA*0.878 (the molar correction factor for CBGA to CBG conversion).
%Decarb. THC and CBD refer to the percentage of Δ9-THC or CBD relative to THCA or CBDA, respectively.
This sample has not undergone random sampling and has not been tested for compliant state, batch representative testing. These results should therefore be used for research and development or quality control purposes only. Results apply to the sample as received.
This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Iron Laboratories, LLC is an ISO/IEC 17025:2017 Testing Laboratory laboratory accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802
Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390
Harvest/Process Date: 04/06/2022 Serving Size (g): 1 Date Received: 04/06/2022 Test Date: 04/05/2022 Valid Through: 04/06/2023 Report Issued: 04/06/2022
Target Compound Name
Method Blank (μg/g)
LCS Spike (μg/g)
LCS Amount (μg/g)
Percent Recovery (%) LCS
LCS Duplicate Amount (μg/g)
Percent Recovery (%) LCSD
Relative Percent Difference (%)
QC Flag
Δ9-THC
0
5.58485
5.57603
99.84
5.61617
100.56
0.72%
THCA
0
5.15914
5.00198
96.95
4.97417
96.41
0.56%
Δ8-THC
0
5.69956
5.75157
100.91
5.65664
99.25
1.66%
CBD
0
5.27989
5.2762
99.93
5.22969
99.05
0.89%
CBDA
0
4.91506
4.89865
99.67
4.91687
100.04
0.37%
CBG
0
6.09092
6.06209
99.53
6.01263
98.71
0.82%
CBGA
0
5.04707
5.01479
99.36
5.01488
99.36
0.00%
CBN
0
5.22827
5.25196
100.45
5.22446
99.93
0.52%
CBC
0
5.82618
5.80784
99.69
5.7813
99.23
0.46%
CBCA
N/A
0
0
0.00
0
0.00
0%
CBL
0
5.81787
5.74302
98.71
5.60626
96.36
2.41%
THCV
0
5.81853
5.81401
99.92
5.77138
99.19
0.74%
CBDV
0
5.7516
5.72788
99.59
5.76227
100.19
0.60%
N.D. = Not Detected
LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.
I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.
Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%
HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.
This sample has not undergone random sampling and has not been tested for compliant state, batch representative testing. These results should therefore be used for research and development or quality control purposes only. Results apply to the sample as received.
This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Iron Laboratories, LLC is an ISO/IEC 17025:2017 Testing Laboratory laboratory accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802
Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390
Harvest/Process Date: 04/06/2022 Serving Size (g): 1 Date Received: 04/06/2022
α-Pinene (0.02%)
β-Ocimene (0.00%)
Camphene (0.01%)
Eucalyptol (1,8-Cineol) (0.00%)
Sabinene (0.00%)
γ-Terpinene (0.00%)
Myrcene (0.06%)
α-Terpinolene (0.00%)
β-Pinene (0.05%)
Linalool (0.05%)
∆3-Carene (0.00%)
Fenchone (0.00%)
α-Terpinene (0.00%)
endo-Fenchol (0.00%)
α-Ocimene (0.00%)
Isopulegol (0.00%)
Limonene (0.10%)
Geraniol (0.00%)
p-Cymene (0.00%)
β-Caryophyllene (0.62%)
α-Humulene (0.19%)
Nerolidol 1 (cis) (0.03%)
Nerolidol 2 (trans) (0.00%)
Guaiol (0.00%)
Caryophyllene Oxide (0.00%)
α-Bisabolol (0.13%)
α-Phellandrene (0.00%)
α-Terpineol (0.00%)
Valenence (0.00%)
Total: 1.260%
Predominant Terpenes
0.62%
β-Caryophyllene
Sweet, woody, spicy, clove
0.19%
α-Humulene
Woody, oceanic-watery, spicy clove
0.13%
α-Bisabolol
Fruity, nutty, coconut
0.10%
Limonene
Citrus, orange, sweet
0.06%
Myrcene
Peppery, spicy balsam
0.05%
β-Pinene
Woody, fresh pine, hay
Results should be interpreted as qualitative only (present/absent). Quantitative values are only estimations for the purpose of research and development, and are not included in Iron Laboratories accredited scope. Eucalyptol, Sabinene, Fenchone, endo-Fenchol, Caryophyllene Oxide, a-Phellandrene, a-Terpineol, and Valencene are not currently tested for by Iron Laboratories Michigan. LOQ = 0.01%. Expanded uncertainty (k=2) for terpene analysis is 25.92%.
Value in parenthesis indicates percentage of terpene present in the total sample (weight percentage, wt/wt%).
Value in doughnut slice indicates individual terpene abundance with respect to the total terpenes detected.
These results should be used for research and development or quality control purposes only. If applicable, results for caregivers apply to the sample as received.
This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Iron Laboratories, LLC is an ISO/IEC 17025:2017 Testing Laboratory laboratory accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802
Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390