ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Marijuana Potency Analysis by
High Performance Liquid Chromatography

Testing Accreditation #: 4092-005 Test Certificate #: 136214-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Crater Lake Live Rosin
License: 030-1009646F7F8
Type: Tincture
Method: FE04U HPLC-UV
Metrc Test Pkg#: 1A4010300003A37000000914
Metrc Source Pkg#: 1A401030002C949000003557

Test Conditions

Prepsheet ID#: ORP220325a
Scale: XS205-OR1
Temp: 22.4 °C
Baro Pressure: 1004 hPa
Analyst: TMR
Technician: TMR

Sample ID#: 136214

Lot #: Crater Lake Live Rosin #1 3.2.2022
Batch #: 136214
Batch Weight (g): 184.4
Harvest/Process Date: 03/02/2022
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 03/29/2022
Test Date: 03/25/2022

Sample #136214
Sample #136214 Sample #136214
Test
Compounds
THC THCA CBD CBDA CBN CBG CBC THCV* CBDV Total
Cannabinoids*
Total THC Total CBD Calc Max Total
Cannabinoids*
Amount (%) 4.10 80.97 N/D 2.37 N/D 0.70 N/D N/D N/D 88.14 75.11 2.08 77.89
Amount (mg/g) 40.97 809.73 N/D 23.70 N/D 7.00 N/D N/D N/D 881.4 751.10 20.78 778.88
Amount per Serving (mg) 2.05 40.49 N\D 1.19 N\D 0.35 N\D N\D N\D 44.07 Serving Size~ (g): 0.05
LOQ (mg/g) 1.9 1.9 1.9 1.9 1.9 1.9 1.9 1.9 1.9   %Decarb. THC CBD
±%RPD 8.58 5.40 1.88 9.73 12.50 7.81 29.70 10.30 12.98 5 0

LOQ = Limit of Quantitation; %RPD = Relative Percent Deviation; %RSD = Relative Standard Deviation; N/D = Not Detected

*Designates values that are not currently included in the accredited scope of Iron Laboratories.

*** Designates tests that use the method FE-45. FE-45 is performed using AOAC 966.02 and 32.004-32.009. FE-45 has relative expanded (k=2) uncertainties of 1.098% for moisture, 1.754% for water activity for unprocessed plant materials, and 13.102% for water activity for infused products. Vitamin E acetate analysis has a relative expanded (k=2) uncertainty of 18.614%.

Total THC and CBD is the calculated sum of THC or CBD and the amount of THC or CBD derived from THCA or CBDA, respectively. These values are calculated by applying a molar correction factor of 0.877 to the THCA or the CBDA value. Calc Max Total Cannabinoids is the sum of Total THC, Total CBD, CBN, CBG, CBC, THCV, and CBDV.

%Decarb. THC and CBD refer to the percentage of THC or CBD relative to THCA or CBDA, respectively.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 1 of 5

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant QC Report

Testing Accreditation #: 4092-005 Test Certificate #: 136214-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Crater Lake Live Rosin
License: 030-1009646F7F8
Type: Tincture
Method: FE04U HPLC-UV
Metrc Test Pkg#: 1A4010300003A37000000914
Metrc Source Pkg#: 1A401030002C949000003557

Test Conditions

Prepsheet ID#: ORP220325a
Scale: XS205-OR1
Temp: 22.4 °C
Baro Pressure: 1004 hPa
Analyst: TMR
Technician: TMR

Sample ID#: 136214

Lot #: Crater Lake Live Rosin #1 3.2.2022
Batch #: 136214
Batch Weight (g): 184.4
Harvest/Process Date: 03/02/2022
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 03/29/2022
Test Date: 03/25/2022

Sample #136214
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Cannabidivarin (CBDV) N.D. 4.55 4.25 93.41 4.84 106.37 12.98
Cannabidiolic Acid (CBDA) N.D. 3.77 3.52 93.37 3.88 102.92 9.73
Cannabigerol (CBG) N.D. 6.01 5.29 88.02 5.72 95.17 7.81
Cannabidiol (CBD) N.D. 5.11 5.28 103.33 5.38 105.28 1.88
Δ9-Tetrahydrocannabivarin (THCV) N.D. 6.09 5.25 86.21 5.82 95.57 10.30
Cannabinol (CBN) N.D. 6.5 5.25 80.77 5.95 91.54 12.50
Δ9-Tetrahydrocannabinol (THC) N.D. 6.12 5.69 92.97 6.2 101.31 8.58
Cannabichromene (CBC) N.D. 0.5 0.58 116.00 0.43 86.00 29.70 Q
Tetrahydrocannabinolic acid (THCA) N.D. 5.83 5.41 92.80 5.71 97.94 5.40

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 2 of 5

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Marijuana Potency Analysis by
High Performance Liquid Chromatography

Testing Accreditation #: 4092-005 Test Certificate #: 136214-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Crater Lake Live Rosin
License: 030-1009646F7F8
Type: Tincture
Method: FE04U HPLC-UV
Metrc Test Pkg#: 1A4010300003A37000000914
Metrc Source Pkg#: 1A401030002C949000003557

Test Conditions

Prepsheet ID#: ORP220325a
Scale: XS205-OR1
Temp: 22.4 °C
Baro Pressure: 1004 hPa
Analyst: TMR
Technician: TMR

Sample ID#: 136214

Lot #: Crater Lake Live Rosin #1 3.2.2022
Batch #: 136214
Batch Weight (g): 184.4
Harvest/Process Date: 03/02/2022
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 03/29/2022
Test Date: 03/25/2022

Sample #136214
Sample #136214 Sample #136214
Test
Compounds
THC THCA CBD CBDA CBN CBG CBC THCV* CBDV Total
Cannabinoids*
Total THC Total CBD Calc Max Total
Cannabinoids*
Amount (%) 4.06 81.50 N/D 2.32 N/D 0.67 N/D N/D N/D 88.55 75.53 2.04 78.24
Amount (mg/g) 40.62 814.95 N/D 23.22 N/D 6.68 N/D N/D N/D 885.47 755.33 20.36 782.37
Amount per Serving (mg) 2.03 40.75 N\D 1.16 N\D 0.33 N\D N\D N\D 44.27 Serving Size~ (g): 0.05
LOQ (mg/g) 1.8 1.8 1.8 1.8 1.8 1.8 1.8 1.8 1.8   %Decarb. THC CBD
±%RPD 8.58 5.40 1.88 9.73 12.50 7.81 29.70 10.30 12.98 0 0

LOQ = Limit of Quantitation; %RPD = Relative Percent Deviation; %RSD = Relative Standard Deviation; N/D = Not Detected

*Designates values that are not currently included in the accredited scope of Iron Laboratories.

*** Designates tests that use the method FE-45. FE-45 is performed using AOAC 966.02 and 32.004-32.009. FE-45 has relative expanded (k=2) uncertainties of 1.098% for moisture, 1.754% for water activity for unprocessed plant materials, and 13.102% for water activity for infused products. Vitamin E acetate analysis has a relative expanded (k=2) uncertainty of 18.614%.

Total THC and CBD is the calculated sum of THC or CBD and the amount of THC or CBD derived from THCA or CBDA, respectively. These values are calculated by applying a molar correction factor of 0.877 to the THCA or the CBDA value. Calc Max Total Cannabinoids is the sum of Total THC, Total CBD, CBN, CBG, CBC, THCV, and CBDV.

%Decarb. THC and CBD refer to the percentage of THC or CBD relative to THCA or CBDA, respectively.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 2 of 5

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant QC Report

Testing Accreditation #: 4092-005 Test Certificate #: 136214-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Crater Lake Live Rosin
License: 030-1009646F7F8
Type: Tincture
Method: FE04U HPLC-UV
Metrc Test Pkg#: 1A4010300003A37000000914
Metrc Source Pkg#: 1A401030002C949000003557

Test Conditions

Prepsheet ID#: ORP220325a
Scale: XS205-OR1
Temp: 22.4 °C
Baro Pressure: 1004 hPa
Analyst: TMR
Technician: TMR

Sample ID#: 136214

Lot #: Crater Lake Live Rosin #1 3.2.2022
Batch #: 136214
Batch Weight (g): 184.4
Harvest/Process Date: 03/02/2022
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 03/29/2022
Test Date: 03/25/2022

Sample #136214
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Cannabidivarin (CBDV) N.D. 4.55 4.25 93.41 4.84 106.37 12.98
Cannabidiolic Acid (CBDA) N.D. 3.77 3.52 93.37 3.88 102.92 9.73
Cannabigerol (CBG) N.D. 6.01 5.29 88.02 5.72 95.17 7.81
Cannabidiol (CBD) N.D. 5.11 5.28 103.33 5.38 105.28 1.88
Δ9-Tetrahydrocannabivarin (THCV) N.D. 6.09 5.25 86.21 5.82 95.57 10.30
Cannabinol (CBN) N.D. 6.5 5.25 80.77 5.95 91.54 12.50
Δ9-Tetrahydrocannabinol (THC) N.D. 6.12 5.69 92.97 6.2 101.31 8.58
Cannabichromene (CBC) N.D. 0.5 0.58 116.00 0.43 86.00 29.70 Q
Tetrahydrocannabinolic acid (THCA) N.D. 5.83 5.41 92.80 5.71 97.94 5.40

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 3 of 5

IRON Laboratories     PJLA

ISO/IEC 17025:2017 Accredited

Oregon Compliant Homogeneity Report by
High Performance Liquid Chromatography

Testing Accreditation #: 77802 Test Certificate #: 136214-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Crater Lake Live Rosin
License: 030-1009646F7F8
Type: Tincture
Metrc Test Pkg#: 1A4010300003A37000000914
Metrc Source Pkg#: 1A401030002C949000003557

Sample ID#: 136214

Lot #: Crater Lake Live Rosin #1 3.2.2022
Batch #: 136214
Batch Weight (g): 184.4
Harvest/Process Date: 03/02/2022
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 03/29/2022

Sample #136214
Increments Tested (mg/g) TOTAL THC TOTAL CBD THC THCA THCV CBD CBC CBDA CBDV CBG CBN
Increment 1 751.10 20.78 40.97 809.73 N.D. N.D. N.D. 23.70 N.D. 7.00 N.D.
Increment 2 755.33 20.36 40.62 814.95 N.D. N.D. N.D. 23.22 N.D. 6.68 N.D.
Average Value 753.22 20.57 40.80 812.34 N.D. N.D. N.D. 23.46 N.D. 6.84 N.D.
Max Value 755.33 20.78 40.97 814.95 N.D. N.D. N.D. 23.70 N.D. 7.00 N.D.
Min Value 751.10 20.36 40.62 809.73 N.D. N.D. N.D. 23.22 N.D. 6.68 N.D.
Relative Percent Difference (RPD) ±0.56 ±2.05 ±0.86 ±0.64 N.D. N.D. N.D. ±2.05 N.D. ±4.68 N.D.
Average Cannabinoids Per Package 753.22 20.57 40.80 812.34 N.D. N.D. N.D. 23.46 N.D. 6.84 N.D.
Average Cannabinoids Per Serving 37.66 1.03 2.04 40.62 N.D. N.D. N.D. 1.17 N.D. 0.34 N.D.
Max Concentration Per Serving (THC)   Not Applicable
Max Concentration Per Package (THC)   Pass
Relative Percent Difference (RPD)   Pass
Control Study   No
Field Duplicate   Pass

N.D. = Not Detected, Min = Minimum, Max = Maximum

RPD is the relative percent difference between increment 1 and increment 2.

RSD is the relative standard deviation between all increments tested.

Total THC and CBD is the calculated sum of CBD or THC and the amount of CBD or THC derived from CBDA or THCA, respectively. These values are calculated by adding a molar correction factor of 0.877 to the CBDA or THCA value.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Terry Rabinowitz Iron laboratories Terry Rabinowitz

Iron Laboratories, LLC is an ISO/IEC 17025:2017 Testing Laboratory laboratory accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 3 of 5

IRON Laboratories

Terpene Report by
Mass Spectrometer

Test Certificate #: 136214-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Crater Lake Live Rosin
License: 030-1009646F7F8
Type: Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A4010300003A37000000914
Metrc Source Pkg#: 1A401030002C949000003557

Test Conditions

Scale: XS205-OR1
Temp: 19.2 °C
Baro Pressure: 999.1 hPa
Analyst: HRM
Technician: HRM

Sample ID#: 136214

Lot #: Crater Lake Live Rosin #1 3.2.2022
Batch #: 136214
Batch Weight (g): 184.4
Harvest/Process Date: 03/02/2022
Serving Size (g): 0.05
Date Received: 03/29/2022

Sample #136214
Sample #136214
  • α-Pinene (0.76%)
  • β-Ocimene (2.13%)
  • Camphene (0.07%)
  • Eucalyptol (1,8-Cineol) (0.22%)
  • Sabinene (0.00%)
  • γ-Terpinene (0.09%)
  • Myrcene (1.09%)
  • α-Terpinolene (0.21%)
  • β-Pinene (1.13%)
  • Linalool (0.45%)
  • ∆3-Carene (0.04%)
  • Fenchone (0.00%)
  • α-Terpinene (0.17%)
  • endo-Fenchol (0.12%)
  • α-Ocimene (0.04%)
  • Isopulegol (0.00%)
  • Limonene (0.81%)
  • Geraniol (0.00%)
  • p-Cymene (0.00%)
  • β-Caryophyllene (1.09%)
  • α-Humulene (1.96%)
  • Nerolidol 1 (cis) (0.00%)
  • Nerolidol 2 (trans) (0.00%)
  • Guaiol (0.00%)
  • Caryophyllene Oxide (0.00%)
  • α-Bisabolol (0.26%)
  • α-Phellandrene (1.03%)
  • α-Terpineol (0.17%)
  • Valenence (0.04%)

Total: 11.880%

Predominant Terpenes

2.13%   β-Ocimene Citrus, tropical, woody, green 1.96%   α-Humulene Woody, oceanic-watery, spicy clove
1.13%   β-Pinene Woody, fresh pine, hay 1.09%   Myrcene Peppery, spicy balsam
1.09%   β-Caryophyllene Sweet, woody, spicy, clove 1.03%   α-Phellandrene Citrus, green, black pepper

Value in parenthesis indicates percentage of terpene present in the total sample (weight percentage, wt/wt%).
Value in doughnut slice indicates individual terpene abundance with respect to the total terpenes detected.

This sample has not been tested according to OAR 333-007. These results should therefore be used for research and development or quality control purposes only.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Himashi Mead Iron laboratories Himashi Mead

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 4 of 5

IRON Laboratories

Terpene Report by
Mass Spectrometer

Test Certificate #: 136214-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Crater Lake Live Rosin
License: 030-1009646F7F8
Type: Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A4010300003A37000000914
Metrc Source Pkg#: 1A401030002C949000003557

Test Conditions

Scale: XS205-OR1
Temp: 19.2 °C
Baro Pressure: 999.1 hPa
Analyst: HRM
Technician: HRM

Sample ID#: 136214

Lot #: Crater Lake Live Rosin #1 3.2.2022
Batch #: 136214
Batch Weight (g): 184.4
Harvest/Process Date: 03/02/2022
Serving Size (g): 0.05
Date Received: 03/29/2022

Sample #136214
Sample #136214
  • α-Pinene (0.76%)
  • β-Ocimene (2.13%)
  • Camphene (0.07%)
  • Eucalyptol (1,8-Cineol) (0.22%)
  • Sabinene (0.00%)
  • γ-Terpinene (0.09%)
  • Myrcene (1.09%)
  • α-Terpinolene (0.21%)
  • β-Pinene (1.13%)
  • Linalool (0.45%)
  • ∆3-Carene (0.04%)
  • Fenchone (0.00%)
  • α-Terpinene (0.17%)
  • endo-Fenchol (0.12%)
  • α-Ocimene (0.04%)
  • Isopulegol (0.00%)
  • Limonene (0.81%)
  • Geraniol (0.00%)
  • p-Cymene (0.00%)
  • β-Caryophyllene (1.09%)
  • α-Humulene (1.96%)
  • Nerolidol 1 (cis) (0.02%)
  • Nerolidol 2 (trans) (0.02%)
  • Guaiol (0.00%)
  • Caryophyllene Oxide (0.00%)
  • α-Bisabolol (0.26%)
  • α-Phellandrene (1.03%)
  • α-Terpineol (0.17%)
  • Valenence (0.04%)

Total: 11.920%

Predominant Terpenes

2.13%   β-Ocimene Citrus, tropical, woody, green 1.96%   α-Humulene Woody, oceanic-watery, spicy clove
1.13%   β-Pinene Woody, fresh pine, hay 1.09%   Myrcene Peppery, spicy balsam
1.09%   β-Caryophyllene Sweet, woody, spicy, clove 1.03%   α-Phellandrene Citrus, green, black pepper

Value in parenthesis indicates percentage of terpene present in the total sample (weight percentage, wt/wt%).
Value in doughnut slice indicates individual terpene abundance with respect to the total terpenes detected.

This sample has not been tested according to OAR 333-007. These results should therefore be used for research and development or quality control purposes only.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Himashi Mead Iron laboratories Himashi Mead

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 5 of 5