ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Marijuana Potency Analysis by
High Performance Liquid Chromatography
Testing Accreditation #: 4092-005 Test Certificate #: 134761-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Gorilla Glue
License: 030-1009646F7F8
Type: AU Tincture
Method: FE04U HPLC-UV
Metrc Test Pkg#: 1A4010300003A37000001276
Metrc Source Pkg#: 1A401030002C949000002555
Test Conditions

Prepsheet ID#: ORP211216a
Scale: XS205-OR1
Temp: 22.3 °C
Baro Pressure: 1004 hPa
Analyst: TMR
Technician: TMR
Sample ID#: 134761

Lot #: Gorilla Glue #1 11.2.2021
Batch #: 134761
Batch Weight (g): 593
Harvest/Process Date: 11/02/2021
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 12/23/2021
Test Date: 12/16/2021
Sample #134761
Sample #134761 Sample #134761
Test
Compounds		 THC THCA CBD CBDA CBN CBG CBC THCV* CBDV Total
Cannabinoids*		 Total THC Total CBD Calc Max Total
Cannabinoids*
Amount (%) 4.22 78.81 N/D 1.75 N/D 0.23 N/D N/D N/D 85.01 73.33 1.54 75.10
Amount (mg/g) 42.16 788.11 N/D 17.51 N/D 2.29 N/D N/D N/D 850.07 733.33 15.36 750.98
Amount per Serving (mg) 2.11 39.41 N\D 0.88 N\D 0.11 N\D N\D N\D 42.50 Serving Size~ (g): 0.05
LOQ (mg/g) 1.9 1.9 1.9 1.9 1.9 1.9 1.9 1.9 1.9   %Decarb. THC CBD
±%RPD 8.48 12.33 7.15 12.97 6.77 6.26 7.13 7.00 7.18 5 0

LOQ = Limit of Quantitation; %RPD = Relative Percent Deviation; %RSD = Relative Standard Deviation; N/D = Not Detected

*Designates values that are not currently included in the accredited scope of Iron Laboratories.

*** Designates tests that use the method FE-45. FE-45 is performed using AOAC 966.02 and 32.004-32.009. FE-45 has relative expanded (k=2) uncertainties of 1.098% for moisture, 1.754% for water activity for unprocessed plant materials, and 13.102% for water activity for infused products. Vitamin E acetate analysis has a relative expanded (k=2) uncertainty of 18.614%.

Total THC and CBD is the calculated sum of THC or CBD and the amount of THC or CBD derived from THCA or CBDA, respectively. These values are calculated by applying a molar correction factor of 0.877 to the THCA or the CBDA value. Calc Max Total Cannabinoids is the sum of Total THC, Total CBD, CBN, CBG, CBC, THCV, and CBDV.

%Decarb. THC and CBD refer to the percentage of THC or CBD relative to THCA or CBDA, respectively.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 1 of 12

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant QC Report
Testing Accreditation #: 4092-005 Test Certificate #: 134761-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Gorilla Glue
License: 030-1009646F7F8
Type: AU Tincture
Method: FE04U HPLC-UV
Metrc Test Pkg#: 1A4010300003A37000001276
Metrc Source Pkg#: 1A401030002C949000002555
Test Conditions

Prepsheet ID#: ORP211216a
Scale: XS205-OR1
Temp: 22.3 °C
Baro Pressure: 1004 hPa
Analyst: TMR
Technician: TMR
Sample ID#: 134761

Lot #: Gorilla Glue #1 11.2.2021
Batch #: 134761
Batch Weight (g): 593
Harvest/Process Date: 11/02/2021
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 12/23/2021
Test Date: 12/16/2021
Sample #134761
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Cannabidivarin (CBDV) N.D. 4.08 4.03 98.77 4.33 106.13 7.18
Cannabidiolic Acid (CBDA) N.D. 3.3 3.1 93.94 3.53 106.97 12.97
Cannabigerol (CBG) N.D. 4.5 4.49 99.78 4.78 106.22 6.26
Cannabidiol (CBD) N.D. 4.22 4.18 99.05 4.49 106.40 7.15
Δ9-Tetrahydrocannabivarin (THCV) N.D. 4.49 4.41 98.22 4.73 105.35 7.00
Cannabinol (CBN) N.D. 4.79 4.71 98.33 5.04 105.22 6.77
Δ9-Tetrahydrocannabinol (THC) N.D. 4.75 4.63 97.47 5.04 106.11 8.48
Cannabichromene (CBC) N.D. 4.44 4.33 97.52 4.65 104.73 7.13
Tetrahydrocannabinolic acid (THCA) N.D. 4.08 3.73 91.42 4.22 103.43 12.33

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 2 of 12

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Marijuana Potency Analysis by
High Performance Liquid Chromatography
Testing Accreditation #: 4092-005 Test Certificate #: 134761-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Gorilla Glue
License: 030-1009646F7F8
Type: AU Tincture
Method: FE04U HPLC-UV
Metrc Test Pkg#: 1A4010300003A37000001276
Metrc Source Pkg#: 1A401030002C949000002555
Test Conditions

Prepsheet ID#: ORP211216a
Scale: XS205-OR1
Temp: 22.3 °C
Baro Pressure: 1004 hPa
Analyst: TMR
Technician: TMR
Sample ID#: 134761

Lot #: Gorilla Glue #1 11.2.2021
Batch #: 134761
Batch Weight (g): 593
Harvest/Process Date: 11/02/2021
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 12/23/2021
Test Date: 12/16/2021
Sample #134761
Sample #134761 Sample #134761
Test
Compounds		 THC THCA CBD CBDA CBN CBG CBC THCV* CBDV Total
Cannabinoids*		 Total THC Total CBD Calc Max Total
Cannabinoids*
Amount (%) 4.78 73.25 N/D 1.86 N/D 0.29 N/D N/D N/D 80.18 69.02 1.63 70.94
Amount (mg/g) 47.80 732.50 N/D 18.59 N/D 2.86 N/D N/D N/D 801.75 690.20 16.30 709.36
Amount per Serving (mg) 2.39 36.63 N\D 0.93 N\D 0.14 N\D N\D N\D 40.09 Serving Size~ (g): 0.05
LOQ (mg/g) 1.8 1.8 1.8 1.8 1.8 1.8 1.8 1.8 1.8   %Decarb. THC CBD
±%RPD 8.48 12.33 7.15 12.97 6.77 6.26 7.13 7.00 7.18 0 0

LOQ = Limit of Quantitation; %RPD = Relative Percent Deviation; %RSD = Relative Standard Deviation; N/D = Not Detected

*Designates values that are not currently included in the accredited scope of Iron Laboratories.

*** Designates tests that use the method FE-45. FE-45 is performed using AOAC 966.02 and 32.004-32.009. FE-45 has relative expanded (k=2) uncertainties of 1.098% for moisture, 1.754% for water activity for unprocessed plant materials, and 13.102% for water activity for infused products. Vitamin E acetate analysis has a relative expanded (k=2) uncertainty of 18.614%.

Total THC and CBD is the calculated sum of THC or CBD and the amount of THC or CBD derived from THCA or CBDA, respectively. These values are calculated by applying a molar correction factor of 0.877 to the THCA or the CBDA value. Calc Max Total Cannabinoids is the sum of Total THC, Total CBD, CBN, CBG, CBC, THCV, and CBDV.

%Decarb. THC and CBD refer to the percentage of THC or CBD relative to THCA or CBDA, respectively.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 2 of 12

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant QC Report
Testing Accreditation #: 4092-005 Test Certificate #: 134761-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Gorilla Glue
License: 030-1009646F7F8
Type: AU Tincture
Method: FE04U HPLC-UV
Metrc Test Pkg#: 1A4010300003A37000001276
Metrc Source Pkg#: 1A401030002C949000002555
Test Conditions

Prepsheet ID#: ORP211216a
Scale: XS205-OR1
Temp: 22.3 °C
Baro Pressure: 1004 hPa
Analyst: TMR
Technician: TMR
Sample ID#: 134761

Lot #: Gorilla Glue #1 11.2.2021
Batch #: 134761
Batch Weight (g): 593
Harvest/Process Date: 11/02/2021
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 12/23/2021
Test Date: 12/16/2021
Sample #134761
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Cannabidivarin (CBDV) N.D. 4.08 4.03 98.77 4.33 106.13 7.18
Cannabidiolic Acid (CBDA) N.D. 3.3 3.1 93.94 3.53 106.97 12.97
Cannabigerol (CBG) N.D. 4.5 4.49 99.78 4.78 106.22 6.26
Cannabidiol (CBD) N.D. 4.22 4.18 99.05 4.49 106.40 7.15
Δ9-Tetrahydrocannabivarin (THCV) N.D. 4.49 4.41 98.22 4.73 105.35 7.00
Cannabinol (CBN) N.D. 4.79 4.71 98.33 5.04 105.22 6.77
Δ9-Tetrahydrocannabinol (THC) N.D. 4.75 4.63 97.47 5.04 106.11 8.48
Cannabichromene (CBC) N.D. 4.44 4.33 97.52 4.65 104.73 7.13
Tetrahydrocannabinolic acid (THCA) N.D. 4.08 3.73 91.42 4.22 103.43 12.33

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 3 of 12

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Pesticide Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-005 Test Certificate #: 134761-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Gorilla Glue
License: 030-1009646F7F8
Type: AU Tincture
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A4010300003A37000001276
Metrc Source Pkg#: 1A401030002C949000002555
Test Conditions

Prepsheet ID#: ORPS211222b
Scale: XS205-OR1
Temp: 22.7 °C
Baro PE: 992.2 hPa
Analyst: HRM
Technician: JBS
Sample ID#: 134761

Lot #: Gorilla Glue #1 11.2.2021
Batch #: 134761
Batch Weight (g): 593
Harvest/Process Date: 11/02/2021
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 12/23/2021
Test Date: 12/22/2021
Sample #134761
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
Aldicarb 0.400 0.117 Pass/<LOD Abamectin**** 0.500 0.117 Pass/<LOD
Acephate 0.400 0.117 Pass/<LOD Acequinocyl 2.000 0.235 Pass/<LOD
Acetamiprid 0.200 0.117 Pass/<LOD Azoxystrobin 0.200 0.117 Pass/<LOD
Bifenazate 0.200 0.117 Pass/<LOD Bifenthrin 0.200 0.117 Pass/<LOD
Boscalid 0.400 0.117 Pass/<LOD Carbaryl 0.200 0.117 Pass/<LOD
Carbofuran 0.200 0.117 Pass/<LOD Chlorantraniliprole 0.200 0.117 Pass/<LOD
Chlorfenapyr 1.000 0.470 Pass/<LOD Chlorpyrifos 0.200 0.117 Pass/<LOD
Clofentezine 0.200 0.117 Pass/<LOD Cyfluthrin** 1.000 0.470 Pass/<LOD
Cypermethrin*** 1.000 0.470 Pass/<LOD Daminozide 1.000 0.117 Pass/<LOD
DDVP (Dichlorvos) 1.000 0.235 Pass/<LOD Diazinon 0.200 0.117 Pass/<LOD
Dimethoate 0.200 0.117 Pass/<LOD Ethoprophos 0.200 0.117 Pass/<LOD
Etofenprox 0.400 0.117 Pass/<LOD Etoxazole 0.200 0.117 Pass/<LOD
Fenoxycarb 0.200 0.117 Pass/<LOD Fenpyroximate 0.400 0.117 Pass/<LOD
Fipronil 0.400 0.117 Pass/<LOD Flonicamid 1.000 0.117 Pass/<LOD
Fludioxonil 0.400 0.117 Pass/<LOD Hexythiazox 1.000 0.117 Pass/<LOD
Imazalil 0.200 0.117 Pass/<LOD Imidacloprid 0.400 0.117 Pass/<LOD
Kresoxim Methyl 0.400 0.117 Pass/<LOD Malathion 0.200 0.117 Pass/<LOD
Metalaxyl 0.200 0.117 Pass/<LOD Methiocarb 0.200 0.117 Pass/<LOD
Methomyl 0.400 0.117 Pass/<LOD Methyl Parathion 0.200 0.117 Pass/<LOD
MGK-264‡ 0.200 0.117 Pass/<LOD Myclobutanil 0.000 0.117 Pass/<LOD
Naled 0.500 0.117 Pass/<LOD Oxamyl 1.000 0.117 Pass/<LOD
Paclobutrazol 0.400 0.117 Pass/<LOD Permethrins† 0.200 0.117 Pass/<LOD
Phosmet 0.200 0.117 Pass/<LOD Piperonyl Butoxide 2.000 0.117 Pass/<LOD
Prallethrin 0.200 0.117 Pass/<LOD Propiconazole 0.400 0.117 Pass/<LOD
Propoxur 0.200 0.117 Pass/<LOD Pyrethrins* 1.000 0.117 Pass/<LOD
Pyridaben 0.200 0.117 Pass/<LOD Spinosad***** 0.200 0.117 Pass/<LOD
Spiromesifen 0.200 0.117 Pass/<LOD Spirotetramat 0.200 0.117 Pass/<LOD
Spiroxamine‡ 0.400 0.117 Pass/<LOD Tebuconazole 0.400 0.117 Pass/<LOD
Thiacloprid 0.200 0.117 Pass/<LOD Thiamethoxam 0.200 0.117 Pass/<LOD
Trifloxystrobin 0.200 0.117 Pass/<LOD

* Pyrethrins are reported as the sum of Jasmolin I, Cinerin I, and Pyrethrin I
** Cyfluthrins are reported as the sum of isomers Cyfluthrin I, II, III, and IV
*** Cypermethrins are reported as the sum of isomers Cypermethrin I, II, III, and IV
**** Abamectin is reported as the sum of Avermectin B1a and Avermectin B1b
***** Spinosad is reported as the sum of Spinosyn A and Spinosyn D
† Permethrin and Prallethrin are reported as the sum of cis and trans isomers
‡ MGK-264 and Spiroximine are reported as the sum of isomers I and II
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 3 of 12

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Pesticide QC Report
Testing Accreditation #: 4092-005 Test Certificate #: 134761-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Gorilla Glue
License: 030-1009646F7F8
Type: AU Tincture
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A4010300003A37000001276
Metrc Source Pkg#: 1A401030002C949000002555
Test Conditions

Prepsheet ID#: ORPS211222b
Scale: XS205-OR1
Temp: 22.7 °C
Baro PE: 992.2 hPa
Analyst: HRM
Technician: JBS
Sample ID#: 134761

Lot #: Gorilla Glue #1 11.2.2021
Batch #: 134761
Batch Weight (g): 593
Harvest/Process Date: 11/02/2021
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 12/23/2021
Test Date: 12/22/2021
Sample #134761
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS recovery% MSD recovery% Relative Percent Difference (%) QC Flag
Acephate N.D. 1 0.307 0.351 30.70 35.10 13.37 LR
Acequinocyl N.D. 1 0.853 1.16 85.30 116.00 30.50 Q
Acetamiprid N.D. 1 0.835 1.05 83.50 105.00 22.81 Q
Aldicarb N.D. 1 0.524 0.949 52.40 94.90 57.71 LR Q
Avermectin B1a N.D. 0.97 2.68 2.25 276.29 231.96 17.44 HR
Azoxystrobin N.D. 1 1.35 1.66 135.00 166.00 20.60 HR Q
Bifenazate N.D. 1 0.21 0.147 21.00 14.70 35.29 LR Q
Bifenthrin N.D. 1 1.1 1.37 110.00 137.00 21.86 HRQ
Boscalid N.D. 1 1.05 1.36 105.00 136.00 25.73 HRQ
Carbaryl N.D. 1 1.22 1.31 122.00 131.00 7.11 HR
Carbofuran N.D. 1 1.42 1.46 142.00 146.00 2.78 HR
Chlorantraniliprole N.D. 1 1.53 1.83 153.00 183.00 17.86 HR
Chlorfenapyr N.D. 1 0.578 0.618 57.80 61.80 6.69 LE
Chlorpyriphos N.D. 1 1.14 1.62 114.00 162.00 34.78 HRQ
Clofentezine N.D. 1 1.4 1.91 140.00 191.00 30.82 HR Q
Cyfluthrin N.D. 1 0.995 1.35 99.50 135.00 30.28 HRQ
Cypermethrin N.D. 1 1.09 1.6 109.00 160.00 37.92 HRQ
Daminoside N.D. 1 3.82 2.61 382.00 261.00 37.64 HR Q
Diazanon N.D. 1 24.7 35.3 2,470.00 3,530.00 35.33 HR Q
Dichlorvos N.D. 1 1.15 1.39 115.00 139.00 18.90 HR
Dimethoate N.D. 1 0.875 0.939 87.50 93.90 7.06
Ethoprophos N.D. 1 1.51 1.63 151.00 163.00 7.64 HR
Etofenprox N.D. 1 1.03 1.56 103.00 156.00 40.93 HRQ
Etoxazole N.D. 1 1.45 1.74 145.00 174.00 18.18 HR
Fenoxycarb N.D. 1 1.61 1.76 161.00 176.00 8.90 HR
Fenpyroximate N.D. 1 1.91 2.24 191.00 224.00 15.90 HR
Fipronil N.D. 1 0.811 0.628 81.10 62.80 25.43 LR Q
Flonicamid N.D. 1 0.583 0.768 58.30 76.80 27.39 LR Q
Fludioxonil N.D. 1 0.904 0.701 90.40 70.10 25.30 Q
Hexythiazox N.D. 1 0.958 1.36 95.80 136.00 34.69 HRQ
Imazalil N.D. 1 1.97 2.46 197.00 246.00 22.12 HR Q
Imidacloprid N.D. 1 0.988 1.52 98.80 152.00 42.42 HRQ
Kresoxim-methyl N.D. 1 1.57 1.72 157.00 172.00 9.12 HR
Malathion N.D. 1 1.67 1.65 167.00 165.00 1.20 HR
Metalaxyl N.D. 1 1.68 1.85 168.00 185.00 9.63 HR
Methiocarb N.D. 1 1.04 1.22 104.00 122.00 15.93
Methomyl N.D. 1 0.445 0.492 44.50 49.20 10.03 LR
MGK-264 N.D. 1 0.761 1.07 76.10 107.00 33.75 Q
Myclobutanil N.D. 1 1.62 1.95 162.00 195.00 18.49 HR
Naled (dibrom) N.D. 1 0.612 0.921 61.20 92.10 40.31 LR Q
Oxamyl N.D. 1 0.383 0.446 38.30 44.60 15.20 LR
Paclobutrazol N.D. 1 1.34 1.96 134.00 196.00 37.58 HR Q
Parathion-methyl N.D. 1 0.683 0.738 68.30 73.80 7.74 LR
Permethrins N.D. 1 1.112 1.333 111.20 133.30 18.08 HR Q
Phosmet N.D. 1 1.41 1.83 141.00 183.00 25.93 HR Q
Piperonyl butoxide N.D. 1 1.31 1.41 131.00 141.00 7.35 HR
Prallethrin N.D. 1 1.63 2.06 163.00 206.00 23.31 HR Q
Propiconazole N.D. 1 1.64 1.85 164.00 185.00 12.03 HR
Propoxur N.D. 1 0.711 1.25 71.10 125.00 54.97 Q
Pyrethrin N.D. 0.65 1.26 1.42 193.85 218.46 11.94 HR
Pyridaben N.D. 1 1.56 1.61 156.00 161.00 3.15 HR
SpinosynA N.D. 0.84 1.26 1.58 150.00 188.10 22.54 HR Q
SpinosynD N.D. 0.16 0.298 0.322 186.25 201.25 7.74 HR
Spiromesifen N.D. 1 1.11 1.15 111.00 115.00 3.54
Spirotetramat N.D. 1 1.28 1.59 128.00 159.00 21.60 HRQ
Spiroxamine N.D. 1 1.91 1.85 191.00 185.00 3.19 HR
Tebuconazole N.D. 1 1.53 2.07 153.00 207.00 30.00 HR Q
Thiacloprid N.D. 1 1.65 1.67 165.00 167.00 1.20 HR
Thiamethoxam N.D. 1 0.782 0.776 78.20 77.60 0.77
Trifloxystrobin N.D. 1 1.06 1.51 106.00 151.00 35.02 HRQ

N.D. = Not Detected

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 30%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (60-120%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 4 of 12

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Pesticide Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-005 Test Certificate #: 134761-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Gorilla Glue
License: 030-1009646F7F8
Type: AU Tincture
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A4010300003A37000001276
Metrc Source Pkg#: 1A401030002C949000002555
Test Conditions

Prepsheet ID#: ORPS211222b
Scale: XS205-OR1
Temp: 22.7 °C
Baro PE: 992.2 hPa
Analyst: HRM
Technician: JBS
Sample ID#: 134761

Lot #: Gorilla Glue #1 11.2.2021
Batch #: 134761
Batch Weight (g): 593
Harvest/Process Date: 11/02/2021
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 12/23/2021
Test Date: 12/22/2021
Sample #134761
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
Aldicarb 0.400 0.126 Pass/<LOD Abamectin**** 0.500 0.126 Pass/<LOD
Acephate 0.400 0.126 Pass/<LOD Acequinocyl 2.000 0.252 Pass/<LOD
Acetamiprid 0.200 0.126 Pass/<LOD Azoxystrobin 0.200 0.126 Pass/<LOD
Bifenazate 0.200 0.126 Pass/<LOD Bifenthrin 0.200 0.126 Pass/<LOD
Boscalid 0.400 0.126 Pass/<LOD Carbaryl 0.200 0.126 Pass/<LOD
Carbofuran 0.200 0.126 Pass/<LOD Chlorantraniliprole 0.200 0.126 Pass/<LOD
Chlorfenapyr 1.000 0.504 Pass/<LOD Chlorpyrifos 0.200 0.126 Pass/<LOD
Clofentezine 0.200 0.126 Pass/<LOD Cyfluthrin** 1.000 0.504 Pass/<LOD
Cypermethrin*** 1.000 0.504 Pass/<LOD Daminozide 1.000 0.126 Pass/<LOD
DDVP (Dichlorvos) 1.000 0.252 Pass/<LOD Diazinon 0.200 0.126 Pass/<LOD
Dimethoate 0.200 0.126 Pass/<LOD Ethoprophos 0.200 0.126 Pass/<LOD
Etofenprox 0.400 0.126 Pass/<LOD Etoxazole 0.200 0.126 Pass/<LOD
Fenoxycarb 0.200 0.126 Pass/<LOD Fenpyroximate 0.400 0.126 Pass/<LOD
Fipronil 0.400 0.126 Pass/<LOD Flonicamid 1.000 0.126 Pass/<LOD
Fludioxonil 0.400 0.126 Pass/<LOD Hexythiazox 1.000 0.126 Pass/<LOD
Imazalil 0.200 0.126 Pass/<LOD Imidacloprid 0.400 0.126 Pass/<LOD
Kresoxim Methyl 0.400 0.126 Pass/<LOD Malathion 0.200 0.126 Pass/<LOD
Metalaxyl 0.200 0.126 Pass/<LOD Methiocarb 0.200 0.126 Pass/<LOD
Methomyl 0.400 0.126 Pass/<LOD Methyl Parathion 0.200 0.126 Pass/<LOD
MGK-264‡ 0.200 0.126 Pass/<LOD Myclobutanil 0.000 0.126 Pass/<LOD
Naled 0.500 0.126 Pass/<LOD Oxamyl 1.000 0.126 Pass/<LOD
Paclobutrazol 0.400 0.126 Pass/<LOD Permethrins† 0.200 0.126 Pass/<LOD
Phosmet 0.200 0.126 Pass/<LOD Piperonyl Butoxide 2.000 0.126 Pass/<LOD
Prallethrin 0.200 0.126 Pass/<LOD Propiconazole 0.400 0.126 Pass/<LOD
Propoxur 0.200 0.126 Pass/<LOD Pyrethrins* 1.000 0.126 Pass/<LOD
Pyridaben 0.200 0.126 Pass/<LOD Spinosad***** 0.200 0.126 Pass/<LOD
Spiromesifen 0.200 0.126 Pass/<LOD Spirotetramat 0.200 0.126 Pass/<LOD
Spiroxamine‡ 0.400 0.126 Pass/<LOD Tebuconazole 0.400 0.126 Pass/<LOD
Thiacloprid 0.200 0.126 Pass/<LOD Thiamethoxam 0.200 0.126 Pass/<LOD
Trifloxystrobin 0.200 0.126 Pass/<LOD

* Pyrethrins are reported as the sum of Jasmolin I, Cinerin I, and Pyrethrin I
** Cyfluthrins are reported as the sum of isomers Cyfluthrin I, II, III, and IV
*** Cypermethrins are reported as the sum of isomers Cypermethrin I, II, III, and IV
**** Abamectin is reported as the sum of Avermectin B1a and Avermectin B1b
***** Spinosad is reported as the sum of Spinosyn A and Spinosyn D
† Permethrin and Prallethrin are reported as the sum of cis and trans isomers
‡ MGK-264 and Spiroximine are reported as the sum of isomers I and II
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 5 of 12

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Pesticide QC Report
Testing Accreditation #: 4092-005 Test Certificate #: 134761-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Gorilla Glue
License: 030-1009646F7F8
Type: AU Tincture
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A4010300003A37000001276
Metrc Source Pkg#: 1A401030002C949000002555
Test Conditions

Prepsheet ID#: ORPS211222b
Scale: XS205-OR1
Temp: 22.7 °C
Baro PE: 992.2 hPa
Analyst: HRM
Technician: JBS
Sample ID#: 134761

Lot #: Gorilla Glue #1 11.2.2021
Batch #: 134761
Batch Weight (g): 593
Harvest/Process Date: 11/02/2021
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 12/23/2021
Test Date: 12/22/2021
Sample #134761
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS recovery% MSD recovery% Relative Percent Difference (%) QC Flag
Acephate N.D. 1 0.307 0.351 30.70 35.10 13.37 LR
Acequinocyl N.D. 1 0.853 1.16 85.30 116.00 30.50 Q
Acetamiprid N.D. 1 0.835 1.05 83.50 105.00 22.81 Q
Aldicarb N.D. 1 0.524 0.949 52.40 94.90 57.71 LR Q
Avermectin B1a N.D. 0.97 2.68 2.25 276.29 231.96 17.44 HR
Azoxystrobin N.D. 1 1.35 1.66 135.00 166.00 20.60 HR Q
Bifenazate N.D. 1 0.21 0.147 21.00 14.70 35.29 LR Q
Bifenthrin N.D. 1 1.1 1.37 110.00 137.00 21.86 HRQ
Boscalid N.D. 1 1.05 1.36 105.00 136.00 25.73 HRQ
Carbaryl N.D. 1 1.22 1.31 122.00 131.00 7.11 HR
Carbofuran N.D. 1 1.42 1.46 142.00 146.00 2.78 HR
Chlorantraniliprole N.D. 1 1.53 1.83 153.00 183.00 17.86 HR
Chlorfenapyr N.D. 1 0.578 0.618 57.80 61.80 6.69 LE
Chlorpyriphos N.D. 1 1.14 1.62 114.00 162.00 34.78 HRQ
Clofentezine N.D. 1 1.4 1.91 140.00 191.00 30.82 HR Q
Cyfluthrin N.D. 1 0.995 1.35 99.50 135.00 30.28 HRQ
Cypermethrin N.D. 1 1.09 1.6 109.00 160.00 37.92 HRQ
Daminoside N.D. 1 3.82 2.61 382.00 261.00 37.64 HR Q
Diazanon N.D. 1 24.7 35.3 2,470.00 3,530.00 35.33 HR Q
Dichlorvos N.D. 1 1.15 1.39 115.00 139.00 18.90 HR
Dimethoate N.D. 1 0.875 0.939 87.50 93.90 7.06
Ethoprophos N.D. 1 1.51 1.63 151.00 163.00 7.64 HR
Etofenprox N.D. 1 1.03 1.56 103.00 156.00 40.93 HRQ
Etoxazole N.D. 1 1.45 1.74 145.00 174.00 18.18 HR
Fenoxycarb N.D. 1 1.61 1.76 161.00 176.00 8.90 HR
Fenpyroximate N.D. 1 1.91 2.24 191.00 224.00 15.90 HR
Fipronil N.D. 1 0.811 0.628 81.10 62.80 25.43 LR Q
Flonicamid N.D. 1 0.583 0.768 58.30 76.80 27.39 LR Q
Fludioxonil N.D. 1 0.904 0.701 90.40 70.10 25.30 Q
Hexythiazox N.D. 1 0.958 1.36 95.80 136.00 34.69 HRQ
Imazalil N.D. 1 1.97 2.46 197.00 246.00 22.12 HR Q
Imidacloprid N.D. 1 0.988 1.52 98.80 152.00 42.42 HRQ
Kresoxim-methyl N.D. 1 1.57 1.72 157.00 172.00 9.12 HR
Malathion N.D. 1 1.67 1.65 167.00 165.00 1.20 HR
Metalaxyl N.D. 1 1.68 1.85 168.00 185.00 9.63 HR
Methiocarb N.D. 1 1.04 1.22 104.00 122.00 15.93
Methomyl N.D. 1 0.445 0.492 44.50 49.20 10.03 LR
MGK-264 N.D. 1 0.761 1.07 76.10 107.00 33.75 Q
Myclobutanil N.D. 1 1.62 1.95 162.00 195.00 18.49 HR
Naled (dibrom) N.D. 1 0.612 0.921 61.20 92.10 40.31 LR Q
Oxamyl N.D. 1 0.383 0.446 38.30 44.60 15.20 LR
Paclobutrazol N.D. 1 1.34 1.96 134.00 196.00 37.58 HR Q
Parathion-methyl N.D. 1 0.683 0.738 68.30 73.80 7.74 LR
Permethrins N.D. 1 1.112 1.333 111.20 133.30 18.08 HR Q
Phosmet N.D. 1 1.41 1.83 141.00 183.00 25.93 HR Q
Piperonyl butoxide N.D. 1 1.31 1.41 131.00 141.00 7.35 HR
Prallethrin N.D. 1 1.63 2.06 163.00 206.00 23.31 HR Q
Propiconazole N.D. 1 1.64 1.85 164.00 185.00 12.03 HR
Propoxur N.D. 1 0.711 1.25 71.10 125.00 54.97 Q
Pyrethrin N.D. 0.65 1.26 1.42 193.85 218.46 11.94 HR
Pyridaben N.D. 1 1.56 1.61 156.00 161.00 3.15 HR
SpinosynA N.D. 0.84 1.26 1.58 150.00 188.10 22.54 HR Q
SpinosynD N.D. 0.16 0.298 0.322 186.25 201.25 7.74 HR
Spiromesifen N.D. 1 1.11 1.15 111.00 115.00 3.54
Spirotetramat N.D. 1 1.28 1.59 128.00 159.00 21.60 HRQ
Spiroxamine N.D. 1 1.91 1.85 191.00 185.00 3.19 HR
Tebuconazole N.D. 1 1.53 2.07 153.00 207.00 30.00 HR Q
Thiacloprid N.D. 1 1.65 1.67 165.00 167.00 1.20 HR
Thiamethoxam N.D. 1 0.782 0.776 78.20 77.60 0.77
Trifloxystrobin N.D. 1 1.06 1.51 106.00 151.00 35.02 HRQ

N.D. = Not Detected

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 30%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (60-120%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 6 of 12

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-005 Test Certificate #: 134761-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Gorilla Glue
License: 030-1009646F7F8
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A4010300003A37000001276
Metrc Source Pkg#: 1A401030002C949000002555
Test Conditions

Prepsheet ID#: ORHS211222a
Scale: XS205-OR2
Temp: 21.2 °C
Baro PE: 989.4 hPa
Analyst: HRM
Technician: JBS
Sample ID#: 134761

Lot #: Gorilla Glue #1 11.2.2021
Batch #: 134761
Batch Weight (g): 593
Harvest/Process Date: 11/02/2021
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 12/23/2021
Test Date: 12/22/2021
Sample #134761
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
1,2-Dichloroethane 2 1 Not Tested 1,2-Dimethoxyethane 100 5 Pass/<LOD
1,4-dioxane 380 200 Pass/<LOD 1-Butanol 5,000 100 Pass/<LOD
1-Pentanol 5,000 100 Pass/<LOD 1-Propanol 5,000 100 Pass/<LOD
2,2-Dimethylpropane (Neopentane) 5,000 100 Pass/<LOD 2,2-Dimethylbutane (Hexanes) 290 100 Pass/<LOD
2,3-Dimethylbutane (Hexanes) 290 100 Pass/<LOD 2-Butanol 5,000 100 Pass/<LOD
2-Butanone (MEK) 5,000 50 Pass/<LOD 2-Ethoxyethanol 160 40 Pass/<LOD
2-Methylbutane (Isopentane) 5,000 50 Pass/<LOD 2-Methylpentane (Hexanes) 290 50 Pass/<LOD
2-Methylpropane (Isobutane) 5,000 100 Pass/<LOD 2-propanol (Isopropyl Alcohol) 5,000 50 Pass/<LOD
2-Propanone (Acetone) 5,000 50 Pass/<LOD 3-Methylpentane (Hexanes) 290 50 Pass/<LOD
Acetonitrile 410 100 Pass/<LOD Benzene 2 1 Pass/<LOD
Butane 5,000 100 Pass/469 Chloroform 2 1 Pass/<LOD
Cumene 70 50 Pass/<LOD Cyclohexane 3,880 1,000 Pass/<LOD
Dichloromethane 600 50 Pass/<LOD Dimethylsulfoxide (DMSO) 5,000 500 Pass/<LOD
Ethanol 5,000 500 Pass/<LOD Ethyl acetate 5,000 50 Pass/<LOD
Ethyl ether 5,000 500 Pass/<LOD Ethylene glycol 620 310 Pass/<LOD
Ethylene oxide 50 50 Pass/<LOD Heptane 5,000 50 Pass/<LOD
Hexane 290 290 Pass/<LOD Isopropyl acetate 5,000 50 Pass/<LOD
Methanol 3,000 500 Pass/<LOD Naptha 400 100 Not Tested
N,N-Dimethylacetamide 1,090 100 Pass/<LOD N,N-Dimethylformamide (DMF) 880 500 Pass/<LOD
Pentane 5,000 50 Pass/<LOD Petroleum Ether 400 100 Not Tested
Propane 5,000 100 Pass/<LOD Pyridine 200 10 Pass/<LOD
Sulfolane 160 200 Pass/<LOD Tetrahydrofuran (THF) 720 200 Pass/<LOD
Toluene 890 50 Pass/<LOD Trichloroethylene 25 5 Not Tested
Xylenes* 2,170 50 Pass/<LOD

Total Butanes = 485 ug/g (PASS); Total Pentanes = 308 ug/g (PASS); Total Hexanes = 0 ug/g (PASS)

* Xylenes are reported as the sum of o-xylene, m-xylene, p-xylene, and ethylbenzene
MRL - Maximum Residue Limit; LOD - Limit of Detection

This sample has not been tested according to OAR 333-007. These results should therefore be used for research and development or quality control purposes only.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 7 of 12

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents QC Report
Testing Accreditation #: 4092-005 Test Certificate #: 134761-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Gorilla Glue
License: 030-1009646F7F8
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A4010300003A37000001276
Metrc Source Pkg#: 1A401030002C949000002555
Test Conditions

Prepsheet ID#: ORHS211222a
Scale: XS205-OR2
Temp: 21.2 °C
Baro PE: 989.4 hPa
Analyst: HRM
Technician: JBS
Sample ID#: 134761

Lot #: Gorilla Glue #1 11.2.2021
Batch #: 134761
Batch Weight (g): 593
Harvest/Process Date: 11/02/2021
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 12/23/2021
Test Date: 12/22/2021
Sample #134761
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS Recovery (%) MSD Recovery (%) Relative Percent Difference (%) QC Flag
1,2-Dichloroethane N.D. 0 0 0 nan nan
n-Propane N.D. 250 131 132 52.40 52.80 0.76 LR
Isobutane N.D. 250 154 152 61.60 60.80 1.31 LR
Methanol N.D. 250 140 143 56.00 57.20 2.12 LR
n-Butane N.D. 250 167 154 66.80 61.60 8.10 LR
2,2-Dimethylpropane N.D. 250 168 168 67.20 67.20 0.00 LR
Ethanol N.D. 250 204 190 81.60 76.00 7.11
Isopentane N.D. 250 176 175 70.40 70.00 0.57
Acetonitrile N.D. 250 201 204 80.40 81.60 1.48
Diethyl ether N.D. 250 194 193 77.60 77.20 0.52
2-propanone N.D. 250 282 316 112.80 126.40 11.37
2-propanol N.D. 250 246 222 98.40 88.80 10.26
n-Pentane N.D. 250 184 132 73.60 52.80 32.91 LRQ
2,2-Dimethylbutane N.D. 250 188 192 75.20 76.80 2.11
2,3-Dimethylbutane N.D. 250 182 193 72.80 77.20 5.87
Methylene chloride N.D. 250 209 211 83.60 84.40 0.95
2-Methylpentane N.D. 250 186 188 74.40 75.20 1.07
3-Methylpentane N.D. 250 191 194 76.40 77.60 1.56
2-Butanol N.D. 250 174 182 69.60 72.80 4.49 LR
n-Hexane N.D. 250 189 185 75.60 74.00 2.14
Ethyl acetate N.D. 250 203 210 81.20 84.00 3.39
Tetrahydrofuran N.D. 250 204 212 0.00 0.00 0.00
Trichloroethylene N.D. 0 0 0 nan nan
Isopropyl acetate N.D. 250 205 211 0.00 0.00 0.00
Benzene N.D. 250 210 214 84.00 85.60 1.89
Chloroform N.D. 0 0 0 nan nan
Cyclohexane N.D. 250 198 206 79.20 82.40 3.96
Ethylene glycol N.D. 250 105 169 42.00 67.60 46.72 LRQ
Heptane N.D. 250 173 122 69.20 48.80 34.58 LRQ
2-Ethoxyethanol N.D. 250 180 174 72.00 69.60 3.39 LR
1,4-Dioxane N.D. 250 207 209 82.80 83.60 0.96
Pyridine N.D. 0 0 0 0.00 0.00 0.00
Toluene N.D. 250 212 219 84.80 87.60 3.25
Chlorobenzene N.D. 0 0 0 0.00 0.00 0.00
Ethylbenzene N.D. 250 209 217 83.60 86.80 3.76
m-Xylene/p-Xylene N.D. 500 420 436 84.00 87.20 3.74
o-Xylene N.D. 250 210 219 84.00 87.60 4.20
Cumene N.D. 250 212 219 84.80 87.60 3.25
Ethylene oxide N.D. 250 186 188 74.40 75.20 1.07

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

N.D. = Not Detected

This sample has not been tested according to OAR 333-007. These results should therefore be used for research and development or quality control purposes only.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 8 of 12

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-005 Test Certificate #: 134761-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Gorilla Glue
License: 030-1009646F7F8
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A4010300003A37000001276
Metrc Source Pkg#: 1A401030002C949000002555
Test Conditions

Prepsheet ID#: ORHS211222a
Scale: XS205-OR4
Temp: 21.2 °C
Baro PE: 989.4 hPa
Analyst: HRM
Technician: JBS
Sample ID#: 134761

Lot #: Gorilla Glue #1 11.2.2021
Batch #: 134761
Batch Weight (g): 593
Harvest/Process Date: 11/02/2021
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 12/23/2021
Test Date: 12/22/2021
Sample #134761
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
1,2-Dichloroethane 2 1 Not Tested 1,2-Dimethoxyethane 100 5 Pass/<LOD
1,4-dioxane 380 200 Pass/<LOD 1-Butanol 5,000 100 Pass/<LOD
1-Pentanol 5,000 100 Pass/<LOD 1-Propanol 5,000 100 Pass/<LOD
2,2-Dimethylpropane (Neopentane) 5,000 100 Pass/<LOD 2,2-Dimethylbutane (Hexanes) 290 100 Pass/<LOD
2,3-Dimethylbutane (Hexanes) 290 100 Pass/<LOD 2-Butanol 5,000 100 Pass/<LOD
2-Butanone (MEK) 5,000 50 Pass/<LOD 2-Ethoxyethanol 160 40 Pass/<LOD
2-Methylbutane (Isopentane) 5,000 50 Pass/<LOD 2-Methylpentane (Hexanes) 290 50 Pass/<LOD
2-Methylpropane (Isobutane) 5,000 100 Pass/<LOD 2-propanol (Isopropyl Alcohol) 5,000 50 Pass/<LOD
2-Propanone (Acetone) 5,000 50 Pass/<LOD 3-Methylpentane (Hexanes) 290 50 Pass/<LOD
Acetonitrile 410 100 Pass/<LOD Benzene 2 1 Pass/<LOD
Butane 5,000 100 Pass/234 Chloroform 2 1 Pass/<LOD
Cumene 70 50 Pass/<LOD Cyclohexane 3,880 1,000 Pass/<LOD
Dichloromethane 600 50 Pass/<LOD Dimethylsulfoxide (DMSO) 5,000 500 Pass/<LOD
Ethanol 5,000 500 Pass/<LOD Ethyl acetate 5,000 50 Pass/<LOD
Ethyl ether 5,000 500 Pass/<LOD Ethylene glycol 620 310 Pass/<LOD
Ethylene oxide 50 50 Pass/<LOD Heptane 5,000 50 Pass/<LOD
Hexane 290 290 Pass/<LOD Isopropyl acetate 5,000 50 Pass/<LOD
Methanol 3,000 500 Pass/<LOD Naptha 400 100 Not Tested
N,N-Dimethylacetamide 1,090 100 Pass/<LOD N,N-Dimethylformamide (DMF) 880 500 Pass/<LOD
Pentane 5,000 50 Pass/<LOD Petroleum Ether 400 100 Not Tested
Propane 5,000 100 Pass/<LOD Pyridine 200 10 Pass/<LOD
Sulfolane 160 200 Pass/<LOD Tetrahydrofuran (THF) 720 200 Pass/<LOD
Toluene 890 50 Pass/<LOD Trichloroethylene 25 5 Not Tested
Xylenes* 2,170 50 Pass/<LOD

Total Butanes = 485 ug/g (PASS); Total Pentanes = 308 ug/g (PASS); Total Hexanes = 0 ug/g (PASS)

* Xylenes are reported as the sum of o-xylene, m-xylene, p-xylene, and ethylbenzene
MRL - Maximum Residue Limit; LOD - Limit of Detection

This sample has not been tested according to OAR 333-007. These results should therefore be used for research and development or quality control purposes only.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 9 of 12

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents QC Report
Testing Accreditation #: 4092-005 Test Certificate #: 134761-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Gorilla Glue
License: 030-1009646F7F8
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A4010300003A37000001276
Metrc Source Pkg#: 1A401030002C949000002555
Test Conditions

Prepsheet ID#: ORHS211222a
Scale: XS205-OR4
Temp: 21.2 °C
Baro PE: 989.4 hPa
Analyst: HRM
Technician: JBS
Sample ID#: 134761

Lot #: Gorilla Glue #1 11.2.2021
Batch #: 134761
Batch Weight (g): 593
Harvest/Process Date: 11/02/2021
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 12/23/2021
Test Date: 12/22/2021
Sample #134761
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS Recovery (%) MSD Recovery (%) Relative Percent Difference (%) QC Flag
1,2-Dichloroethane N.D. 0 0 0 nan nan
n-Propane N.D. 250 131 132 52.40 52.80 0.76 LR
Isobutane N.D. 250 154 152 61.60 60.80 1.31 LR
Methanol N.D. 250 140 143 56.00 57.20 2.12 LR
n-Butane N.D. 250 167 154 66.80 61.60 8.10 LR
2,2-Dimethylpropane N.D. 250 168 168 67.20 67.20 0.00 LR
Ethanol N.D. 250 204 190 81.60 76.00 7.11
Isopentane N.D. 250 176 175 70.40 70.00 0.57
Acetonitrile N.D. 250 201 204 80.40 81.60 1.48
Diethyl ether N.D. 250 194 193 77.60 77.20 0.52
2-propanone N.D. 250 282 316 112.80 126.40 11.37
2-propanol N.D. 250 246 222 98.40 88.80 10.26
n-Pentane N.D. 250 184 132 73.60 52.80 32.91 LRQ
2,2-Dimethylbutane N.D. 250 188 192 75.20 76.80 2.11
2,3-Dimethylbutane N.D. 250 182 193 72.80 77.20 5.87
Methylene chloride N.D. 250 209 211 83.60 84.40 0.95
2-Methylpentane N.D. 250 186 188 74.40 75.20 1.07
3-Methylpentane N.D. 250 191 194 76.40 77.60 1.56
2-Butanol N.D. 250 174 182 69.60 72.80 4.49 LR
n-Hexane N.D. 250 189 185 75.60 74.00 2.14
Ethyl acetate N.D. 250 203 210 81.20 84.00 3.39
Tetrahydrofuran N.D. 250 204 212 0.00 0.00 0.00
Trichloroethylene N.D. 0 0 0 nan nan
Isopropyl acetate N.D. 250 205 211 0.00 0.00 0.00
Benzene N.D. 250 210 214 84.00 85.60 1.89
Chloroform N.D. 0 0 0 nan nan
Cyclohexane N.D. 250 198 206 79.20 82.40 3.96
Ethylene glycol N.D. 250 105 169 42.00 67.60 46.72 LRQ
Heptane N.D. 250 173 122 69.20 48.80 34.58 LRQ
2-Ethoxyethanol N.D. 250 180 174 72.00 69.60 3.39 LR
1,4-Dioxane N.D. 250 207 209 82.80 83.60 0.96
Pyridine N.D. 0 0 0 0.00 0.00 0.00
Toluene N.D. 250 212 219 84.80 87.60 3.25
Chlorobenzene N.D. 0 0 0 0.00 0.00 0.00
Ethylbenzene N.D. 250 209 217 83.60 86.80 3.76
m-Xylene/p-Xylene N.D. 500 420 436 84.00 87.20 3.74
o-Xylene N.D. 250 210 219 84.00 87.60 4.20
Cumene N.D. 250 212 219 84.80 87.60 3.25
Ethylene oxide N.D. 250 186 188 74.40 75.20 1.07

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

N.D. = Not Detected

This sample has not been tested according to OAR 333-007. These results should therefore be used for research and development or quality control purposes only.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 10 of 12

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Homogeneity Report by
High Performance Liquid Chromatography
Testing Accreditation #: 4092-005 Test Certificate #: 134761-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Gorilla Glue
License: 030-1009646F7F8
Type: AU Tincture
Metrc Test Pkg#: 1A4010300003A37000001276
Metrc Source Pkg#: 1A401030002C949000002555
Sample ID#: 134761

Lot #: Gorilla Glue #1 11.2.2021
Batch #: 134761
Batch Weight (g): 593
Harvest/Process Date: 11/02/2021
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 12/23/2021
Sample #134761
Increments Tested (mg/g) TOTAL THC TOTAL CBD THC THCA THCV CBD CBC CBDA CBDV CBG CBN
Increment 1 733.33 15.36 42.16 788.11 N.D. N.D. N.D. 17.51 N.D. 2.29 N.D.
Increment 2 690.20 16.30 47.80 732.50 N.D. N.D. N.D. 18.59 N.D. 2.86 N.D.
Average Value 711.77 15.83 44.98 760.31 N.D. N.D. N.D. 18.05 N.D. 2.58 N.D.
Max Value 733.33 16.30 47.80 788.11 N.D. N.D. N.D. 18.59 N.D. 2.86 N.D.
Min Value 690.20 15.36 42.16 732.50 N.D. N.D. N.D. 17.51 N.D. 2.29 N.D.
Relative Percent Difference (RPD) ±6.06 ±5.98 ±12.54 ±7.31 N.D. N.D. N.D. ±5.98 N.D. ±22.14 N.D.
Average Cannabinoids Per Package 711.77 15.83 44.98 760.31 N.D. N.D. N.D. 18.05 N.D. 2.58 N.D.
Average Cannabinoids Per Serving 35.59 0.79 2.25 38.02 N.D. N.D. N.D. 0.90 N.D. 0.13 N.D.
Max Concentration Per Serving (THC)   Not Applicable
Max Concentration Per Package (THC)   Pass
Relative Percent Difference (RPD)   Pass
Control Study   Yes, MJ1957
Field Duplicate   Pass

N.D. = Not Detected, Min = Minimum, Max = Maximum

RPD is the relative percent difference between increment 1 and increment 2.

RSD is the relative standard deviation between all increments tested.

Total THC and CBD is the calculated sum of CBD or THC and the amount of CBD or THC derived from CBDA or THCA, respectively. These values are calculated by adding a molar correction factor of 0.877 to the CBDA or THCA value.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 11 of 12
IRON Laboratories

Terpene Report by
Mass Spectrometer
Test Certificate #: 134761-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Gorilla Glue
License: 030-1009646F7F8
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A4010300003A37000001276
Metrc Source Pkg#: 1A401030002C949000002555

Test Conditions

Scale: XS205-OR1
Temp: 21.2 °C
Baro Pressure: 989.4 hPa
Analyst: HRM
Technician: JBS

Sample ID#: 134761

Lot #: Gorilla Glue #1 11.2.2021
Batch #: 134761
Batch Weight (g): 593
Harvest/Process Date: 11/02/2021
Serving Size (g): 0.05
Date Received: 12/23/2021

Sample #134761
Sample #134761
  • α-Pinene (0.22%)
  • β-Ocimene (0.42%)
  • Camphene (0.02%)
  • Eucalyptol (1,8-Cineol) (0.00%)
  • Sabinene (0.00%)
  • γ-Terpinene (0.94%)
  • Myrcene (0.82%)
  • α-Terpinolene (1.20%)
  • β-Pinene (0.63%)
  • Linalool (0.34%)
  • ∆3-Carene (0.19%)
  • Fenchone (0.00%)
  • α-Terpinene (1.93%)
  • endo-Fenchol (0.02%)
  • α-Ocimene (0.02%)
  • Isopulegol (0.00%)
  • Limonene (0.70%)
  • Geraniol (0.00%)
  • p-Cymene (0.00%)
  • β-Caryophyllene (0.10%)
  • α-Humulene (4.22%)
  • Nerolidol 1 (cis) (0.00%)
  • Nerolidol 2 (trans) (0.05%)
  • Guaiol (0.00%)
  • Caryophyllene Oxide (0.40%)
  • α-Bisabolol (0.92%)
  • α-Phellandrene (1.02%)
  • α-Terpineol (0.00%)
  • Valenence (0.20%)

Total: 14.360%

Predominant Terpenes

4.22%   α-Humulene Woody, oceanic-watery, spicy clove 1.93%   α-Terpinene Woody, lemon, citrus
1.20%   α-Terpinolene Fresh wood, sweet, pine, citrus 1.02%   α-Phellandrene Citrus, green, black pepper
0.94%   γ-Terpinene Woody, lemon/lime, tropical 0.92%   α-Bisabolol Fruity, nutty, coconut

Value in parenthesis indicates percentage of terpene present in the total sample (weight percentage, wt/wt%).
Value in doughnut slice indicates individual terpene abundance with respect to the total terpenes detected.

This sample has not been tested according to OAR 333-007. These results should therefore be used for research and development or quality control purposes only.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Himashi Mead Iron laboratories Himashi Mead

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 12 of 12