ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Marijuana Potency Analysis by
High Performance Liquid Chromatography
Testing Accreditation #: 4092-005 Test Certificate #: 134752-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Elephant Ears
License: 030-1009646F7F8
Type: AU Tincture
Method: FE04U HPLC-UV
Metrc Test Pkg#: 1A4010300003A37000001267
Metrc Source Pkg#: 1A401030002C949000002705
Test Conditions

Prepsheet ID#: ORP211216a
Scale: XS205-OR1
Temp: 22.3 °C
Baro Pressure: 1004 hPa
Analyst: TMR
Technician: TMR
Sample ID#: 134752

Lot #: Elephant Ears #1 12.12.2021
Batch #: 134752
Batch Weight (g): 468.7
Harvest/Process Date: 12/12/2021
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 12/23/2021
Test Date: 12/16/2021
Sample #134752
Sample #134752 Sample #134752
Test
Compounds		 THC THCA CBD CBDA CBN CBG CBC THCV* CBDV Total
Cannabinoids*		 Total THC Total CBD Calc Max Total
Cannabinoids*
Amount (%) 10.16 63.20 N/D 0.74 N/D 0.25 N/D N/D N/D 74.35 65.58 0.65 66.48
Amount (mg/g) 101.55 631.98 N/D 7.42 N/D 2.53 N/D N/D N/D 743.48 655.80 6.51 664.84
Amount per Serving (mg) 5.08 31.60 N\D 0.37 N\D 0.13 N\D N\D N\D 37.17 Serving Size~ (g): 0.05
LOQ (mg/g) 1.8 1.8 1.8 1.8 1.8 1.8 1.8 1.8 1.8   %Decarb. THC CBD
±%RPD 5.24 5.50 0.95 6.53 2.51 +/-5% 3.15 1.35 0.49 14 0

LOQ = Limit of Quantitation; %RPD = Relative Percent Deviation; %RSD = Relative Standard Deviation; N/D = Not Detected

*Designates values that are not currently included in the accredited scope of Iron Laboratories.

*** Designates tests that use the method FE-45. FE-45 is performed using AOAC 966.02 and 32.004-32.009. FE-45 has relative expanded (k=2) uncertainties of 1.098% for moisture, 1.754% for water activity for unprocessed plant materials, and 13.102% for water activity for infused products. Vitamin E acetate analysis has a relative expanded (k=2) uncertainty of 18.614%.

Total THC and CBD is the calculated sum of THC or CBD and the amount of THC or CBD derived from THCA or CBDA, respectively. These values are calculated by applying a molar correction factor of 0.877 to the THCA or the CBDA value. Calc Max Total Cannabinoids is the sum of Total THC, Total CBD, CBN, CBG, CBC, THCV, and CBDV.

%Decarb. THC and CBD refer to the percentage of THC or CBD relative to THCA or CBDA, respectively.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 1 of 12

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant QC Report
Testing Accreditation #: 4092-005 Test Certificate #: 134752-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Elephant Ears
License: 030-1009646F7F8
Type: AU Tincture
Method: FE04U HPLC-UV
Metrc Test Pkg#: 1A4010300003A37000001267
Metrc Source Pkg#: 1A401030002C949000002705
Test Conditions

Prepsheet ID#: ORP211216a
Scale: XS205-OR1
Temp: 22.3 °C
Baro Pressure: 1004 hPa
Analyst: TMR
Technician: TMR
Sample ID#: 134752

Lot #: Elephant Ears #1 12.12.2021
Batch #: 134752
Batch Weight (g): 468.7
Harvest/Process Date: 12/12/2021
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 12/23/2021
Test Date: 12/16/2021
Sample #134752
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Cannabidivarin (CBDV) N.D. 4.07 4.05 99.51 4.07 100.00 0.49
Cannabidiolic Acid (CBDA) N.D. 3.32 3.11 93.67 3.32 100.00 6.53
Cannabigerol (CBG) N.D. 4.54 4.5 99.12 4.5 99.12 0.00
Cannabidiol (CBD) N.D. 4.24 4.18 98.58 4.22 99.53 0.95
Δ9-Tetrahydrocannabivarin (THCV) N.D. 4.5 4.43 98.44 4.49 99.78 1.35
Cannabinol (CBN) N.D. 4.8 4.73 98.54 4.85 101.04 2.51
Δ9-Tetrahydrocannabinol (THC) N.D. 4.81 4.65 96.67 4.9 101.87 5.24
Cannabichromene (CBC) N.D. 4.48 4.37 97.54 4.51 100.67 3.15
Tetrahydrocannabinolic acid (THCA) N.D. 4.1 3.71 90.49 3.92 95.61 5.50

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 2 of 12

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Marijuana Potency Analysis by
High Performance Liquid Chromatography
Testing Accreditation #: 4092-005 Test Certificate #: 134752-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Elephant Ears
License: 030-1009646F7F8
Type: AU Tincture
Method: FE04U HPLC-UV
Metrc Test Pkg#: 1A4010300003A37000001267
Metrc Source Pkg#: 1A401030002C949000002705
Test Conditions

Prepsheet ID#: ORP211216a
Scale: XS205-OR1
Temp: 22.3 °C
Baro Pressure: 1004 hPa
Analyst: TMR
Technician: TMR
Sample ID#: 134752

Lot #: Elephant Ears #1 12.12.2021
Batch #: 134752
Batch Weight (g): 468.7
Harvest/Process Date: 12/12/2021
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 12/23/2021
Test Date: 12/16/2021
Sample #134752
Sample #134752 Sample #134752
Test
Compounds		 THC THCA CBD CBDA CBN CBG CBC THCV* CBDV Total
Cannabinoids*		 Total THC Total CBD Calc Max Total
Cannabinoids*
Amount (%) 13.07 60.82 N/D 0.65 N/D 0.35 0.25 N/D N/D 75.14 66.41 0.57 67.58
Amount (mg/g) 130.68 608.24 N/D 6.46 N/D 3.50 2.48 N/D N/D 751.36 664.11 5.67 675.76
Amount per Serving (mg) 6.53 30.41 N\D 0.32 N\D 0.18 0.12 N\D N\D 37.57 Serving Size~ (g): 0.05
LOQ (mg/g) 1.9 1.9 1.9 1.9 1.9 1.9 1.9 1.9 1.9   %Decarb. THC CBD
±%RPD 5.24 5.50 0.95 6.53 2.51 +/-5% 3.15 1.35 0.49 0 0

LOQ = Limit of Quantitation; %RPD = Relative Percent Deviation; %RSD = Relative Standard Deviation; N/D = Not Detected

*Designates values that are not currently included in the accredited scope of Iron Laboratories.

*** Designates tests that use the method FE-45. FE-45 is performed using AOAC 966.02 and 32.004-32.009. FE-45 has relative expanded (k=2) uncertainties of 1.098% for moisture, 1.754% for water activity for unprocessed plant materials, and 13.102% for water activity for infused products. Vitamin E acetate analysis has a relative expanded (k=2) uncertainty of 18.614%.

Total THC and CBD is the calculated sum of THC or CBD and the amount of THC or CBD derived from THCA or CBDA, respectively. These values are calculated by applying a molar correction factor of 0.877 to the THCA or the CBDA value. Calc Max Total Cannabinoids is the sum of Total THC, Total CBD, CBN, CBG, CBC, THCV, and CBDV.

%Decarb. THC and CBD refer to the percentage of THC or CBD relative to THCA or CBDA, respectively.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 2 of 12

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant QC Report
Testing Accreditation #: 4092-005 Test Certificate #: 134752-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Elephant Ears
License: 030-1009646F7F8
Type: AU Tincture
Method: FE04U HPLC-UV
Metrc Test Pkg#: 1A4010300003A37000001267
Metrc Source Pkg#: 1A401030002C949000002705
Test Conditions

Prepsheet ID#: ORP211216a
Scale: XS205-OR1
Temp: 22.3 °C
Baro Pressure: 1004 hPa
Analyst: TMR
Technician: TMR
Sample ID#: 134752

Lot #: Elephant Ears #1 12.12.2021
Batch #: 134752
Batch Weight (g): 468.7
Harvest/Process Date: 12/12/2021
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 12/23/2021
Test Date: 12/16/2021
Sample #134752
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Cannabidivarin (CBDV) N.D. 4.07 4.05 99.51 4.07 100.00 0.49
Cannabidiolic Acid (CBDA) N.D. 3.32 3.11 93.67 3.32 100.00 6.53
Cannabigerol (CBG) N.D. 4.54 4.5 99.12 4.5 99.12 0.00
Cannabidiol (CBD) N.D. 4.24 4.18 98.58 4.22 99.53 0.95
Δ9-Tetrahydrocannabivarin (THCV) N.D. 4.5 4.43 98.44 4.49 99.78 1.35
Cannabinol (CBN) N.D. 4.8 4.73 98.54 4.85 101.04 2.51
Δ9-Tetrahydrocannabinol (THC) N.D. 4.81 4.65 96.67 4.9 101.87 5.24
Cannabichromene (CBC) N.D. 4.48 4.37 97.54 4.51 100.67 3.15
Tetrahydrocannabinolic acid (THCA) N.D. 4.1 3.71 90.49 3.92 95.61 5.50

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 3 of 12

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Pesticide Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-005 Test Certificate #: 134752-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Elephant Ears
License: 030-1009646F7F8
Type: AU Tincture
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A4010300003A37000001267
Metrc Source Pkg#: 1A401030002C949000002705
Test Conditions

Prepsheet ID#: ORPS211222a
Scale: XS205-OR1
Temp: 22.7 °C
Baro PE: 992.2 hPa
Analyst: HRM
Technician: JBS
Sample ID#: 134752

Lot #: Elephant Ears #1 12.12.2021
Batch #: 134752
Batch Weight (g): 468.7
Harvest/Process Date: 12/12/2021
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 12/23/2021
Test Date: 12/22/2021
Sample #134752
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
Aldicarb 0.400 0.120 Pass/<LOD Abamectin**** 0.500 0.120 Pass/<LOD
Acephate 0.400 0.120 Pass/<LOD Acequinocyl 2.000 0.240 Pass/<LOD
Acetamiprid 0.200 0.120 Pass/<LOD Azoxystrobin 0.200 0.120 Pass/<LOD
Bifenazate 0.200 0.120 Pass/<LOD Bifenthrin 0.200 0.120 Pass/<LOD
Boscalid 0.400 0.120 Pass/<LOD Carbaryl 0.200 0.120 Pass/<LOD
Carbofuran 0.200 0.120 Pass/<LOD Chlorantraniliprole 0.200 0.120 Pass/<LOD
Chlorfenapyr 1.000 0.480 Pass/<LOD Chlorpyrifos 0.200 0.120 Pass/<LOD
Clofentezine 0.200 0.120 Pass/<LOD Cyfluthrin** 1.000 0.480 Pass/<LOD
Cypermethrin*** 1.000 0.480 Pass/<LOD Daminozide 1.000 0.120 Pass/<LOD
DDVP (Dichlorvos) 1.000 0.240 Pass/<LOD Diazinon 0.200 0.120 Pass/<LOD
Dimethoate 0.200 0.120 Pass/<LOD Ethoprophos 0.200 0.120 Pass/<LOD
Etofenprox 0.400 0.120 Pass/<LOD Etoxazole 0.200 0.120 Pass/<LOD
Fenoxycarb 0.200 0.120 Pass/<LOD Fenpyroximate 0.400 0.120 Pass/<LOD
Fipronil 0.400 0.120 Pass/<LOD Flonicamid 1.000 0.120 Pass/<LOD
Fludioxonil 0.400 0.120 Pass/<LOD Hexythiazox 1.000 0.120 Pass/<LOD
Imazalil 0.200 0.120 Pass/<LOD Imidacloprid 0.400 0.120 Pass/<LOD
Kresoxim Methyl 0.400 0.120 Pass/<LOD Malathion 0.200 0.120 Pass/<LOD
Metalaxyl 0.200 0.120 Pass/<LOD Methiocarb 0.200 0.120 Pass/<LOD
Methomyl 0.400 0.120 Pass/<LOD Methyl Parathion 0.200 0.120 Pass/<LOD
MGK-264‡ 0.200 0.120 Pass/<LOD Myclobutanil 0.000 0.120 Pass/<LOD
Naled 0.500 0.120 Pass/<LOD Oxamyl 1.000 0.120 Pass/<LOD
Paclobutrazol 0.400 0.120 Pass/<LOD Permethrins† 0.200 0.120 Pass/<LOD
Phosmet 0.200 0.120 Pass/<LOD Piperonyl Butoxide 2.000 0.120 Pass/<LOD
Prallethrin 0.200 0.120 Pass/<LOD Propiconazole 0.400 0.120 Pass/<LOD
Propoxur 0.200 0.120 Pass/<LOD Pyrethrins* 1.000 0.120 Pass/<LOD
Pyridaben 0.200 0.120 Pass/<LOD Spinosad***** 0.200 0.120 Pass/<LOD
Spiromesifen 0.200 0.120 Pass/<LOD Spirotetramat 0.200 0.120 Pass/<LOD
Spiroxamine‡ 0.400 0.120 Pass/<LOD Tebuconazole 0.400 0.120 Pass/<LOD
Thiacloprid 0.200 0.120 Pass/<LOD Thiamethoxam 0.200 0.120 Pass/<LOD
Trifloxystrobin 0.200 0.120 Pass/<LOD

* Pyrethrins are reported as the sum of Jasmolin I, Cinerin I, and Pyrethrin I
** Cyfluthrins are reported as the sum of isomers Cyfluthrin I, II, III, and IV
*** Cypermethrins are reported as the sum of isomers Cypermethrin I, II, III, and IV
**** Abamectin is reported as the sum of Avermectin B1a and Avermectin B1b
***** Spinosad is reported as the sum of Spinosyn A and Spinosyn D
† Permethrin and Prallethrin are reported as the sum of cis and trans isomers
‡ MGK-264 and Spiroximine are reported as the sum of isomers I and II
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 3 of 12

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Pesticide QC Report
Testing Accreditation #: 4092-005 Test Certificate #: 134752-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Elephant Ears
License: 030-1009646F7F8
Type: AU Tincture
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A4010300003A37000001267
Metrc Source Pkg#: 1A401030002C949000002705
Test Conditions

Prepsheet ID#: ORPS211222a
Scale: XS205-OR1
Temp: 22.7 °C
Baro PE: 992.2 hPa
Analyst: HRM
Technician: JBS
Sample ID#: 134752

Lot #: Elephant Ears #1 12.12.2021
Batch #: 134752
Batch Weight (g): 468.7
Harvest/Process Date: 12/12/2021
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 12/23/2021
Test Date: 12/22/2021
Sample #134752
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS recovery% MSD recovery% Relative Percent Difference (%) QC Flag
Acephate N.D. 1 1.46 1.25 146.00 125.00 15.50 HR
Acequinocyl N.D. 1 0.889 1.06 88.90 106.00 17.55
Acetamiprid N.D. 1 1.21 1.5 121.00 150.00 21.40 HRQ
Aldicarb N.D. 1 0.904 1.19 90.40 119.00 27.32 Q
Avermectin B1a N.D. 0.97 2.31 1.92 238.14 197.94 18.44 HR
Azoxystrobin N.D. 1 1.51 1.32 151.00 132.00 13.43 HR
Bifenazate N.D. 1 1.59 1.63 159.00 163.00 2.48 HR
Bifenthrin N.D. 1 0.903 1.29 90.30 129.00 35.29 Q
Boscalid N.D. 1 1.38 1.4 138.00 140.00 1.44 HR
Carbaryl N.D. 1 1.07 1.52 107.00 152.00 34.75 HRQ
Carbofuran N.D. 1 1.46 1.43 146.00 143.00 2.08 HR
Chlorantraniliprole N.D. 1 2.2 1.72 220.00 172.00 24.49 HR Q
Chlorfenapyr N.D. 1 0.766 1.05 76.60 105.00 31.28 Q
Chlorpyriphos N.D. 1 1.25 1.39 125.00 139.00 10.61 HR
Clofentezine N.D. 1 1.43 1.81 143.00 181.00 23.46 HR Q
Cyfluthrin N.D. 1 0.955 1.16 95.50 116.00 19.39
Cypermethrin N.D. 1 1.09 1.19 109.00 119.00 8.77
Daminoside N.D. 1 2.2 10.5 220.00 1,050.00 130.71 HR Q
Diazanon N.D. 1 32.6 29.7 3,260.00 2,970.00 9.31 HR
Dichlorvos N.D. 1 1.77 1.65 177.00 165.00 7.02 HR
Dimethoate N.D. 1 1.33 1.32 133.00 132.00 0.75 HR
Ethoprophos N.D. 1 1.46 1.51 146.00 151.00 3.37 HR
Etofenprox N.D. 1 1.1 1.08 110.00 108.00 1.83
Etoxazole N.D. 1 1.76 1.8 176.00 180.00 2.25 HR
Fenoxycarb N.D. 1 1.86 1.92 186.00 192.00 3.17 HR
Fenpyroximate N.D. 1 1.62 1.91 162.00 191.00 16.43 HR
Fipronil N.D. 1 1.2 0.878 120.00 87.80 30.99 Q
Flonicamid N.D. 1 0.99 1.52 99.00 152.00 42.23 HRQ
Fludioxonil N.D. 1 1.17 0.89 117.00 89.00 27.18 Q
Hexythiazox N.D. 1 1.04 1.18 104.00 118.00 12.61
Imazalil N.D. 1 2.71 2.36 271.00 236.00 13.81 HR
Imidacloprid N.D. 1 1.54 1.81 154.00 181.00 16.12 HR
Kresoxim-methyl N.D. 1 1.72 2 172.00 200.00 15.05 HR
Malathion N.D. 1 1.48 1.37 148.00 137.00 7.72 HR
Metalaxyl N.D. 1 1.82 1.89 182.00 189.00 3.77 HR
Methiocarb N.D. 1 1.36 1.1 136.00 110.00 21.14 HR Q
Methomyl N.D. 1 1.25 1.59 125.00 159.00 23.94 HRQ
MGK-264 N.D. 1 1.1 1.33 110.00 133.00 18.93 HR
Myclobutanil N.D. 1 2.13 1.9 213.00 190.00 11.41 HR
Naled (dibrom) N.D. 1 0.819 0.706 81.90 70.60 14.82
Oxamyl N.D. 1 1.35 0.917 135.00 91.70 38.20 HR Q
Paclobutrazol N.D. 1 2.65 2.69 265.00 269.00 1.50 HR
Parathion-methyl N.D. 1 1.06 0.975 106.00 97.50 8.35
Permethrins N.D. 1 1.129 1.226 112.90 122.60 8.24
Phosmet N.D. 1 1.78 1.86 178.00 186.00 4.40 HR
Piperonyl butoxide N.D. 1 1.16 1.21 116.00 121.00 4.22
Prallethrin N.D. 1 1.85 1.9 185.00 190.00 2.67 HR
Propiconazole N.D. 1 1.99 1.95 199.00 195.00 2.03 HR
Propoxur N.D. 1 1.07 1.29 107.00 129.00 18.64
Pyrethrin N.D. 0.65 0.858 1.07 132.00 164.62 21.99 HR Q
Pyridaben N.D. 1 1.32 1.4 132.00 140.00 5.88 HR
SpinosynA N.D. 0.84 1.69 1.46 201.19 173.81 14.60 HR
SpinosynD N.D. 0.16 0.283 0.294 176.88 183.75 3.81 HR
Spiromesifen N.D. 1 0.925 0.992 92.50 99.20 6.99
Spirotetramat N.D. 1 1.51 1.33 151.00 133.00 12.68 HR
Spiroxamine N.D. 1 2.54 2.24 254.00 224.00 12.55 HR
Tebuconazole N.D. 1 2.02 2.15 202.00 215.00 6.24 HR
Thiacloprid N.D. 1 1.84 2.03 184.00 203.00 9.82 HR
Thiamethoxam N.D. 1 1.59 1.85 159.00 185.00 15.12 HR
Trifloxystrobin N.D. 1 1.25 1.27 125.00 127.00 1.59

N.D. = Not Detected

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 30%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (60-120%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 4 of 12

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Pesticide Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-005 Test Certificate #: 134752-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Elephant Ears
License: 030-1009646F7F8
Type: AU Tincture
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A4010300003A37000001267
Metrc Source Pkg#: 1A401030002C949000002705
Test Conditions

Prepsheet ID#: ORPS211222a
Scale: XS205-OR1
Temp: 22.7 °C
Baro PE: 992.2 hPa
Analyst: HRM
Technician: JBS
Sample ID#: 134752

Lot #: Elephant Ears #1 12.12.2021
Batch #: 134752
Batch Weight (g): 468.7
Harvest/Process Date: 12/12/2021
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 12/23/2021
Test Date: 12/22/2021
Sample #134752
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
Aldicarb 0.400 0.125 Pass/<LOD Abamectin**** 0.500 0.125 Pass/<LOD
Acephate 0.400 0.125 Pass/<LOD Acequinocyl 2.000 0.250 Pass/<LOD
Acetamiprid 0.200 0.125 Pass/<LOD Azoxystrobin 0.200 0.125 Pass/<LOD
Bifenazate 0.200 0.125 Pass/<LOD Bifenthrin 0.200 0.125 Pass/<LOD
Boscalid 0.400 0.125 Pass/<LOD Carbaryl 0.200 0.125 Pass/<LOD
Carbofuran 0.200 0.125 Pass/<LOD Chlorantraniliprole 0.200 0.125 Pass/<LOD
Chlorfenapyr 1.000 0.499 Pass/<LOD Chlorpyrifos 0.200 0.125 Pass/<LOD
Clofentezine 0.200 0.125 Pass/<LOD Cyfluthrin** 1.000 0.499 Pass/<LOD
Cypermethrin*** 1.000 0.499 Pass/<LOD Daminozide 1.000 0.125 Pass/<LOD
DDVP (Dichlorvos) 1.000 0.250 Pass/<LOD Diazinon 0.200 0.125 Pass/<LOD
Dimethoate 0.200 0.125 Pass/<LOD Ethoprophos 0.200 0.125 Pass/<LOD
Etofenprox 0.400 0.125 Pass/<LOD Etoxazole 0.200 0.125 Pass/<LOD
Fenoxycarb 0.200 0.125 Pass/<LOD Fenpyroximate 0.400 0.125 Pass/<LOD
Fipronil 0.400 0.125 Pass/<LOD Flonicamid 1.000 0.125 Pass/<LOD
Fludioxonil 0.400 0.125 Pass/<LOD Hexythiazox 1.000 0.125 Pass/<LOD
Imazalil 0.200 0.125 Pass/<LOD Imidacloprid 0.400 0.125 Pass/<LOD
Kresoxim Methyl 0.400 0.125 Pass/<LOD Malathion 0.200 0.125 Pass/<LOD
Metalaxyl 0.200 0.125 Pass/<LOD Methiocarb 0.200 0.125 Pass/<LOD
Methomyl 0.400 0.125 Pass/<LOD Methyl Parathion 0.200 0.125 Pass/<LOD
MGK-264‡ 0.200 0.125 Pass/<LOD Myclobutanil 0.000 0.125 Pass/<LOD
Naled 0.500 0.125 Pass/<LOD Oxamyl 1.000 0.125 Pass/<LOD
Paclobutrazol 0.400 0.125 Pass/<LOD Permethrins† 0.200 0.125 Pass/<LOD
Phosmet 0.200 0.125 Pass/<LOD Piperonyl Butoxide 2.000 0.125 Pass/<LOD
Prallethrin 0.200 0.125 Pass/<LOD Propiconazole 0.400 0.125 Pass/<LOD
Propoxur 0.200 0.125 Pass/<LOD Pyrethrins* 1.000 0.125 Pass/<LOD
Pyridaben 0.200 0.125 Pass/<LOD Spinosad***** 0.200 0.125 Pass/<LOD
Spiromesifen 0.200 0.125 Pass/<LOD Spirotetramat 0.200 0.125 Pass/<LOD
Spiroxamine‡ 0.400 0.125 Pass/<LOD Tebuconazole 0.400 0.125 Pass/<LOD
Thiacloprid 0.200 0.125 Pass/<LOD Thiamethoxam 0.200 0.125 Pass/<LOD
Trifloxystrobin 0.200 0.125 Pass/<LOD

* Pyrethrins are reported as the sum of Jasmolin I, Cinerin I, and Pyrethrin I
** Cyfluthrins are reported as the sum of isomers Cyfluthrin I, II, III, and IV
*** Cypermethrins are reported as the sum of isomers Cypermethrin I, II, III, and IV
**** Abamectin is reported as the sum of Avermectin B1a and Avermectin B1b
***** Spinosad is reported as the sum of Spinosyn A and Spinosyn D
† Permethrin and Prallethrin are reported as the sum of cis and trans isomers
‡ MGK-264 and Spiroximine are reported as the sum of isomers I and II
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 5 of 12

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Pesticide QC Report
Testing Accreditation #: 4092-005 Test Certificate #: 134752-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Elephant Ears
License: 030-1009646F7F8
Type: AU Tincture
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A4010300003A37000001267
Metrc Source Pkg#: 1A401030002C949000002705
Test Conditions

Prepsheet ID#: ORPS211222a
Scale: XS205-OR1
Temp: 22.7 °C
Baro PE: 992.2 hPa
Analyst: HRM
Technician: JBS
Sample ID#: 134752

Lot #: Elephant Ears #1 12.12.2021
Batch #: 134752
Batch Weight (g): 468.7
Harvest/Process Date: 12/12/2021
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 12/23/2021
Test Date: 12/22/2021
Sample #134752
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS recovery% MSD recovery% Relative Percent Difference (%) QC Flag
Acephate N.D. 1 1.46 1.25 146.00 125.00 15.50 HR
Acequinocyl N.D. 1 0.889 1.06 88.90 106.00 17.55
Acetamiprid N.D. 1 1.21 1.5 121.00 150.00 21.40 HRQ
Aldicarb N.D. 1 0.904 1.19 90.40 119.00 27.32 Q
Avermectin B1a N.D. 0.97 2.31 1.92 238.14 197.94 18.44 HR
Azoxystrobin N.D. 1 1.51 1.32 151.00 132.00 13.43 HR
Bifenazate N.D. 1 1.59 1.63 159.00 163.00 2.48 HR
Bifenthrin N.D. 1 0.903 1.29 90.30 129.00 35.29 Q
Boscalid N.D. 1 1.38 1.4 138.00 140.00 1.44 HR
Carbaryl N.D. 1 1.07 1.52 107.00 152.00 34.75 HRQ
Carbofuran N.D. 1 1.46 1.43 146.00 143.00 2.08 HR
Chlorantraniliprole N.D. 1 2.2 1.72 220.00 172.00 24.49 HR Q
Chlorfenapyr N.D. 1 0.766 1.05 76.60 105.00 31.28 Q
Chlorpyriphos N.D. 1 1.25 1.39 125.00 139.00 10.61 HR
Clofentezine N.D. 1 1.43 1.81 143.00 181.00 23.46 HR Q
Cyfluthrin N.D. 1 0.955 1.16 95.50 116.00 19.39
Cypermethrin N.D. 1 1.09 1.19 109.00 119.00 8.77
Daminoside N.D. 1 2.2 10.5 220.00 1,050.00 130.71 HR Q
Diazanon N.D. 1 32.6 29.7 3,260.00 2,970.00 9.31 HR
Dichlorvos N.D. 1 1.77 1.65 177.00 165.00 7.02 HR
Dimethoate N.D. 1 1.33 1.32 133.00 132.00 0.75 HR
Ethoprophos N.D. 1 1.46 1.51 146.00 151.00 3.37 HR
Etofenprox N.D. 1 1.1 1.08 110.00 108.00 1.83
Etoxazole N.D. 1 1.76 1.8 176.00 180.00 2.25 HR
Fenoxycarb N.D. 1 1.86 1.92 186.00 192.00 3.17 HR
Fenpyroximate N.D. 1 1.62 1.91 162.00 191.00 16.43 HR
Fipronil N.D. 1 1.2 0.878 120.00 87.80 30.99 Q
Flonicamid N.D. 1 0.99 1.52 99.00 152.00 42.23 HRQ
Fludioxonil N.D. 1 1.17 0.89 117.00 89.00 27.18 Q
Hexythiazox N.D. 1 1.04 1.18 104.00 118.00 12.61
Imazalil N.D. 1 2.71 2.36 271.00 236.00 13.81 HR
Imidacloprid N.D. 1 1.54 1.81 154.00 181.00 16.12 HR
Kresoxim-methyl N.D. 1 1.72 2 172.00 200.00 15.05 HR
Malathion N.D. 1 1.48 1.37 148.00 137.00 7.72 HR
Metalaxyl N.D. 1 1.82 1.89 182.00 189.00 3.77 HR
Methiocarb N.D. 1 1.36 1.1 136.00 110.00 21.14 HR Q
Methomyl N.D. 1 1.25 1.59 125.00 159.00 23.94 HRQ
MGK-264 N.D. 1 1.1 1.33 110.00 133.00 18.93 HR
Myclobutanil N.D. 1 2.13 1.9 213.00 190.00 11.41 HR
Naled (dibrom) N.D. 1 0.819 0.706 81.90 70.60 14.82
Oxamyl N.D. 1 1.35 0.917 135.00 91.70 38.20 HR Q
Paclobutrazol N.D. 1 2.65 2.69 265.00 269.00 1.50 HR
Parathion-methyl N.D. 1 1.06 0.975 106.00 97.50 8.35
Permethrins N.D. 1 1.129 1.226 112.90 122.60 8.24
Phosmet N.D. 1 1.78 1.86 178.00 186.00 4.40 HR
Piperonyl butoxide N.D. 1 1.16 1.21 116.00 121.00 4.22
Prallethrin N.D. 1 1.85 1.9 185.00 190.00 2.67 HR
Propiconazole N.D. 1 1.99 1.95 199.00 195.00 2.03 HR
Propoxur N.D. 1 1.07 1.29 107.00 129.00 18.64
Pyrethrin N.D. 0.65 0.858 1.07 132.00 164.62 21.99 HR Q
Pyridaben N.D. 1 1.32 1.4 132.00 140.00 5.88 HR
SpinosynA N.D. 0.84 1.69 1.46 201.19 173.81 14.60 HR
SpinosynD N.D. 0.16 0.283 0.294 176.88 183.75 3.81 HR
Spiromesifen N.D. 1 0.925 0.992 92.50 99.20 6.99
Spirotetramat N.D. 1 1.51 1.33 151.00 133.00 12.68 HR
Spiroxamine N.D. 1 2.54 2.24 254.00 224.00 12.55 HR
Tebuconazole N.D. 1 2.02 2.15 202.00 215.00 6.24 HR
Thiacloprid N.D. 1 1.84 2.03 184.00 203.00 9.82 HR
Thiamethoxam N.D. 1 1.59 1.85 159.00 185.00 15.12 HR
Trifloxystrobin N.D. 1 1.25 1.27 125.00 127.00 1.59

N.D. = Not Detected

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 30%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (60-120%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 6 of 12

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-005 Test Certificate #: 134752-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Elephant Ears
License: 030-1009646F7F8
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A4010300003A37000001267
Metrc Source Pkg#: 1A401030002C949000002705
Test Conditions

Prepsheet ID#: MIHS211229a
Scale: XS205-OR1
Temp: 21.2 °C
Baro PE: 976.3 hPa
Analyst: HRM
Technician: MEH
Sample ID#: 134752

Lot #: Elephant Ears #1 12.12.2021
Batch #: 134752
Batch Weight (g): 468.7
Harvest/Process Date: 12/12/2021
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 12/23/2021
Test Date: 12/22/2021
Sample #134752
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
1,2-Dichloroethane 2 1 Not Tested 1,2-Dimethoxyethane 100 5 Pass/<LOD
1,4-dioxane 380 200 Pass/<LOD 1-Butanol 5,000 100 Pass/<LOD
1-Pentanol 5,000 100 Pass/<LOD 1-Propanol 5,000 100 Pass/<LOD
2,2-Dimethylpropane (Neopentane) 5,000 100 Pass/<LOD 2,2-Dimethylbutane (Hexanes) 290 100 Pass/<LOD
2,3-Dimethylbutane (Hexanes) 290 100 Pass/<LOD 2-Butanol 5,000 100 Pass/<LOD
2-Butanone (MEK) 5,000 50 Pass/<LOD 2-Ethoxyethanol 160 40 Pass/<LOD
2-Methylbutane (Isopentane) 5,000 50 Pass/315 2-Methylpentane (Hexanes) 290 50 Pass/<LOD
2-Methylpropane (Isobutane) 5,000 100 Pass/<LOD 2-propanol (Isopropyl Alcohol) 5,000 50 Pass/<LOD
2-Propanone (Acetone) 5,000 50 Pass/<LOD 3-Methylpentane (Hexanes) 290 50 Pass/<LOD
Acetonitrile 410 100 Pass/<LOD Benzene 2 1 Pass/<LOD
Butane 5,000 100 Pass/544 Chloroform 2 1 Pass/<LOD
Cumene 70 50 Pass/<LOD Cyclohexane 3,880 1,000 Pass/<LOD
Dichloromethane 600 50 Pass/<LOD Dimethylsulfoxide (DMSO) 5,000 500 Pass/<LOD
Ethanol 5,000 500 Pass/<LOD Ethyl acetate 5,000 50 Pass/<LOD
Ethyl ether 5,000 500 Pass/<LOD Ethylene glycol 620 310 Pass/<LOD
Ethylene oxide 50 50 Pass/<LOD Heptane 5,000 50 Pass/<LOD
Hexane 290 290 Pass/<LOD Isopropyl acetate 5,000 50 Pass/<LOD
Methanol 3,000 500 Pass/<LOD Naptha 400 100 Not Tested
N,N-Dimethylacetamide 1,090 100 Pass/<LOD N,N-Dimethylformamide (DMF) 880 500 Pass/<LOD
Pentane 5,000 50 Pass/<LOD Petroleum Ether 400 100 Not Tested
Propane 5,000 100 Pass/<LOD Pyridine 200 10 Pass/<LOD
Sulfolane 160 200 Pass/<LOD Tetrahydrofuran (THF) 720 200 Pass/<LOD
Toluene 890 50 Pass/<LOD Trichloroethylene 25 5 Not Tested
Xylenes* 2,170 50 Pass/<LOD

Total Butanes = 544 ug/g (PASS); Total Pentanes = 317 ug/g (PASS); Total Hexanes = 0 ug/g (PASS)

* Xylenes are reported as the sum of o-xylene, m-xylene, p-xylene, and ethylbenzene
MRL - Maximum Residue Limit; LOD - Limit of Detection

This sample has not been tested according to OAR 333-007. These results should therefore be used for research and development or quality control purposes only.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 7 of 12

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents QC Report
Testing Accreditation #: 4092-005 Test Certificate #: 134752-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Elephant Ears
License: 030-1009646F7F8
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A4010300003A37000001267
Metrc Source Pkg#: 1A401030002C949000002705
Test Conditions

Prepsheet ID#: MIHS211229a
Scale: XS205-OR1
Temp: 21.2 °C
Baro PE: 976.3 hPa
Analyst: HRM
Technician: MEH
Sample ID#: 134752

Lot #: Elephant Ears #1 12.12.2021
Batch #: 134752
Batch Weight (g): 468.7
Harvest/Process Date: 12/12/2021
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 12/23/2021
Test Date: 12/22/2021
Sample #134752
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS Recovery (%) MSD Recovery (%) Relative Percent Difference (%) QC Flag
1,2-Dichloroethane N.D. 250 208 200 83.20 80.00 3.92
n-Propane N.D. 250 96 107 38.40 42.80 10.84 LRLR
Isobutane N.D. 250 118 126 47.20 50.40 6.56 LRLR
Methanol N.D. 250 181 179 72.40 71.60 1.11
n-Butane N.D. 250 259 271 103.60 108.40 4.53
2,2-Dimethylpropane N.D. 250 181 190 72.40 76.00 4.85
Ethanol N.D. 250 186 193 74.40 77.20 3.69
Isopentane N.D. 250 228 235 91.20 94.00 3.02
Acetonitrile N.D. 250 185 182 74.00 72.80 1.63
Diethyl ether N.D. 250 192 193 76.80 77.20 0.52
2-propanone N.D. 250 194 194 77.60 77.60 0.00
2-propanol N.D. 250 202 200 80.80 80.00 1.00
n-Pentane N.D. 250 182 206 72.80 82.40 12.37
2,2-Dimethylbutane N.D. 250 159 162 63.60 64.80 1.87 LRLR
2,3-Dimethylbutane N.D. 250 180 177 72.00 70.80 1.68
Methylene chloride N.D. 250 189 189 75.60 75.60 0.00
2-Methylpentane N.D. 250 179 170 71.60 68.00 5.16 LR
3-Methylpentane N.D. 250 199 177 79.60 70.80 11.70
2-Butanol N.D. 0 0 0 0.00 0.00 0.00
n-Hexane N.D. 250 179 182 71.60 72.80 1.66
Ethyl acetate N.D. 250 188 188 75.20 75.20 0.00
Tetrahydrofuran N.D. 0 0 0 0.00 0.00 0.00
Trichloroethylene N.D. 250 216 206 86.40 82.40 4.74
Isopropyl acetate N.D. 0 0 0 0.00 0.00 0.00
Benzene N.D. 250 198 191 79.20 76.40 3.60
Chloroform N.D. 250 205 206 82.00 82.40 0.49
Cyclohexane N.D. 0 0 0 0.00 0.00 0.00
Ethylene glycol N.D. 0 0 0 0.00 0.00 0.00
Heptane N.D. 250 198 194 79.20 77.60 2.04
2-Ethoxyethanol N.D. 0 0 0 0.00 0.00 0.00
1,4-Dioxane N.D. 0 0 0 0.00 0.00 0.00
Pyridine N.D. 0 0 0 0.00 0.00 0.00
Toluene N.D. 250 210 209 84.00 83.60 0.48
Chlorobenzene N.D. 0 0 0 0.00 0.00 0.00
Ethylbenzene N.D. 0 0 0 0.00 0.00 0.00
m-Xylene/p-Xylene N.D. 500 454 437 90.80 87.40 3.82
o-Xylene N.D. 250 238 224 95.20 89.60 6.06
Cumene N.D. 0 0 0 0.00 0.00 0.00
Ethylene oxide N.D. 250 178 190 71.20 76.00 6.52

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

N.D. = Not Detected

This sample has not been tested according to OAR 333-007. These results should therefore be used for research and development or quality control purposes only.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 8 of 12

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-005 Test Certificate #: 134752-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Elephant Ears
License: 030-1009646F7F8
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A4010300003A37000001267
Metrc Source Pkg#: 1A401030002C949000002705
Test Conditions

Prepsheet ID#: MIHS211229a
Scale: XS205-OR1
Temp: 21.2 °C
Baro PE: 976.3 hPa
Analyst: HRM
Technician: MEH
Sample ID#: 134752

Lot #: Elephant Ears #1 12.12.2021
Batch #: 134752
Batch Weight (g): 468.7
Harvest/Process Date: 12/12/2021
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 12/23/2021
Test Date: 12/22/2021
Sample #134752
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
1,2-Dichloroethane 2 1 Not Tested 1,2-Dimethoxyethane 100 5 Pass/<LOD
1,4-dioxane 380 200 Pass/<LOD 1-Butanol 5,000 100 Pass/<LOD
1-Pentanol 5,000 100 Pass/<LOD 1-Propanol 5,000 100 Pass/<LOD
2,2-Dimethylpropane (Neopentane) 5,000 100 Pass/<LOD 2,2-Dimethylbutane (Hexanes) 290 100 Pass/<LOD
2,3-Dimethylbutane (Hexanes) 290 100 Pass/<LOD 2-Butanol 5,000 100 Pass/<LOD
2-Butanone (MEK) 5,000 50 Pass/<LOD 2-Ethoxyethanol 160 40 Pass/<LOD
2-Methylbutane (Isopentane) 5,000 50 Pass/390 2-Methylpentane (Hexanes) 290 50 Pass/<LOD
2-Methylpropane (Isobutane) 5,000 100 Pass/<LOD 2-propanol (Isopropyl Alcohol) 5,000 50 Pass/<LOD
2-Propanone (Acetone) 5,000 50 Pass/<LOD 3-Methylpentane (Hexanes) 290 50 Pass/<LOD
Acetonitrile 410 100 Pass/<LOD Benzene 2 1 Pass/<LOD
Butane 5,000 100 Pass/<LOD Chloroform 2 1 Pass/<LOD
Cumene 70 50 Pass/<LOD Cyclohexane 3,880 1,000 Pass/<LOD
Dichloromethane 600 50 Pass/<LOD Dimethylsulfoxide (DMSO) 5,000 500 Pass/<LOD
Ethanol 5,000 500 Pass/<LOD Ethyl acetate 5,000 50 Pass/<LOD
Ethyl ether 5,000 500 Pass/<LOD Ethylene glycol 620 310 Pass/<LOD
Ethylene oxide 50 50 Pass/<LOD Heptane 5,000 50 Pass/<LOD
Hexane 290 290 Pass/<LOD Isopropyl acetate 5,000 50 Pass/<LOD
Methanol 3,000 500 Pass/<LOD Naptha 400 100 Not Tested
N,N-Dimethylacetamide 1,090 100 Pass/<LOD N,N-Dimethylformamide (DMF) 880 500 Pass/<LOD
Pentane 5,000 50 Pass/<LOD Petroleum Ether 400 100 Not Tested
Propane 5,000 100 Pass/<LOD Pyridine 200 10 Pass/<LOD
Sulfolane 160 200 Pass/<LOD Tetrahydrofuran (THF) 720 200 Pass/<LOD
Toluene 890 50 Pass/<LOD Trichloroethylene 25 5 Not Tested
Xylenes* 2,170 50 Pass/<LOD

Total Butanes = 72 ug/g (PASS); Total Pentanes = 390 ug/g (PASS); Total Hexanes = 0 ug/g (PASS)

* Xylenes are reported as the sum of o-xylene, m-xylene, p-xylene, and ethylbenzene
MRL - Maximum Residue Limit; LOD - Limit of Detection

This sample has not been tested according to OAR 333-007. These results should therefore be used for research and development or quality control purposes only.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 9 of 12

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents QC Report
Testing Accreditation #: 4092-005 Test Certificate #: 134752-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Elephant Ears
License: 030-1009646F7F8
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A4010300003A37000001267
Metrc Source Pkg#: 1A401030002C949000002705
Test Conditions

Prepsheet ID#: MIHS211229a
Scale: XS205-OR1
Temp: 21.2 °C
Baro PE: 976.3 hPa
Analyst: HRM
Technician: MEH
Sample ID#: 134752

Lot #: Elephant Ears #1 12.12.2021
Batch #: 134752
Batch Weight (g): 468.7
Harvest/Process Date: 12/12/2021
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 12/23/2021
Test Date: 12/22/2021
Sample #134752
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS Recovery (%) MSD Recovery (%) Relative Percent Difference (%) QC Flag
1,2-Dichloroethane N.D. 250 208 200 83.20 80.00 3.92
n-Propane N.D. 250 96 107 38.40 42.80 10.84 LRLR
Isobutane N.D. 250 118 126 47.20 50.40 6.56 LRLR
Methanol N.D. 250 181 179 72.40 71.60 1.11
n-Butane N.D. 250 259 271 103.60 108.40 4.53
2,2-Dimethylpropane N.D. 250 181 190 72.40 76.00 4.85
Ethanol N.D. 250 186 193 74.40 77.20 3.69
Isopentane N.D. 250 228 235 91.20 94.00 3.02
Acetonitrile N.D. 250 185 182 74.00 72.80 1.63
Diethyl ether N.D. 250 192 193 76.80 77.20 0.52
2-propanone N.D. 250 194 194 77.60 77.60 0.00
2-propanol N.D. 250 202 200 80.80 80.00 1.00
n-Pentane N.D. 250 182 206 72.80 82.40 12.37
2,2-Dimethylbutane N.D. 250 159 162 63.60 64.80 1.87 LRLR
2,3-Dimethylbutane N.D. 250 180 177 72.00 70.80 1.68
Methylene chloride N.D. 250 189 189 75.60 75.60 0.00
2-Methylpentane N.D. 250 179 170 71.60 68.00 5.16 LR
3-Methylpentane N.D. 250 199 177 79.60 70.80 11.70
2-Butanol N.D. 0 0 0 0.00 0.00 0.00
n-Hexane N.D. 250 179 182 71.60 72.80 1.66
Ethyl acetate N.D. 250 188 188 75.20 75.20 0.00
Tetrahydrofuran N.D. 0 0 0 0.00 0.00 0.00
Trichloroethylene N.D. 250 216 206 86.40 82.40 4.74
Isopropyl acetate N.D. 0 0 0 0.00 0.00 0.00
Benzene N.D. 250 198 191 79.20 76.40 3.60
Chloroform N.D. 250 205 206 82.00 82.40 0.49
Cyclohexane N.D. 0 0 0 0.00 0.00 0.00
Ethylene glycol N.D. 0 0 0 0.00 0.00 0.00
Heptane N.D. 250 198 194 79.20 77.60 2.04
2-Ethoxyethanol N.D. 0 0 0 0.00 0.00 0.00
1,4-Dioxane N.D. 0 0 0 0.00 0.00 0.00
Pyridine N.D. 0 0 0 0.00 0.00 0.00
Toluene N.D. 250 210 209 84.00 83.60 0.48
Chlorobenzene N.D. 0 0 0 0.00 0.00 0.00
Ethylbenzene N.D. 0 0 0 0.00 0.00 0.00
m-Xylene/p-Xylene N.D. 500 454 437 90.80 87.40 3.82
o-Xylene N.D. 250 238 224 95.20 89.60 6.06
Cumene N.D. 0 0 0 0.00 0.00 0.00
Ethylene oxide N.D. 250 178 190 71.20 76.00 6.52

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

N.D. = Not Detected

This sample has not been tested according to OAR 333-007. These results should therefore be used for research and development or quality control purposes only.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 10 of 12

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Homogeneity Report by
High Performance Liquid Chromatography
Testing Accreditation #: 4092-005 Test Certificate #: 134752-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Elephant Ears
License: 030-1009646F7F8
Type: AU Tincture
Metrc Test Pkg#: 1A4010300003A37000001267
Metrc Source Pkg#: 1A401030002C949000002705
Sample ID#: 134752

Lot #: Elephant Ears #1 12.12.2021
Batch #: 134752
Batch Weight (g): 468.7
Harvest/Process Date: 12/12/2021
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 12/23/2021
Sample #134752
Increments Tested (mg/g) TOTAL THC TOTAL CBD THC THCA THCV CBD CBC CBDA CBDV CBG CBN
Increment 1 655.80 6.51 101.55 631.98 N.D. N.D. N.D. 7.42 N.D. 2.53 N.D.
Increment 2 664.11 5.67 130.68 608.24 N.D. N.D. 2.48 6.46 N.D. 3.50 N.D.
Average Value 659.95 6.09 116.12 620.11 N.D. N.D. 1.24 6.94 N.D. 3.02 N.D.
Max Value 664.11 6.51 130.68 631.98 N.D. N.D. 2.48 7.42 N.D. 3.50 N.D.
Min Value 655.80 5.67 101.55 608.24 N.D. N.D. N.D. 6.46 N.D. 2.53 N.D.
Relative Percent Difference (RPD) ±1.26 ±13.83 ±25.09 ±3.83 N.D. N.D. ±200.00 ±13.83 N.D. ±32.17 N.D.
Average Cannabinoids Per Package 659.95 6.09 116.12 620.11 N.D. N.D. 1.24 6.94 N.D. 3.02 N.D.
Average Cannabinoids Per Serving 33.00 0.30 5.81 31.01 N.D. N.D. 0.06 0.35 N.D. 0.15 N.D.
Max Concentration Per Serving (THC)   Not Applicable
Max Concentration Per Package (THC)   Pass
Relative Percent Difference (RPD)   Pass
Control Study   Yes, MJ1957
Field Duplicate   Pass

N.D. = Not Detected, Min = Minimum, Max = Maximum

RPD is the relative percent difference between increment 1 and increment 2.

RSD is the relative standard deviation between all increments tested.

Total THC and CBD is the calculated sum of CBD or THC and the amount of CBD or THC derived from CBDA or THCA, respectively. These values are calculated by adding a molar correction factor of 0.877 to the CBDA or THCA value.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Terry Rabinowitz Iron laboratories Terry Rabinowitz

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 11 of 12
IRON Laboratories

Terpene Report by
Mass Spectrometer
Test Certificate #: 134752-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Elephant Ears
License: 030-1009646F7F8
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A4010300003A37000001267
Metrc Source Pkg#: 1A401030002C949000002705

Test Conditions

Scale: XS205-OR1
Temp: 21.2 °C
Baro Pressure: 989.4 hPa
Analyst: HRM
Technician: JBS

Sample ID#: 134752

Lot #: Elephant Ears #1 12.12.2021
Batch #: 134752
Batch Weight (g): 468.7
Harvest/Process Date: 12/12/2021
Serving Size (g): 0.05
Date Received: 12/23/2021

Sample #134752
Sample #134752
  • α-Pinene (0.22%)
  • β-Ocimene (0.00%)
  • Camphene (0.06%)
  • Eucalyptol (1,8-Cineol) (0.00%)
  • Sabinene (0.00%)
  • γ-Terpinene (0.04%)
  • Myrcene (1.14%)
  • α-Terpinolene (0.14%)
  • β-Pinene (0.56%)
  • Linalool (0.63%)
  • ∆3-Carene (0.00%)
  • Fenchone (0.00%)
  • α-Terpinene (0.07%)
  • endo-Fenchol (0.35%)
  • α-Ocimene (0.00%)
  • Isopulegol (0.00%)
  • Limonene (0.82%)
  • Geraniol (0.00%)
  • p-Cymene (0.00%)
  • β-Caryophyllene (0.06%)
  • α-Humulene (3.76%)
  • Nerolidol 1 (cis) (0.00%)
  • Nerolidol 2 (trans) (0.10%)
  • Guaiol (0.00%)
  • Caryophyllene Oxide (0.09%)
  • α-Bisabolol (0.42%)
  • α-Phellandrene (0.20%)
  • α-Terpineol (0.00%)
  • Valenence (0.89%)

Total: 9.550%

Predominant Terpenes

3.76%   α-Humulene Woody, oceanic-watery, spicy clove 1.14%   Myrcene Peppery, spicy balsam
0.89%   Valenence Sweet, citrus, grapefruit, woody, orange 0.82%   Limonene Citrus, orange, sweet
0.63%   Linalool Citrus, floral, sweet, bois de rose, woody, green, blueberry 0.56%   β-Pinene Woody, fresh pine, hay

Value in parenthesis indicates percentage of terpene present in the total sample (weight percentage, wt/wt%).
Value in doughnut slice indicates individual terpene abundance with respect to the total terpenes detected.

This sample has not been tested according to OAR 333-007. These results should therefore be used for research and development or quality control purposes only.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Himashi Mead Iron laboratories Himashi Mead

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 12 of 12