ORELAP NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Marijuana Potency Analysis by
High Performance Liquid Chromatography

Testing Accreditation #: 4092-005

Test Certificate #: 134746-001

Client Name, Sample Details
Hash Hamilton Extracts Salem, OR 97301 Sample: Garlic Puff Live Rosin License: 030-1009646F7F8 Type: Tincture Method: FE04U HPLC-UV Metrc Test Pkg#: 1A4010300003A37000001261 Metrc Source Pkg#: 1A401030002C949000002563

Test Conditions
Prepsheet ID#: ORP211216a Scale: XS205-OR1 Temp: 22.3 °C Baro Pressure: 1004 hPa Analyst: TMR Technician: TMR

Sample ID#: 134746
Lot #: Garlic Puff 10-26-21 Batch #: 134746 Batch Weight (g): 200.9 Harvest/Process Date: 11/12/2021 Serving Size (g): 0.05 Package Weight (g):1 Date Received: 12/23/2021 Test Date: 12/16/2021

Test Compounds	THC	THCA	CBD	CBDA	CBN	CBG	CBC	THCV*	CBDV	Total Cannabinoids*	Total THC	Total CBD	Calc Max Total Cannabinoids*
Amount (%)	1.21	78.68	N/D	10.05	N/D	0.20	N/D	N/D	N/D	90.13	70.21	8.81	79.22
Amount (mg/g)	12.05	786.77	N/D	100.47	N/D	2.04	N/D	N/D	N/D	901.33	702.05	88.11	792.20
Amount per Serving (mg)	0.60	39.34	N\D	5.02	N\D	0.10	N\D	N\D	N\D	45.07	Serving Size~ (g):		0.05
LOQ (mg/g)	2	2	2	2	2	2	2	2	2		%Decarb.	THC	CBD
±%RPD	5.24	5.50	0.95	6.53	2.51	+/-5%	3.15	1.35	0.49		%Decarb.	2	0

LOQ = Limit of Quantitation; %RPD = Relative Percent Deviation; %RSD = Relative Standard Deviation; N/D = Not Detected

*Designates values that are not currently included in the accredited scope of Iron Laboratories.

*** Designates tests that use the method FE-45. FE-45 is performed using AOAC 966.02 and 32.004-32.009. FE-45 has relative expanded (k=2) uncertainties of 1.098% for moisture, 1.754% for water activity for unprocessed plant materials, and 13.102% for water activity for infused products. Vitamin E acetate analysis has a relative expanded (k=2) uncertainty of 18.614%.

Total THC and CBD is the calculated sum of THC or CBD and the amount of THC or CBD derived from THCA or CBDA, respectively. These values are calculated by applying a molar correction factor of 0.877 to the THCA or the CBDA value. Calc Max Total Cannabinoids is the sum of Total THC, Total CBD, CBN, CBG, CBC, THCV, and CBDV.

%Decarb. THC and CBD refer to the percentage of THC or CBD relative to THCA or CBDA, respectively.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.
This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.
Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401
Page 1 of 8

ORELAP NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant QC Report

Testing Accreditation #: 4092-005

Test Certificate #: 134746-001

Client Name, Sample Details
Hash Hamilton Extracts Salem, OR 97301 Sample: Garlic Puff Live Rosin License: 030-1009646F7F8 Type: Tincture Method: FE04U HPLC-UV Metrc Test Pkg#: 1A4010300003A37000001261 Metrc Source Pkg#: 1A401030002C949000002563

Test Conditions
Prepsheet ID#: ORP211216a Scale: XS205-OR1 Temp: 22.3 °C Baro Pressure: 1004 hPa Analyst: TMR Technician: TMR

Sample ID#: 134746
Lot #: Garlic Puff 10-26-21 Batch #: 134746 Batch Weight (g): 200.9 Harvest/Process Date: 11/12/2021 Serving Size (g): 0.05 Package Weight (g):1 Date Received: 12/23/2021 Test Date: 12/16/2021

Target Compound Name	Method Blank (μg/g)	LCS Spike (μg/g)	LCS Amount (μg/g)	Percent Recovery (%) LCS	LCS Duplicate Amount (μg/g)	Percent Recovery (%) LCSD	Relative Percent Difference (%)
Cannabidivarin (CBDV)	N.D.	4.07	4.05	99.51	4.07	100.00	0.49
Cannabidiolic Acid (CBDA)	N.D.	3.32	3.11	93.67	3.32	100.00	6.53
Cannabigerol (CBG)	N.D.	4.54	4.5	99.12	4.5	99.12	0.00
Cannabidiol (CBD)	N.D.	4.24	4.18	98.58	4.22	99.53	0.95
Δ9-Tetrahydrocannabivarin (THCV)	N.D.	4.5	4.43	98.44	4.49	99.78	1.35
Cannabinol (CBN)	N.D.	4.8	4.73	98.54	4.85	101.04	2.51
Δ9-Tetrahydrocannabinol (THC)	N.D.	4.81	4.65	96.67	4.9	101.87	5.24
Cannabichromene (CBC)	N.D.	4.48	4.37	97.54	4.51	100.67	3.15
Tetrahydrocannabinolic acid (THCA)	N.D.	4.1	3.71	90.49	3.92	95.61	5.50

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.
This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.
Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401
Page 2 of 8

ORELAP NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Marijuana Potency Analysis by
High Performance Liquid Chromatography

Testing Accreditation #: 4092-005

Test Certificate #: 134746-001

Client Name, Sample Details
Hash Hamilton Extracts Salem, OR 97301 Sample: Garlic Puff Live Rosin License: 030-1009646F7F8 Type: Tincture Method: FE04U HPLC-UV Metrc Test Pkg#: 1A4010300003A37000001261 Metrc Source Pkg#: 1A401030002C949000002563

Test Conditions
Prepsheet ID#: ORP211216a Scale: XS205-OR1 Temp: 22.3 °C Baro Pressure: 1004 hPa Analyst: TMR Technician: TMR

Sample ID#: 134746
Lot #: Garlic Puff 10-26-21 Batch #: 134746 Batch Weight (g): 200.9 Harvest/Process Date: 11/12/2021 Serving Size (g): 0.05 Package Weight (g):1 Date Received: 12/23/2021 Test Date: 12/16/2021

Test Compounds	THC	THCA	CBD	CBDA	CBN	CBG	CBC	THCV*	CBDV	Total Cannabinoids*	Total THC	Total CBD	Calc Max Total Cannabinoids*
Amount (%)	1.26	79.76	N/D	10.21	N/D	0.23	N/D	N/D	N/D	91.45	71.20	8.96	80.39
Amount (mg/g)	12.56	797.57	N/D	102.14	N/D	2.25	N/D	N/D	N/D	914.52	712.03	89.58	803.86
Amount per Serving (mg)	0.63	39.88	N\D	5.11	N\D	0.11	N\D	N\D	N\D	45.73	Serving Size~ (g):		0.05
LOQ (mg/g)	1.9	1.9	1.9	1.9	1.9	1.9	1.9	1.9	1.9		%Decarb.	THC	CBD
±%RPD	5.24	5.50	0.95	6.53	2.51	+/-5%	3.15	1.35	0.49		%Decarb.	0	0

LOQ = Limit of Quantitation; %RPD = Relative Percent Deviation; %RSD = Relative Standard Deviation; N/D = Not Detected

*Designates values that are not currently included in the accredited scope of Iron Laboratories.

%Decarb. THC and CBD refer to the percentage of THC or CBD relative to THCA or CBDA, respectively.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.
This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.
Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401
Page 2 of 8

ORELAP NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant QC Report

Testing Accreditation #: 4092-005

Test Certificate #: 134746-001

Client Name, Sample Details
Hash Hamilton Extracts Salem, OR 97301 Sample: Garlic Puff Live Rosin License: 030-1009646F7F8 Type: Tincture Method: FE04U HPLC-UV Metrc Test Pkg#: 1A4010300003A37000001261 Metrc Source Pkg#: 1A401030002C949000002563

Test Conditions
Prepsheet ID#: ORP211216a Scale: XS205-OR1 Temp: 22.3 °C Baro Pressure: 1004 hPa Analyst: TMR Technician: TMR

Sample ID#: 134746
Lot #: Garlic Puff 10-26-21 Batch #: 134746 Batch Weight (g): 200.9 Harvest/Process Date: 11/12/2021 Serving Size (g): 0.05 Package Weight (g):1 Date Received: 12/23/2021 Test Date: 12/16/2021

Target Compound Name	Method Blank (μg/g)	LCS Spike (μg/g)	LCS Amount (μg/g)	Percent Recovery (%) LCS	LCS Duplicate Amount (μg/g)	Percent Recovery (%) LCSD	Relative Percent Difference (%)
Cannabidivarin (CBDV)	N.D.	4.07	4.05	99.51	4.07	100.00	0.49
Cannabidiolic Acid (CBDA)	N.D.	3.32	3.11	93.67	3.32	100.00	6.53
Cannabigerol (CBG)	N.D.	4.54	4.5	99.12	4.5	99.12	0.00
Cannabidiol (CBD)	N.D.	4.24	4.18	98.58	4.22	99.53	0.95
Δ9-Tetrahydrocannabivarin (THCV)	N.D.	4.5	4.43	98.44	4.49	99.78	1.35
Cannabinol (CBN)	N.D.	4.8	4.73	98.54	4.85	101.04	2.51
Δ9-Tetrahydrocannabinol (THC)	N.D.	4.81	4.65	96.67	4.9	101.87	5.24
Cannabichromene (CBC)	N.D.	4.48	4.37	97.54	4.51	100.67	3.15
Tetrahydrocannabinolic acid (THCA)	N.D.	4.1	3.71	90.49	3.92	95.61	5.50

N.D. = Not Detected

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.
This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.
Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401
Page 3 of 8

ORELAP NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Pesticide Analysis by
Mass Spectrometer

Testing Accreditation #: 4092-005

Test Certificate #: 134746-001

Client Name, Sample Details
Hash Hamilton Extracts Salem, OR 97301 Sample: Garlic Puff Live Rosin License: 030-1009646F7F8 Type: Tincture Method: FE-52 (EN 15662 & AOAC 2007.01) Metrc Test Pkg#: 1A4010300003A37000001261 Metrc Source Pkg#: 1A401030002C949000002563

Test Conditions
Prepsheet ID#: ORPS211222a Scale: XS205-OR1 Temp: 22.7 °C Baro PE: 992.2 hPa Analyst: HRM Technician: JBS

Sample ID#: 134746
Lot #: Garlic Puff 10-26-21 Batch #: 134746 Batch Weight (g): 200.9 Harvest/Process Date: 11/12/2021 Serving Size (g): 0.05 Package Weight (g):1 Date Received: 12/23/2021 Test Date: 12/22/2021

Compound	MRL (µg/g)	LOD (µg/g)	Status (µg/g)	Compound	MRL (µg/g)	LOD (µg/g)	Status (µg/g)
Aldicarb	0.400	0.122	Pass/<LOD	Abamectin****	0.500	0.122	Pass/<LOD
Acephate	0.400	0.122	Pass/<LOD	Acequinocyl	2.000	0.245	Pass/<LOD
Acetamiprid	0.200	0.122	Pass/<LOD	Azoxystrobin	0.200	0.122	Pass/<LOD
Bifenazate	0.200	0.122	Pass/<LOD	Bifenthrin	0.200	0.122	Pass/<LOD
Boscalid	0.400	0.122	Pass/<LOD	Carbaryl	0.200	0.122	Pass/<LOD
Carbofuran	0.200	0.122	Pass/<LOD	Chlorantraniliprole	0.200	0.122	Pass/<LOD
Chlorfenapyr	1.000	0.489	Pass/<LOD	Chlorpyrifos	0.200	0.122	Pass/<LOD
Clofentezine	0.200	0.122	Pass/<LOD	Cyfluthrin**	1.000	0.489	Pass/<LOD
Cypermethrin***	1.000	0.489	Pass/<LOD	Daminozide	1.000	0.122	Pass/<LOD
DDVP (Dichlorvos)	1.000	0.245	Pass/<LOD	Diazinon	0.200	0.122	Pass/<LOD
Dimethoate	0.200	0.122	Pass/<LOD	Ethoprophos	0.200	0.122	Pass/<LOD
Etofenprox	0.400	0.122	Pass/<LOD	Etoxazole	0.200	0.122	Pass/<LOD
Fenoxycarb	0.200	0.122	Pass/<LOD	Fenpyroximate	0.400	0.122	Pass/<LOD
Fipronil	0.400	0.122	Pass/<LOD	Flonicamid	1.000	0.122	Pass/<LOD
Fludioxonil	0.400	0.122	Pass/<LOD	Hexythiazox	1.000	0.122	Pass/<LOD
Imazalil	0.200	0.122	Pass/<LOD	Imidacloprid	0.400	0.122	Pass/<LOD
Kresoxim Methyl	0.400	0.122	Pass/<LOD	Malathion	0.200	0.122	Pass/<LOD
Metalaxyl	0.200	0.122	Pass/<LOD	Methiocarb	0.200	0.122	Pass/<LOD
Methomyl	0.400	0.122	Pass/<LOD	Methyl Parathion	0.200	0.122	Pass/<LOD
MGK-264‡	0.200	0.122	Pass/<LOD	Myclobutanil	0.000	0.122	Pass/<LOD
Naled	0.500	0.122	Pass/<LOD	Oxamyl	1.000	0.122	Pass/<LOD
Paclobutrazol	0.400	0.122	Pass/<LOD	Permethrins†	0.200	0.122	Pass/<LOD
Phosmet	0.200	0.122	Pass/<LOD	Piperonyl Butoxide	2.000	0.122	Pass/<LOD
Prallethrin	0.200	0.122	Pass/<LOD	Propiconazole	0.400	0.122	Pass/<LOD
Propoxur	0.200	0.122	Pass/<LOD	Pyrethrins*	1.000	0.122	Pass/<LOD
Pyridaben	0.200	0.122	Pass/<LOD	Spinosad*****	0.200	0.122	Pass/<LOD
Spiromesifen	0.200	0.122	Pass/<LOD	Spirotetramat	0.200	0.122	Pass/<LOD
Spiroxamine‡	0.400	0.122	Pass/<LOD	Tebuconazole	0.400	0.122	Pass/<LOD
Thiacloprid	0.200	0.122	Pass/<LOD	Thiamethoxam	0.200	0.122	Pass/<LOD
Trifloxystrobin	0.200	0.122	Pass/<LOD

* Pyrethrins are reported as the sum of Jasmolin I, Cinerin I, and Pyrethrin I
** Cyfluthrins are reported as the sum of isomers Cyfluthrin I, II, III, and IV
*** Cypermethrins are reported as the sum of isomers Cypermethrin I, II, III, and IV
**** Abamectin is reported as the sum of Avermectin B1a and Avermectin B1b
***** Spinosad is reported as the sum of Spinosyn A and Spinosyn D
† Permethrin and Prallethrin are reported as the sum of cis and trans isomers
‡ MGK-264 and Spiroximine are reported as the sum of isomers I and II
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.
This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.
Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401
Page 3 of 8

ORELAP NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Pesticide QC Report

Testing Accreditation #: 4092-005

Test Certificate #: 134746-001

Client Name, Sample Details
Hash Hamilton Extracts Salem, OR 97301 Sample: Garlic Puff Live Rosin License: 030-1009646F7F8 Type: Tincture Method: FE-52 (EN 15662 & AOAC 2007.01) Metrc Test Pkg#: 1A4010300003A37000001261 Metrc Source Pkg#: 1A401030002C949000002563

Test Conditions
Prepsheet ID#: ORPS211222a Scale: XS205-OR1 Temp: 22.7 °C Baro PE: 992.2 hPa Analyst: HRM Technician: JBS

Sample ID#: 134746
Lot #: Garlic Puff 10-26-21 Batch #: 134746 Batch Weight (g): 200.9 Harvest/Process Date: 11/12/2021 Serving Size (g): 0.05 Package Weight (g):1 Date Received: 12/23/2021 Test Date: 12/22/2021

Target Compound Name	Method Blank (μg/g)	QC Spike (μg/g)	Matrix Spike (μg/g)	Matrix Spike Duplicate (μg/g)	MS recovery%	MSD recovery%	Relative Percent Difference (%)	QC Flag
Acephate	N.D.	1	1.46	1.25	146.00	125.00	15.50	HR
Acequinocyl	N.D.	1	0.889	1.06	88.90	106.00	17.55
Acetamiprid	N.D.	1	1.21	1.5	121.00	150.00	21.40	HRQ
Aldicarb	N.D.	1	0.904	1.19	90.40	119.00	27.32	Q
Avermectin B1a	N.D.	0.97	2.31	1.92	238.14	197.94	18.44	HR
Azoxystrobin	N.D.	1	1.51	1.32	151.00	132.00	13.43	HR
Bifenazate	N.D.	1	1.59	1.63	159.00	163.00	2.48	HR
Bifenthrin	N.D.	1	0.903	1.29	90.30	129.00	35.29	Q
Boscalid	N.D.	1	1.38	1.4	138.00	140.00	1.44	HR
Carbaryl	N.D.	1	1.07	1.52	107.00	152.00	34.75	HRQ
Carbofuran	N.D.	1	1.46	1.43	146.00	143.00	2.08	HR
Chlorantraniliprole	N.D.	1	2.2	1.72	220.00	172.00	24.49	HR Q
Chlorfenapyr	N.D.	1	0.766	1.05	76.60	105.00	31.28	Q
Chlorpyriphos	N.D.	1	1.25	1.39	125.00	139.00	10.61	HR
Clofentezine	N.D.	1	1.43	1.81	143.00	181.00	23.46	HR Q
Cyfluthrin	N.D.	1	0.955	1.16	95.50	116.00	19.39
Cypermethrin	N.D.	1	1.09	1.19	109.00	119.00	8.77
Daminoside	N.D.	1	2.2	10.5	220.00	1,050.00	130.71	HR Q
Diazanon	N.D.	1	32.6	29.7	3,260.00	2,970.00	9.31	HR
Dichlorvos	N.D.	1	1.77	1.65	177.00	165.00	7.02	HR
Dimethoate	N.D.	1	1.33	1.32	133.00	132.00	0.75	HR
Ethoprophos	N.D.	1	1.46	1.51	146.00	151.00	3.37	HR
Etofenprox	N.D.	1	1.1	1.08	110.00	108.00	1.83
Etoxazole	N.D.	1	1.76	1.8	176.00	180.00	2.25	HR
Fenoxycarb	N.D.	1	1.86	1.92	186.00	192.00	3.17	HR
Fenpyroximate	N.D.	1	1.62	1.91	162.00	191.00	16.43	HR
Fipronil	N.D.	1	1.2	0.878	120.00	87.80	30.99	Q
Flonicamid	N.D.	1	0.99	1.52	99.00	152.00	42.23	HRQ
Fludioxonil	N.D.	1	1.17	0.89	117.00	89.00	27.18	Q
Hexythiazox	N.D.	1	1.04	1.18	104.00	118.00	12.61
Imazalil	N.D.	1	2.71	2.36	271.00	236.00	13.81	HR
Imidacloprid	N.D.	1	1.54	1.81	154.00	181.00	16.12	HR
Kresoxim-methyl	N.D.	1	1.72	2	172.00	200.00	15.05	HR
Malathion	N.D.	1	1.48	1.37	148.00	137.00	7.72	HR
Metalaxyl	N.D.	1	1.82	1.89	182.00	189.00	3.77	HR
Methiocarb	N.D.	1	1.36	1.1	136.00	110.00	21.14	HR Q
Methomyl	N.D.	1	1.25	1.59	125.00	159.00	23.94	HRQ
MGK-264	N.D.	1	1.1	1.33	110.00	133.00	18.93	HR
Myclobutanil	N.D.	1	2.13	1.9	213.00	190.00	11.41	HR
Naled (dibrom)	N.D.	1	0.819	0.706	81.90	70.60	14.82
Oxamyl	N.D.	1	1.35	0.917	135.00	91.70	38.20	HR Q
Paclobutrazol	N.D.	1	2.65	2.69	265.00	269.00	1.50	HR
Parathion-methyl	N.D.	1	1.06	0.975	106.00	97.50	8.35
Permethrins	N.D.	1	1.129	1.226	112.90	122.60	8.24
Phosmet	N.D.	1	1.78	1.86	178.00	186.00	4.40	HR
Piperonyl butoxide	N.D.	1	1.16	1.21	116.00	121.00	4.22
Prallethrin	N.D.	1	1.85	1.9	185.00	190.00	2.67	HR
Propiconazole	N.D.	1	1.99	1.95	199.00	195.00	2.03	HR
Propoxur	N.D.	1	1.07	1.29	107.00	129.00	18.64
Pyrethrin	N.D.	0.65	0.858	1.07	132.00	164.62	21.99	HR Q
Pyridaben	N.D.	1	1.32	1.4	132.00	140.00	5.88	HR
SpinosynA	N.D.	0.84	1.69	1.46	201.19	173.81	14.60	HR
SpinosynD	N.D.	0.16	0.283	0.294	176.88	183.75	3.81	HR
Spiromesifen	N.D.	1	0.925	0.992	92.50	99.20	6.99
Spirotetramat	N.D.	1	1.51	1.33	151.00	133.00	12.68	HR
Spiroxamine	N.D.	1	2.54	2.24	254.00	224.00	12.55	HR
Tebuconazole	N.D.	1	2.02	2.15	202.00	215.00	6.24	HR
Thiacloprid	N.D.	1	1.84	2.03	184.00	203.00	9.82	HR
Thiamethoxam	N.D.	1	1.59	1.85	159.00	185.00	15.12	HR
Trifloxystrobin	N.D.	1	1.25	1.27	125.00	127.00	1.59

N.D. = Not Detected

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 30%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (60-120%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.
This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.
Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401
Page 4 of 8

ORELAP NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Pesticide Analysis by
Mass Spectrometer

Testing Accreditation #: 4092-005

Test Certificate #: 134746-001

Client Name, Sample Details
Hash Hamilton Extracts Salem, OR 97301 Sample: Garlic Puff Live Rosin License: 030-1009646F7F8 Type: Tincture Method: FE-52 (EN 15662 & AOAC 2007.01) Metrc Test Pkg#: 1A4010300003A37000001261 Metrc Source Pkg#: 1A401030002C949000002563

Test Conditions
Prepsheet ID#: ORPS211222a Scale: XS205-OR1 Temp: 22.7 °C Baro PE: 992.2 hPa Analyst: HRM Technician: JBS

Sample ID#: 134746
Lot #: Garlic Puff 10-26-21 Batch #: 134746 Batch Weight (g): 200.9 Harvest/Process Date: 11/12/2021 Serving Size (g): 0.05 Package Weight (g):1 Date Received: 12/23/2021 Test Date: 12/22/2021

Compound	MRL (µg/g)	LOD (µg/g)	Status (µg/g)	Compound	MRL (µg/g)	LOD (µg/g)	Status (µg/g)
Aldicarb	0.400	0.117	Pass/<LOD	Abamectin****	0.500	0.117	Pass/<LOD
Acephate	0.400	0.117	Pass/<LOD	Acequinocyl	2.000	0.235	Pass/<LOD
Acetamiprid	0.200	0.117	Pass/<LOD	Azoxystrobin	0.200	0.117	Pass/<LOD
Bifenazate	0.200	0.117	Pass/<LOD	Bifenthrin	0.200	0.117	Pass/<LOD
Boscalid	0.400	0.117	Pass/<LOD	Carbaryl	0.200	0.117	Pass/<LOD
Carbofuran	0.200	0.117	Pass/<LOD	Chlorantraniliprole	0.200	0.117	Pass/<LOD
Chlorfenapyr	1.000	0.470	Pass/<LOD	Chlorpyrifos	0.200	0.117	Pass/<LOD
Clofentezine	0.200	0.117	Pass/<LOD	Cyfluthrin**	1.000	0.470	Pass/<LOD
Cypermethrin***	1.000	0.470	Pass/<LOD	Daminozide	1.000	0.117	Pass/<LOD
DDVP (Dichlorvos)	1.000	0.235	Pass/<LOD	Diazinon	0.200	0.117	Pass/<LOD
Dimethoate	0.200	0.117	Pass/<LOD	Ethoprophos	0.200	0.117	Pass/<LOD
Etofenprox	0.400	0.117	Pass/<LOD	Etoxazole	0.200	0.117	Pass/<LOD
Fenoxycarb	0.200	0.117	Pass/<LOD	Fenpyroximate	0.400	0.117	Pass/<LOD
Fipronil	0.400	0.117	Pass/<LOD	Flonicamid	1.000	0.117	Pass/<LOD
Fludioxonil	0.400	0.117	Pass/<LOD	Hexythiazox	1.000	0.117	Pass/<LOD
Imazalil	0.200	0.117	Pass/<LOD	Imidacloprid	0.400	0.117	Pass/<LOD
Kresoxim Methyl	0.400	0.117	Pass/<LOD	Malathion	0.200	0.117	Pass/<LOD
Metalaxyl	0.200	0.117	Pass/<LOD	Methiocarb	0.200	0.117	Pass/<LOD
Methomyl	0.400	0.117	Pass/<LOD	Methyl Parathion	0.200	0.117	Pass/<LOD
MGK-264‡	0.200	0.117	Pass/<LOD	Myclobutanil	0.000	0.117	Pass/<LOD
Naled	0.500	0.117	Pass/<LOD	Oxamyl	1.000	0.117	Pass/<LOD
Paclobutrazol	0.400	0.117	Pass/<LOD	Permethrins†	0.200	0.117	Pass/<LOD
Phosmet	0.200	0.117	Pass/<LOD	Piperonyl Butoxide	2.000	0.117	Pass/<LOD
Prallethrin	0.200	0.117	Pass/<LOD	Propiconazole	0.400	0.117	Pass/<LOD
Propoxur	0.200	0.117	Pass/<LOD	Pyrethrins*	1.000	0.117	Pass/<LOD
Pyridaben	0.200	0.117	Pass/<LOD	Spinosad*****	0.200	0.117	Pass/<LOD
Spiromesifen	0.200	0.117	Pass/<LOD	Spirotetramat	0.200	0.117	Pass/<LOD
Spiroxamine‡	0.400	0.117	Pass/<LOD	Tebuconazole	0.400	0.117	Pass/<LOD
Thiacloprid	0.200	0.117	Pass/<LOD	Thiamethoxam	0.200	0.117	Pass/<LOD
Trifloxystrobin	0.200	0.117	Pass/<LOD

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.
This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.
Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401
Page 5 of 8

ORELAP NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Pesticide QC Report

Testing Accreditation #: 4092-005

Test Certificate #: 134746-001

Client Name, Sample Details
Hash Hamilton Extracts Salem, OR 97301 Sample: Garlic Puff Live Rosin License: 030-1009646F7F8 Type: Tincture Method: FE-52 (EN 15662 & AOAC 2007.01) Metrc Test Pkg#: 1A4010300003A37000001261 Metrc Source Pkg#: 1A401030002C949000002563

Test Conditions
Prepsheet ID#: ORPS211222a Scale: XS205-OR1 Temp: 22.7 °C Baro PE: 992.2 hPa Analyst: HRM Technician: JBS

Sample ID#: 134746
Lot #: Garlic Puff 10-26-21 Batch #: 134746 Batch Weight (g): 200.9 Harvest/Process Date: 11/12/2021 Serving Size (g): 0.05 Package Weight (g):1 Date Received: 12/23/2021 Test Date: 12/22/2021

Target Compound Name	Method Blank (μg/g)	QC Spike (μg/g)	Matrix Spike (μg/g)	Matrix Spike Duplicate (μg/g)	MS recovery%	MSD recovery%	Relative Percent Difference (%)	QC Flag
Acephate	N.D.	1	1.46	1.25	146.00	125.00	15.50	HR
Acequinocyl	N.D.	1	0.889	1.06	88.90	106.00	17.55
Acetamiprid	N.D.	1	1.21	1.5	121.00	150.00	21.40	HRQ
Aldicarb	N.D.	1	0.904	1.19	90.40	119.00	27.32	Q
Avermectin B1a	N.D.	0.97	2.31	1.92	238.14	197.94	18.44	HR
Azoxystrobin	N.D.	1	1.51	1.32	151.00	132.00	13.43	HR
Bifenazate	N.D.	1	1.59	1.63	159.00	163.00	2.48	HR
Bifenthrin	N.D.	1	0.903	1.29	90.30	129.00	35.29	Q
Boscalid	N.D.	1	1.38	1.4	138.00	140.00	1.44	HR
Carbaryl	N.D.	1	1.07	1.52	107.00	152.00	34.75	HRQ
Carbofuran	N.D.	1	1.46	1.43	146.00	143.00	2.08	HR
Chlorantraniliprole	N.D.	1	2.2	1.72	220.00	172.00	24.49	HR Q
Chlorfenapyr	N.D.	1	0.766	1.05	76.60	105.00	31.28	Q
Chlorpyriphos	N.D.	1	1.25	1.39	125.00	139.00	10.61	HR
Clofentezine	N.D.	1	1.43	1.81	143.00	181.00	23.46	HR Q
Cyfluthrin	N.D.	1	0.955	1.16	95.50	116.00	19.39
Cypermethrin	N.D.	1	1.09	1.19	109.00	119.00	8.77
Daminoside	N.D.	1	2.2	10.5	220.00	1,050.00	130.71	HR Q
Diazanon	N.D.	1	32.6	29.7	3,260.00	2,970.00	9.31	HR
Dichlorvos	N.D.	1	1.77	1.65	177.00	165.00	7.02	HR
Dimethoate	N.D.	1	1.33	1.32	133.00	132.00	0.75	HR
Ethoprophos	N.D.	1	1.46	1.51	146.00	151.00	3.37	HR
Etofenprox	N.D.	1	1.1	1.08	110.00	108.00	1.83
Etoxazole	N.D.	1	1.76	1.8	176.00	180.00	2.25	HR
Fenoxycarb	N.D.	1	1.86	1.92	186.00	192.00	3.17	HR
Fenpyroximate	N.D.	1	1.62	1.91	162.00	191.00	16.43	HR
Fipronil	N.D.	1	1.2	0.878	120.00	87.80	30.99	Q
Flonicamid	N.D.	1	0.99	1.52	99.00	152.00	42.23	HRQ
Fludioxonil	N.D.	1	1.17	0.89	117.00	89.00	27.18	Q
Hexythiazox	N.D.	1	1.04	1.18	104.00	118.00	12.61
Imazalil	N.D.	1	2.71	2.36	271.00	236.00	13.81	HR
Imidacloprid	N.D.	1	1.54	1.81	154.00	181.00	16.12	HR
Kresoxim-methyl	N.D.	1	1.72	2	172.00	200.00	15.05	HR
Malathion	N.D.	1	1.48	1.37	148.00	137.00	7.72	HR
Metalaxyl	N.D.	1	1.82	1.89	182.00	189.00	3.77	HR
Methiocarb	N.D.	1	1.36	1.1	136.00	110.00	21.14	HR Q
Methomyl	N.D.	1	1.25	1.59	125.00	159.00	23.94	HRQ
MGK-264	N.D.	1	1.1	1.33	110.00	133.00	18.93	HR
Myclobutanil	N.D.	1	2.13	1.9	213.00	190.00	11.41	HR
Naled (dibrom)	N.D.	1	0.819	0.706	81.90	70.60	14.82
Oxamyl	N.D.	1	1.35	0.917	135.00	91.70	38.20	HR Q
Paclobutrazol	N.D.	1	2.65	2.69	265.00	269.00	1.50	HR
Parathion-methyl	N.D.	1	1.06	0.975	106.00	97.50	8.35
Permethrins	N.D.	1	1.129	1.226	112.90	122.60	8.24
Phosmet	N.D.	1	1.78	1.86	178.00	186.00	4.40	HR
Piperonyl butoxide	N.D.	1	1.16	1.21	116.00	121.00	4.22
Prallethrin	N.D.	1	1.85	1.9	185.00	190.00	2.67	HR
Propiconazole	N.D.	1	1.99	1.95	199.00	195.00	2.03	HR
Propoxur	N.D.	1	1.07	1.29	107.00	129.00	18.64
Pyrethrin	N.D.	0.65	0.858	1.07	132.00	164.62	21.99	HR Q
Pyridaben	N.D.	1	1.32	1.4	132.00	140.00	5.88	HR
SpinosynA	N.D.	0.84	1.69	1.46	201.19	173.81	14.60	HR
SpinosynD	N.D.	0.16	0.283	0.294	176.88	183.75	3.81	HR
Spiromesifen	N.D.	1	0.925	0.992	92.50	99.20	6.99
Spirotetramat	N.D.	1	1.51	1.33	151.00	133.00	12.68	HR
Spiroxamine	N.D.	1	2.54	2.24	254.00	224.00	12.55	HR
Tebuconazole	N.D.	1	2.02	2.15	202.00	215.00	6.24	HR
Thiacloprid	N.D.	1	1.84	2.03	184.00	203.00	9.82	HR
Thiamethoxam	N.D.	1	1.59	1.85	159.00	185.00	15.12	HR
Trifloxystrobin	N.D.	1	1.25	1.27	125.00	127.00	1.59

N.D. = Not Detected

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 30%

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.
This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.
Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401
Page 6 of 8

ORELAP NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Homogeneity Report by
High Performance Liquid Chromatography

Testing Accreditation #: 4092-005

Test Certificate #: 134746-001

Client Name, Sample Details
Hash Hamilton Extracts Salem, OR 97301 Sample: Garlic Puff Live Rosin License: 030-1009646F7F8 Type: Tincture Metrc Test Pkg#: 1A4010300003A37000001261 Metrc Source Pkg#: 1A401030002C949000002563

Sample ID#: 134746
Lot #: Garlic Puff 10-26-21 Batch #: 134746 Batch Weight (g): 200.9 Harvest/Process Date: 11/12/2021 Serving Size (g): 0.05 Package Weight (g):1 Date Received: 12/23/2021

Increments Tested (mg/g)	TOTAL THC	TOTAL CBD	THC	THCA	THCV	CBD	CBC	CBDA	CBDV	CBG	CBN
Increment 1	702.05	88.11	12.05	786.77	N.D.	N.D.	N.D.	100.47	N.D.	2.04	N.D.
Increment 2	712.03	89.58	12.56	797.57	N.D.	N.D.	N.D.	102.14	N.D.	2.25	N.D.
Average Value	707.04	88.84	12.31	792.17	N.D.	N.D.	N.D.	101.31	N.D.	2.15	N.D.
Max Value	712.03	89.58	12.56	797.57	N.D.	N.D.	N.D.	102.14	N.D.	2.25	N.D.
Min Value	702.05	88.11	12.05	786.77	N.D.	N.D.	N.D.	100.47	N.D.	2.04	N.D.
Relative Percent Difference (RPD)	±1.41	±1.65	±4.14	±1.36	N.D.	N.D.	N.D.	±1.65	N.D.	±9.79	N.D.
Average Cannabinoids Per Package	707.04	88.84	12.31	792.17	N.D.	N.D.	N.D.	101.31	N.D.	2.15	N.D.
Average Cannabinoids Per Serving	35.35	4.44	0.62	39.61	N.D.	N.D.	N.D.	5.07	N.D.	0.11	N.D.

Max Concentration Per Serving (THC)	Not Applicable
Max Concentration Per Package (THC)	Pass
Relative Percent Difference (RPD)	Pass
Control Study	Yes, MJ2136
Field Duplicate	Pass

N.D. = Not Detected, Min = Minimum, Max = Maximum

RPD is the relative percent difference between increment 1 and increment 2.

RSD is the relative standard deviation between all increments tested.

Total THC and CBD is the calculated sum of CBD or THC and the amount of CBD or THC derived from CBDA or THCA, respectively. These values are calculated by adding a molar correction factor of 0.877 to the CBDA or THCA value.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.
This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.
Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401
Page 7 of 8

Terpene Report by
Mass Spectrometer

Test Certificate #: 134746-001

Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Garlic Puff Live Rosin
License: 030-1009646F7F8
Type: Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A4010300003A37000001261
Metrc Source Pkg#: 1A401030002C949000002563

Test Conditions

Scale: XS205-OR1
Temp: 19.9 °C
Baro Pressure: 1001 hPa
Analyst: HRM
Technician: JBS

Sample ID#: 134746

Lot #: Garlic Puff 10-26-21
Batch #: 134746
Batch Weight (g): 200.9
Harvest/Process Date: 11/12/2021
Serving Size (g): 0.05
Date Received: 12/23/2021

α-Pinene (0.16%)
β-Ocimene (0.03%)
Camphene (0.04%)
Eucalyptol (1,8-Cineol) (0.00%)
Sabinene (0.00%)
γ-Terpinene (0.03%)
Myrcene (0.64%)
α-Terpinolene (0.14%)
β-Pinene (0.41%)
Linalool (0.06%)
∆3-Carene (0.00%)
Fenchone (0.00%)
α-Terpinene (0.04%)
endo-Fenchol (0.15%)
α-Ocimene (0.00%)
Isopulegol (0.00%)
Limonene (1.08%)
Geraniol (0.00%)
p-Cymene (0.00%)
β-Caryophyllene (0.00%)
α-Humulene (7.55%)
Nerolidol 1 (cis) (0.00%)
Nerolidol 2 (trans) (0.07%)
Guaiol (0.00%)
Caryophyllene Oxide (0.02%)
α-Bisabolol (0.58%)
α-Phellandrene (0.04%)
α-Terpineol (0.22%)
Valenence (1.15%)

Total: 12.410%

Predominant Terpenes

7.55%	α-Humulene	Woody, oceanic-watery, spicy clove	1.15%	Valenence	Sweet, citrus, grapefruit, woody, orange
1.08%	Limonene	Citrus, orange, sweet	0.64%	Myrcene	Peppery, spicy balsam
0.58%	α-Bisabolol	Fruity, nutty, coconut	0.41%	β-Pinene	Woody, fresh pine, hay
Value in parenthesis indicates percentage of terpene present in the total sample (weight percentage, wt/wt%). Value in doughnut slice indicates individual terpene abundance with respect to the total terpenes detected.

This sample has not been tested according to OAR 333-007. These results should therefore be used for research and development or quality control purposes only.
This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401
Page 8 of 8

ORELAP Cert No. 4092-005OLCC No. 1002158CD2E

Oregon Compliant Marijuana Potency Analysis byHigh Performance Liquid Chromatography

Client Name, Sample Details

Test Conditions

Sample ID#: 134746

ORELAP Cert No. 4092-005OLCC No. 1002158CD2E

Oregon Compliant QC Report

Client Name, Sample Details

Test Conditions

Sample ID#: 134746

ORELAP Cert No. 4092-005OLCC No. 1002158CD2E

Oregon Compliant Marijuana Potency Analysis byHigh Performance Liquid Chromatography

Client Name, Sample Details

Test Conditions

Sample ID#: 134746

ORELAP Cert No. 4092-005OLCC No. 1002158CD2E

Oregon Compliant QC Report

Client Name, Sample Details

Test Conditions

Sample ID#: 134746

ORELAP Cert No. 4092-005OLCC No. 1002158CD2E

Oregon Compliant Pesticide Analysis byMass Spectrometer

Client Name, Sample Details

Test Conditions

Sample ID#: 134746

ORELAP Cert No. 4092-005OLCC No. 1002158CD2E

Oregon Compliant Pesticide QC Report

Client Name, Sample Details

Test Conditions

Sample ID#: 134746

ORELAP Cert No. 4092-005OLCC No. 1002158CD2E

Oregon Compliant Pesticide Analysis byMass Spectrometer

Client Name, Sample Details

Test Conditions

Sample ID#: 134746

ORELAP Cert No. 4092-005OLCC No. 1002158CD2E

Oregon Compliant Pesticide QC Report

Client Name, Sample Details

Test Conditions

Sample ID#: 134746

ORELAP Cert No. 4092-005OLCC No. 1002158CD2E

Oregon Compliant Homogeneity Report byHigh Performance Liquid Chromatography

Client Name, Sample Details

Sample ID#: 134746

Terpene Report byMass Spectrometer

Client Name, Sample Details

Test Conditions

Sample ID#: 134746

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Marijuana Potency Analysis by
High Performance Liquid Chromatography

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Marijuana Potency Analysis by
High Performance Liquid Chromatography

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Pesticide Analysis by
Mass Spectrometer

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Pesticide Analysis by
Mass Spectrometer

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Homogeneity Report by
High Performance Liquid Chromatography

Terpene Report by
Mass Spectrometer