ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Marijuana Potency Analysis by
High Performance Liquid Chromatography
Testing Accreditation #: 4092-005 Test Certificate #: 132796-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Supreme Ruckus
License: 030-1009646F7F8
Type: AU Tincture
Method: FE04U HPLC-UV
Metrc Test Pkg#: 1A401030002C949000002383
Metrc Source Pkg#: 1A401030002C949000002342
Test Conditions

Prepsheet ID#: ORP210826B
Scale: XS205-OR1
Temp: 21.5 °C
Baro Pressure: 998 hPa
Analyst: TMR
Technician: TMR
Sample ID#: 132796

Lot #: Supreme Ruckus #1 8.9.2021
Batch #: 132796
Batch Weight (g): 252.6
Harvest/Process Date: 08/09/2021
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 08/24/2021
Test Date: 08/26/2021
Sample #132796
Sample #132796 Sample #132796
Test
Compounds		 THC THCA CBD CBDA CBN CBG CBC THCV* CBDV Total
Cannabinoids*		 Total THC Total CBD Calc Max Total
Cannabinoids*
Amount (%) 7.40 77.28 N/D 4.95 N/D 0.36 N/D N/D N/D 89.99 75.18 4.34 79.87
Amount (mg/g) 73.99 772.82 N/D 49.50 N/D 3.57 N/D N/D N/D 899.88 751.75 43.41 798.73
Amount per Serving (mg) 3.70 38.64 N\D 2.48 N\D 0.18 N\D N\D N\D 44.99 Serving Size~ (g): 0.05
LOQ (mg/g) 1.9 1.9 1.9 1.9 1.9 1.9 1.9 1.9 1.9   %Decarb. THC CBD
±%RPD 0.90 1.01 0.57 +/-5% 0.18 0.37 0.16 +/-5% +/-5% 9 0

LOQ = Limit of Quantitation; %RPD = Relative Percent Deviation; %RSD = Relative Standard Deviation; N/D = Not Detected

*Designates values that are not currently included in the accredited scope of Iron Laboratories.

*** Designates tests that use the method FE-45. FE-45 is performed using AOAC 966.02 and 32.004-32.009. FE-45 has relative expanded (k=2) uncertainties of 1.098% for moisture, 1.754% for water activity for unprocessed plant materials, and 13.102% for water activity for infused products. Vitamin E acetate analysis has a relative expanded (k=2) uncertainty of 18.614%.

Total THC and CBD is the calculated sum of THC or CBD and the amount of THC or CBD derived from THCA or CBDA, respectively. These values are calculated by applying a molar correction factor of 0.877 to the THCA or the CBDA value. Calc Max Total Cannabinoids is the sum of Total THC, Total CBD, CBN, CBG, CBC, THCV, and CBDV.

%Decarb. THC and CBD refer to the percentage of THC or CBD relative to THCA or CBDA, respectively.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 1 of 12

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant QC Report
Testing Accreditation #: 4092-005 Test Certificate #: 132796-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Supreme Ruckus
License: 030-1009646F7F8
Type: AU Tincture
Method: FE04U HPLC-UV
Metrc Test Pkg#: 1A401030002C949000002383
Metrc Source Pkg#: 1A401030002C949000002342
Test Conditions

Prepsheet ID#: ORP210826B
Scale: XS205-OR1
Temp: 21.5 °C
Baro Pressure: 998 hPa
Analyst: TMR
Technician: TMR
Sample ID#: 132796

Lot #: Supreme Ruckus #1 8.9.2021
Batch #: 132796
Batch Weight (g): 252.6
Harvest/Process Date: 08/09/2021
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 08/24/2021
Test Date: 08/26/2021
Sample #132796
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Cannabidivarin (CBDV) N.D. 5.15 5.03 97.67 5.03 97.67 0.00
Cannabidiolic Acid (CBDA) N.D. 4.03 3.9 96.77 3.9 96.77 0.00
Cannabigerol (CBG) N.D. 5.59 5.44 97.32 5.42 96.96 0.37
Cannabidiol (CBD) N.D. 5.45 5.26 96.51 5.29 97.06 0.57
Δ9-Tetrahydrocannabivarin (THCV) N.D. 5.55 5.4 97.30 5.4 97.30 0.00
Cannabinol (CBN) N.D. 5.72 5.55 97.03 5.56 97.20 0.18
Δ9-Tetrahydrocannabinol (THC) N.D. 5.8 5.56 95.86 5.61 96.72 0.90
Cannabichromene (CBC) N.D. 6.3 6.11 96.98 6.1 96.83 0.16
Tetrahydrocannabinolic acid (THCA) N.D. 4.09 3.98 97.31 3.94 96.33 1.01

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 2 of 12

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Marijuana Potency Analysis by
High Performance Liquid Chromatography
Testing Accreditation #: 4092-005 Test Certificate #: 132796-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Supreme Ruckus
License: 030-1009646F7F8
Type: AU Tincture
Method: FE04U HPLC-UV
Metrc Test Pkg#: 1A401030002C949000002383
Metrc Source Pkg#: 1A401030002C949000002342
Test Conditions

Prepsheet ID#: ORP210826B
Scale: XS205-OR1
Temp: 21.5 °C
Baro Pressure: 998 hPa
Analyst: TMR
Technician: TMR
Sample ID#: 132796

Lot #: Supreme Ruckus #1 8.9.2021
Batch #: 132796
Batch Weight (g): 252.6
Harvest/Process Date: 08/09/2021
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 08/24/2021
Test Date: 08/26/2021
Sample #132796
Sample #132796 Sample #132796
Test
Compounds		 THC THCA CBD CBDA CBN CBG CBC THCV* CBDV Total
Cannabinoids*		 Total THC Total CBD Calc Max Total
Cannabinoids*
Amount (%) 7.39 75.77 N/D 4.87 N/D 0.35 N/D N/D N/D 88.38 73.84 4.27 78.46
Amount (mg/g) 73.89 757.66 N/D 48.74 N/D 3.51 N/D N/D N/D 883.8 738.36 42.74 784.61
Amount per Serving (mg) 3.69 37.88 N\D 2.44 N\D 0.18 N\D N\D N\D 44.19 Serving Size~ (g): 0.05
LOQ (mg/g) 2 2 2 2 2 2 2 2 2   %Decarb. THC CBD
±%RPD 0.90 1.01 0.57 +/-5% 0.18 0.37 0.16 +/-5% +/-5% 0 0

LOQ = Limit of Quantitation; %RPD = Relative Percent Deviation; %RSD = Relative Standard Deviation; N/D = Not Detected

*Designates values that are not currently included in the accredited scope of Iron Laboratories.

*** Designates tests that use the method FE-45. FE-45 is performed using AOAC 966.02 and 32.004-32.009. FE-45 has relative expanded (k=2) uncertainties of 1.098% for moisture, 1.754% for water activity for unprocessed plant materials, and 13.102% for water activity for infused products. Vitamin E acetate analysis has a relative expanded (k=2) uncertainty of 18.614%.

Total THC and CBD is the calculated sum of THC or CBD and the amount of THC or CBD derived from THCA or CBDA, respectively. These values are calculated by applying a molar correction factor of 0.877 to the THCA or the CBDA value. Calc Max Total Cannabinoids is the sum of Total THC, Total CBD, CBN, CBG, CBC, THCV, and CBDV.

%Decarb. THC and CBD refer to the percentage of THC or CBD relative to THCA or CBDA, respectively.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 2 of 12

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant QC Report
Testing Accreditation #: 4092-005 Test Certificate #: 132796-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Supreme Ruckus
License: 030-1009646F7F8
Type: AU Tincture
Method: FE04U HPLC-UV
Metrc Test Pkg#: 1A401030002C949000002383
Metrc Source Pkg#: 1A401030002C949000002342
Test Conditions

Prepsheet ID#: ORP210826B
Scale: XS205-OR1
Temp: 21.5 °C
Baro Pressure: 998 hPa
Analyst: TMR
Technician: TMR
Sample ID#: 132796

Lot #: Supreme Ruckus #1 8.9.2021
Batch #: 132796
Batch Weight (g): 252.6
Harvest/Process Date: 08/09/2021
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 08/24/2021
Test Date: 08/26/2021
Sample #132796
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Cannabidivarin (CBDV) N.D. 5.15 5.03 97.67 5.03 97.67 0.00
Cannabidiolic Acid (CBDA) N.D. 4.03 3.9 96.77 3.9 96.77 0.00
Cannabigerol (CBG) N.D. 5.59 5.44 97.32 5.42 96.96 0.37
Cannabidiol (CBD) N.D. 5.45 5.26 96.51 5.29 97.06 0.57
Δ9-Tetrahydrocannabivarin (THCV) N.D. 5.55 5.4 97.30 5.4 97.30 0.00
Cannabinol (CBN) N.D. 5.72 5.55 97.03 5.56 97.20 0.18
Δ9-Tetrahydrocannabinol (THC) N.D. 5.8 5.56 95.86 5.61 96.72 0.90
Cannabichromene (CBC) N.D. 6.3 6.11 96.98 6.1 96.83 0.16
Tetrahydrocannabinolic acid (THCA) N.D. 4.09 3.98 97.31 3.94 96.33 1.01

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 3 of 12

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Pesticide Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-005 Test Certificate #: 132796-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Supreme Ruckus
License: 030-1009646F7F8
Type: AU Tincture
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A401030002C949000002383
Metrc Source Pkg#: 1A401030002C949000002342
Test Conditions

Prepsheet ID#: ORPS210826b
Scale: XS205-OR1
Temp: 21.3 °C
Baro PE: 1003 hPa
Analyst: HRM
Technician: JBS
Sample ID#: 132796

Lot #: Supreme Ruckus #1 8.9.2021
Batch #: 132796
Batch Weight (g): 252.6
Harvest/Process Date: 08/09/2021
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 08/24/2021
Test Date: 08/26/2021
Sample #132796
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
Aldicarb 0.400 0.123 Pass/<LOD Abamectin**** 0.500 0.123 Pass/<LOD
Acephate 0.400 0.123 Pass/<LOD Acequinocyl 2.000 0.245 Pass/<LOD
Acetamiprid 0.200 0.123 Pass/<LOD Azoxystrobin 0.200 0.123 Pass/<LOD
Bifenazate 0.200 0.123 Pass/<LOD Bifenthrin 0.200 0.123 Pass/<LOD
Boscalid 0.400 0.123 Pass/<LOD Carbaryl 0.200 0.123 Pass/<LOD
Carbofuran 0.200 0.123 Pass/<LOD Chlorantraniliprole 0.200 0.123 Pass/<LOD
Chlorfenapyr 1.000 0.490 Pass/<LOD Chlorpyrifos 0.200 0.123 Pass/<LOD
Clofentezine 0.200 0.123 Pass/<LOD Cyfluthrin** 1.000 0.490 Pass/<LOD
Cypermethrin*** 1.000 0.490 Pass/<LOD Daminozide 1.000 0.123 Pass/<LOD
DDVP (Dichlorvos) 1.000 0.245 Pass/<LOD Diazinon 0.200 0.123 Pass/<LOD
Dimethoate 0.200 0.123 Pass/<LOD Ethoprophos 0.200 0.123 Pass/<LOD
Etofenprox 0.400 0.123 Pass/<LOD Etoxazole 0.200 0.123 Pass/<LOD
Fenoxycarb 0.200 0.123 Pass/<LOD Fenpyroximate 0.400 0.123 Pass/<LOD
Fipronil 0.400 0.123 Pass/<LOD Flonicamid 1.000 0.123 Pass/<LOD
Fludioxonil 0.400 0.123 Pass/<LOD Hexythiazox 1.000 0.123 Pass/<LOD
Imazalil 0.200 0.123 Pass/<LOD Imidacloprid 0.400 0.123 Pass/<LOD
Kresoxim Methyl 0.400 0.123 Pass/<LOD Malathion 0.200 0.123 Pass/<LOD
Metalaxyl 0.200 0.123 Pass/<LOD Methiocarb 0.200 0.123 Pass/<LOD
Methomyl 0.400 0.123 Pass/<LOD Methyl Parathion 0.200 0.123 Pass/<LOD
MGK-264‡ 0.200 0.123 Pass/<LOD Myclobutanil 0.000 0.123 Pass/<LOD
Naled 0.500 0.123 Pass/<LOD Oxamyl 1.000 0.123 Pass/<LOD
Paclobutrazol 0.400 0.123 Pass/<LOD Permethrins† 0.200 0.123 Pass/<LOD
Phosmet 0.200 0.123 Pass/<LOD Piperonyl Butoxide 2.000 0.123 Pass/<LOD
Prallethrin 0.200 0.123 Pass/<LOD Propiconazole 0.400 0.123 Pass/<LOD
Propoxur 0.200 0.123 Pass/<LOD Pyrethrins* 1.000 0.123 Pass/<LOD
Pyridaben 0.200 0.123 Pass/<LOD Spinosad***** 0.200 0.123 Pass/<LOD
Spiromesifen 0.200 0.123 Pass/<LOD Spirotetramat 0.200 0.123 Pass/<LOD
Spiroxamine‡ 0.400 0.123 Pass/<LOD Tebuconazole 0.400 0.123 Pass/<LOD
Thiacloprid 0.200 0.123 Pass/<LOD Thiamethoxam 0.200 0.123 Pass/<LOD
Trifloxystrobin 0.200 0.123 Pass/<LOD

* Pyrethrins are reported as the sum of Jasmolin I, Cinerin I, and Pyrethrin I
** Cyfluthrins are reported as the sum of isomers Cyfluthrin I, II, III, and IV
*** Cypermethrins are reported as the sum of isomers Cypermethrin I, II, III, and IV
**** Abamectin is reported as the sum of Avermectin B1a and Avermectin B1b
***** Spinosad is reported as the sum of Spinosyn A and Spinosyn D
† Permethrin and Prallethrin are reported as the sum of cis and trans isomers
‡ MGK-264 and Spiroximine are reported as the sum of isomers I and II
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 3 of 12

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Pesticide QC Report
Testing Accreditation #: 4092-005 Test Certificate #: 132796-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Supreme Ruckus
License: 030-1009646F7F8
Type: AU Tincture
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A401030002C949000002383
Metrc Source Pkg#: 1A401030002C949000002342
Test Conditions

Prepsheet ID#: ORPS210826b
Scale: XS205-OR1
Temp: 21.3 °C
Baro PE: 1003 hPa
Analyst: HRM
Technician: JBS
Sample ID#: 132796

Lot #: Supreme Ruckus #1 8.9.2021
Batch #: 132796
Batch Weight (g): 252.6
Harvest/Process Date: 08/09/2021
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 08/24/2021
Test Date: 08/26/2021
Sample #132796
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS recovery% MSD recovery% Relative Percent Difference (%) QC Flag
Acephate N.D. 1 1.54 1.5 154.00 150.00 2.63 HR
Acequinocyl N.D. 1 0.518 0.447 51.80 44.70 14.72 LR
Acetamiprid N.D. 1 1.79 1.67 179.00 167.00 6.94 HR
Aldicarb N.D. 1 1.68 1.52 168.00 152.00 10.00 HR
Avermectin B1a N.D. 0.97 2.61 2.52 269.07 259.79 3.51 HR
Azoxystrobin N.D. 1 2.17 2.12 217.00 212.00 2.33 HR
Bifenazate N.D. 1 2.05 1.05 205.00 105.00 64.52 HR Q
Bifenthrin N.D. 1 1.53 1.36 153.00 136.00 11.76 HR
Boscalid N.D. 1 1.91 1.29 191.00 129.00 38.75 HR Q
Carbaryl N.D. 1 1.83 1.77 183.00 177.00 3.33 HR
Carbofuran N.D. 1 2.31 2.01 231.00 201.00 13.89 HR
Chlorantraniliprole N.D. 1 2.47 2.27 247.00 227.00 8.44 HR
Chlorfenapyr N.D. 1 1.39 1.29 139.00 129.00 7.46 HR
Chlorpyriphos N.D. 1 1.07 0.998 107.00 99.80 6.96
Clofentezine N.D. 1 1.27 1.19 127.00 119.00 6.50
Cyfluthrin N.D. 1 1.66 1.58 166.00 158.00 4.94 HR
Cypermethrin N.D. 1 1.55 1.51 155.00 151.00 2.61 HR
Daminoside N.D. 1 1.21 0.889 121.00 88.90 30.59 Q
Diazanon N.D. 1 4.91 4.48 491.00 448.00 9.16 HR
Dichlorvos N.D. 1 3.21 2.98 321.00 298.00 7.43 HR
Dimethoate N.D. 1 2.8 2.52 280.00 252.00 10.53 HR
Ethoprophos N.D. 1 1.79 1.81 179.00 181.00 1.11 HR
Etofenprox N.D. 1 1.5 1.39 150.00 139.00 7.61 HR
Etoxazole N.D. 1 1.59 1.47 159.00 147.00 7.84 HR
Fenoxycarb N.D. 1 2.44 1.97 244.00 197.00 21.32 HR Q
Fenpyroximate N.D. 1 2 1.83 200.00 183.00 8.88 HR
Fipronil N.D. 1 1.49 1.44 149.00 144.00 3.41 HR
Flonicamid N.D. 1 2.02 2.41 202.00 241.00 17.61 HR
Fludioxonil N.D. 1 1.63 1.57 163.00 157.00 3.75 HR
Hexythiazox N.D. 1 0.93 0.868 93.00 86.80 6.90
Imazalil N.D. 1 2.57 2.41 257.00 241.00 6.43 HR
Imidacloprid N.D. 1 2.26 2.15 226.00 215.00 4.99 HR
Kresoxim-methyl N.D. 1 1.72 1.59 172.00 159.00 7.85 HR
Malathion N.D. 1 1.59 1.53 159.00 153.00 3.85 HR
Metalaxyl N.D. 1 2.45 2.23 245.00 223.00 9.40 HR
Methiocarb N.D. 1 2.16 2.02 216.00 202.00 6.70 HR
Methomyl N.D. 1 1.35 1.25 135.00 125.00 7.69 HR
MGK-264 N.D. 1 1.89 1.87 189.00 187.00 1.06 HR
Myclobutanil N.D. 1 3.15 2.45 315.00 245.00 25.00 HR Q
Naled (dibrom) N.D. 1 1.26 1.32 126.00 132.00 4.65 HR
Oxamyl N.D. 1 2.44 2.34 244.00 234.00 4.18 HR
Paclobutrazol N.D. 1 2.37 2.02 237.00 202.00 15.95 HR
Parathion-methyl N.D. 1 1.3 1.1 130.00 110.00 16.67
Permethrins N.D. 1 1.726 1.456 172.60 145.60 16.97 HR
Phosmet N.D. 1 1.96 1.88 196.00 188.00 4.17 HR
Piperonyl butoxide N.D. 1 1.66 1.57 166.00 157.00 5.57 HR
Prallethrin N.D. 1 2.32 2.05 232.00 205.00 12.36 HR
Propiconazole N.D. 1 1.63 1.55 163.00 155.00 5.03 HR
Propoxur N.D. 1 2.28 2.12 228.00 212.00 7.27 HR
Pyrethrin N.D. 0.65 0.952 0.854 146.46 131.38 10.85 HR
Pyridaben N.D. 1 1.45 1.28 145.00 128.00 12.45 HR
SpinosynA N.D. 0.84 2.35 2.29 279.76 272.62 2.59 HR
SpinosynD N.D. 0.16 0.397 0.352 248.13 220.00 12.02 HR
Spiromesifen N.D. 1 1.05 0.958 105.00 95.80 9.16
Spirotetramat N.D. 1 2.06 1.87 206.00 187.00 9.67 HR
Spiroxamine N.D. 1 2.15 2.04 215.00 204.00 5.25 HR
Tebuconazole N.D. 1 1.87 1.6 187.00 160.00 15.56 HR
Thiacloprid N.D. 1 2.31 2.24 231.00 224.00 3.08 HR
Thiamethoxam N.D. 1 2.12 2.01 212.00 201.00 5.33 HR
Trifloxystrobin N.D. 1 1.87 1.78 187.00 178.00 4.93 HR

N.D. = Not Detected

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 30%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (60-120%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 4 of 12

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Pesticide Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-005 Test Certificate #: 132796-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Supreme Ruckus
License: 030-1009646F7F8
Type: AU Tincture
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A401030002C949000002383
Metrc Source Pkg#: 1A401030002C949000002342
Test Conditions

Prepsheet ID#: ORPS210826b
Scale: XS205-OR1
Temp: 21.3 °C
Baro PE: 1003 hPa
Analyst: HRM
Technician: JBS
Sample ID#: 132796

Lot #: Supreme Ruckus #1 8.9.2021
Batch #: 132796
Batch Weight (g): 252.6
Harvest/Process Date: 08/09/2021
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 08/24/2021
Test Date: 08/26/2021
Sample #132796
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
Aldicarb 0.400 0.124 Pass/<LOD Abamectin**** 0.500 0.124 Pass/<LOD
Acephate 0.400 0.124 Pass/<LOD Acequinocyl 2.000 0.248 Pass/<LOD
Acetamiprid 0.200 0.124 Pass/<LOD Azoxystrobin 0.200 0.124 Pass/<LOD
Bifenazate 0.200 0.124 Pass/<LOD Bifenthrin 0.200 0.124 Pass/<LOD
Boscalid 0.400 0.124 Pass/<LOD Carbaryl 0.200 0.124 Pass/<LOD
Carbofuran 0.200 0.124 Pass/<LOD Chlorantraniliprole 0.200 0.124 Pass/<LOD
Chlorfenapyr 1.000 0.496 Pass/<LOD Chlorpyrifos 0.200 0.124 Pass/<LOD
Clofentezine 0.200 0.124 Pass/<LOD Cyfluthrin** 1.000 0.496 Pass/<LOD
Cypermethrin*** 1.000 0.496 Pass/<LOD Daminozide 1.000 0.124 Pass/<LOD
DDVP (Dichlorvos) 1.000 0.248 Pass/<LOD Diazinon 0.200 0.124 Pass/<LOD
Dimethoate 0.200 0.124 Pass/<LOD Ethoprophos 0.200 0.124 Pass/<LOD
Etofenprox 0.400 0.124 Pass/<LOD Etoxazole 0.200 0.124 Pass/<LOD
Fenoxycarb 0.200 0.124 Pass/<LOD Fenpyroximate 0.400 0.124 Pass/<LOD
Fipronil 0.400 0.124 Pass/<LOD Flonicamid 1.000 0.124 Pass/<LOD
Fludioxonil 0.400 0.124 Pass/<LOD Hexythiazox 1.000 0.124 Pass/<LOD
Imazalil 0.200 0.124 Pass/<LOD Imidacloprid 0.400 0.124 Pass/<LOD
Kresoxim Methyl 0.400 0.124 Pass/<LOD Malathion 0.200 0.124 Pass/<LOD
Metalaxyl 0.200 0.124 Pass/<LOD Methiocarb 0.200 0.124 Pass/<LOD
Methomyl 0.400 0.124 Pass/<LOD Methyl Parathion 0.200 0.124 Pass/<LOD
MGK-264‡ 0.200 0.124 Pass/<LOD Myclobutanil 0.000 0.124 Pass/<LOD
Naled 0.500 0.124 Pass/<LOD Oxamyl 1.000 0.124 Pass/<LOD
Paclobutrazol 0.400 0.124 Pass/<LOD Permethrins† 0.200 0.124 Pass/<LOD
Phosmet 0.200 0.124 Pass/<LOD Piperonyl Butoxide 2.000 0.124 Pass/<LOD
Prallethrin 0.200 0.124 Pass/<LOD Propiconazole 0.400 0.124 Pass/<LOD
Propoxur 0.200 0.124 Pass/<LOD Pyrethrins* 1.000 0.124 Pass/<LOD
Pyridaben 0.200 0.124 Pass/<LOD Spinosad***** 0.200 0.124 Pass/<LOD
Spiromesifen 0.200 0.124 Pass/<LOD Spirotetramat 0.200 0.124 Pass/<LOD
Spiroxamine‡ 0.400 0.124 Pass/<LOD Tebuconazole 0.400 0.124 Pass/<LOD
Thiacloprid 0.200 0.124 Pass/<LOD Thiamethoxam 0.200 0.124 Pass/<LOD
Trifloxystrobin 0.200 0.124 Pass/<LOD

* Pyrethrins are reported as the sum of Jasmolin I, Cinerin I, and Pyrethrin I
** Cyfluthrins are reported as the sum of isomers Cyfluthrin I, II, III, and IV
*** Cypermethrins are reported as the sum of isomers Cypermethrin I, II, III, and IV
**** Abamectin is reported as the sum of Avermectin B1a and Avermectin B1b
***** Spinosad is reported as the sum of Spinosyn A and Spinosyn D
† Permethrin and Prallethrin are reported as the sum of cis and trans isomers
‡ MGK-264 and Spiroximine are reported as the sum of isomers I and II
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 5 of 12

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Pesticide QC Report
Testing Accreditation #: 4092-005 Test Certificate #: 132796-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Supreme Ruckus
License: 030-1009646F7F8
Type: AU Tincture
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A401030002C949000002383
Metrc Source Pkg#: 1A401030002C949000002342
Test Conditions

Prepsheet ID#: ORPS210826b
Scale: XS205-OR1
Temp: 21.3 °C
Baro PE: 1003 hPa
Analyst: HRM
Technician: JBS
Sample ID#: 132796

Lot #: Supreme Ruckus #1 8.9.2021
Batch #: 132796
Batch Weight (g): 252.6
Harvest/Process Date: 08/09/2021
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 08/24/2021
Test Date: 08/26/2021
Sample #132796
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS recovery% MSD recovery% Relative Percent Difference (%) QC Flag
Acephate N.D. 1 1.54 1.5 154.00 150.00 2.63 HR
Acequinocyl N.D. 1 0.518 0.447 51.80 44.70 14.72 LR
Acetamiprid N.D. 1 1.79 1.67 179.00 167.00 6.94 HR
Aldicarb N.D. 1 1.68 1.52 168.00 152.00 10.00 HR
Avermectin B1a N.D. 0.97 2.61 2.52 269.07 259.79 3.51 HR
Azoxystrobin N.D. 1 2.17 2.12 217.00 212.00 2.33 HR
Bifenazate N.D. 1 2.05 1.05 205.00 105.00 64.52 HR Q
Bifenthrin N.D. 1 1.53 1.36 153.00 136.00 11.76 HR
Boscalid N.D. 1 1.91 1.29 191.00 129.00 38.75 HR Q
Carbaryl N.D. 1 1.83 1.77 183.00 177.00 3.33 HR
Carbofuran N.D. 1 2.31 2.01 231.00 201.00 13.89 HR
Chlorantraniliprole N.D. 1 2.47 2.27 247.00 227.00 8.44 HR
Chlorfenapyr N.D. 1 1.39 1.29 139.00 129.00 7.46 HR
Chlorpyriphos N.D. 1 1.07 0.998 107.00 99.80 6.96
Clofentezine N.D. 1 1.27 1.19 127.00 119.00 6.50
Cyfluthrin N.D. 1 1.66 1.58 166.00 158.00 4.94 HR
Cypermethrin N.D. 1 1.55 1.51 155.00 151.00 2.61 HR
Daminoside N.D. 1 1.21 0.889 121.00 88.90 30.59 Q
Diazanon N.D. 1 4.91 4.48 491.00 448.00 9.16 HR
Dichlorvos N.D. 1 3.21 2.98 321.00 298.00 7.43 HR
Dimethoate N.D. 1 2.8 2.52 280.00 252.00 10.53 HR
Ethoprophos N.D. 1 1.79 1.81 179.00 181.00 1.11 HR
Etofenprox N.D. 1 1.5 1.39 150.00 139.00 7.61 HR
Etoxazole N.D. 1 1.59 1.47 159.00 147.00 7.84 HR
Fenoxycarb N.D. 1 2.44 1.97 244.00 197.00 21.32 HR Q
Fenpyroximate N.D. 1 2 1.83 200.00 183.00 8.88 HR
Fipronil N.D. 1 1.49 1.44 149.00 144.00 3.41 HR
Flonicamid N.D. 1 2.02 2.41 202.00 241.00 17.61 HR
Fludioxonil N.D. 1 1.63 1.57 163.00 157.00 3.75 HR
Hexythiazox N.D. 1 0.93 0.868 93.00 86.80 6.90
Imazalil N.D. 1 2.57 2.41 257.00 241.00 6.43 HR
Imidacloprid N.D. 1 2.26 2.15 226.00 215.00 4.99 HR
Kresoxim-methyl N.D. 1 1.72 1.59 172.00 159.00 7.85 HR
Malathion N.D. 1 1.59 1.53 159.00 153.00 3.85 HR
Metalaxyl N.D. 1 2.45 2.23 245.00 223.00 9.40 HR
Methiocarb N.D. 1 2.16 2.02 216.00 202.00 6.70 HR
Methomyl N.D. 1 1.35 1.25 135.00 125.00 7.69 HR
MGK-264 N.D. 1 1.89 1.87 189.00 187.00 1.06 HR
Myclobutanil N.D. 1 3.15 2.45 315.00 245.00 25.00 HR Q
Naled (dibrom) N.D. 1 1.26 1.32 126.00 132.00 4.65 HR
Oxamyl N.D. 1 2.44 2.34 244.00 234.00 4.18 HR
Paclobutrazol N.D. 1 2.37 2.02 237.00 202.00 15.95 HR
Parathion-methyl N.D. 1 1.3 1.1 130.00 110.00 16.67
Permethrins N.D. 1 1.726 1.456 172.60 145.60 16.97 HR
Phosmet N.D. 1 1.96 1.88 196.00 188.00 4.17 HR
Piperonyl butoxide N.D. 1 1.66 1.57 166.00 157.00 5.57 HR
Prallethrin N.D. 1 2.32 2.05 232.00 205.00 12.36 HR
Propiconazole N.D. 1 1.63 1.55 163.00 155.00 5.03 HR
Propoxur N.D. 1 2.28 2.12 228.00 212.00 7.27 HR
Pyrethrin N.D. 0.65 0.952 0.854 146.46 131.38 10.85 HR
Pyridaben N.D. 1 1.45 1.28 145.00 128.00 12.45 HR
SpinosynA N.D. 0.84 2.35 2.29 279.76 272.62 2.59 HR
SpinosynD N.D. 0.16 0.397 0.352 248.13 220.00 12.02 HR
Spiromesifen N.D. 1 1.05 0.958 105.00 95.80 9.16
Spirotetramat N.D. 1 2.06 1.87 206.00 187.00 9.67 HR
Spiroxamine N.D. 1 2.15 2.04 215.00 204.00 5.25 HR
Tebuconazole N.D. 1 1.87 1.6 187.00 160.00 15.56 HR
Thiacloprid N.D. 1 2.31 2.24 231.00 224.00 3.08 HR
Thiamethoxam N.D. 1 2.12 2.01 212.00 201.00 5.33 HR
Trifloxystrobin N.D. 1 1.87 1.78 187.00 178.00 4.93 HR

N.D. = Not Detected

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 30%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (60-120%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 6 of 12

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-005 Test Certificate #: 132796-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Supreme Ruckus
License: 030-1009646F7F8
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A401030002C949000002383
Metrc Source Pkg#: 1A401030002C949000002342
Test Conditions

Prepsheet ID#: ORHS210824a
Scale: XS205-OR1
Temp: 20.7 °C
Baro PE: 1002 hPa
Analyst: HRM
Technician: JBS
Sample ID#: 132796

Lot #: Supreme Ruckus #1 8.9.2021
Batch #: 132796
Batch Weight (g): 252.6
Harvest/Process Date: 08/09/2021
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 08/24/2021
Test Date: 08/24/2021
Sample #132796
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
1,2-Dichloroethane 2 1 Not Tested 1,2-Dimethoxyethane 100 5 Pass/<LOD
1,4-dioxane 380 200 Pass/<LOD 1-Butanol 5,000 100 Pass/<LOD
1-Pentanol 5,000 100 Pass/<LOD 1-Propanol 5,000 100 Pass/<LOD
2,2-Dimethylpropane (Neopentane) 5,000 100 Pass/<LOD 2,2-Dimethylbutane (Hexanes) 290 100 Pass/<LOD
2,3-Dimethylbutane (Hexanes) 290 100 Pass/<LOD 2-Butanol 5,000 100 Pass/<LOD
2-Butanone (MEK) 5,000 50 Pass/<LOD 2-Ethoxyethanol 160 40 Pass/<LOD
2-Methylbutane (Isopentane) 5,000 50 Pass/<LOD 2-Methylpentane (Hexanes) 290 50 Pass/<LOD
2-Methylpropane (Isobutane) 5,000 100 Pass/<LOD 2-propanol (Isopropyl Alcohol) 5,000 50 Pass/<LOD
2-Propanone (Acetone) 5,000 50 Pass/<LOD 3-Methylpentane (Hexanes) 290 50 Pass/<LOD
Acetonitrile 410 100 Pass/<LOD Benzene 2 1 Pass/<LOD
Butane 5,000 100 Pass/640 Chloroform 2 1 Pass/<LOD
Cumene 70 50 Pass/<LOD Cyclohexane 3,880 1,000 Pass/<LOD
Dichloromethane 600 50 Pass/<LOD Dimethylsulfoxide (DMSO) 5,000 500 Pass/<LOD
Ethanol 5,000 500 Pass/<LOD Ethyl acetate 5,000 50 Pass/<LOD
Ethyl ether 5,000 500 Pass/<LOD Ethylene glycol 620 310 Pass/<LOD
Ethylene oxide 50 50 Pass/<LOD Heptane 5,000 50 Pass/<LOD
Hexane 290 290 Pass/<LOD Isopropyl acetate 5,000 50 Pass/<LOD
Methanol 3,000 500 Pass/<LOD Naptha 400 100 Not Tested
N,N-Dimethylacetamide 1,090 100 Pass/<LOD N,N-Dimethylformamide (DMF) 880 500 Pass/<LOD
Pentane 5,000 50 Pass/<LOD Petroleum Ether 400 100 Not Tested
Propane 5,000 100 Pass/<LOD Pyridine 200 10 Pass/<LOD
Sulfolane 160 200 Pass/<LOD Tetrahydrofuran (THF) 720 200 Pass/<LOD
Toluene 890 50 Pass/<LOD Trichloroethylene 25 5 Not Tested
Xylenes* 2,170 50 Pass/<LOD

Total Butanes = 640 ug/g (PASS); Total Pentanes = 0 ug/g (PASS); Total Hexanes = 0 ug/g (PASS)

* Xylenes are reported as the sum of o-xylene, m-xylene, p-xylene, and ethylbenzene
MRL - Maximum Residue Limit; LOD - Limit of Detection

This sample has not been tested according to OAR 333-007. These results should therefore be used for research and development or quality control purposes only.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 7 of 12

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents QC Report
Testing Accreditation #: 4092-005 Test Certificate #: 132796-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Supreme Ruckus
License: 030-1009646F7F8
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A401030002C949000002383
Metrc Source Pkg#: 1A401030002C949000002342
Test Conditions

Prepsheet ID#: ORHS210824a
Scale: XS205-OR1
Temp: 20.7 °C
Baro PE: 1002 hPa
Analyst: HRM
Technician: JBS
Sample ID#: 132796

Lot #: Supreme Ruckus #1 8.9.2021
Batch #: 132796
Batch Weight (g): 252.6
Harvest/Process Date: 08/09/2021
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 08/24/2021
Test Date: 08/24/2021
Sample #132796
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS Recovery (%) MSD Recovery (%) Relative Percent Difference (%) QC Flag
1,2-Dichloroethane N.D. 0 0 0 nan nan
n-Propane N.D. 250 126 124 50.40 49.60 1.60 LRLR
Isobutane N.D. 250 224 142 89.60 56.80 44.81 LRQ
Methanol N.D. 250 89 85 35.60 34.00 4.60 LRLR
n-Butane N.D. 250 262 165 104.80 66.00 45.43 LRQ
2,2-Dimethylpropane N.D. 250 206 205 82.40 82.00 0.49
Ethanol N.D. 250 317 317 126.80 126.80 0.00
Isopentane N.D. 250 248 261 99.20 104.40 5.11
Acetonitrile N.D. 250 228 235 91.20 94.00 3.02
Diethyl ether N.D. 250 252 258 100.80 103.20 2.35
2-propanone N.D. 250 280 184 112.00 73.60 41.38 Q
2-propanol N.D. 250 213 262 85.20 104.80 20.63 Q
n-Pentane 704.06 250 0 852 0.00 340.80 200.00 LRHRQI
2,2-Dimethylbutane N.D. 250 244 246 97.60 98.40 0.82
2,3-Dimethylbutane N.D. 250 246 250 98.40 100.00 1.61
Methylene chloride N.D. 250 264 263 105.60 105.20 0.38
2-Methylpentane N.D. 250 246 259 98.40 103.60 5.15
3-Methylpentane N.D. 250 248 243 99.20 97.20 2.04
2-Butanol N.D. 250 257 264 102.80 105.60 2.69
n-Hexane N.D. 250 228 233 91.20 93.20 2.17
Ethyl acetate N.D. 250 272 277 108.80 110.80 1.82
Tetrahydrofuran N.D. 250 274 275 0.00 0.00 0.00
Trichloroethylene N.D. 0 0 0 nan nan
Isopropyl acetate N.D. 250 258 257 0.00 0.00 0.00
Benzene N.D. 250 259 264 103.60 105.60 1.91
Chloroform N.D. 0 0 0 nan nan
Cyclohexane N.D. 250 265 268 106.00 107.20 1.13
Ethylene glycol N.D. 250 207 192 82.80 76.80 7.52
Heptane N.D. 250 307 253 122.80 101.20 19.29
2-Ethoxyethanol N.D. 250 393 259 157.20 103.60 41.10 HRQ
1,4-Dioxane N.D. 250 287 291 114.80 116.40 1.38
Pyridine N.D. 0 0 0 0.00 0.00 0.00
Toluene N.D. 250 251 254 100.40 101.60 1.19
Chlorobenzene N.D. 0 0 0 0.00 0.00 0.00
Ethylbenzene N.D. 250 256 259 102.40 103.60 1.17
m-Xylene/p-Xylene N.D. 500 529 527 105.80 105.40 0.38
o-Xylene N.D. 250 296 293 118.40 117.20 1.02
Cumene N.D. 250 283 282 113.20 112.80 0.35
Ethylene oxide N.D. 250 289 414 115.60 165.60 35.56 HRQ

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

N.D. = Not Detected

This sample has not been tested according to OAR 333-007. These results should therefore be used for research and development or quality control purposes only.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 8 of 12

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-005 Test Certificate #: 132796-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Supreme Ruckus
License: 030-1009646F7F8
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A401030002C949000002383
Metrc Source Pkg#: 1A401030002C949000002342
Test Conditions

Prepsheet ID#: ORHS210824a
Scale: XS205-OR1
Temp: 20.7 °C
Baro PE: 1002 hPa
Analyst: HRM
Technician: JBS
Sample ID#: 132796

Lot #: Supreme Ruckus #1 8.9.2021
Batch #: 132796
Batch Weight (g): 252.6
Harvest/Process Date: 08/09/2021
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 08/24/2021
Test Date: 08/24/2021
Sample #132796
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
1,2-Dichloroethane 2 1 Not Tested 1,2-Dimethoxyethane 100 5 Pass/<LOD
1,4-dioxane 380 200 Pass/<LOD 1-Butanol 5,000 100 Pass/<LOD
1-Pentanol 5,000 100 Pass/<LOD 1-Propanol 5,000 100 Pass/<LOD
2,2-Dimethylpropane (Neopentane) 5,000 100 Pass/<LOD 2,2-Dimethylbutane (Hexanes) 290 100 Pass/<LOD
2,3-Dimethylbutane (Hexanes) 290 100 Pass/<LOD 2-Butanol 5,000 100 Pass/<LOD
2-Butanone (MEK) 5,000 50 Pass/<LOD 2-Ethoxyethanol 160 40 Pass/<LOD
2-Methylbutane (Isopentane) 5,000 50 Pass/<LOD 2-Methylpentane (Hexanes) 290 50 Pass/<LOD
2-Methylpropane (Isobutane) 5,000 100 Pass/<LOD 2-propanol (Isopropyl Alcohol) 5,000 50 Pass/<LOD
2-Propanone (Acetone) 5,000 50 Pass/<LOD 3-Methylpentane (Hexanes) 290 50 Pass/<LOD
Acetonitrile 410 100 Pass/<LOD Benzene 2 1 Pass/<LOD
Butane 5,000 100 Pass/763 Chloroform 2 1 Pass/<LOD
Cumene 70 50 Pass/<LOD Cyclohexane 3,880 1,000 Pass/<LOD
Dichloromethane 600 50 Pass/<LOD Dimethylsulfoxide (DMSO) 5,000 500 Pass/<LOD
Ethanol 5,000 500 Pass/<LOD Ethyl acetate 5,000 50 Pass/<LOD
Ethyl ether 5,000 500 Pass/<LOD Ethylene glycol 620 310 Pass/<LOD
Ethylene oxide 50 50 Pass/<LOD Heptane 5,000 50 Pass/<LOD
Hexane 290 290 Pass/<LOD Isopropyl acetate 5,000 50 Pass/<LOD
Methanol 3,000 500 Pass/<LOD Naptha 400 100 Not Tested
N,N-Dimethylacetamide 1,090 100 Pass/<LOD N,N-Dimethylformamide (DMF) 880 500 Pass/<LOD
Pentane 5,000 50 Pass/<LOD Petroleum Ether 400 100 Not Tested
Propane 5,000 100 Pass/<LOD Pyridine 200 10 Pass/<LOD
Sulfolane 160 200 Pass/<LOD Tetrahydrofuran (THF) 720 200 Pass/<LOD
Toluene 890 50 Pass/<LOD Trichloroethylene 25 5 Not Tested
Xylenes* 2,170 50 Pass/<LOD

Total Butanes = 763 ug/g (PASS); Total Pentanes = 0 ug/g (PASS); Total Hexanes = 0 ug/g (PASS)

* Xylenes are reported as the sum of o-xylene, m-xylene, p-xylene, and ethylbenzene
MRL - Maximum Residue Limit; LOD - Limit of Detection

This sample has not been tested according to OAR 333-007. These results should therefore be used for research and development or quality control purposes only.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 9 of 12

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents QC Report
Testing Accreditation #: 4092-005 Test Certificate #: 132796-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Supreme Ruckus
License: 030-1009646F7F8
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A401030002C949000002383
Metrc Source Pkg#: 1A401030002C949000002342
Test Conditions

Prepsheet ID#: ORHS210824a
Scale: XS205-OR1
Temp: 20.7 °C
Baro PE: 1002 hPa
Analyst: HRM
Technician: JBS
Sample ID#: 132796

Lot #: Supreme Ruckus #1 8.9.2021
Batch #: 132796
Batch Weight (g): 252.6
Harvest/Process Date: 08/09/2021
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 08/24/2021
Test Date: 08/24/2021
Sample #132796
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS Recovery (%) MSD Recovery (%) Relative Percent Difference (%) QC Flag
1,2-Dichloroethane N.D. 0 0 0 nan nan
n-Propane N.D. 250 126 124 50.40 49.60 1.60 LRLR
Isobutane N.D. 250 224 142 89.60 56.80 44.81 LRQ
Methanol N.D. 250 89 85 35.60 34.00 4.60 LRLR
n-Butane N.D. 250 262 165 104.80 66.00 45.43 LRQ
2,2-Dimethylpropane N.D. 250 206 205 82.40 82.00 0.49
Ethanol N.D. 250 317 317 126.80 126.80 0.00
Isopentane N.D. 250 248 261 99.20 104.40 5.11
Acetonitrile N.D. 250 228 235 91.20 94.00 3.02
Diethyl ether N.D. 250 252 258 100.80 103.20 2.35
2-propanone N.D. 250 280 184 112.00 73.60 41.38 Q
2-propanol N.D. 250 213 262 85.20 104.80 20.63 Q
n-Pentane 704.06 250 0 852 0.00 340.80 200.00 LRHRQI
2,2-Dimethylbutane N.D. 250 244 246 97.60 98.40 0.82
2,3-Dimethylbutane N.D. 250 246 250 98.40 100.00 1.61
Methylene chloride N.D. 250 264 263 105.60 105.20 0.38
2-Methylpentane N.D. 250 246 259 98.40 103.60 5.15
3-Methylpentane N.D. 250 248 243 99.20 97.20 2.04
2-Butanol N.D. 250 257 264 102.80 105.60 2.69
n-Hexane N.D. 250 228 233 91.20 93.20 2.17
Ethyl acetate N.D. 250 272 277 108.80 110.80 1.82
Tetrahydrofuran N.D. 250 274 275 0.00 0.00 0.00
Trichloroethylene N.D. 0 0 0 nan nan
Isopropyl acetate N.D. 250 258 257 0.00 0.00 0.00
Benzene N.D. 250 259 264 103.60 105.60 1.91
Chloroform N.D. 0 0 0 nan nan
Cyclohexane N.D. 250 265 268 106.00 107.20 1.13
Ethylene glycol N.D. 250 207 192 82.80 76.80 7.52
Heptane N.D. 250 307 253 122.80 101.20 19.29
2-Ethoxyethanol N.D. 250 393 259 157.20 103.60 41.10 HRQ
1,4-Dioxane N.D. 250 287 291 114.80 116.40 1.38
Pyridine N.D. 0 0 0 0.00 0.00 0.00
Toluene N.D. 250 251 254 100.40 101.60 1.19
Chlorobenzene N.D. 0 0 0 0.00 0.00 0.00
Ethylbenzene N.D. 250 256 259 102.40 103.60 1.17
m-Xylene/p-Xylene N.D. 500 529 527 105.80 105.40 0.38
o-Xylene N.D. 250 296 293 118.40 117.20 1.02
Cumene N.D. 250 283 282 113.20 112.80 0.35
Ethylene oxide N.D. 250 289 414 115.60 165.60 35.56 HRQ

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

N.D. = Not Detected

This sample has not been tested according to OAR 333-007. These results should therefore be used for research and development or quality control purposes only.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 10 of 12

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Homogeneity Report by
High Performance Liquid Chromatography
Testing Accreditation #: 4092-005 Test Certificate #: 132796-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Supreme Ruckus
License: 030-1009646F7F8
Type: AU Tincture
Metrc Test Pkg#: 1A401030002C949000002383
Metrc Source Pkg#: 1A401030002C949000002342
Sample ID#: 132796

Lot #: Supreme Ruckus #1 8.9.2021
Batch #: 132796
Batch Weight (g): 252.6
Harvest/Process Date: 08/09/2021
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 08/24/2021
Sample #132796
Increments Tested (mg/g) TOTAL THC TOTAL CBD THC THCA THCV CBD CBC CBDA CBDV CBG CBN
Increment 1 751.75 43.41 73.99 772.82 N.D. N.D. N.D. 49.50 N.D. 3.57 N.D.
Increment 2 738.36 42.74 73.89 757.66 N.D. N.D. N.D. 48.74 N.D. 3.51 N.D.
Average Value 745.06 43.08 73.94 765.24 N.D. N.D. N.D. 49.12 N.D. 3.54 N.D.
Max Value 751.75 43.41 73.99 772.82 N.D. N.D. N.D. 49.50 N.D. 3.57 N.D.
Min Value 738.36 42.74 73.89 757.66 N.D. N.D. N.D. 48.74 N.D. 3.51 N.D.
Relative Percent Difference (RPD) ±1.80 ±1.55 ±0.14 ±1.98 N.D. N.D. N.D. ±1.55 N.D. ±1.69 N.D.
Average Cannabinoids Per Package 745.06 43.08 73.94 765.24 N.D. N.D. N.D. 49.12 N.D. 3.54 N.D.
Average Cannabinoids Per Serving 37.25 2.15 3.70 38.26 N.D. N.D. N.D. 2.46 N.D. 0.18 N.D.
Max Concentration Per Serving (THC)   Not Applicable
Max Concentration Per Package (THC)   Pass
Relative Percent Difference (RPD)   Pass
Control Study   Yes, MJ1957
Field Duplicate   Pass

N.D. = Not Detected, Min = Minimum, Max = Maximum

RPD is the relative percent difference between increment 1 and increment 2.

RSD is the relative standard deviation between all increments tested.

Total THC and CBD is the calculated sum of CBD or THC and the amount of CBD or THC derived from CBDA or THCA, respectively. These values are calculated by adding a molar correction factor of 0.877 to the CBDA or THCA value.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Terry Rabinowitz Iron laboratories Terry Rabinowitz

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 11 of 12
IRON Laboratories

Terpene Report by
Mass Spectrometer
Test Certificate #: 132796-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Supreme Ruckus
License: 030-1009646F7F8
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A401030002C949000002383
Metrc Source Pkg#: 1A401030002C949000002342

Test Conditions

Scale: XS205-OR1
Temp: 20.7 °C
Baro Pressure: 1002 hPa
Analyst: HRM
Technician: JBS

Sample ID#: 132796

Lot #: Supreme Ruckus #1 8.9.2021
Batch #: 132796
Batch Weight (g): 252.6
Harvest/Process Date: 08/09/2021
Serving Size (g): 0.05
Date Received: 08/24/2021

Sample #132796
Sample #132796
  • α-Pinene (0.09%)
  • β-Ocimene (0.10%)
  • Camphene (0.02%)
  • Eucalyptol (1,8-Cineol) (0.00%)
  • Sabinene (0.00%)
  • γ-Terpinene (0.02%)
  • Myrcene (0.30%)
  • α-Terpinolene (0.03%)
  • β-Pinene (0.24%)
  • Linalool (0.52%)
  • ∆3-Carene (0.00%)
  • Fenchone (0.00%)
  • α-Terpinene (0.02%)
  • endo-Fenchol (0.23%)
  • α-Ocimene (0.00%)
  • Isopulegol (0.00%)
  • Limonene (0.23%)
  • Geraniol (0.00%)
  • p-Cymene (0.00%)
  • β-Caryophyllene (0.14%)
  • α-Humulene (2.79%)
  • Nerolidol 1 (cis) (0.00%)
  • Nerolidol 2 (trans) (0.12%)
  • Guaiol (0.09%)
  • Caryophyllene Oxide (0.17%)
  • α-Bisabolol (0.36%)
  • α-Phellandrene (0.00%)
  • α-Terpineol (0.44%)
  • Valenence (0.28%)

Total: 6.190%

Predominant Terpenes

2.79%   α-Humulene Woody, oceanic-watery, spicy clove 0.52%   Linalool Citrus, floral, sweet, bois de rose, woody, green, blueberry
0.44%   α-Terpineol Pine, woody, lemon, lime, citrus, floral 0.36%   α-Bisabolol Fruity, nutty, coconut
0.30%   Myrcene Peppery, spicy balsam 0.28%   Valenence Sweet, citrus, grapefruit, woody, orange

Value in parenthesis indicates percentage of terpene present in the total sample (weight percentage, wt/wt%).
Value in doughnut slice indicates individual terpene abundance with respect to the total terpenes detected.

This sample has not been tested according to OAR 333-007. These results should therefore be used for research and development or quality control purposes only.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Himashi Mead Iron laboratories Himashi Mead

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 12 of 12