ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Marijuana Potency Analysis by
High Performance Liquid Chromatography

Testing Accreditation #: 4092-005 Test Certificate #: 131491-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Azazel
License: 030-1009646F7F8
Type: Extract
Method: FE04U HPLC-UV
Metrc Test Pkg#: 1A401030002C949000002138
Metrc Source Pkg#: 1A401030002C949000001987

Test Conditions

Prepsheet ID#: ORP210615b
Scale: XS205-OR1
Temp: 22.3 °C
Baro Pressure: 1004 hPa
Analyst: TMR
Technician: TMR

Sample ID#: 131491

Lot #: Azazel #1 5.26.2021
Batch #: 131491
Batch Weight (g): 196.6
Harvest/Process Date: 05/26/2021
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 06/15/2021
Test Date: 06/15/2021

Sample #131491
Sample #131491 Sample #131491
Test
Compounds
THC THCA CBD CBDA CBN CBG CBC THCV* CBDV Total
Cannabinoids*
Total THC Total CBD Calc Max Total
Cannabinoids*
Amount (%) 5.78 82.30 N/D 3.46 N/D 0.37 0.44 N/D N/D 92.35 77.96 3.03 80.99
Amount (mg/g) 57.81 822.99 N/D 34.56 N/D 3.69 4.43 N/D N/D 923.48 779.57 30.31 818.00
Amount per Serving (mg) 2.89 41.15 N\D 1.73 N\D 0.18 0.22 N\D N\D 46.17 Serving Size~ (g): 0.05
LOQ (mg/g) 1.9 1.9 1.9 1.9 1.9 1.9 1.9 1.9 1.9   %Decarb. THC CBD
±%RPD 0.50 0.93 0.58 0.34 0.48 1.29 1.22 +/-5% 0.62 7 0

LOQ = Limit of Quantitation; %RPD = Relative Percent Deviation; %RSD = Relative Standard Deviation; N/D = Not Detected

*Designates values that are not currently included in the accredited scope of Iron Laboratories.

*** Designates tests that use the method FE-45. FE-45 is performed using AOAC 966.02 and 32.004-32.009. FE-45 has relative expanded (k=2) uncertainties of 1.098% for moisture, 1.754% for water activity for unprocessed plant materials, and 13.102% for water activity for infused products. Vitamin E acetate analysis has a relative expanded (k=2) uncertainty of 18.614%.

Total THC and CBD is the calculated sum of THC or CBD and the amount of THC or CBD derived from THCA or CBDA, respectively. These values are calculated by applying a molar correction factor of 0.877 to the THCA or the CBDA value. Calc Max Total Cannabinoids is the sum of Total THC, Total CBD, CBN, CBG, CBC, THCV, and CBDV.

%Decarb. THC and CBD refer to the percentage of THC or CBD relative to THCA or CBDA, respectively.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 1 of 12

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant QC Report

Testing Accreditation #: 4092-005 Test Certificate #: 131491-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Azazel
License: 030-1009646F7F8
Type: Extract
Method: FE04U HPLC-UV
Metrc Test Pkg#: 1A401030002C949000002138
Metrc Source Pkg#: 1A401030002C949000001987

Test Conditions

Prepsheet ID#: ORP210615b
Scale: XS205-OR1
Temp: 22.3 °C
Baro Pressure: 1004 hPa
Analyst: TMR
Technician: TMR

Sample ID#: 131491

Lot #: Azazel #1 5.26.2021
Batch #: 131491
Batch Weight (g): 196.6
Harvest/Process Date: 05/26/2021
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 06/15/2021
Test Date: 06/15/2021

Sample #131491
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Cannabidivarin (CBDV) N.D. 3.20 3.19 99.69 3.21 100.31 0.62
Cannabidiolic Acid (CBDA) N.D. 2.92 2.92 100.00 2.93 100.34 0.34
Cannabigerol (CBG) N.D. 3.89 3.89 100.00 3.84 98.71 1.29
Cannabidiol (CBD) N.D. 3.42 3.41 99.71 3.43 100.29 0.58
Δ9-Tetrahydrocannabivarin (THCV) N.D. 3.84 3.84 100.00 3.84 100.00 0.00
Cannabinol (CBN) N.D. 4.14 4.15 100.24 4.13 99.76 0.48
Δ9-Tetrahydrocannabinol (THC) N.D. 4.02 4.02 100.00 4.00 99.50 0.50
Cannabichromene (CBC) N.D. 4.04 4.06 100.50 4.11 101.73 1.22
Tetrahydrocannabinolic acid (THCA) N.D. 3.22 3.21 99.69 3.24 100.62 0.93

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 2 of 12

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Marijuana Potency Analysis by
High Performance Liquid Chromatography

Testing Accreditation #: 4092-005 Test Certificate #: 131491-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Azazel
License: 030-1009646F7F8
Type: Extract
Method: FE04U HPLC-UV
Metrc Test Pkg#: 1A401030002C949000002138
Metrc Source Pkg#: 1A401030002C949000001987

Test Conditions

Prepsheet ID#: ORP210615b
Scale: XS205-OR1
Temp: 22.3 °C
Baro Pressure: 1004 hPa
Analyst: TMR
Technician: TMR

Sample ID#: 131491

Lot #: Azazel #1 5.26.2021
Batch #: 131491
Batch Weight (g): 196.6
Harvest/Process Date: 05/26/2021
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 06/15/2021
Test Date: 06/15/2021

Sample #131491
Sample #131491 Sample #131491
Test
Compounds
THC THCA CBD CBDA CBN CBG CBC THCV* CBDV Total
Cannabinoids*
Total THC Total CBD Calc Max Total
Cannabinoids*
Amount (%) 5.73 81.52 N/D 3.56 N/D 0.38 0.43 N/D N/D 91.61 77.22 3.12 80.34
Amount (mg/g) 57.26 815.16 N/D 35.62 N/D 3.76 4.32 N/D N/D 916.12 772.16 31.24 811.48
Amount per Serving (mg) 2.86 40.76 N\D 1.78 N\D 0.19 0.22 N\D N\D 45.81 Serving Size~ (g): 0.05
LOQ (mg/g) 1.9 1.9 1.9 1.9 1.9 1.9 1.9 1.9 1.9   %Decarb. THC CBD
±%RPD 0.50 0.93 0.58 0.34 0.48 1.29 1.22 +/-5% 0.62 0

LOQ = Limit of Quantitation; %RPD = Relative Percent Deviation; %RSD = Relative Standard Deviation; N/D = Not Detected

*Designates values that are not currently included in the accredited scope of Iron Laboratories.

*** Designates tests that use the method FE-45. FE-45 is performed using AOAC 966.02 and 32.004-32.009. FE-45 has relative expanded (k=2) uncertainties of 1.098% for moisture, 1.754% for water activity for unprocessed plant materials, and 13.102% for water activity for infused products. Vitamin E acetate analysis has a relative expanded (k=2) uncertainty of 18.614%.

Total THC and CBD is the calculated sum of THC or CBD and the amount of THC or CBD derived from THCA or CBDA, respectively. These values are calculated by applying a molar correction factor of 0.877 to the THCA or the CBDA value. Calc Max Total Cannabinoids is the sum of Total THC, Total CBD, CBN, CBG, CBC, THCV, and CBDV.

%Decarb. THC and CBD refer to the percentage of THC or CBD relative to THCA or CBDA, respectively.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 2 of 12

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant QC Report

Testing Accreditation #: 4092-005 Test Certificate #: 131491-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Azazel
License: 030-1009646F7F8
Type: Extract
Method: FE04U HPLC-UV
Metrc Test Pkg#: 1A401030002C949000002138
Metrc Source Pkg#: 1A401030002C949000001987

Test Conditions

Prepsheet ID#: ORP210615b
Scale: XS205-OR1
Temp: 22.3 °C
Baro Pressure: 1004 hPa
Analyst: TMR
Technician: TMR

Sample ID#: 131491

Lot #: Azazel #1 5.26.2021
Batch #: 131491
Batch Weight (g): 196.6
Harvest/Process Date: 05/26/2021
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 06/15/2021
Test Date: 06/15/2021

Sample #131491
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Cannabidivarin (CBDV) N.D. 3.20 3.19 99.69 3.21 100.31 0.62
Cannabidiolic Acid (CBDA) N.D. 2.92 2.92 100.00 2.93 100.34 0.34
Cannabigerol (CBG) N.D. 3.89 3.89 100.00 3.84 98.71 1.29
Cannabidiol (CBD) N.D. 3.42 3.41 99.71 3.43 100.29 0.58
Δ9-Tetrahydrocannabivarin (THCV) N.D. 3.84 3.84 100.00 3.84 100.00 0.00
Cannabinol (CBN) N.D. 4.14 4.15 100.24 4.13 99.76 0.48
Δ9-Tetrahydrocannabinol (THC) N.D. 4.02 4.02 100.00 4.00 99.50 0.50
Cannabichromene (CBC) N.D. 4.04 4.06 100.50 4.11 101.73 1.22
Tetrahydrocannabinolic acid (THCA) N.D. 3.22 3.21 99.69 3.24 100.62 0.93

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 3 of 12

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Pesticide Analysis by
Mass Spectrometer

Testing Accreditation #: 4092-005 Test Certificate #: 131491-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Azazel
License: 030-1009646F7F8
Type: Extract
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A401030002C949000002138
Metrc Source Pkg#: 1A401030002C949000001987

Test Conditions

Prepsheet ID#: ORPS210622b
Scale: XS205-OR1
Temp: 21.5 °C
Baro PE: 993.1 hPa
Analyst: HRM
Technician: JBS

Sample ID#: 131491

Lot #: Azazel #1 5.26.2021
Batch #: 131491
Batch Weight (g): 196.6
Harvest/Process Date: 05/26/2021
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 06/15/2021
Test Date: 06/22/2021

Sample #131491
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
Aldicarb 0.400 0.112 Pass/<LOD Abamectin**** 0.500 0.112 Pass/<LOD
Acephate 0.400 0.112 Pass/<LOD Acequinocyl 2.000 0.225 Pass/<LOD
Acetamiprid 0.200 0.112 Pass/<LOD Azoxystrobin 0.200 0.112 Pass/<LOD
Bifenazate 0.200 0.112 Pass/<LOD Bifenthrin 0.200 0.112 Pass/<LOD
Boscalid 0.400 0.112 Pass/<LOD Carbaryl 0.200 0.112 Pass/<LOD
Carbofuran 0.200 0.112 Pass/<LOD Chlorantraniliprole 0.200 0.112 Pass/<LOD
Chlorfenapyr 1.000 0.450 Pass/<LOD Chlorpyrifos 0.200 0.112 Pass/<LOD
Clofentezine 0.200 0.112 Pass/<LOD Cyfluthrin** 1.000 0.450 Pass/<LOD
Cypermethrin*** 1.000 0.450 Pass/<LOD Daminozide 1.000 0.112 Pass/<LOD
DDVP (Dichlorvos) 1.000 0.225 Pass/<LOD Diazinon 0.200 0.112 Pass/<LOD
Dimethoate 0.200 0.112 Pass/<LOD Ethoprophos 0.200 0.112 Pass/<LOD
Etofenprox 0.400 0.112 Pass/<LOD Etoxazole 0.200 0.112 Pass/<LOD
Fenoxycarb 0.200 0.112 Pass/<LOD Fenpyroximate 0.400 0.112 Pass/<LOD
Fipronil 0.400 0.112 Pass/<LOD Flonicamid 1.000 0.112 Pass/<LOD
Fludioxonil 0.400 0.112 Pass/<LOD Hexythiazox 1.000 0.112 Pass/<LOD
Imazalil 0.200 0.112 Pass/<LOD Imidacloprid 0.400 0.112 Pass/<LOD
Kresoxim Methyl 0.400 0.112 Pass/<LOD Malathion 0.200 0.112 Pass/<LOD
Metalaxyl 0.200 0.112 Pass/<LOD Methiocarb 0.200 0.112 Pass/<LOD
Methomyl 0.400 0.112 Pass/<LOD Methyl Parathion 0.200 0.112 Pass/<LOD
MGK-264‡ 0.200 0.112 Pass/<LOD Myclobutanil 0.000 0.112 Pass/<LOD
Naled 0.500 0.112 Pass/<LOD Oxamyl 1.000 0.112 Pass/<LOD
Paclobutrazol 0.400 0.112 Pass/<LOD Permethrins† 0.200 0.112 Pass/<LOD
Phosmet 0.200 0.112 Pass/<LOD Piperonyl Butoxide 2.000 0.112 Pass/<LOD
Prallethrin 0.200 0.112 Pass/<LOD Propiconazole 0.400 0.112 Pass/<LOD
Propoxur 0.200 0.112 Pass/<LOD Pyrethrins* 1.000 0.112 Pass/<LOD
Pyridaben 0.200 0.112 Pass/<LOD Spinosad***** 0.200 0.112 Pass/<LOD
Spiromesifen 0.200 0.112 Pass/<LOD Spirotetramat 0.200 0.112 Pass/<LOD
Spiroxamine‡ 0.400 0.112 Pass/<LOD Tebuconazole 0.400 0.112 Pass/<LOD
Thiacloprid 0.200 0.112 Pass/<LOD Thiamethoxam 0.200 0.112 Pass/<LOD
Trifloxystrobin 0.200 0.112 Pass/<LOD

* Pyrethrins are reported as the sum of Jasmolin I, Cinerin I, and Pyrethrin I
** Cyfluthrins are reported as the sum of isomers Cyfluthrin I, II, III, and IV
*** Cypermethrins are reported as the sum of isomers Cypermethrin I, II, III, and IV
**** Abamectin is reported as the sum of Avermectin B1a and Avermectin B1b
***** Spinosad is reported as the sum of Spinosyn A and Spinosyn D
† Permethrin and Prallethrin are reported as the sum of cis and trans isomers
‡ MGK-264 and Spiroximine are reported as the sum of isomers I and II
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 3 of 12

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Pesticide QC Report

Testing Accreditation #: 4092-005 Test Certificate #: 131491-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Azazel
License: 030-1009646F7F8
Type: Extract
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A401030002C949000002138
Metrc Source Pkg#: 1A401030002C949000001987

Test Conditions

Prepsheet ID#: ORPS210622b
Scale: XS205-OR1
Temp: 21.5 °C
Baro PE: 993.1 hPa
Analyst: HRM
Technician: JBS

Sample ID#: 131491

Lot #: Azazel #1 5.26.2021
Batch #: 131491
Batch Weight (g): 196.6
Harvest/Process Date: 05/26/2021
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 06/15/2021
Test Date: 06/22/2021

Sample #131491
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS recovery% MSD recovery% Relative Percent Difference (%) QC Flag
Acephate N.D. 1 0.676 0.867 67.60 86.70 24.76 LR Q
Acequinocyl N.D. 1 0.292 0.432 29.20 43.20 38.67 LR Q
Acetamiprid N.D. 1 1.37 1.55 137.00 155.00 12.33 HR
Aldicarb N.D. 1 1.41 1.3 141.00 130.00 8.12 HR
Avermectin B1a N.D. 0.97 1.86 1.77 191.75 182.47 4.96 HR
Azoxystrobin N.D. 1 1.56 1.66 156.00 166.00 6.21 HR
Bifenazate N.D. 1 0.383 0.384 38.30 38.40 0.26 LR
Bifenthrin N.D. 1 0.735 0.974 73.50 97.40 27.97 Q
Boscalid N.D. 1 0.735 0.963 73.50 96.30 26.86 Q
Carbaryl N.D. 1 1.17 1.33 117.00 133.00 12.80 HR
Carbofuran N.D. 1 1.64 1.79 164.00 179.00 8.75 HR
Chlorantraniliprole N.D. 1 1.4 1.66 140.00 166.00 16.99 HR
Chlorfenapyr N.D. 1 0.512 0.909 51.20 90.90 55.88 LR Q
Chlorpyriphos N.D. 1 0.827 0.855 82.70 85.50 3.33
Clofentezine N.D. 1 0.812 1.07 81.20 107.00 27.42 Q
Cyfluthrin N.D. 1 1.08 1.39 108.00 139.00 25.10 HRQ
Cypermethrin N.D. 1 1.16 1.48 116.00 148.00 24.24 HRQ
Daminoside N.D. 1 0.922 0.814 92.20 81.40 12.44
Diazanon N.D. 1 1.34 1.41 134.00 141.00 5.09 HR
Dichlorvos N.D. 1 1.28 1.75 128.00 175.00 31.02 HRQ
Dimethoate N.D. 1 2.01 1.96 201.00 196.00 2.52 HR
Ethoprophos N.D. 1 1.72 1.63 172.00 163.00 5.37 HR
Etofenprox N.D. 1 0.757 1.11 75.70 111.00 37.81 Q
Etoxazole N.D. 1 1.25 1.18 125.00 118.00 5.76
Fenoxycarb N.D. 1 1.29 1.51 129.00 151.00 15.71 HR
Fenpyroximate N.D. 1 1.26 1.45 126.00 145.00 14.02 HR
Fipronil N.D. 1 1.31 1.24 131.00 124.00 5.49 HR
Flonicamid N.D. 1 1.42 1.78 142.00 178.00 22.50 HRQ
Fludioxonil N.D. 1 1.26 1.19 126.00 119.00 5.71
Hexythiazox N.D. 1 0.54 0.743 54.00 74.30 31.64 LR Q
Imazalil N.D. 1 1.92 1.74 192.00 174.00 9.84 HR
Imidacloprid N.D. 1 1.13 1.58 113.00 158.00 33.21 HRQ
Kresoxim-methyl N.D. 1 1.09 1.25 109.00 125.00 13.68
Malathion N.D. 1 1.25 1.44 125.00 144.00 14.13 HR
Metalaxyl N.D. 1 2 1.89 200.00 189.00 5.66 HR
Methiocarb N.D. 1 1.8 1.85 180.00 185.00 2.74 HR
Methomyl N.D. 1 1.05 1.01 105.00 101.00 3.88
MGK-264 N.D. 1 1.12 1.12 112.00 112.00 0.00
Myclobutanil N.D. 1 1.51 1.77 151.00 177.00 15.85 HR
Naled (dibrom) N.D. 1 1.07 1.22 107.00 122.00 13.10
Oxamyl N.D. 1 2.12 2.05 212.00 205.00 3.36 HR
Paclobutrazol N.D. 1 1.61 1.69 161.00 169.00 4.85 HR
Parathion-methyl N.D. 1 0.925 0.922 92.50 92.20 0.32
Permethrins N.D. 1 0.823 1.149 82.30 114.90 33.06 LRQ
Phosmet N.D. 1 1.14 1.36 114.00 136.00 17.60 HR
Piperonyl butoxide N.D. 1 0.996 1.16 99.60 116.00 15.21
Prallethrin N.D. 1 1.38 1.53 138.00 153.00 10.31 HR
Propiconazole N.D. 1 0.983 1.08 98.30 108.00 9.40
Propoxur N.D. 1 1.16 1.31 116.00 131.00 12.15 HR
Pyrethrin N.D. 0.65 0.68 0.817 104.62 125.69 18.30
Pyridaben N.D. 1 0.883 1.05 88.30 105.00 17.28
SpinosynA N.D. 0.84 1.26 1.34 150.00 159.52 6.15 HR
SpinosynD N.D. 0.16 0.244 0.265 152.50 165.63 8.25 HR
Spiromesifen N.D. 1 1.24 1.22 124.00 122.00 1.63
Spirotetramat N.D. 1 1.28 1.45 128.00 145.00 12.45 HR
Spiroxamine N.D. 1 1.39 1.44 139.00 144.00 3.53 HR
Tebuconazole N.D. 1 1.19 1.19 119.00 119.00 0.00
Thiacloprid N.D. 1 1.6 1.66 160.00 166.00 3.68 HR
Thiamethoxam N.D. 1 1.23 1.51 123.00 151.00 20.44 HRQ
Trifloxystrobin N.D. 1 1.5 1.61 150.00 161.00 7.07 HR

N.D. = Not Detected

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 30%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (60-120%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 4 of 12

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Pesticide Analysis by
Mass Spectrometer

Testing Accreditation #: 4092-005 Test Certificate #: 131491-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Azazel
License: 030-1009646F7F8
Type: Extract
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A401030002C949000002138
Metrc Source Pkg#: 1A401030002C949000001987

Test Conditions

Prepsheet ID#: ORPS210622b
Scale: XS205-OR1
Temp: 21.5 °C
Baro PE: 993.1 hPa
Analyst: HRM
Technician: JBS

Sample ID#: 131491

Lot #: Azazel #1 5.26.2021
Batch #: 131491
Batch Weight (g): 196.6
Harvest/Process Date: 05/26/2021
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 06/15/2021
Test Date: 06/22/2021

Sample #131491
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
Aldicarb 0.400 0.124 Pass/<LOD Abamectin**** 0.500 0.124 Pass/<LOD
Acephate 0.400 0.124 Pass/<LOD Acequinocyl 2.000 0.249 Pass/<LOD
Acetamiprid 0.200 0.124 Pass/<LOD Azoxystrobin 0.200 0.124 Pass/<LOD
Bifenazate 0.200 0.124 Pass/<LOD Bifenthrin 0.200 0.124 Pass/<LOD
Boscalid 0.400 0.124 Pass/<LOD Carbaryl 0.200 0.124 Pass/<LOD
Carbofuran 0.200 0.124 Pass/<LOD Chlorantraniliprole 0.200 0.124 Pass/<LOD
Chlorfenapyr 1.000 0.497 Pass/<LOD Chlorpyrifos 0.200 0.124 Pass/<LOD
Clofentezine 0.200 0.124 Pass/<LOD Cyfluthrin** 1.000 0.497 Pass/<LOD
Cypermethrin*** 1.000 0.497 Pass/<LOD Daminozide 1.000 0.124 Pass/<LOD
DDVP (Dichlorvos) 1.000 0.249 Pass/<LOD Diazinon 0.200 0.124 Pass/<LOD
Dimethoate 0.200 0.124 Pass/<LOD Ethoprophos 0.200 0.124 Pass/<LOD
Etofenprox 0.400 0.124 Pass/<LOD Etoxazole 0.200 0.124 Pass/<LOD
Fenoxycarb 0.200 0.124 Pass/<LOD Fenpyroximate 0.400 0.124 Pass/<LOD
Fipronil 0.400 0.124 Pass/<LOD Flonicamid 1.000 0.124 Pass/<LOD
Fludioxonil 0.400 0.124 Pass/<LOD Hexythiazox 1.000 0.124 Pass/<LOD
Imazalil 0.200 0.124 Pass/<LOD Imidacloprid 0.400 0.124 Pass/<LOD
Kresoxim Methyl 0.400 0.124 Pass/<LOD Malathion 0.200 0.124 Pass/<LOD
Metalaxyl 0.200 0.124 Pass/<LOD Methiocarb 0.200 0.124 Pass/<LOD
Methomyl 0.400 0.124 Pass/<LOD Methyl Parathion 0.200 0.124 Pass/<LOD
MGK-264‡ 0.200 0.124 Pass/<LOD Myclobutanil 0.000 0.124 Pass/<LOD
Naled 0.500 0.124 Pass/<LOD Oxamyl 1.000 0.124 Pass/<LOD
Paclobutrazol 0.400 0.124 Pass/<LOD Permethrins† 0.200 0.124 Pass/<LOD
Phosmet 0.200 0.124 Pass/<LOD Piperonyl Butoxide 2.000 0.124 Pass/<LOD
Prallethrin 0.200 0.124 Pass/<LOD Propiconazole 0.400 0.124 Pass/<LOD
Propoxur 0.200 0.124 Pass/<LOD Pyrethrins* 1.000 0.124 Pass/<LOD
Pyridaben 0.200 0.124 Pass/<LOD Spinosad***** 0.200 0.124 Pass/<LOD
Spiromesifen 0.200 0.124 Pass/<LOD Spirotetramat 0.200 0.124 Pass/<LOD
Spiroxamine‡ 0.400 0.124 Pass/<LOD Tebuconazole 0.400 0.124 Pass/<LOD
Thiacloprid 0.200 0.124 Pass/<LOD Thiamethoxam 0.200 0.124 Pass/<LOD
Trifloxystrobin 0.200 0.124 Pass/<LOD

* Pyrethrins are reported as the sum of Jasmolin I, Cinerin I, and Pyrethrin I
** Cyfluthrins are reported as the sum of isomers Cyfluthrin I, II, III, and IV
*** Cypermethrins are reported as the sum of isomers Cypermethrin I, II, III, and IV
**** Abamectin is reported as the sum of Avermectin B1a and Avermectin B1b
***** Spinosad is reported as the sum of Spinosyn A and Spinosyn D
† Permethrin and Prallethrin are reported as the sum of cis and trans isomers
‡ MGK-264 and Spiroximine are reported as the sum of isomers I and II
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 5 of 12

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Pesticide QC Report

Testing Accreditation #: 4092-005 Test Certificate #: 131491-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Azazel
License: 030-1009646F7F8
Type: Extract
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A401030002C949000002138
Metrc Source Pkg#: 1A401030002C949000001987

Test Conditions

Prepsheet ID#: ORPS210622b
Scale: XS205-OR1
Temp: 21.5 °C
Baro PE: 993.1 hPa
Analyst: HRM
Technician: JBS

Sample ID#: 131491

Lot #: Azazel #1 5.26.2021
Batch #: 131491
Batch Weight (g): 196.6
Harvest/Process Date: 05/26/2021
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 06/15/2021
Test Date: 06/22/2021

Sample #131491
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS recovery% MSD recovery% Relative Percent Difference (%) QC Flag
Acephate N.D. 1 0.676 0.867 67.60 86.70 24.76 LR Q
Acequinocyl N.D. 1 0.292 0.432 29.20 43.20 38.67 LR Q
Acetamiprid N.D. 1 1.37 1.55 137.00 155.00 12.33 HR
Aldicarb N.D. 1 1.41 1.3 141.00 130.00 8.12 HR
Avermectin B1a N.D. 0.97 1.86 1.77 191.75 182.47 4.96 HR
Azoxystrobin N.D. 1 1.56 1.66 156.00 166.00 6.21 HR
Bifenazate N.D. 1 0.383 0.384 38.30 38.40 0.26 LR
Bifenthrin N.D. 1 0.735 0.974 73.50 97.40 27.97 Q
Boscalid N.D. 1 0.735 0.963 73.50 96.30 26.86 Q
Carbaryl N.D. 1 1.17 1.33 117.00 133.00 12.80 HR
Carbofuran N.D. 1 1.64 1.79 164.00 179.00 8.75 HR
Chlorantraniliprole N.D. 1 1.4 1.66 140.00 166.00 16.99 HR
Chlorfenapyr N.D. 1 0.512 0.909 51.20 90.90 55.88 LR Q
Chlorpyriphos N.D. 1 0.827 0.855 82.70 85.50 3.33
Clofentezine N.D. 1 0.812 1.07 81.20 107.00 27.42 Q
Cyfluthrin N.D. 1 1.08 1.39 108.00 139.00 25.10 HRQ
Cypermethrin N.D. 1 1.16 1.48 116.00 148.00 24.24 HRQ
Daminoside N.D. 1 0.922 0.814 92.20 81.40 12.44
Diazanon N.D. 1 1.34 1.41 134.00 141.00 5.09 HR
Dichlorvos N.D. 1 1.28 1.75 128.00 175.00 31.02 HRQ
Dimethoate N.D. 1 2.01 1.96 201.00 196.00 2.52 HR
Ethoprophos N.D. 1 1.72 1.63 172.00 163.00 5.37 HR
Etofenprox N.D. 1 0.757 1.11 75.70 111.00 37.81 Q
Etoxazole N.D. 1 1.25 1.18 125.00 118.00 5.76
Fenoxycarb N.D. 1 1.29 1.51 129.00 151.00 15.71 HR
Fenpyroximate N.D. 1 1.26 1.45 126.00 145.00 14.02 HR
Fipronil N.D. 1 1.31 1.24 131.00 124.00 5.49 HR
Flonicamid N.D. 1 1.42 1.78 142.00 178.00 22.50 HRQ
Fludioxonil N.D. 1 1.26 1.19 126.00 119.00 5.71
Hexythiazox N.D. 1 0.54 0.743 54.00 74.30 31.64 LR Q
Imazalil N.D. 1 1.92 1.74 192.00 174.00 9.84 HR
Imidacloprid N.D. 1 1.13 1.58 113.00 158.00 33.21 HRQ
Kresoxim-methyl N.D. 1 1.09 1.25 109.00 125.00 13.68
Malathion N.D. 1 1.25 1.44 125.00 144.00 14.13 HR
Metalaxyl N.D. 1 2 1.89 200.00 189.00 5.66 HR
Methiocarb N.D. 1 1.8 1.85 180.00 185.00 2.74 HR
Methomyl N.D. 1 1.05 1.01 105.00 101.00 3.88
MGK-264 N.D. 1 1.12 1.12 112.00 112.00 0.00
Myclobutanil N.D. 1 1.51 1.77 151.00 177.00 15.85 HR
Naled (dibrom) N.D. 1 1.07 1.22 107.00 122.00 13.10
Oxamyl N.D. 1 2.12 2.05 212.00 205.00 3.36 HR
Paclobutrazol N.D. 1 1.61 1.69 161.00 169.00 4.85 HR
Parathion-methyl N.D. 1 0.925 0.922 92.50 92.20 0.32
Permethrins N.D. 1 0.823 1.149 82.30 114.90 33.06 LRQ
Phosmet N.D. 1 1.14 1.36 114.00 136.00 17.60 HR
Piperonyl butoxide N.D. 1 0.996 1.16 99.60 116.00 15.21
Prallethrin N.D. 1 1.38 1.53 138.00 153.00 10.31 HR
Propiconazole N.D. 1 0.983 1.08 98.30 108.00 9.40
Propoxur N.D. 1 1.16 1.31 116.00 131.00 12.15 HR
Pyrethrin N.D. 0.65 0.68 0.817 104.62 125.69 18.30
Pyridaben N.D. 1 0.883 1.05 88.30 105.00 17.28
SpinosynA N.D. 0.84 1.26 1.34 150.00 159.52 6.15 HR
SpinosynD N.D. 0.16 0.244 0.265 152.50 165.63 8.25 HR
Spiromesifen N.D. 1 1.24 1.22 124.00 122.00 1.63
Spirotetramat N.D. 1 1.28 1.45 128.00 145.00 12.45 HR
Spiroxamine N.D. 1 1.39 1.44 139.00 144.00 3.53 HR
Tebuconazole N.D. 1 1.19 1.19 119.00 119.00 0.00
Thiacloprid N.D. 1 1.6 1.66 160.00 166.00 3.68 HR
Thiamethoxam N.D. 1 1.23 1.51 123.00 151.00 20.44 HRQ
Trifloxystrobin N.D. 1 1.5 1.61 150.00 161.00 7.07 HR

N.D. = Not Detected

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 30%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (60-120%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 6 of 12

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents Analysis by
Mass Spectrometer

Testing Accreditation #: 4092-005 Test Certificate #: 131491-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Azazel
License: 030-1009646F7F8
Type: Extract
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A401030002C949000002138
Metrc Source Pkg#: 1A401030002C949000001987

Test Conditions

Prepsheet ID#: ORHS210617b
Scale: XS205-OR1
Temp: 22.3 °C
Baro PE: 1004 hPa
Analyst: HRM
Technician: JBS

Sample ID#: 131491

Lot #: Azazel #1 5.26.2021
Batch #: 131491
Batch Weight (g): 196.6
Harvest/Process Date: 05/26/2021
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 06/15/2021
Test Date: 06/17/2021

Sample #131491
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
1,2-Dichloroethane 2 1 Not Tested 1,2-Dimethoxyethane 100 5 Pass/<LOD
1,4-dioxane 380 200 Pass/<LOD 1-Butanol 5,000 100 Pass/<LOD
1-Pentanol 5,000 100 Pass/<LOD 1-Propanol 5,000 100 Pass/<LOD
2,2-Dimethylpropane (Neopentane) 5,000 100 Pass/<LOD 2,2-Dimethylbutane (Hexanes) 290 100 Pass/<LOD
2,3-Dimethylbutane (Hexanes) 290 100 Pass/<LOD 2-Butanol 5,000 100 Pass/<LOD
2-Butanone (MEK) 5,000 50 Pass/<LOD 2-Ethoxyethanol 160 40 Pass/<LOD
2-Methylbutane (Isopentane) 5,000 50 Pass/<LOD 2-Methylpentane (Hexanes) 290 50 Pass/<LOD
2-Methylpropane (Isobutane) 5,000 100 Pass/<LOD 2-propanol (Isopropyl Alcohol) 5,000 50 Pass/<LOD
2-Propanone (Acetone) 5,000 50 Pass/<LOD 3-Methylpentane (Hexanes) 290 50 Pass/<LOD
Acetonitrile 410 100 Pass/<LOD Benzene 2 1 Pass/<LOD
Butane 5,000 100 Pass/180 Chloroform 2 1 Pass/<LOD
Cumene 70 50 Pass/<LOD Cyclohexane 3,880 1,000 Pass/<LOD
Dichloromethane 600 50 Pass/<LOD Dimethylsulfoxide (DMSO) 5,000 500 Pass/<LOD
Ethanol 5,000 500 Pass/<LOD Ethyl acetate 5,000 50 Pass/<LOD
Ethyl ether 5,000 500 Pass/<LOD Ethylene glycol 620 310 Pass/<LOD
Ethylene oxide 50 50 Pass/<LOD Heptane 5,000 50 Pass/<LOD
Hexane 290 290 Pass/<LOD Isopropyl acetate 5,000 50 Pass/<LOD
Methanol 3,000 500 Pass/<LOD Naptha 400 100 Not Tested
N,N-Dimethylacetamide 1,090 100 Pass/<LOD N,N-Dimethylformamide (DMF) 880 500 Pass/<LOD
Pentane 5,000 50 Pass/<LOD Petroleum Ether 400 100 Not Tested
Propane 5,000 100 Pass/<LOD Pyridine 200 10 Pass/<LOD
Sulfolane 160 200 Pass/<LOD Tetrahydrofuran (THF) 720 200 Pass/<LOD
Toluene 890 50 Pass/<LOD Trichloroethylene 25 5 Not Tested
Xylenes* 2,170 50 Pass/<LOD

Total Butanes = 180 ug/g (PASS); Total Pentanes = 0 ug/g (PASS); Total Hexanes = 0 ug/g (PASS)

* Xylenes are reported as the sum of o-xylene, m-xylene, p-xylene, and ethylbenzene
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 7 of 12

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents QC Report

Testing Accreditation #: 4092-005 Test Certificate #: 131491-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Azazel
License: 030-1009646F7F8
Type: Extract
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A401030002C949000002138
Metrc Source Pkg#: 1A401030002C949000001987

Test Conditions

Prepsheet ID#: ORHS210617b
Scale: XS205-OR1
Temp: 22.3 °C
Baro PE: 1004 hPa
Analyst: HRM
Technician: JBS

Sample ID#: 131491

Lot #: Azazel #1 5.26.2021
Batch #: 131491
Batch Weight (g): 196.6
Harvest/Process Date: 05/26/2021
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 06/15/2021
Test Date: 06/17/2021

Sample #131491
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS Recovery (%) MSD Recovery (%) Relative Percent Difference (%) QC Flag
1,2-Dichloroethane N.D. 0 0 0 nan nan
n-Propane N.D. 250 168 161 67.20 64.40 4.26 LR
Isobutane N.D. 250 194 203 77.60 81.20 4.53
Methanol N.D. 250 252 263 100.80 105.20 4.27
n-Butane N.D. 250 219 216 87.60 86.40 1.38
2,2-Dimethylpropane N.D. 250 212 214 84.80 85.60 0.94
Ethanol N.D. 250 248 271 99.20 108.40 8.86
Isopentane N.D. 250 218 224 87.20 89.60 2.71
Acetonitrile N.D. 250 260 283 104.00 113.20 8.47
Diethyl ether N.D. 250 247 255 98.80 102.00 3.19
2-propanone N.D. 250 183 194 73.20 77.60 5.84
2-propanol N.D. 250 0 0 0.00 0.00 LR
n-Pentane N.D. 250 654 723 261.60 289.20 10.02 HR
2,2-Dimethylbutane N.D. 250 230 234 92.00 93.60 1.72
2,3-Dimethylbutane N.D. 250 216 231 86.40 92.40 6.71
Methylene chloride N.D. 250 239 252 95.60 100.80 5.30
2-Methylpentane N.D. 250 234 245 93.60 98.00 4.59
3-Methylpentane N.D. 250 227 248 90.80 99.20 8.84
2-Butanol N.D. 250 249 257 99.60 102.80 3.16
n-Hexane N.D. 250 243 256 97.20 102.40 5.21
Ethyl acetate N.D. 250 249 284 99.60 113.60 13.13
Tetrahydrofuran N.D. 250 261 292 0.00 0.00 0.00
Trichloroethylene N.D. 0 0 0 nan nan
Isopropyl acetate N.D. 250 239 272 0.00 0.00 0.00
Benzene N.D. 250 252 272 100.80 108.80 7.63
Chloroform N.D. 0 0 0 nan nan
Cyclohexane N.D. 250 255 263 102.00 105.20 3.09
Ethylene glycol N.D. 250 234 310 93.60 124.00 27.94 Q
Heptane N.D. 250 428 420 171.20 168.00 1.89 HR
2-Ethoxyethanol N.D. 250 337 304 134.80 121.60 10.30 HR
1,4-Dioxane N.D. 250 282 289 112.80 115.60 2.45
Pyridine N.D. 0 0 0 0.00 0.00 0.00
Toluene N.D. 250 272 281 108.80 112.40 3.25
Chlorobenzene N.D. 0 0 0 0.00 0.00 0.00
Ethylbenzene N.D. 250 263 273 105.20 109.20 3.73
m-Xylene/p-Xylene N.D. 500 539 539 107.80 107.80 0.00
o-Xylene N.D. 250 266 276 106.40 110.40 3.69
Cumene N.D. 250 262 269 104.80 107.60 2.64
Ethylene oxide N.D. 250 234 236 93.60 94.40 0.85

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

N.D. = Not Detected

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 8 of 12

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents Analysis by
Mass Spectrometer

Testing Accreditation #: 4092-005 Test Certificate #: 131491-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Azazel
License: 030-1009646F7F8
Type: Extract
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A401030002C949000002138
Metrc Source Pkg#: 1A401030002C949000001987

Test Conditions

Prepsheet ID#: ORHS210617b
Scale: XS205-OR1
Temp: 22.3 °C
Baro PE: 1004 hPa
Analyst: HRM
Technician: JBS

Sample ID#: 131491

Lot #: Azazel #1 5.26.2021
Batch #: 131491
Batch Weight (g): 196.6
Harvest/Process Date: 05/26/2021
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 06/15/2021
Test Date: 06/17/2021

Sample #131491
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
1,2-Dichloroethane 2 1 Not Tested 1,2-Dimethoxyethane 100 5 Pass/<LOD
1,4-dioxane 380 200 Pass/<LOD 1-Butanol 5,000 100 Pass/<LOD
1-Pentanol 5,000 100 Pass/<LOD 1-Propanol 5,000 100 Pass/<LOD
2,2-Dimethylpropane (Neopentane) 5,000 100 Pass/<LOD 2,2-Dimethylbutane (Hexanes) 290 100 Pass/<LOD
2,3-Dimethylbutane (Hexanes) 290 100 Pass/<LOD 2-Butanol 5,000 100 Pass/<LOD
2-Butanone (MEK) 5,000 50 Pass/<LOD 2-Ethoxyethanol 160 40 Pass/<LOD
2-Methylbutane (Isopentane) 5,000 50 Pass/<LOD 2-Methylpentane (Hexanes) 290 50 Pass/<LOD
2-Methylpropane (Isobutane) 5,000 100 Pass/<LOD 2-propanol (Isopropyl Alcohol) 5,000 50 Pass/<LOD
2-Propanone (Acetone) 5,000 50 Pass/<LOD 3-Methylpentane (Hexanes) 290 50 Pass/<LOD
Acetonitrile 410 100 Pass/<LOD Benzene 2 1 Pass/<LOD
Butane 5,000 100 Pass/226 Chloroform 2 1 Pass/<LOD
Cumene 70 50 Pass/<LOD Cyclohexane 3,880 1,000 Pass/<LOD
Dichloromethane 600 50 Pass/<LOD Dimethylsulfoxide (DMSO) 5,000 500 Pass/<LOD
Ethanol 5,000 500 Pass/<LOD Ethyl acetate 5,000 50 Pass/<LOD
Ethyl ether 5,000 500 Pass/<LOD Ethylene glycol 620 310 Pass/<LOD
Ethylene oxide 50 50 Pass/<LOD Heptane 5,000 50 Pass/<LOD
Hexane 290 290 Pass/<LOD Isopropyl acetate 5,000 50 Pass/<LOD
Methanol 3,000 500 Pass/<LOD Naptha 400 100 Not Tested
N,N-Dimethylacetamide 1,090 100 Pass/<LOD N,N-Dimethylformamide (DMF) 880 500 Pass/<LOD
Pentane 5,000 50 Pass/<LOD Petroleum Ether 400 100 Not Tested
Propane 5,000 100 Pass/<LOD Pyridine 200 10 Pass/<LOD
Sulfolane 160 200 Pass/<LOD Tetrahydrofuran (THF) 720 200 Pass/<LOD
Toluene 890 50 Pass/<LOD Trichloroethylene 25 5 Not Tested
Xylenes* 2,170 50 Pass/<LOD

Total Butanes = 226 ug/g (PASS); Total Pentanes = 0 ug/g (PASS); Total Hexanes = 0 ug/g (PASS)

* Xylenes are reported as the sum of o-xylene, m-xylene, p-xylene, and ethylbenzene
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 9 of 12

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents QC Report

Testing Accreditation #: 4092-005 Test Certificate #: 131491-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Azazel
License: 030-1009646F7F8
Type: Extract
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A401030002C949000002138
Metrc Source Pkg#: 1A401030002C949000001987

Test Conditions

Prepsheet ID#: ORHS210617b
Scale: XS205-OR1
Temp: 22.3 °C
Baro PE: 1004 hPa
Analyst: HRM
Technician: JBS

Sample ID#: 131491

Lot #: Azazel #1 5.26.2021
Batch #: 131491
Batch Weight (g): 196.6
Harvest/Process Date: 05/26/2021
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 06/15/2021
Test Date: 06/17/2021

Sample #131491
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS Recovery (%) MSD Recovery (%) Relative Percent Difference (%) QC Flag
1,2-Dichloroethane N.D. 0 0 0 nan nan
n-Propane N.D. 250 168 161 67.20 64.40 4.26 LR
Isobutane N.D. 250 194 203 77.60 81.20 4.53
Methanol N.D. 250 252 263 100.80 105.20 4.27
n-Butane N.D. 250 219 216 87.60 86.40 1.38
2,2-Dimethylpropane N.D. 250 212 214 84.80 85.60 0.94
Ethanol N.D. 250 248 271 99.20 108.40 8.86
Isopentane N.D. 250 218 224 87.20 89.60 2.71
Acetonitrile N.D. 250 260 283 104.00 113.20 8.47
Diethyl ether N.D. 250 247 255 98.80 102.00 3.19
2-propanone N.D. 250 183 194 73.20 77.60 5.84
2-propanol N.D. 250 0 0 0.00 0.00 LR
n-Pentane N.D. 250 654 723 261.60 289.20 10.02 HR
2,2-Dimethylbutane N.D. 250 230 234 92.00 93.60 1.72
2,3-Dimethylbutane N.D. 250 216 231 86.40 92.40 6.71
Methylene chloride N.D. 250 239 252 95.60 100.80 5.30
2-Methylpentane N.D. 250 234 245 93.60 98.00 4.59
3-Methylpentane N.D. 250 227 248 90.80 99.20 8.84
2-Butanol N.D. 250 249 257 99.60 102.80 3.16
n-Hexane N.D. 250 243 256 97.20 102.40 5.21
Ethyl acetate N.D. 250 249 284 99.60 113.60 13.13
Tetrahydrofuran N.D. 250 261 292 0.00 0.00 0.00
Trichloroethylene N.D. 0 0 0 nan nan
Isopropyl acetate N.D. 250 239 272 0.00 0.00 0.00
Benzene N.D. 250 252 272 100.80 108.80 7.63
Chloroform N.D. 0 0 0 nan nan
Cyclohexane N.D. 250 255 263 102.00 105.20 3.09
Ethylene glycol N.D. 250 234 310 93.60 124.00 27.94 Q
Heptane N.D. 250 428 420 171.20 168.00 1.89 HR
2-Ethoxyethanol N.D. 250 337 304 134.80 121.60 10.30 HR
1,4-Dioxane N.D. 250 282 289 112.80 115.60 2.45
Pyridine N.D. 0 0 0 0.00 0.00 0.00
Toluene N.D. 250 272 281 108.80 112.40 3.25
Chlorobenzene N.D. 0 0 0 0.00 0.00 0.00
Ethylbenzene N.D. 250 263 273 105.20 109.20 3.73
m-Xylene/p-Xylene N.D. 500 539 539 107.80 107.80 0.00
o-Xylene N.D. 250 266 276 106.40 110.40 3.69
Cumene N.D. 250 262 269 104.80 107.60 2.64
Ethylene oxide N.D. 250 234 236 93.60 94.40 0.85

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

N.D. = Not Detected

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

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ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Homogeneity Report by
High Performance Liquid Chromatography

Testing Accreditation #: 4092-005 Test Certificate #: 131491-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Azazel
License: 030-1009646F7F8
Type: Extract
Metrc Test Pkg#: 1A401030002C949000002138
Metrc Source Pkg#: 1A401030002C949000001987

Sample ID#: 131491

Lot #: Azazel #1 5.26.2021
Batch #: 131491
Batch Weight (g): 196.6
Harvest/Process Date: 05/26/2021
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 06/15/2021

Sample #131491
Increments Tested (mg/g) TOTAL THC TOTAL CBD THC THCA THCV CBD CBC CBDA CBDV CBG CBN
Increment 1 779.57 30.31 57.81 822.99 N.D. N.D. 4.43 34.56 N.D. 3.69 N.D.
Increment 2 772.16 31.24 57.26 815.16 N.D. N.D. 4.32 35.62 N.D. 3.76 N.D.
Average Value 775.86 30.77 57.54 819.08 N.D. N.D. 4.38 35.09 N.D. 3.73 N.D.
Max Value 779.57 31.24 57.81 822.99 N.D. N.D. 4.43 35.62 N.D. 3.76 N.D.
Min Value 772.16 30.31 57.26 815.16 N.D. N.D. 4.32 34.56 N.D. 3.69 N.D.
Relative Percent Difference (RPD) ±0.96 ±3.02 ±0.96 ±0.96 N.D. N.D. ±2.51 ±3.02 N.D. ±1.88 N.D.
Average Cannabinoids Per Package 775.86 30.77 57.54 819.08 N.D. N.D. 4.38 35.09 N.D. 3.73 N.D.
Average Cannabinoids Per Serving 38.79 1.54 2.88 40.95 N.D. N.D. 0.22 1.75 N.D. 0.19 N.D.
Max Concentration Per Serving (THC)   Not Applicable
Max Concentration Per Package (THC)   Pass
Relative Percent Difference (RPD)   Pass
Control Study   Yes, MJ1957
Field Duplicate   Pass

N.D. = Not Detected, Min = Minimum, Max = Maximum

RPD is the relative percent difference between increment 1 and increment 2.

RSD is the relative standard deviation between all increments tested.

Total THC and CBD is the calculated sum of CBD or THC and the amount of CBD or THC derived from CBDA or THCA, respectively. These values are calculated by adding a molar correction factor of 0.877 to the CBDA or THCA value.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Terry Rabinowitz Iron laboratories Terry Rabinowitz

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

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IRON Laboratories

Terpene Report by
Mass Spectrometer

Test Certificate #: 131491-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Azazel
License: 030-1009646F7F8
Type: Extract
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A401030002C949000002138
Metrc Source Pkg#: 1A401030002C949000001987

Test Conditions

Scale: XS205-OR1
Temp: 22.3 °C
Baro Pressure: 1004 hPa
Analyst: HRM
Technician: JBS

Sample ID#: 131491

Lot #: Azazel #1 5.26.2021
Batch #: 131491
Batch Weight (g): 196.6
Harvest/Process Date: 05/26/2021
Serving Size (g): 0.05
Date Received: 06/15/2021

Sample #131491
Sample #131491
  • α-Pinene (0.69%)
  • β-Ocimene (0.31%)
  • Camphene (0.10%)
  • Eucalyptol (1,8-Cineol) (0.00%)
  • Sabinene (0.00%)
  • γ-Terpinene (0.13%)
  • Myrcene (0.83%)
  • α-Terpinolene (0.35%)
  • β-Pinene (0.83%)
  • Linalool (0.91%)
  • ∆3-Carene (0.00%)
  • Fenchone (0.00%)
  • α-Terpinene (0.22%)
  • endo-Fenchol (0.35%)
  • α-Ocimene (0.00%)
  • Isopulegol (0.00%)
  • Limonene (0.88%)
  • Geraniol (0.00%)
  • p-Cymene (0.00%)
  • β-Caryophyllene (0.00%)
  • α-Humulene (2.67%)
  • Nerolidol 1 (cis) (0.00%)
  • Nerolidol 2 (trans) (0.06%)
  • Guaiol (0.52%)
  • Caryophyllene Oxide (0.02%)
  • α-Bisabolol (0.00%)
  • α-Phellandrene (1.95%)
  • α-Terpineol (0.70%)
  • Valenence (0.00%)

Total: 11.520%

Predominant Terpenes

2.67%   α-Humulene Woody, oceanic-watery, spicy clove 1.95%   α-Phellandrene Citrus, green, black pepper
0.91%   Linalool Citrus, floral, sweet, bois de rose, woody, green, blueberry 0.88%   Limonene Citrus, orange, sweet
0.83%   β-Pinene Woody, fresh pine, hay 0.83%   Myrcene Peppery, spicy balsam

Value in parenthesis indicates percentage of terpene present in the total sample (weight percentage, wt/wt%).
Value in doughnut slice indicates individual terpene abundance with respect to the total terpenes detected.

This sample has not been tested according to OAR 333-007. These results should therefore be used for research and development or quality control purposes only.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Himashi Mead Iron laboratories Himashi Mead

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

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