ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Marijuana Potency Analysis by
High Performance Liquid Chromatography
Testing Accreditation #: 4092-005 Test Certificate #: 130726-001
Client Name, Sample Details

45th Parallel Farms LLC
Dallas, OR 97338
Sample: Northern Wreck Shake
License: 010-100164183CE
Type: Adult Use Flower
Method: FE04U HPLC-UV
Metrc Test Pkg#: 1A4010300000DAD000003894
Metrc Source Pkg#: 1A4010300000DAD000003893
***Water Activity: 0.516
***Moisture: 10.79%
Test Conditions

Prepsheet ID#: ORP210505a
Scale: XS205-OR1
Temp: 21.5 °C
Baro Pressure: 1001 hPa
Analyst: TMR
Technician: TMR
Sample ID#: 130726

Lot #: Northern Wreck 10-8-20
Batch #: 130726
Batch Weight (g): 6810
Harvest/Process Date: 10/08/2020
Date Received: 05/05/2021
Test Date: 05/05/2021
Sample #130726
Sample #130726 Sample #130726
Test
Compounds		 THC THCA CBD CBDA CBN CBG CBC THCV* CBDV Total
Cannabinoids*		 Total THC Total CBD Calc Max Total
Cannabinoids*
Amount (%) 2.06 31.14 N/D 1.12 N/D 0.22 N/D N/D N/D 34.53 29.37 0.98 30.56
Amount (mg/g) 20.58 311.37 N/D 11.19 N/D 2.17 N/D N/D N/D 345.31 293.65 9.81 305.63
Amount per Serving (mg) N\D N\D N\D N\D N\D N\D N\D N\D N\D 0.00 Serving Size~ (g): 0.00
LOQ (mg/g) 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5   %Decarb. THC CBD
±%RPD 0.79 0.75 0.78 1.83 10.53 0.98 1.60 +/-5% +/-5% 6 0

LOQ = Limit of Quantitation; %RPD = Relative Percent Deviation; %RSD = Relative Standard Deviation; N/D = Not Detected

*Designates values that are not currently included in the accredited scope of Iron Laboratories.

*** Designates tests that use the method FE-45. FE-45 is performed using AOAC 966.02 and 32.004-32.009. FE-45 has relative expanded (k=2) uncertainties of 1.098% for moisture, 1.754% for water activity for unprocessed plant materials, and 13.102% for water activity for infused products. Vitamin E acetate analysis has a relative expanded (k=2) uncertainty of 18.614%.

Total THC and CBD is the calculated sum of THC or CBD and the amount of THC or CBD derived from THCA or CBDA, respectively. These values are calculated by applying a molar correction factor of 0.877 to the THCA or the CBDA value. Calc Max Total Cannabinoids is the sum of Total THC, Total CBD, CBN, CBG, CBC, THCV, and CBDV.

%Decarb. THC and CBD refer to the percentage of THC or CBD relative to THCA or CBDA, respectively.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 1 of 4

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant QC Report
Testing Accreditation #: 4092-005 Test Certificate #: 130726-001
Client Name, Sample Details

45th Parallel Farms LLC
Dallas, OR 97338
Sample: Northern Wreck Shake
License: 010-100164183CE
Type: Adult Use Flower
Method: FE04U HPLC-UV
Metrc Test Pkg#: 1A4010300000DAD000003894
Metrc Source Pkg#: 1A4010300000DAD000003893
***Water Activity: 0.516
***Moisture: 10.79%
Test Conditions

Prepsheet ID#: ORP210505a
Scale: XS205-OR1
Temp: 21.5 °C
Baro Pressure: 1001 hPa
Analyst: TMR
Technician: TMR
Sample ID#: 130726

Lot #: Northern Wreck 10-8-20
Batch #: 130726
Batch Weight (g): 6810
Harvest/Process Date: 10/08/2020
Date Received: 05/05/2021
Test Date: 05/05/2021
Sample #130726
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Cannabidivarin (CBDV) N.D. 1 0 0.00 0 0.00 0
Cannabidiolic Acid (CBDA) N.D. 11.56 11.91 103.03 12.13 104.93 1.83
Cannabigerol (CBG) N.D. 1.09 1.03 94.50 1.02 93.58 0.98
Cannabidiol (CBD) N.D. 6.5 6.43 98.92 6.38 98.15 0.78
Δ9-Tetrahydrocannabivarin (THCV) N.D. 1 0 0.00 0 0.00 0
Cannabinol (CBN) N.D. 0.44 0.2 45.45 0.18 40.91 10.53 LR
Δ9-Tetrahydrocannabinol (THC) N.D. 29.39 30.6 104.12 30.36 103.30 0.79
Cannabichromene (CBC) N.D. 0.65 0.63 96.92 0.62 95.38 1.60
Tetrahydrocannabinolic acid (THCA) N.D. 57.25 60.47 105.62 60.02 104.84 0.75

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 2 of 4

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Pesticide Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-005 Test Certificate #: 130726-001
Client Name, Sample Details

45th Parallel Farms LLC
Dallas, OR 97338
Sample: Northern Wreck Shake
License: 010-100164183CE
Type: Adult Use Flower
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A4010300000DAD000003894
Metrc Source Pkg#: 1A4010300000DAD000003893
Test Conditions

Prepsheet ID#: ORPS210507a
Scale: XS205-OR1
Temp: 22.7 °C
Baro PE: 1011 hPa
Analyst: HRM
Technician: JBS
Sample ID#: 130726

Lot #: Northern Wreck 10-8-20
Batch #: 130726
Batch Weight (g): 6810
Harvest/Process Date: 10/08/2020
Date Received: 05/05/2021
Test Date: 05/07/2021
Sample #130726
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
Aldicarb 0.400 0.124 Pass/<LOD Abamectin**** 0.500 0.124 Pass/<LOD
Acephate 0.400 0.124 Pass/<LOD Acequinocyl 2.000 0.248 Pass/<LOD
Acetamiprid 0.200 0.124 Pass/<LOD Azoxystrobin 0.200 0.124 Pass/<LOD
Bifenazate 0.200 0.124 Pass/<LOD Bifenthrin 0.200 0.124 Pass/<LOD
Boscalid 0.400 0.124 Pass/<LOD Carbaryl 0.200 0.124 Pass/<LOD
Carbofuran 0.200 0.124 Pass/<LOD Chlorantraniliprole 0.200 0.124 Pass/<LOD
Chlorfenapyr 1.000 0.496 Pass/<LOD Chlorpyrifos 0.200 0.124 Pass/<LOD
Clofentezine 0.200 0.124 Pass/<LOD Cyfluthrin** 1.000 0.496 Pass/<LOD
Cypermethrin*** 1.000 0.496 Pass/<LOD Daminozide 1.000 0.124 Pass/<LOD
DDVP (Dichlorvos) 1.000 0.248 Pass/<LOD Diazinon 0.200 0.124 Pass/<LOD
Dimethoate 0.200 0.124 Pass/<LOD Ethoprophos 0.200 0.124 Pass/<LOD
Etofenprox 0.400 0.124 Pass/<LOD Etoxazole 0.200 0.124 Pass/<LOD
Fenoxycarb 0.200 0.124 Pass/<LOD Fenpyroximate 0.400 0.124 Pass/<LOD
Fipronil 0.400 0.124 Pass/<LOD Flonicamid 1.000 0.124 Pass/<LOD
Fludioxonil 0.400 0.124 Pass/<LOD Hexythiazox 1.000 0.124 Pass/<LOD
Imazalil 0.200 0.124 Pass/<LOD Imidacloprid 0.400 0.124 Pass/<LOD
Kresoxim Methyl 0.400 0.124 Pass/<LOD Malathion 0.200 0.124 Pass/<LOD
Metalaxyl 0.200 0.124 Pass/<LOD Methiocarb 0.200 0.124 Pass/<LOD
Methomyl 0.400 0.124 Pass/<LOD Methyl Parathion 0.200 0.124 Pass/<LOD
MGK-264‡ 0.200 0.124 Pass/<LOD Myclobutanil 0.000 0.124 Pass/<LOD
Naled 0.500 0.124 Pass/<LOD Oxamyl 1.000 0.124 Pass/<LOD
Paclobutrazol 0.400 0.124 Pass/<LOD Permethrins† 0.200 0.124 Pass/<LOD
Phosmet 0.200 0.124 Pass/<LOD Piperonyl Butoxide 2.000 0.124 Pass/<LOD
Prallethrin 0.200 0.124 Pass/<LOD Propiconazole 0.400 0.124 Pass/<LOD
Propoxur 0.200 0.124 Pass/<LOD Pyrethrins* 1.000 0.124 Pass/<LOD
Pyridaben 0.200 0.124 Pass/<LOD Spinosad***** 0.200 0.124 Pass/<LOD
Spiromesifen 0.200 0.124 Pass/<LOD Spirotetramat 0.200 0.124 Pass/<LOD
Spiroxamine‡ 0.400 0.124 Pass/<LOD Tebuconazole 0.400 0.124 Pass/<LOD
Thiacloprid 0.200 0.124 Pass/<LOD Thiamethoxam 0.200 0.124 Pass/<LOD
Trifloxystrobin 0.200 0.124 Pass/<LOD

* Pyrethrins are reported as the sum of Jasmolin I, Cinerin I, and Pyrethrin I
** Cyfluthrins are reported as the sum of isomers Cyfluthrin I, II, III, and IV
*** Cypermethrins are reported as the sum of isomers Cypermethrin I, II, III, and IV
**** Abamectin is reported as the sum of Avermectin B1a and Avermectin B1b
***** Spinosad is reported as the sum of Spinosyn A and Spinosyn D
† Permethrin and Prallethrin are reported as the sum of cis and trans isomers
‡ MGK-264 and Spiroximine are reported as the sum of isomers I and II
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 2 of 4

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Pesticide QC Report
Testing Accreditation #: 4092-005 Test Certificate #: 130726-001
Client Name, Sample Details

45th Parallel Farms LLC
Dallas, OR 97338
Sample: Northern Wreck Shake
License: 010-100164183CE
Type: Adult Use Flower
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A4010300000DAD000003894
Metrc Source Pkg#: 1A4010300000DAD000003893
Test Conditions

Prepsheet ID#: ORPS210507a
Scale: XS205-OR1
Temp: 22.7 °C
Baro PE: 1011 hPa
Analyst: HRM
Technician: JBS
Sample ID#: 130726

Lot #: Northern Wreck 10-8-20
Batch #: 130726
Batch Weight (g): 6810
Harvest/Process Date: 10/08/2020
Date Received: 05/05/2021
Test Date: 05/07/2021
Sample #130726
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS recovery% MSD recovery% Relative Percent Difference (%) QC Flag
Acephate N.D. 1 1.29 1.06 129.00 106.00 19.57
Acequinocyl N.D. 1 0.733 0.616 73.30 61.60 17.35 LR
Acetamiprid N.D. 1 1.4 1.45 140.00 145.00 3.51 HR
Aldicarb N.D. 1 1.39 1.45 139.00 145.00 4.23 HR
Avermectin B1a N.D. 0.97 1.4 1.36 144.33 140.21 2.90 HR
Azoxystrobin N.D. 1 1.19 1.14 119.00 114.00 4.29
Bifenazate N.D. 1 1.02 1.03 102.00 103.00 0.98
Bifenthrin N.D. 1 1.11 1.1 111.00 110.00 0.90
Boscalid N.D. 1 0.971 1 97.10 100.00 2.94
Carbaryl N.D. 1 1.27 1.25 127.00 125.00 1.59
Carbofuran N.D. 1 1.29 1.28 129.00 128.00 0.78
Chlorantraniliprole N.D. 1 0.964 0.969 96.40 96.90 0.52
Chlorfenapyr N.D. 1 0.715 0.949 71.50 94.90 28.13 Q
Chlorpyriphos N.D. 1 1.13 1.13 113.00 113.00 0.00
Clofentezine N.D. 1 1.01 0.932 101.00 93.20 8.03
Cyfluthrin N.D. 1 1.22 1.22 122.00 122.00 0.00
Cypermethrin N.D. 1 1.21 1.16 121.00 116.00 4.22
Daminoside N.D. 1 0.275 0.259 27.50 25.90 5.99 LR
Diazanon N.D. 1 32.2 30.1 3,220.00 3,010.00 6.74 HR
Dichlorvos N.D. 1 1.1 0.954 110.00 95.40 14.22
Dimethoate N.D. 1 1.21 1.24 121.00 124.00 2.45
Ethoprophos N.D. 1 0.996 1.09 99.60 109.00 9.01
Etofenprox N.D. 1 1.5 1.45 150.00 145.00 3.39 HR
Etoxazole N.D. 1 1.34 1.37 134.00 137.00 2.21 HR
Fenoxycarb N.D. 1 0.973 1.01 97.30 101.00 3.73
Fenpyroximate N.D. 1 1.54 1.45 154.00 145.00 6.02 HR
Fipronil N.D. 1 1.6 1.56 160.00 156.00 2.53 HR
Flonicamid N.D. 1 1.3 1.21 130.00 121.00 7.17
Fludioxonil N.D. 1 1.77 1.76 177.00 176.00 0.57 HR
Hexythiazox N.D. 1 1.01 0.982 101.00 98.20 2.81
Imazalil N.D. 1 0.96 1.01 96.00 101.00 5.08
Imidacloprid N.D. 1 1.13 1.23 113.00 123.00 8.47
Kresoxim-methyl N.D. 1 0.92 0.873 92.00 87.30 5.24
Malathion N.D. 1 0.912 0.899 91.20 89.90 1.44
Metalaxyl N.D. 1 0.993 1.09 99.30 109.00 9.31
Methiocarb N.D. 1 1.21 1.24 121.00 124.00 2.45
Methomyl N.D. 1 1.08 1.12 108.00 112.00 3.64
MGK-264 N.D. 1 0.94 0.944 94.00 94.40 0.42
Myclobutanil N.D. 1 1.02 1.06 102.00 106.00 3.85
Naled (dibrom) N.D. 1 0.248 0.242 24.80 24.20 2.45 LR
Oxamyl N.D. 1 1.36 1.32 136.00 132.00 2.99 HR
Paclobutrazol N.D. 1 0.973 0.984 97.30 98.40 1.12
Parathion-methyl N.D. 1 1.41 1.28 141.00 128.00 9.67 HR
Permethrins N.D. 1 1.26 1.219 126.00 121.90 3.31
Phosmet N.D. 1 0.974 0.896 97.40 89.60 8.34
Piperonyl butoxide N.D. 1 1.25 1.21 125.00 121.00 3.25
Prallethrin N.D. 1 0.973 0.901 97.30 90.10 7.68
Propiconazole N.D. 1 1.01 0.935 101.00 93.50 7.71
Propoxur N.D. 1 1.44 1.24 144.00 124.00 14.93 HR
Pyrethrin N.D. 0.65 0.539 0.561 82.92 86.31 4.00
Pyridaben N.D. 1 1.47 1.41 147.00 141.00 4.17 HR
SpinosynA N.D. 0.84 0.83 0.79 98.81 94.05 4.94
SpinosynD N.D. 0.16 0.133 0.127 83.13 79.38 4.62
Spiromesifen N.D. 1 0.0822 0.0544 8.22 5.44 40.70 LR Q
Spirotetramat N.D. 1 0.854 0.881 85.40 88.10 3.11
Spiroxamine N.D. 1 0.974 0.962 97.40 96.20 1.24
Tebuconazole N.D. 1 0.898 0.965 89.80 96.50 7.19
Thiacloprid N.D. 1 1.14 1.12 114.00 112.00 1.77
Thiamethoxam N.D. 1 1.01 1.01 101.00 101.00 0.00
Trifloxystrobin N.D. 1 1.35 1.34 135.00 134.00 0.74 HR

N.D. = Not Detected

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 30%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (60-120%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 3 of 4
IRON Laboratories

Terpene Report by
Mass Spectrometer
Test Certificate #: 130726-001
Client Name, Sample Details

45th Parallel Farms LLC
Dallas, OR 97338
Sample: Northern Wreck Shake
License: 010-100164183CE
Type: Adult Use Flower
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A4010300000DAD000003894
Metrc Source Pkg#: 1A4010300000DAD000003893

Test Conditions

Scale: XS205-OR1
Analyst: HRM
Technician: JBS

Sample ID#: 130726

Lot #: Northern Wreck 10-8-20
Batch #: 130726
Batch Weight (g): 6810
Harvest/Process Date: 10/08/2020
Date Received: 05/05/2021

Sample #130726
Sample #130726
  • α-Pinene (0.00%)
  • β-Ocimene (0.05%)
  • Camphene (0.00%)
  • Eucalyptol (1,8-Cineol) (0.00%)
  • Sabinene (0.00%)
  • γ-Terpinene (0.02%)
  • Myrcene (0.16%)
  • α-Terpinolene (0.00%)
  • β-Pinene (0.17%)
  • Linalool (0.32%)
  • ∆3-Carene (0.00%)
  • Fenchone (0.00%)
  • α-Terpinene (0.02%)
  • endo-Fenchol (0.04%)
  • α-Ocimene (0.00%)
  • Isopulegol (0.00%)
  • Limonene (0.10%)
  • Geraniol (0.00%)
  • p-Cymene (0.00%)
  • β-Caryophyllene (0.35%)
  • α-Humulene (1.75%)
  • Nerolidol 1 (cis) (0.00%)
  • Nerolidol 2 (trans) (0.08%)
  • Guaiol (0.90%)
  • Caryophyllene Oxide (0.18%)
  • α-Bisabolol (0.60%)
  • α-Phellandrene (0.02%)
  • α-Terpineol (0.08%)
  • Valenence (0.00%)

Total: 4.840%

Predominant Terpenes

1.75%   α-Humulene Woody, oceanic-watery, spicy clove 0.90%   Guaiol Mild, guaiacwood, tea, rose
0.60%   α-Bisabolol Fruity, nutty, coconut 0.35%   β-Caryophyllene Sweet, woody, spicy, clove
0.32%   Linalool Citrus, floral, sweet, bois de rose, woody, green, blueberry 0.18%   Caryophyllene Oxide Sweet, fresh, woody, spicy

Value in parenthesis indicates percentage of terpene present in the total sample (weight percentage, wt/wt%).
Value in doughnut slice indicates individual terpene abundance with respect to the total terpenes detected.

This sample has not been tested according to OAR 333-007. These results should therefore be used for research and development or quality control purposes only.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Himashi Mead Iron laboratories Himashi Mead

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 4 of 4