ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Marijuana Potency Analysis by
High Performance Liquid Chromatography

Testing Accreditation #: 4092-005 Test Certificate #: 130388-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Food Grade Production Batch #2
License: 030-1009646F7F8
Type: Concentrate
Method: FE04U HPLC-UV
Metrc Test Pkg#: 1A401030002C949000001844
Metrc Source Pkg#: 1A401030002C949000001835

Test Conditions

Prepsheet ID#: ORP210416a
Scale: XS205-OR1
Temp: 22.1 °C
Baro Pressure: 1004 hPa
Analyst: TMR
Technician: TMR

Sample ID#: 130388

Lot #: Food Grade Rosin Batch #1 4.8.2021
Batch #: 130388
Batch Weight (g): 819.9
Harvest/Process Date: 04/08/2021
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 04/14/2021
Test Date: 04/16/2021

Sample #130388
Sample #130388 Sample #130388
Test
Compounds
THC THCA CBD CBDA CBN CBG CBC THCV* CBDV Total
Cannabinoids*
Total THC Total CBD Calc Max Total
Cannabinoids*
Amount (%) 57.12 33.20 N/D 2.30 N/D 1.01 1.04 N/D N/D 94.66 86.24 2.01 88.25
Amount (mg/g) 571.22 331.96 N/D 22.97 N/D 10.09 10.36 N/D N/D 946.6 862.35 20.14 902.94
Amount per Serving (mg) 28.56 16.60 N\D 1.15 N\D 0.50 0.52 N\D N\D 47.33 Serving Size~ (g): 0.05
LOQ (mg/g) 2 2 2 2 2 2 2 2 2   %Decarb. THC CBD
±%RPD 1.50 3.42 0.89 10.76 0.54 0.30 1.09 +/-5% 0.58 63 0

LOQ = Limit of Quantitation; %RPD = Relative Percent Deviation; %RSD = Relative Standard Deviation; N/D = Not Detected

*Designates values that are not currently included in the accredited scope of Iron Laboratories.

*** Designates tests that use the method FE-45. FE-45 is performed using AOAC 966.02 and 32.004-32.009. FE-45 has relative expanded (k=2) uncertainties of 1.098% for moisture, 1.754% for water activity for unprocessed plant materials, and 13.102% for water activity for infused products. Vitamin E acetate analysis has a relative expanded (k=2) uncertainty of 18.614%.

Total THC and CBD is the calculated sum of THC or CBD and the amount of THC or CBD derived from THCA or CBDA, respectively. These values are calculated by applying a molar correction factor of 0.877 to the THCA or the CBDA value. Calc Max Total Cannabinoids is the sum of Total THC, Total CBD, CBN, CBG, CBC, THCV, and CBDV.

%Decarb. THC and CBD refer to the percentage of THC or CBD relative to THCA or CBDA, respectively.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 1 of 8

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant QC Report

Testing Accreditation #: 4092-005 Test Certificate #: 130388-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Food Grade Production Batch #2
License: 030-1009646F7F8
Type: Concentrate
Method: FE04U HPLC-UV
Metrc Test Pkg#: 1A401030002C949000001844
Metrc Source Pkg#: 1A401030002C949000001835

Test Conditions

Prepsheet ID#: ORP210416a
Scale: XS205-OR1
Temp: 22.1 °C
Baro Pressure: 1004 hPa
Analyst: TMR
Technician: TMR

Sample ID#: 130388

Lot #: Food Grade Rosin Batch #1 4.8.2021
Batch #: 130388
Batch Weight (g): 819.9
Harvest/Process Date: 04/08/2021
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 04/14/2021
Test Date: 04/16/2021

Sample #130388
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Cannabidivarin (CBDV) N.D. 3.46 3.46 100.00 3.44 99.42 0.58
Cannabidiolic Acid (CBDA) N.D. 2.94 2.84 96.60 2.55 86.73 10.76
Cannabigerol (CBG) N.D. 3.37 3.36 99.70 3.35 99.41 0.30
Cannabidiol (CBD) N.D. 3.37 3.38 100.30 3.35 99.41 0.89
Δ9-Tetrahydrocannabivarin (THCV) N.D. 3.64 3.61 99.18 3.61 99.18 0.00
Cannabinol (CBN) N.D. 3.68 3.68 100.00 3.66 99.46 0.54
Δ9-Tetrahydrocannabinol (THC) N.D. 3.35 3.35 100.00 3.30 98.51 1.50
Cannabichromene (CBC) N.D. 3.69 3.68 99.73 3.64 98.64 1.09
Tetrahydrocannabinolic acid (THCA) N.D. 3.25 3.27 100.62 3.16 97.23 3.42

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 2 of 8

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Marijuana Potency Analysis by
High Performance Liquid Chromatography

Testing Accreditation #: 4092-005 Test Certificate #: 130388-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Food Grade Production Batch #2
License: 030-1009646F7F8
Type: Concentrate
Method: FE04U HPLC-UV
Metrc Test Pkg#: 1A401030002C949000001844
Metrc Source Pkg#: 1A401030002C949000001835

Test Conditions

Prepsheet ID#: ORP210416a
Scale: XS205-OR1
Temp: 22.1 °C
Baro Pressure: 1004 hPa
Analyst: TMR
Technician: TMR

Sample ID#: 130388

Lot #: Food Grade Rosin Batch #1 4.8.2021
Batch #: 130388
Batch Weight (g): 819.9
Harvest/Process Date: 04/08/2021
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 04/14/2021
Test Date: 04/16/2021

Sample #130388
Sample #130388 Sample #130388
Test
Compounds
THC THCA CBD CBDA CBN CBG CBC THCV* CBDV Total
Cannabinoids*
Total THC Total CBD Calc Max Total
Cannabinoids*
Amount (%) 52.57 31.29 N/D 2.20 N/D 0.95 0.71 N/D N/D 87.72 80.02 1.93 81.95
Amount (mg/g) 525.74 312.90 N/D 22.01 N/D 9.53 7.06 N/D N/D 877.24 800.15 19.30 836.04
Amount per Serving (mg) 26.29 15.65 N\D 1.10 N\D 0.48 0.35 N\D N\D 43.86 Serving Size~ (g): 0.05
LOQ (mg/g) 2 2 2 2 2 2 2 2 2   %Decarb. THC CBD
±%RPD 1.50 3.42 0.89 10.76 0.54 0.30 1.09 +/-5% 0.58 0

LOQ = Limit of Quantitation; %RPD = Relative Percent Deviation; %RSD = Relative Standard Deviation; N/D = Not Detected

*Designates values that are not currently included in the accredited scope of Iron Laboratories.

*** Designates tests that use the method FE-45. FE-45 is performed using AOAC 966.02 and 32.004-32.009. FE-45 has relative expanded (k=2) uncertainties of 1.098% for moisture, 1.754% for water activity for unprocessed plant materials, and 13.102% for water activity for infused products. Vitamin E acetate analysis has a relative expanded (k=2) uncertainty of 18.614%.

Total THC and CBD is the calculated sum of THC or CBD and the amount of THC or CBD derived from THCA or CBDA, respectively. These values are calculated by applying a molar correction factor of 0.877 to the THCA or the CBDA value. Calc Max Total Cannabinoids is the sum of Total THC, Total CBD, CBN, CBG, CBC, THCV, and CBDV.

%Decarb. THC and CBD refer to the percentage of THC or CBD relative to THCA or CBDA, respectively.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 2 of 8

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant QC Report

Testing Accreditation #: 4092-005 Test Certificate #: 130388-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Food Grade Production Batch #2
License: 030-1009646F7F8
Type: Concentrate
Method: FE04U HPLC-UV
Metrc Test Pkg#: 1A401030002C949000001844
Metrc Source Pkg#: 1A401030002C949000001835

Test Conditions

Prepsheet ID#: ORP210416a
Scale: XS205-OR1
Temp: 22.1 °C
Baro Pressure: 1004 hPa
Analyst: TMR
Technician: TMR

Sample ID#: 130388

Lot #: Food Grade Rosin Batch #1 4.8.2021
Batch #: 130388
Batch Weight (g): 819.9
Harvest/Process Date: 04/08/2021
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 04/14/2021
Test Date: 04/16/2021

Sample #130388
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Cannabidivarin (CBDV) N.D. 3.46 3.46 100.00 3.44 99.42 0.58
Cannabidiolic Acid (CBDA) N.D. 2.94 2.84 96.60 2.55 86.73 10.76
Cannabigerol (CBG) N.D. 3.37 3.36 99.70 3.35 99.41 0.30
Cannabidiol (CBD) N.D. 3.37 3.38 100.30 3.35 99.41 0.89
Δ9-Tetrahydrocannabivarin (THCV) N.D. 3.64 3.61 99.18 3.61 99.18 0.00
Cannabinol (CBN) N.D. 3.68 3.68 100.00 3.66 99.46 0.54
Δ9-Tetrahydrocannabinol (THC) N.D. 3.35 3.35 100.00 3.30 98.51 1.50
Cannabichromene (CBC) N.D. 3.69 3.68 99.73 3.64 98.64 1.09
Tetrahydrocannabinolic acid (THCA) N.D. 3.25 3.27 100.62 3.16 97.23 3.42

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 3 of 8

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents Analysis by
Mass Spectrometer

Testing Accreditation #: 4092-005 Test Certificate #: 130388-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Food Grade Production Batch #2
License: 030-1009646F7F8
Type: Concentrate
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A401030002C949000001844
Metrc Source Pkg#: 1A401030002C949000001835

Test Conditions

Prepsheet ID#: ORHS210418b
Scale: XS205-OR1
Analyst: HRM
Technician: JBS

Sample ID#: 130388

Lot #: Food Grade Rosin Batch #1 4.8.2021
Batch #: 130388
Batch Weight (g): 819.9
Harvest/Process Date: 04/08/2021
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 04/14/2021
Test Date: 04/18/2021

Sample #130388
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
1,2-Dichloroethane 2 1 Not Tested 1,2-Dimethoxyethane 100 5 Pass/<LOD
1,4-dioxane 380 200 Pass/<LOD 1-Butanol 5,000 100 Pass/<LOD
1-Pentanol 5,000 100 Pass/<LOD 1-Propanol 5,000 100 Pass/<LOD
2,2-Dimethylpropane (Neopentane) 5,000 100 Pass/<LOD 2,2-Dimethylbutane (Hexanes) 290 100 Pass/<LOD
2,3-Dimethylbutane (Hexanes) 290 100 Pass/<LOD 2-Butanol 5,000 100 Pass/<LOD
2-Butanone (MEK) 5,000 50 Pass/<LOD 2-Ethoxyethanol 160 40 Pass/<LOD
2-Methylbutane (Isopentane) 5,000 50 Pass/<LOD 2-Methylpentane (Hexanes) 290 50 Pass/<LOD
2-Methylpropane (Isobutane) 5,000 100 Pass/<LOD 2-propanol (Isopropyl Alcohol) 5,000 50 Pass/<LOD
2-Propanone (Acetone) 5,000 50 Pass/<LOD 3-Methylpentane (Hexanes) 290 50 Pass/<LOD
Acetonitrile 410 100 Pass/<LOD Benzene 2 1 Pass/<LOD
Butane 5,000 100 Pass/<LOD Chloroform 2 1 Pass/<LOD
Cumene 70 50 Pass/<LOD Cyclohexane 3,880 1,000 Pass/<LOD
Dichloromethane 600 50 Pass/<LOD Dimethylsulfoxide (DMSO) 5,000 500 Pass/<LOD
Ethanol 5,000 500 Pass/<LOD Ethyl acetate 5,000 50 Pass/<LOD
Ethyl ether 5,000 500 Pass/<LOD Ethylene glycol 620 310 Pass/<LOD
Ethylene oxide 50 50 Pass/<LOD Heptane 5,000 50 Pass/<LOD
Hexane 290 290 Pass/<LOD Isopropyl acetate 5,000 50 Pass/<LOD
Methanol 3,000 500 Pass/<LOD Naptha 400 100 Not Tested
N,N-Dimethylacetamide 1,090 100 Pass/<LOD N,N-Dimethylformamide (DMF) 880 500 Pass/<LOD
Pentane 5,000 50 Pass/<LOD Petroleum Ether 400 100 Not Tested
Propane 5,000 100 Pass/<LOD Pyridine 200 10 Pass/<LOD
Sulfolane 160 200 Pass/<LOD Tetrahydrofuran (THF) 720 200 Pass/<LOD
Toluene 890 50 Pass/<LOD Trichloroethylene 25 5 Not Tested
Xylenes* 2,170 50 Pass/<LOD

Total Butanes = 0 ug/g (PASS); Total Pentanes = 0 ug/g (PASS); Total Hexanes = 0 ug/g (PASS)

* Xylenes are reported as the sum of o-xylene, m-xylene, p-xylene, and ethylbenzene
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 3 of 8

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents QC Report

Testing Accreditation #: 4092-005 Test Certificate #: 130388-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Food Grade Production Batch #2
License: 030-1009646F7F8
Type: Concentrate
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A401030002C949000001844
Metrc Source Pkg#: 1A401030002C949000001835

Test Conditions

Prepsheet ID#: ORHS210418b
Scale: XS205-OR1
Analyst: HRM
Technician: JBS

Sample ID#: 130388

Lot #: Food Grade Rosin Batch #1 4.8.2021
Batch #: 130388
Batch Weight (g): 819.9
Harvest/Process Date: 04/08/2021
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 04/14/2021
Test Date: 04/18/2021

Sample #130388
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS Recovery (%) MSD Recovery (%) Relative Percent Difference (%) QC Flag
1,2-Dichloroethane N.D. 0 0 0 nan nan
n-Propane N.D. 250 321 272 128.40 108.80 16.53
Isobutane N.D. 250 294 266 117.60 106.40 10.00
Methanol N.D. 250 278 269 111.20 107.60 3.29
n-Butane N.D. 250 286 278 114.40 111.20 2.84
2,2-Dimethylpropane N.D. 250 283 273 113.20 109.20 3.60
Ethanol N.D. 250 269 255 107.60 102.00 5.34
Isopentane N.D. 250 278 274 111.20 109.60 1.45
Acetonitrile N.D. 250 295 284 118.00 113.60 3.80
Diethyl ether N.D. 250 286 272 114.40 108.80 5.02
2-propanone N.D. 250 306 293 122.40 117.20 4.34
2-propanol N.D. 250 674 411 269.60 164.40 48.48 HRQ
n-Pentane N.D. 250 375 277 150.00 110.80 30.06 HRQ
2,2-Dimethylbutane N.D. 250 279 277 111.60 110.80 0.72
2,3-Dimethylbutane N.D. 250 288 265 115.20 106.00 8.32
Methylene chloride N.D. 250 271 266 108.40 106.40 1.86
2-Methylpentane N.D. 250 273 283 109.20 113.20 3.60
3-Methylpentane N.D. 250 283 283 113.20 113.20 0.00
2-Butanol N.D. 250 264 260 105.60 104.00 1.53
n-Hexane N.D. 250 292 284 116.80 113.60 2.78
Ethyl acetate N.D. 250 262 270 104.80 108.00 3.01
Tetrahydrofuran N.D. 250 269 277 0.00 0.00 0.00
Trichloroethylene N.D. 0 0 0 nan nan
Isopropyl acetate N.D. 250 263 272 0.00 0.00 0.00
Benzene N.D. 250 273 278 109.20 111.20 1.81
Chloroform N.D. 0 0 0 nan nan
Cyclohexane N.D. 250 268 278 107.20 111.20 3.66
Ethylene glycol N.D. 250 263 286 105.20 114.40 8.38
Heptane N.D. 250 290 274 116.00 109.60 5.67
2-Ethoxyethanol N.D. 250 327 259 130.80 103.60 23.21 HRQ
1,4-Dioxane N.D. 250 287 283 114.80 113.20 1.40
Pyridine N.D. 0 0 0 0.00 0.00 0.00
Toluene N.D. 250 275 276 110.00 110.40 0.36
Chlorobenzene N.D. 0 0 0 0.00 0.00 0.00
Ethylbenzene N.D. 250 273 280 109.20 112.00 2.53
m-Xylene/p-Xylene N.D. 500 552 559 110.40 111.80 1.26
o-Xylene N.D. 250 280 284 112.00 113.60 1.42
Cumene N.D. 250 281 284 112.40 113.60 1.06
Ethylene oxide N.D. 250 269 253 107.60 101.20 6.13

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

N.D. = Not Detected

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 4 of 8

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents Analysis by
Mass Spectrometer

Testing Accreditation #: 4092-005 Test Certificate #: 130388-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Food Grade Production Batch #2
License: 030-1009646F7F8
Type: Concentrate
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A401030002C949000001844
Metrc Source Pkg#: 1A401030002C949000001835

Test Conditions

Prepsheet ID#: ORHS210418b
Scale: XS205-OR1
Analyst: HRM
Technician: JBS

Sample ID#: 130388

Lot #: Food Grade Rosin Batch #1 4.8.2021
Batch #: 130388
Batch Weight (g): 819.9
Harvest/Process Date: 04/08/2021
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 04/14/2021
Test Date: 04/18/2021

Sample #130388
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
1,2-Dichloroethane 2 1 Not Tested 1,2-Dimethoxyethane 100 5 Pass/<LOD
1,4-dioxane 380 200 Pass/<LOD 1-Butanol 5,000 100 Pass/<LOD
1-Pentanol 5,000 100 Pass/<LOD 1-Propanol 5,000 100 Pass/<LOD
2,2-Dimethylpropane (Neopentane) 5,000 100 Pass/<LOD 2,2-Dimethylbutane (Hexanes) 290 100 Pass/<LOD
2,3-Dimethylbutane (Hexanes) 290 100 Pass/<LOD 2-Butanol 5,000 100 Pass/<LOD
2-Butanone (MEK) 5,000 50 Pass/<LOD 2-Ethoxyethanol 160 40 Pass/<LOD
2-Methylbutane (Isopentane) 5,000 50 Pass/<LOD 2-Methylpentane (Hexanes) 290 50 Pass/<LOD
2-Methylpropane (Isobutane) 5,000 100 Pass/<LOD 2-propanol (Isopropyl Alcohol) 5,000 50 Pass/<LOD
2-Propanone (Acetone) 5,000 50 Pass/<LOD 3-Methylpentane (Hexanes) 290 50 Pass/<LOD
Acetonitrile 410 100 Pass/<LOD Benzene 2 1 Pass/<LOD
Butane 5,000 100 Pass/<LOD Chloroform 2 1 Pass/<LOD
Cumene 70 50 Pass/<LOD Cyclohexane 3,880 1,000 Pass/<LOD
Dichloromethane 600 50 Pass/<LOD Dimethylsulfoxide (DMSO) 5,000 500 Pass/<LOD
Ethanol 5,000 500 Pass/<LOD Ethyl acetate 5,000 50 Pass/<LOD
Ethyl ether 5,000 500 Pass/<LOD Ethylene glycol 620 310 Pass/<LOD
Ethylene oxide 50 50 Pass/<LOD Heptane 5,000 50 Pass/<LOD
Hexane 290 290 Pass/<LOD Isopropyl acetate 5,000 50 Pass/<LOD
Methanol 3,000 500 Pass/<LOD Naptha 400 100 Not Tested
N,N-Dimethylacetamide 1,090 100 Pass/<LOD N,N-Dimethylformamide (DMF) 880 500 Pass/<LOD
Pentane 5,000 50 Pass/<LOD Petroleum Ether 400 100 Not Tested
Propane 5,000 100 Pass/<LOD Pyridine 200 10 Pass/<LOD
Sulfolane 160 200 Pass/<LOD Tetrahydrofuran (THF) 720 200 Pass/<LOD
Toluene 890 50 Pass/<LOD Trichloroethylene 25 5 Not Tested
Xylenes* 2,170 50 Pass/<LOD

Total Butanes = 0 ug/g (PASS); Total Pentanes = 0 ug/g (PASS); Total Hexanes = 0 ug/g (PASS)

* Xylenes are reported as the sum of o-xylene, m-xylene, p-xylene, and ethylbenzene
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 5 of 8

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents QC Report

Testing Accreditation #: 4092-005 Test Certificate #: 130388-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Food Grade Production Batch #2
License: 030-1009646F7F8
Type: Concentrate
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A401030002C949000001844
Metrc Source Pkg#: 1A401030002C949000001835

Test Conditions

Prepsheet ID#: ORHS210418b
Scale: XS205-OR1
Analyst: HRM
Technician: JBS

Sample ID#: 130388

Lot #: Food Grade Rosin Batch #1 4.8.2021
Batch #: 130388
Batch Weight (g): 819.9
Harvest/Process Date: 04/08/2021
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 04/14/2021
Test Date: 04/18/2021

Sample #130388
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS Recovery (%) MSD Recovery (%) Relative Percent Difference (%) QC Flag
1,2-Dichloroethane N.D. 0 0 0 nan nan
n-Propane N.D. 250 321 272 128.40 108.80 16.53
Isobutane N.D. 250 294 266 117.60 106.40 10.00
Methanol N.D. 250 278 269 111.20 107.60 3.29
n-Butane N.D. 250 286 278 114.40 111.20 2.84
2,2-Dimethylpropane N.D. 250 283 273 113.20 109.20 3.60
Ethanol N.D. 250 269 255 107.60 102.00 5.34
Isopentane N.D. 250 278 274 111.20 109.60 1.45
Acetonitrile N.D. 250 295 284 118.00 113.60 3.80
Diethyl ether N.D. 250 286 272 114.40 108.80 5.02
2-propanone N.D. 250 306 293 122.40 117.20 4.34
2-propanol N.D. 250 674 411 269.60 164.40 48.48 HRQ
n-Pentane N.D. 250 375 277 150.00 110.80 30.06 HRQ
2,2-Dimethylbutane N.D. 250 279 277 111.60 110.80 0.72
2,3-Dimethylbutane N.D. 250 288 265 115.20 106.00 8.32
Methylene chloride N.D. 250 271 266 108.40 106.40 1.86
2-Methylpentane N.D. 250 273 283 109.20 113.20 3.60
3-Methylpentane N.D. 250 283 283 113.20 113.20 0.00
2-Butanol N.D. 250 264 260 105.60 104.00 1.53
n-Hexane N.D. 250 292 284 116.80 113.60 2.78
Ethyl acetate N.D. 250 262 270 104.80 108.00 3.01
Tetrahydrofuran N.D. 250 269 277 0.00 0.00 0.00
Trichloroethylene N.D. 0 0 0 nan nan
Isopropyl acetate N.D. 250 263 272 0.00 0.00 0.00
Benzene N.D. 250 273 278 109.20 111.20 1.81
Chloroform N.D. 0 0 0 nan nan
Cyclohexane N.D. 250 268 278 107.20 111.20 3.66
Ethylene glycol N.D. 250 263 286 105.20 114.40 8.38
Heptane N.D. 250 290 274 116.00 109.60 5.67
2-Ethoxyethanol N.D. 250 327 259 130.80 103.60 23.21 HRQ
1,4-Dioxane N.D. 250 287 283 114.80 113.20 1.40
Pyridine N.D. 0 0 0 0.00 0.00 0.00
Toluene N.D. 250 275 276 110.00 110.40 0.36
Chlorobenzene N.D. 0 0 0 0.00 0.00 0.00
Ethylbenzene N.D. 250 273 280 109.20 112.00 2.53
m-Xylene/p-Xylene N.D. 500 552 559 110.40 111.80 1.26
o-Xylene N.D. 250 280 284 112.00 113.60 1.42
Cumene N.D. 250 281 284 112.40 113.60 1.06
Ethylene oxide N.D. 250 269 253 107.60 101.20 6.13

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

N.D. = Not Detected

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

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ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Homogeneity Report by
High Performance Liquid Chromatography

Testing Accreditation #: 4092-005 Test Certificate #: 130388-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Food Grade Production Batch #2
License: 030-1009646F7F8
Type: Concentrate
Metrc Test Pkg#: 1A401030002C949000001844
Metrc Source Pkg#: 1A401030002C949000001835

Sample ID#: 130388

Lot #: Food Grade Rosin Batch #1 4.8.2021
Batch #: 130388
Batch Weight (g): 819.9
Harvest/Process Date: 04/08/2021
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 04/14/2021

Sample #130388
Increments Tested (mg/g) TOTAL THC TOTAL CBD THC THCA THCV CBD CBC CBDA CBDV CBG CBN
Increment 1 862.35 20.14 571.22 331.96 N.D. N.D. 10.36 22.97 N.D. 10.09 N.D.
Increment 2 800.15 19.30 525.74 312.90 N.D. N.D. 7.06 22.01 N.D. 9.53 N.D.
Average Value 831.25 19.72 548.48 322.43 N.D. N.D. 8.71 22.49 N.D. 9.81 N.D.
Max Value 862.35 20.14 571.22 331.96 N.D. N.D. 10.36 22.97 N.D. 10.09 N.D.
Min Value 800.15 19.30 525.74 312.90 N.D. N.D. 7.06 22.01 N.D. 9.53 N.D.
Relative Percent Difference (RPD) ±7.48 ±4.27 ±8.29 ±5.91 N.D. N.D. ±37.89 ±4.27 N.D. ±5.71 N.D.
Average Cannabinoids Per Package 831.25 19.72 548.48 322.43 N.D. N.D. 8.71 22.49 N.D. 9.81 N.D.
Average Cannabinoids Per Serving 41.56 0.99 27.42 16.12 N.D. N.D. 0.44 1.12 N.D. 0.49 N.D.
Max Concentration Per Serving (THC)   Not Applicable
Max Concentration Per Package (THC)   Pass
Relative Percent Difference (RPD)   Pass
Control Study   Yes, MJ2136
Field Duplicate   Pass

N.D. = Not Detected, Min = Minimum, Max = Maximum

RPD is the relative percent difference between increment 1 and increment 2.

RSD is the relative standard deviation between all increments tested.

Total THC and CBD is the calculated sum of CBD or THC and the amount of CBD or THC derived from CBDA or THCA, respectively. These values are calculated by adding a molar correction factor of 0.877 to the CBDA or THCA value.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Terry Rabinowitz Iron laboratories Terry Rabinowitz

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

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IRON Laboratories

Terpene Report by
Mass Spectrometer

Test Certificate #: 130388-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Food Grade Production Batch #2
License: 030-1009646F7F8
Type: Concentrate
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A401030002C949000001844
Metrc Source Pkg#: 1A401030002C949000001835

Test Conditions

Scale: XS205-OR1
Analyst: HRM
Technician: JBS

Sample ID#: 130388

Lot #: Food Grade Rosin Batch #1 4.8.2021
Batch #: 130388
Batch Weight (g): 819.9
Harvest/Process Date: 04/08/2021
Serving Size (g): 0.05
Date Received: 04/14/2021

Sample #130388
Sample #130388
  • α-Pinene (0.40%)
  • β-Ocimene (0.46%)
  • Camphene (0.07%)
  • Eucalyptol (1,8-Cineol) (0.00%)
  • Sabinene (0.00%)
  • γ-Terpinene (0.05%)
  • Myrcene (0.47%)
  • α-Terpinolene (0.25%)
  • β-Pinene (0.44%)
  • Linalool (0.50%)
  • ∆3-Carene (0.00%)
  • Fenchone (0.02%)
  • α-Terpinene (0.06%)
  • endo-Fenchol (0.26%)
  • α-Ocimene (0.00%)
  • Isopulegol (0.00%)
  • Limonene (0.93%)
  • Geraniol (0.00%)
  • p-Cymene (0.00%)
  • β-Caryophyllene (0.07%)
  • α-Humulene (2.84%)
  • Nerolidol 1 (cis) (0.00%)
  • Nerolidol 2 (trans) (0.05%)
  • Guaiol (0.16%)
  • Caryophyllene Oxide (0.18%)
  • α-Bisabolol (0.26%)
  • α-Phellandrene (0.14%)
  • α-Terpineol (0.35%)
  • Valenence (0.00%)

Total: 7.960%

Predominant Terpenes

2.84%   α-Humulene Woody, oceanic-watery, spicy clove 0.93%   Limonene Citrus, orange, sweet
0.50%   Linalool Citrus, floral, sweet, bois de rose, woody, green, blueberry 0.47%   Myrcene Peppery, spicy balsam
0.46%   β-Ocimene Citrus, tropical, woody, green 0.44%   β-Pinene Woody, fresh pine, hay

Value in parenthesis indicates percentage of terpene present in the total sample (weight percentage, wt/wt%).
Value in doughnut slice indicates individual terpene abundance with respect to the total terpenes detected.

This sample has not been tested according to OAR 333-007. These results should therefore be used for research and development or quality control purposes only.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Himashi Mead Iron laboratories Himashi Mead

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

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