ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Marijuana Potency Analysis by
High Performance Liquid Chromatography
Testing Accreditation #: 4092-005 Test Certificate #: 129768-001
Client Name, Sample Details

Nakd Farms
Cottage Grove, OR 97424
Sample: Viola - Papaya
License: 060-1007418AD59
Type: AU Tincture
Method: FE04U HPLC-UV
Metrc Test Pkg#: 1A4010300011621000007505
Metrc Source Pkg#: 1A4010300011621000007467
Test Conditions

Prepsheet ID#: ORP210318c
Scale: XS205-OR1
Temp: 22.4 °C
Baro Pressure: 1004 hPa
Analyst: TMR
Technician: TMR
Sample ID#: 129768

Lot #: Papaya 1/14/21
Batch #: 129768
Batch Weight (g): 2015
Harvest/Process Date: 01/14/2021
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 03/17/2021
Test Date: 03/18/2021
Sample #129768
Sample #129768 Sample #129768
Test
Compounds		 THC THCA CBD CBDA CBN CBG CBC THCV* CBDV Total
Cannabinoids*		 Total THC Total CBD Calc Max Total
Cannabinoids*
Amount (%) 3.50 77.69 N/D 2.15 N/D 0.59 N/D N/D N/D 83.94 71.64 1.89 74.11
Amount (mg/g) 34.97 776.94 N/D 21.51 N/D 5.93 N/D N/D N/D 839.35 716.35 18.86 741.14
Amount per Serving (mg) 1.75 38.85 N\D 1.08 N\D 0.30 N\D N\D N\D 41.97 Serving Size~ (g): 0.05
LOQ (mg/g) 2 2 2 2 2 2 2 2 2   %Decarb. THC CBD
±%RPD 16.35 8.35 16.94 8.70 12.02 17.24 11.05 11.67 10.92 4 0

LOQ = Limit of Quantitation; %RPD = Relative Percent Deviation; %RSD = Relative Standard Deviation; N/D = Not Detected

*Designates values that are not currently included in the accredited scope of Iron Laboratories.

*** Designates tests that use the method FE-45. FE-45 is performed using AOAC 966.02 and 32.004-32.009. FE-45 has relative expanded (k=2) uncertainties of 1.098% for moisture, 1.754% for water activity for unprocessed plant materials, and 13.102% for water activity for infused products. Vitamin E acetate analysis has a relative expanded (k=2) uncertainty of 18.614%.

Total THC and CBD is the calculated sum of THC or CBD and the amount of THC or CBD derived from THCA or CBDA, respectively. These values are calculated by applying a molar correction factor of 0.877 to the THCA or the CBDA value. Calc Max Total Cannabinoids is the sum of Total THC, Total CBD, CBN, CBG, CBC, THCV, and CBDV.

%Decarb. THC and CBD refer to the percentage of THC or CBD relative to THCA or CBDA, respectively.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 1 of 12

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant QC Report
Testing Accreditation #: 4092-005 Test Certificate #: 129768-001
Client Name, Sample Details

Nakd Farms
Cottage Grove, OR 97424
Sample: Viola - Papaya
License: 060-1007418AD59
Type: AU Tincture
Method: FE04U HPLC-UV
Metrc Test Pkg#: 1A4010300011621000007505
Metrc Source Pkg#: 1A4010300011621000007467
Test Conditions

Prepsheet ID#: ORP210318c
Scale: XS205-OR1
Temp: 22.4 °C
Baro Pressure: 1004 hPa
Analyst: TMR
Technician: TMR
Sample ID#: 129768

Lot #: Papaya 1/14/21
Batch #: 129768
Batch Weight (g): 2015
Harvest/Process Date: 01/14/2021
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 03/17/2021
Test Date: 03/18/2021
Sample #129768
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Cannabidivarin (CBDV) N.D. 4.29 3.55 82.75 3.96 92.31 10.92
Cannabidiolic Acid (CBDA) N.D. 3.29 2.75 83.59 3 91.19 8.70
Cannabigerol (CBG) N.D. 5.53 4.4 79.57 5.23 94.58 17.24
Cannabidiol (CBD) N.D. 5.81 4.81 82.79 5.7 98.11 16.94
Δ9-Tetrahydrocannabivarin (THCV) N.D. 5.7 4.6 80.70 5.17 90.70 11.67
Cannabinol (CBN) N.D. 5.82 4.69 80.58 5.29 90.89 12.02
Δ9-Tetrahydrocannabinol (THC) N.D. 7.16 5.56 77.65 6.55 91.48 16.35
Cannabichromene (CBC) N.D. 6.07 4.96 81.71 5.54 91.27 11.05
Tetrahydrocannabinolic acid (THCA) N.D. 3.57 2.87 80.39 3.12 87.39 8.35

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 2 of 12

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Marijuana Potency Analysis by
High Performance Liquid Chromatography
Testing Accreditation #: 4092-005 Test Certificate #: 129768-001
Client Name, Sample Details

Nakd Farms
Cottage Grove, OR 97424
Sample: Viola - Papaya
License: 060-1007418AD59
Type: AU Tincture
Method: FE04U HPLC-UV
Metrc Test Pkg#: 1A4010300011621000007505
Metrc Source Pkg#: 1A4010300011621000007467
Test Conditions

Prepsheet ID#: ORP210318c
Scale: XS205-OR1
Temp: 22.4 °C
Baro Pressure: 1004 hPa
Analyst: TMR
Technician: TMR
Sample ID#: 129768

Lot #: Papaya 1/14/21
Batch #: 129768
Batch Weight (g): 2015
Harvest/Process Date: 01/14/2021
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 03/17/2021
Test Date: 03/18/2021
Sample #129768
Sample #129768 Sample #129768
Test
Compounds		 THC THCA CBD CBDA CBN CBG CBC THCV* CBDV Total
Cannabinoids*		 Total THC Total CBD Calc Max Total
Cannabinoids*
Amount (%) 3.78 75.76 N/D 2.47 N/D 0.72 N/D N/D N/D 82.74 70.23 2.17 73.12
Amount (mg/g) 37.84 757.60 N/D 24.70 N/D 7.24 N/D N/D N/D 827.38 702.26 21.66 731.16
Amount per Serving (mg) 1.89 37.88 N\D 1.24 N\D 0.36 N\D N\D N\D 41.37 Serving Size~ (g): 0.05
LOQ (mg/g) 1.8 1.8 1.8 1.8 1.8 1.8 1.8 1.8 1.8   %Decarb. THC CBD
±%RPD 16.35 8.35 16.94 8.70 12.02 17.24 11.05 11.67 10.92 0 0

LOQ = Limit of Quantitation; %RPD = Relative Percent Deviation; %RSD = Relative Standard Deviation; N/D = Not Detected

*Designates values that are not currently included in the accredited scope of Iron Laboratories.

*** Designates tests that use the method FE-45. FE-45 is performed using AOAC 966.02 and 32.004-32.009. FE-45 has relative expanded (k=2) uncertainties of 1.098% for moisture, 1.754% for water activity for unprocessed plant materials, and 13.102% for water activity for infused products. Vitamin E acetate analysis has a relative expanded (k=2) uncertainty of 18.614%.

Total THC and CBD is the calculated sum of THC or CBD and the amount of THC or CBD derived from THCA or CBDA, respectively. These values are calculated by applying a molar correction factor of 0.877 to the THCA or the CBDA value. Calc Max Total Cannabinoids is the sum of Total THC, Total CBD, CBN, CBG, CBC, THCV, and CBDV.

%Decarb. THC and CBD refer to the percentage of THC or CBD relative to THCA or CBDA, respectively.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 2 of 12

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant QC Report
Testing Accreditation #: 4092-005 Test Certificate #: 129768-001
Client Name, Sample Details

Nakd Farms
Cottage Grove, OR 97424
Sample: Viola - Papaya
License: 060-1007418AD59
Type: AU Tincture
Method: FE04U HPLC-UV
Metrc Test Pkg#: 1A4010300011621000007505
Metrc Source Pkg#: 1A4010300011621000007467
Test Conditions

Prepsheet ID#: ORP210318c
Scale: XS205-OR1
Temp: 22.4 °C
Baro Pressure: 1004 hPa
Analyst: TMR
Technician: TMR
Sample ID#: 129768

Lot #: Papaya 1/14/21
Batch #: 129768
Batch Weight (g): 2015
Harvest/Process Date: 01/14/2021
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 03/17/2021
Test Date: 03/18/2021
Sample #129768
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Cannabidivarin (CBDV) N.D. 4.29 3.55 82.75 3.96 92.31 10.92
Cannabidiolic Acid (CBDA) N.D. 3.29 2.75 83.59 3 91.19 8.70
Cannabigerol (CBG) N.D. 5.53 4.4 79.57 5.23 94.58 17.24
Cannabidiol (CBD) N.D. 5.81 4.81 82.79 5.7 98.11 16.94
Δ9-Tetrahydrocannabivarin (THCV) N.D. 5.7 4.6 80.70 5.17 90.70 11.67
Cannabinol (CBN) N.D. 5.82 4.69 80.58 5.29 90.89 12.02
Δ9-Tetrahydrocannabinol (THC) N.D. 7.16 5.56 77.65 6.55 91.48 16.35
Cannabichromene (CBC) N.D. 6.07 4.96 81.71 5.54 91.27 11.05
Tetrahydrocannabinolic acid (THCA) N.D. 3.57 2.87 80.39 3.12 87.39 8.35

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 3 of 12

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Pesticide Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-005 Test Certificate #: 129768-001
Client Name, Sample Details

Nakd Farms
Cottage Grove, OR 97424
Sample: Viola - Papaya
License: 060-1007418AD59
Type: AU Tincture
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A4010300011621000007505
Metrc Source Pkg#: 1A4010300011621000007467
Test Conditions

Prepsheet ID#: ORPS210319b
Scale: XS205-OR1
Temp: 21.9 °C
Baro PE: 1002 hPa
Analyst: HRM
Technician: JBS
Sample ID#: 129768

Lot #: Papaya 1/14/21
Batch #: 129768
Batch Weight (g): 2015
Harvest/Process Date: 01/14/2021
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 03/17/2021
Test Date: 03/19/2021
Sample #129768
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
Aldicarb 0.400 0.124 Pass/<LOD Abamectin**** 0.500 0.124 Pass/<LOD
Acephate 0.400 0.124 Pass/<LOD Acequinocyl 2.000 0.249 Pass/<LOD
Acetamiprid 0.200 0.124 Pass/<LOD Azoxystrobin 0.200 0.124 Pass/<LOD
Bifenazate 0.200 0.124 Pass/<LOD Bifenthrin 0.200 0.124 Pass/<LOD
Boscalid 0.400 0.124 Pass/<LOD Carbaryl 0.200 0.124 Pass/<LOD
Carbofuran 0.200 0.124 Pass/<LOD Chlorantraniliprole 0.200 0.124 Pass/<LOD
Chlorfenapyr 1.000 0.497 Pass/<LOD Chlorpyrifos 0.200 0.124 Pass/<LOD
Clofentezine 0.200 0.124 Pass/<LOD Cyfluthrin** 1.000 0.497 Pass/<LOD
Cypermethrin*** 1.000 0.497 Pass/<LOD Daminozide 1.000 0.124 Pass/<LOD
DDVP (Dichlorvos) 1.000 0.249 Pass/<LOD Diazinon 0.200 0.124 Pass/<LOD
Dimethoate 0.200 0.124 Pass/<LOD Ethoprophos 0.200 0.124 Pass/<LOD
Etofenprox 0.400 0.124 Pass/<LOD Etoxazole 0.200 0.124 Pass/<LOD
Fenoxycarb 0.200 0.124 Pass/<LOD Fenpyroximate 0.400 0.124 Pass/<LOD
Fipronil 0.400 0.124 Pass/<LOD Flonicamid 1.000 0.124 Pass/<LOD
Fludioxonil 0.400 0.124 Pass/<LOD Hexythiazox 1.000 0.124 Pass/<LOD
Imazalil 0.200 0.124 Pass/<LOD Imidacloprid 0.400 0.124 Pass/<LOD
Kresoxim Methyl 0.400 0.124 Pass/<LOD Malathion 0.200 0.124 Pass/<LOD
Metalaxyl 0.200 0.124 Pass/<LOD Methiocarb 0.200 0.124 Pass/<LOD
Methomyl 0.400 0.124 Pass/<LOD Methyl Parathion 0.200 0.124 Pass/<LOD
MGK-264‡ 0.200 0.124 Pass/<LOD Myclobutanil 0.000 0.124 Pass/<LOD
Naled 0.500 0.124 Pass/<LOD Oxamyl 1.000 0.124 Pass/<LOD
Paclobutrazol 0.400 0.124 Pass/<LOD Permethrins† 0.200 0.124 Pass/<LOD
Phosmet 0.200 0.124 Pass/<LOD Piperonyl Butoxide 2.000 0.124 Pass/<LOD
Prallethrin 0.200 0.124 Pass/<LOD Propiconazole 0.400 0.124 Pass/<LOD
Propoxur 0.200 0.124 Pass/<LOD Pyrethrins* 1.000 0.124 Pass/<LOD
Pyridaben 0.200 0.124 Pass/<LOD Spinosad***** 0.200 0.124 Pass/<LOD
Spiromesifen 0.200 0.124 Pass/<LOD Spirotetramat 0.200 0.124 Pass/<LOD
Spiroxamine‡ 0.400 0.124 Pass/<LOD Tebuconazole 0.400 0.124 Pass/<LOD
Thiacloprid 0.200 0.124 Pass/<LOD Thiamethoxam 0.200 0.124 Pass/<LOD
Trifloxystrobin 0.200 0.124 Pass/<LOD

* Pyrethrins are reported as the sum of Jasmolin I, Cinerin I, and Pyrethrin I
** Cyfluthrins are reported as the sum of isomers Cyfluthrin I, II, III, and IV
*** Cypermethrins are reported as the sum of isomers Cypermethrin I, II, III, and IV
**** Abamectin is reported as the sum of Avermectin B1a and Avermectin B1b
***** Spinosad is reported as the sum of Spinosyn A and Spinosyn D
† Permethrin and Prallethrin are reported as the sum of cis and trans isomers
‡ MGK-264 and Spiroximine are reported as the sum of isomers I and II
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 3 of 12

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Pesticide QC Report
Testing Accreditation #: 4092-005 Test Certificate #: 129768-001
Client Name, Sample Details

Nakd Farms
Cottage Grove, OR 97424
Sample: Viola - Papaya
License: 060-1007418AD59
Type: AU Tincture
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A4010300011621000007505
Metrc Source Pkg#: 1A4010300011621000007467
Test Conditions

Prepsheet ID#: ORPS210319b
Scale: XS205-OR1
Temp: 21.9 °C
Baro PE: 1002 hPa
Analyst: HRM
Technician: JBS
Sample ID#: 129768

Lot #: Papaya 1/14/21
Batch #: 129768
Batch Weight (g): 2015
Harvest/Process Date: 01/14/2021
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 03/17/2021
Test Date: 03/19/2021
Sample #129768
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS recovery% MSD recovery% Relative Percent Difference (%) QC Flag
Acephate N.D. 1 1.83 1.97 183.00 197.00 7.37 HR
Acequinocyl N.D. 1 0.277 0.376 27.70 37.60 30.32 LR Q
Acetamiprid N.D. 1 1.36 1.4 136.00 140.00 2.90 HR
Aldicarb N.D. 1 1.93 1.89 193.00 189.00 2.09 HR
Avermectin B1a N.D. 0.97 7.8 8.9 804.12 917.53 13.17 HR
Azoxystrobin N.D. 1 1.45 1.53 145.00 153.00 5.37 HR
Bifenazate N.D. 1 0.917 0.939 91.70 93.90 2.37
Bifenthrin N.D. 1 3.93 6.92 393.00 692.00 55.12 HRQ
Boscalid N.D. 1 1.12 1.17 112.00 117.00 4.37
Carbaryl N.D. 1 1.34 1.35 134.00 135.00 0.74 HR
Carbofuran N.D. 1 1.54 1.55 154.00 155.00 0.65 HR
Chlorantraniliprole N.D. 1 2.27 2.32 227.00 232.00 2.18 HR
Chlorfenapyr N.D. 1 0.925 1.02 92.50 102.00 9.77
Chlorpyriphos N.D. 1 0.929 1.02 92.90 102.00 9.34
Clofentezine N.D. 1 1.56 1.81 156.00 181.00 14.84 HR
Cyfluthrin N.D. 1 1.86 2.01 186.00 201.00 7.75 HR
Cypermethrin N.D. 1 1.39 1.51 139.00 151.00 8.28 HR
Daminoside N.D. 1 0.474 0.512 47.40 51.20 7.71 LR
Diazanon N.D. 1 19.2 19.2 1,920.00 1,920.00 0.00 HR
Dichlorvos N.D. 1 3.85 3.54 385.00 354.00 8.39 HR
Dimethoate N.D. 1 1.63 1.52 163.00 152.00 6.98 HR
Ethoprophos N.D. 1 1.43 1.44 143.00 144.00 0.70 HR
Etofenprox N.D. 1 0.838 0.94 83.80 94.00 11.47
Etoxazole N.D. 1 1.31 1.26 131.00 126.00 3.89 HR
Fenoxycarb N.D. 1 1.79 1.93 179.00 193.00 7.53 HR
Fenpyroximate N.D. 1 1.32 1.44 132.00 144.00 8.70 HR
Fipronil N.D. 1 1.39 1.4 139.00 140.00 0.72 HR
Flonicamid N.D. 1 1.96 1.95 196.00 195.00 0.51 HR
Fludioxonil N.D. 1 1.5 1.5 150.00 150.00 0.00 HR
Hexythiazox N.D. 1 0.866 0.964 86.60 96.40 10.71
Imazalil N.D. 1 1.88 1.98 188.00 198.00 5.18 HR
Imidacloprid N.D. 1 1.69 1.64 169.00 164.00 3.00 HR
Kresoxim-methyl N.D. 1 2.04 2.08 204.00 208.00 1.94 HR
Malathion N.D. 1 2.28 2.56 228.00 256.00 11.57 HR
Metalaxyl N.D. 1 2.55 2.57 255.00 257.00 0.78 HR
Methiocarb N.D. 1 1.49 1.55 149.00 155.00 3.95 HR
Methomyl N.D. 1 2.85 2.86 285.00 286.00 0.35 HR
MGK-264 N.D. 1 1.17 1.25 117.00 125.00 6.61
Myclobutanil N.D. 1 1.57 1.61 157.00 161.00 2.52 HR
Naled (dibrom) N.D. 1 0.645 0.651 64.50 65.10 0.93 LR
Oxamyl N.D. 1 3.14 3.03 314.00 303.00 3.57 HR
Paclobutrazol N.D. 1 2.03 2.04 203.00 204.00 0.49 HR
Parathion-methyl N.D. 1 1.21 1.2 121.00 120.00 0.83
Permethrins N.D. 1 4.914 6.73 491.40 673.00 31.19 HR Q
Phosmet N.D. 1 1.68 1.77 168.00 177.00 5.22 HR
Piperonyl butoxide N.D. 1 1.08 1.13 108.00 113.00 4.52
Prallethrin N.D. 1 1.9 1.93 190.00 193.00 1.57 HR
Propiconazole N.D. 1 1.47 1.51 147.00 151.00 2.68 HR
Propoxur N.D. 1 1.42 1.43 142.00 143.00 0.70 HR
Pyrethrin N.D. 0.65 0.805 0.876 123.85 134.77 8.45 HR
Pyridaben N.D. 1 2.07 2.61 207.00 261.00 23.08 HR Q
SpinosynA N.D. 0.84 1.81 1.9 215.48 226.19 4.85 HR
SpinosynD N.D. 0.16 0.384 0.4 240.00 250.00 4.08 HR
Spiromesifen N.D. 1 0.101 0.108 10.10 10.80 6.70 LR
Spirotetramat N.D. 1 1.26 1.3 126.00 130.00 3.13
Spiroxamine N.D. 1 2.92 2.8 292.00 280.00 4.20 HR
Tebuconazole N.D. 1 2.33 2.39 233.00 239.00 2.54 HR
Thiacloprid N.D. 1 1.68 1.63 168.00 163.00 3.02 HR
Thiamethoxam N.D. 1 2.22 2.1 222.00 210.00 5.56 HR
Trifloxystrobin N.D. 1 1.38 1.43 138.00 143.00 3.56 HR

N.D. = Not Detected

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 30%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (60-120%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 4 of 12

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Pesticide Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-005 Test Certificate #: 129768-001
Client Name, Sample Details

Nakd Farms
Cottage Grove, OR 97424
Sample: Viola - Papaya
License: 060-1007418AD59
Type: AU Tincture
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A4010300011621000007505
Metrc Source Pkg#: 1A4010300011621000007467
Test Conditions

Prepsheet ID#: ORPS210319b
Scale: XS205-OR1
Temp: 21.9 °C
Baro PE: 1002 hPa
Analyst: HRM
Technician: JBS
Sample ID#: 129768

Lot #: Papaya 1/14/21
Batch #: 129768
Batch Weight (g): 2015
Harvest/Process Date: 01/14/2021
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 03/17/2021
Test Date: 03/19/2021
Sample #129768
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
Aldicarb 0.400 0.121 Pass/<LOD Abamectin**** 0.500 0.121 Pass/<LOD
Acephate 0.400 0.121 Pass/<LOD Acequinocyl 2.000 0.243 Pass/<LOD
Acetamiprid 0.200 0.121 Pass/<LOD Azoxystrobin 0.200 0.121 Pass/<LOD
Bifenazate 0.200 0.121 Pass/<LOD Bifenthrin 0.200 0.121 Pass/<LOD
Boscalid 0.400 0.121 Pass/<LOD Carbaryl 0.200 0.121 Pass/<LOD
Carbofuran 0.200 0.121 Pass/<LOD Chlorantraniliprole 0.200 0.121 Pass/<LOD
Chlorfenapyr 1.000 0.485 Pass/<LOD Chlorpyrifos 0.200 0.121 Pass/<LOD
Clofentezine 0.200 0.121 Pass/<LOD Cyfluthrin** 1.000 0.485 Pass/<LOD
Cypermethrin*** 1.000 0.485 Pass/<LOD Daminozide 1.000 0.121 Pass/<LOD
DDVP (Dichlorvos) 1.000 0.243 Pass/<LOD Diazinon 0.200 0.121 Pass/<LOD
Dimethoate 0.200 0.121 Pass/<LOD Ethoprophos 0.200 0.121 Pass/<LOD
Etofenprox 0.400 0.121 Pass/<LOD Etoxazole 0.200 0.121 Pass/<LOD
Fenoxycarb 0.200 0.121 Pass/<LOD Fenpyroximate 0.400 0.121 Pass/<LOD
Fipronil 0.400 0.121 Pass/<LOD Flonicamid 1.000 0.121 Pass/<LOD
Fludioxonil 0.400 0.121 Pass/<LOD Hexythiazox 1.000 0.121 Pass/<LOD
Imazalil 0.200 0.121 Pass/<LOD Imidacloprid 0.400 0.121 Pass/<LOD
Kresoxim Methyl 0.400 0.121 Pass/<LOD Malathion 0.200 0.121 Pass/<LOD
Metalaxyl 0.200 0.121 Pass/<LOD Methiocarb 0.200 0.121 Pass/<LOD
Methomyl 0.400 0.121 Pass/<LOD Methyl Parathion 0.200 0.121 Pass/<LOD
MGK-264‡ 0.200 0.121 Pass/<LOD Myclobutanil 0.000 0.121 Pass/<LOD
Naled 0.500 0.121 Pass/<LOD Oxamyl 1.000 0.121 Pass/<LOD
Paclobutrazol 0.400 0.121 Pass/<LOD Permethrins† 0.200 0.121 Pass/<LOD
Phosmet 0.200 0.121 Pass/<LOD Piperonyl Butoxide 2.000 0.121 Pass/<LOD
Prallethrin 0.200 0.121 Pass/<LOD Propiconazole 0.400 0.121 Pass/<LOD
Propoxur 0.200 0.121 Pass/<LOD Pyrethrins* 1.000 0.121 Pass/<LOD
Pyridaben 0.200 0.121 Pass/<LOD Spinosad***** 0.200 0.121 Pass/<LOD
Spiromesifen 0.200 0.121 Pass/<LOD Spirotetramat 0.200 0.121 Pass/<LOD
Spiroxamine‡ 0.400 0.121 Pass/<LOD Tebuconazole 0.400 0.121 Pass/<LOD
Thiacloprid 0.200 0.121 Pass/<LOD Thiamethoxam 0.200 0.121 Pass/<LOD
Trifloxystrobin 0.200 0.121 Pass/<LOD

* Pyrethrins are reported as the sum of Jasmolin I, Cinerin I, and Pyrethrin I
** Cyfluthrins are reported as the sum of isomers Cyfluthrin I, II, III, and IV
*** Cypermethrins are reported as the sum of isomers Cypermethrin I, II, III, and IV
**** Abamectin is reported as the sum of Avermectin B1a and Avermectin B1b
***** Spinosad is reported as the sum of Spinosyn A and Spinosyn D
† Permethrin and Prallethrin are reported as the sum of cis and trans isomers
‡ MGK-264 and Spiroximine are reported as the sum of isomers I and II
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 5 of 12

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Pesticide QC Report
Testing Accreditation #: 4092-005 Test Certificate #: 129768-001
Client Name, Sample Details

Nakd Farms
Cottage Grove, OR 97424
Sample: Viola - Papaya
License: 060-1007418AD59
Type: AU Tincture
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A4010300011621000007505
Metrc Source Pkg#: 1A4010300011621000007467
Test Conditions

Prepsheet ID#: ORPS210319b
Scale: XS205-OR1
Temp: 21.9 °C
Baro PE: 1002 hPa
Analyst: HRM
Technician: JBS
Sample ID#: 129768

Lot #: Papaya 1/14/21
Batch #: 129768
Batch Weight (g): 2015
Harvest/Process Date: 01/14/2021
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 03/17/2021
Test Date: 03/19/2021
Sample #129768
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS recovery% MSD recovery% Relative Percent Difference (%) QC Flag
Acephate N.D. 1 1.83 1.97 183.00 197.00 7.37 HR
Acequinocyl N.D. 1 0.277 0.376 27.70 37.60 30.32 LR Q
Acetamiprid N.D. 1 1.36 1.4 136.00 140.00 2.90 HR
Aldicarb N.D. 1 1.93 1.89 193.00 189.00 2.09 HR
Avermectin B1a N.D. 0.97 7.8 8.9 804.12 917.53 13.17 HR
Azoxystrobin N.D. 1 1.45 1.53 145.00 153.00 5.37 HR
Bifenazate N.D. 1 0.917 0.939 91.70 93.90 2.37
Bifenthrin N.D. 1 3.93 6.92 393.00 692.00 55.12 HRQ
Boscalid N.D. 1 1.12 1.17 112.00 117.00 4.37
Carbaryl N.D. 1 1.34 1.35 134.00 135.00 0.74 HR
Carbofuran N.D. 1 1.54 1.55 154.00 155.00 0.65 HR
Chlorantraniliprole N.D. 1 2.27 2.32 227.00 232.00 2.18 HR
Chlorfenapyr N.D. 1 0.925 1.02 92.50 102.00 9.77
Chlorpyriphos N.D. 1 0.929 1.02 92.90 102.00 9.34
Clofentezine N.D. 1 1.56 1.81 156.00 181.00 14.84 HR
Cyfluthrin N.D. 1 1.86 2.01 186.00 201.00 7.75 HR
Cypermethrin N.D. 1 1.39 1.51 139.00 151.00 8.28 HR
Daminoside N.D. 1 0.474 0.512 47.40 51.20 7.71 LR
Diazanon N.D. 1 19.2 19.2 1,920.00 1,920.00 0.00 HR
Dichlorvos N.D. 1 3.85 3.54 385.00 354.00 8.39 HR
Dimethoate N.D. 1 1.63 1.52 163.00 152.00 6.98 HR
Ethoprophos N.D. 1 1.43 1.44 143.00 144.00 0.70 HR
Etofenprox N.D. 1 0.838 0.94 83.80 94.00 11.47
Etoxazole N.D. 1 1.31 1.26 131.00 126.00 3.89 HR
Fenoxycarb N.D. 1 1.79 1.93 179.00 193.00 7.53 HR
Fenpyroximate N.D. 1 1.32 1.44 132.00 144.00 8.70 HR
Fipronil N.D. 1 1.39 1.4 139.00 140.00 0.72 HR
Flonicamid N.D. 1 1.96 1.95 196.00 195.00 0.51 HR
Fludioxonil N.D. 1 1.5 1.5 150.00 150.00 0.00 HR
Hexythiazox N.D. 1 0.866 0.964 86.60 96.40 10.71
Imazalil N.D. 1 1.88 1.98 188.00 198.00 5.18 HR
Imidacloprid N.D. 1 1.69 1.64 169.00 164.00 3.00 HR
Kresoxim-methyl N.D. 1 2.04 2.08 204.00 208.00 1.94 HR
Malathion N.D. 1 2.28 2.56 228.00 256.00 11.57 HR
Metalaxyl N.D. 1 2.55 2.57 255.00 257.00 0.78 HR
Methiocarb N.D. 1 1.49 1.55 149.00 155.00 3.95 HR
Methomyl N.D. 1 2.85 2.86 285.00 286.00 0.35 HR
MGK-264 N.D. 1 1.17 1.25 117.00 125.00 6.61
Myclobutanil N.D. 1 1.57 1.61 157.00 161.00 2.52 HR
Naled (dibrom) N.D. 1 0.645 0.651 64.50 65.10 0.93 LR
Oxamyl N.D. 1 3.14 3.03 314.00 303.00 3.57 HR
Paclobutrazol N.D. 1 2.03 2.04 203.00 204.00 0.49 HR
Parathion-methyl N.D. 1 1.21 1.2 121.00 120.00 0.83
Permethrins N.D. 1 4.914 6.73 491.40 673.00 31.19 HR Q
Phosmet N.D. 1 1.68 1.77 168.00 177.00 5.22 HR
Piperonyl butoxide N.D. 1 1.08 1.13 108.00 113.00 4.52
Prallethrin N.D. 1 1.9 1.93 190.00 193.00 1.57 HR
Propiconazole N.D. 1 1.47 1.51 147.00 151.00 2.68 HR
Propoxur N.D. 1 1.42 1.43 142.00 143.00 0.70 HR
Pyrethrin N.D. 0.65 0.805 0.876 123.85 134.77 8.45 HR
Pyridaben N.D. 1 2.07 2.61 207.00 261.00 23.08 HR Q
SpinosynA N.D. 0.84 1.81 1.9 215.48 226.19 4.85 HR
SpinosynD N.D. 0.16 0.384 0.4 240.00 250.00 4.08 HR
Spiromesifen N.D. 1 0.101 0.108 10.10 10.80 6.70 LR
Spirotetramat N.D. 1 1.26 1.3 126.00 130.00 3.13
Spiroxamine N.D. 1 2.92 2.8 292.00 280.00 4.20 HR
Tebuconazole N.D. 1 2.33 2.39 233.00 239.00 2.54 HR
Thiacloprid N.D. 1 1.68 1.63 168.00 163.00 3.02 HR
Thiamethoxam N.D. 1 2.22 2.1 222.00 210.00 5.56 HR
Trifloxystrobin N.D. 1 1.38 1.43 138.00 143.00 3.56 HR

N.D. = Not Detected

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 30%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (60-120%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 6 of 12

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-005 Test Certificate #: 129768-001
Client Name, Sample Details

Nakd Farms
Cottage Grove, OR 97424
Sample: Viola - Papaya
License: 060-1007418AD59
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A4010300011621000007505
Metrc Source Pkg#: 1A4010300011621000007467
Test Conditions

Prepsheet ID#: ORHS210317c
Scale: XS205-OR1
Temp: 22.1 °C
Baro PE: 1012 hPa
Analyst: HRM
Technician: JBS
Sample ID#: 129768

Lot #: Papaya 1/14/21
Batch #: 129768
Batch Weight (g): 2015
Harvest/Process Date: 01/14/2021
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 03/17/2021
Test Date: 03/17/2021
Sample #129768
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
1,2-Dichloroethane 2 1 Not Tested 1,2-Dimethoxyethane 100 5 Pass/<LOD
1,4-dioxane 380 200 Pass/<LOD 1-Butanol 5,000 100 Pass/<LOD
1-Pentanol 5,000 100 Pass/<LOD 1-Propanol 5,000 100 Pass/<LOD
2,2-Dimethylpropane (Neopentane) 5,000 100 Pass/<LOD 2,2-Dimethylbutane (Hexanes) 290 100 Pass/<LOD
2,3-Dimethylbutane (Hexanes) 290 100 Pass/<LOD 2-Butanol 5,000 100 Pass/<LOD
2-Butanone (MEK) 5,000 50 Pass/<LOD 2-Ethoxyethanol 160 40 Pass/<LOD
2-Methylbutane (Isopentane) 5,000 50 Pass/<LOD 2-Methylpentane (Hexanes) 290 50 Pass/<LOD
2-Methylpropane (Isobutane) 5,000 100 Pass/<LOD 2-propanol (Isopropyl Alcohol) 5,000 50 Pass/<LOD
2-Propanone (Acetone) 5,000 50 Pass/53 3-Methylpentane (Hexanes) 290 50 Pass/<LOD
Acetonitrile 410 100 Pass/<LOD Benzene 2 1 Pass/<LOD
Butane 5,000 100 Pass/<LOD Chloroform 2 1 Pass/<LOD
Cumene 70 50 Pass/<LOD Cyclohexane 3,880 1,000 Pass/<LOD
Dichloromethane 600 50 Pass/<LOD Dimethylsulfoxide (DMSO) 5,000 500 Pass/<LOD
Ethanol 5,000 500 Pass/<LOD Ethyl acetate 5,000 50 Pass/<LOD
Ethyl ether 5,000 500 Pass/<LOD Ethylene glycol 620 310 Pass/<LOD
Ethylene oxide 50 50 Pass/<LOD Heptane 5,000 50 Pass/<LOD
Hexane 290 290 Pass/<LOD Isopropyl acetate 5,000 50 Pass/<LOD
Methanol 3,000 500 Pass/<LOD Naptha 400 100 Not Tested
N,N-Dimethylacetamide 1,090 100 Pass/<LOD N,N-Dimethylformamide (DMF) 880 500 Pass/<LOD
Pentane 5,000 50 Pass/<LOD Petroleum Ether 400 100 Not Tested
Propane 5,000 100 Pass/<LOD Pyridine 200 10 Pass/<LOD
Sulfolane 160 200 Pass/<LOD Tetrahydrofuran (THF) 720 200 Pass/<LOD
Toluene 890 50 Pass/<LOD Trichloroethylene 25 5 Not Tested
Xylenes* 2,170 50 Pass/<LOD

Total Butanes = 0 ug/g (PASS); Total Pentanes = 0 ug/g (PASS); Total Hexanes = 0 ug/g (PASS)

* Xylenes are reported as the sum of o-xylene, m-xylene, p-xylene, and ethylbenzene
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 7 of 12

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents QC Report
Testing Accreditation #: 4092-005 Test Certificate #: 129768-001
Client Name, Sample Details

Nakd Farms
Cottage Grove, OR 97424
Sample: Viola - Papaya
License: 060-1007418AD59
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A4010300011621000007505
Metrc Source Pkg#: 1A4010300011621000007467
Test Conditions

Prepsheet ID#: ORHS210317c
Scale: XS205-OR1
Temp: 22.1 °C
Baro PE: 1012 hPa
Analyst: HRM
Technician: JBS
Sample ID#: 129768

Lot #: Papaya 1/14/21
Batch #: 129768
Batch Weight (g): 2015
Harvest/Process Date: 01/14/2021
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 03/17/2021
Test Date: 03/17/2021
Sample #129768
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS Recovery (%) MSD Recovery (%) Relative Percent Difference (%) QC Flag
1,2-Dichloroethane N.D. 0 0 0 nan nan
n-Propane N.D. 250 155 171 62.00 68.40 9.82 LR
Isobutane N.D. 250 155 186 62.00 74.40 18.18 LR
Methanol N.D. 250 33 60 13.20 24.00 58.06 LRQ
n-Butane N.D. 250 151 180 60.40 72.00 17.52 LR
2,2-Dimethylpropane N.D. 250 166 205 66.40 82.00 21.02 LRQ
Ethanol N.D. 250 137 207 54.80 82.80 40.70 LRQ
Isopentane N.D. 250 167 205 66.80 82.00 20.43 LRQ
Acetonitrile N.D. 250 170 230 68.00 92.00 30.00 LRQ
Diethyl ether N.D. 250 168 229 67.20 91.60 30.73 LRQ
2-propanone N.D. 250 157 218 62.80 87.20 32.53 LRQ
2-propanol N.D. 250 168 172 67.20 68.80 2.35 LR
n-Pentane N.D. 250 0 67 0.00 26.80 200.00 LRQ
2,2-Dimethylbutane N.D. 250 175 219 70.00 87.60 22.34 Q
2,3-Dimethylbutane N.D. 250 166 227 66.40 90.80 31.04 LRQ
Methylene chloride N.D. 250 176 232 70.40 92.80 27.45 Q
2-Methylpentane N.D. 250 161 215 64.40 86.00 28.72 LRQ
3-Methylpentane N.D. 250 171 223 68.40 89.20 26.40 LRQ
2-Butanol N.D. 250 168 221 67.20 88.40 27.25 LRQ
n-Hexane N.D. 250 146 206 58.40 82.40 34.09 LRQ
Ethyl acetate N.D. 250 165 232 66.00 92.80 33.75 LRQ
Tetrahydrofuran N.D. 250 165 237 0.00 0.00 0.00 LRQ
Trichloroethylene N.D. 0 0 0 nan nan
Isopropyl acetate N.D. 250 157 238 0.00 0.00 0.00 LRQ
Benzene N.D. 250 175 242 70.00 96.80 32.13 Q
Chloroform N.D. 0 0 0 nan nan
Cyclohexane N.D. 250 154 217 61.60 86.80 33.96 LRQ
Ethylene glycol N.D. 250 77 152 30.80 60.80 65.50 LRQ
Heptane N.D. 250 98 175 39.20 70.00 56.41 LRQ
2-Ethoxyethanol N.D. 250 147 226 58.80 90.40 42.36 LRQ
1,4-Dioxane N.D. 250 158 246 63.20 98.40 43.56 LRQ
Pyridine N.D. 0 0 0 0.00 0.00 0.00
Toluene N.D. 250 170 237 68.00 94.80 32.92 LRQ
Chlorobenzene N.D. 0 0 0 0.00 0.00 0.00
Ethylbenzene N.D. 250 168 236 67.20 94.40 33.66 LRQ
m-Xylene/p-Xylene N.D. 500 330 470 66.00 94.00 35.00 LRQ
o-Xylene N.D. 250 172 239 68.80 95.60 32.60 LRQ
Cumene N.D. 250 173 238 69.20 95.20 31.63 LRQ
Ethylene oxide N.D. 250 157 219 62.80 87.60 32.98 LRQ

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

N.D. = Not Detected

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 8 of 12

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-005 Test Certificate #: 129768-001
Client Name, Sample Details

Nakd Farms
Cottage Grove, OR 97424
Sample: Viola - Papaya
License: 060-1007418AD59
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A4010300011621000007505
Metrc Source Pkg#: 1A4010300011621000007467
Test Conditions

Prepsheet ID#: ORHS210317c
Scale: XS205-OR1
Temp: 22.1 °C
Baro PE: 1012 hPa
Analyst: HRM
Technician: JBS
Sample ID#: 129768

Lot #: Papaya 1/14/21
Batch #: 129768
Batch Weight (g): 2015
Harvest/Process Date: 01/14/2021
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 03/17/2021
Test Date: 03/17/2021
Sample #129768
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
1,2-Dichloroethane 2 1 Not Tested 1,2-Dimethoxyethane 100 5 Pass/<LOD
1,4-dioxane 380 200 Pass/<LOD 1-Butanol 5,000 100 Pass/<LOD
1-Pentanol 5,000 100 Pass/<LOD 1-Propanol 5,000 100 Pass/<LOD
2,2-Dimethylpropane (Neopentane) 5,000 100 Pass/<LOD 2,2-Dimethylbutane (Hexanes) 290 100 Pass/<LOD
2,3-Dimethylbutane (Hexanes) 290 100 Pass/<LOD 2-Butanol 5,000 100 Pass/<LOD
2-Butanone (MEK) 5,000 50 Pass/<LOD 2-Ethoxyethanol 160 40 Pass/<LOD
2-Methylbutane (Isopentane) 5,000 50 Pass/<LOD 2-Methylpentane (Hexanes) 290 50 Pass/<LOD
2-Methylpropane (Isobutane) 5,000 100 Pass/<LOD 2-propanol (Isopropyl Alcohol) 5,000 50 Pass/<LOD
2-Propanone (Acetone) 5,000 50 Pass/<LOD 3-Methylpentane (Hexanes) 290 50 Pass/<LOD
Acetonitrile 410 100 Pass/<LOD Benzene 2 1 Pass/<LOD
Butane 5,000 100 Pass/<LOD Chloroform 2 1 Pass/<LOD
Cumene 70 50 Pass/<LOD Cyclohexane 3,880 1,000 Pass/<LOD
Dichloromethane 600 50 Pass/<LOD Dimethylsulfoxide (DMSO) 5,000 500 Pass/<LOD
Ethanol 5,000 500 Pass/<LOD Ethyl acetate 5,000 50 Pass/<LOD
Ethyl ether 5,000 500 Pass/<LOD Ethylene glycol 620 310 Pass/<LOD
Ethylene oxide 50 50 Pass/<LOD Heptane 5,000 50 Pass/<LOD
Hexane 290 290 Pass/<LOD Isopropyl acetate 5,000 50 Pass/<LOD
Methanol 3,000 500 Pass/<LOD Naptha 400 100 Not Tested
N,N-Dimethylacetamide 1,090 100 Pass/<LOD N,N-Dimethylformamide (DMF) 880 500 Pass/<LOD
Pentane 5,000 50 Pass/<LOD Petroleum Ether 400 100 Not Tested
Propane 5,000 100 Pass/<LOD Pyridine 200 10 Pass/<LOD
Sulfolane 160 200 Pass/<LOD Tetrahydrofuran (THF) 720 200 Pass/<LOD
Toluene 890 50 Pass/<LOD Trichloroethylene 25 5 Not Tested
Xylenes* 2,170 50 Pass/<LOD

Total Butanes = 59 ug/g (PASS); Total Pentanes = 0 ug/g (PASS); Total Hexanes = 0 ug/g (PASS)

* Xylenes are reported as the sum of o-xylene, m-xylene, p-xylene, and ethylbenzene
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 9 of 12

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents QC Report
Testing Accreditation #: 4092-005 Test Certificate #: 129768-001
Client Name, Sample Details

Nakd Farms
Cottage Grove, OR 97424
Sample: Viola - Papaya
License: 060-1007418AD59
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A4010300011621000007505
Metrc Source Pkg#: 1A4010300011621000007467
Test Conditions

Prepsheet ID#: ORHS210317c
Scale: XS205-OR1
Temp: 22.1 °C
Baro PE: 1012 hPa
Analyst: HRM
Technician: JBS
Sample ID#: 129768

Lot #: Papaya 1/14/21
Batch #: 129768
Batch Weight (g): 2015
Harvest/Process Date: 01/14/2021
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 03/17/2021
Test Date: 03/17/2021
Sample #129768
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS Recovery (%) MSD Recovery (%) Relative Percent Difference (%) QC Flag
1,2-Dichloroethane N.D. 0 0 0 nan nan
n-Propane N.D. 250 155 171 62.00 68.40 9.82 LR
Isobutane N.D. 250 155 186 62.00 74.40 18.18 LR
Methanol N.D. 250 33 60 13.20 24.00 58.06 LRQ
n-Butane N.D. 250 151 180 60.40 72.00 17.52 LR
2,2-Dimethylpropane N.D. 250 166 205 66.40 82.00 21.02 LRQ
Ethanol N.D. 250 137 207 54.80 82.80 40.70 LRQ
Isopentane N.D. 250 167 205 66.80 82.00 20.43 LRQ
Acetonitrile N.D. 250 170 230 68.00 92.00 30.00 LRQ
Diethyl ether N.D. 250 168 229 67.20 91.60 30.73 LRQ
2-propanone N.D. 250 157 218 62.80 87.20 32.53 LRQ
2-propanol N.D. 250 168 172 67.20 68.80 2.35 LR
n-Pentane N.D. 250 0 67 0.00 26.80 200.00 LRQ
2,2-Dimethylbutane N.D. 250 175 219 70.00 87.60 22.34 Q
2,3-Dimethylbutane N.D. 250 166 227 66.40 90.80 31.04 LRQ
Methylene chloride N.D. 250 176 232 70.40 92.80 27.45 Q
2-Methylpentane N.D. 250 161 215 64.40 86.00 28.72 LRQ
3-Methylpentane N.D. 250 171 223 68.40 89.20 26.40 LRQ
2-Butanol N.D. 250 168 221 67.20 88.40 27.25 LRQ
n-Hexane N.D. 250 146 206 58.40 82.40 34.09 LRQ
Ethyl acetate N.D. 250 165 232 66.00 92.80 33.75 LRQ
Tetrahydrofuran N.D. 250 165 237 0.00 0.00 0.00 LRQ
Trichloroethylene N.D. 0 0 0 nan nan
Isopropyl acetate N.D. 250 157 238 0.00 0.00 0.00 LRQ
Benzene N.D. 250 175 242 70.00 96.80 32.13 Q
Chloroform N.D. 0 0 0 nan nan
Cyclohexane N.D. 250 154 217 61.60 86.80 33.96 LRQ
Ethylene glycol N.D. 250 77 152 30.80 60.80 65.50 LRQ
Heptane N.D. 250 98 175 39.20 70.00 56.41 LRQ
2-Ethoxyethanol N.D. 250 147 226 58.80 90.40 42.36 LRQ
1,4-Dioxane N.D. 250 158 246 63.20 98.40 43.56 LRQ
Pyridine N.D. 0 0 0 0.00 0.00 0.00
Toluene N.D. 250 170 237 68.00 94.80 32.92 LRQ
Chlorobenzene N.D. 0 0 0 0.00 0.00 0.00
Ethylbenzene N.D. 250 168 236 67.20 94.40 33.66 LRQ
m-Xylene/p-Xylene N.D. 500 330 470 66.00 94.00 35.00 LRQ
o-Xylene N.D. 250 172 239 68.80 95.60 32.60 LRQ
Cumene N.D. 250 173 238 69.20 95.20 31.63 LRQ
Ethylene oxide N.D. 250 157 219 62.80 87.60 32.98 LRQ

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

N.D. = Not Detected

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

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ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Homogeneity Report by
High Performance Liquid Chromatography
Testing Accreditation #: 4092-005 Test Certificate #: 129768-001
Client Name, Sample Details

Nakd Farms
Cottage Grove, OR 97424
Sample: Viola - Papaya
License: 060-1007418AD59
Type: AU Tincture
Metrc Test Pkg#: 1A4010300011621000007505
Metrc Source Pkg#: 1A4010300011621000007467
Sample ID#: 129768

Lot #: Papaya 1/14/21
Batch #: 129768
Batch Weight (g): 2015
Harvest/Process Date: 01/14/2021
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 03/17/2021
Sample #129768
Increments Tested (mg/g) TOTAL THC TOTAL CBD THC THCA THCV CBD CBC CBDA CBDV CBG CBN
Increment 1 716.35 18.86 34.97 776.94 N.D. N.D. N.D. 21.51 N.D. 5.93 N.D.
Increment 2 702.26 21.66 37.84 757.60 N.D. N.D. N.D. 24.70 N.D. 7.24 N.D.
Average Value 709.30 20.26 36.41 767.27 N.D. N.D. N.D. 23.11 N.D. 6.59 N.D.
Max Value 716.35 21.66 37.84 776.94 N.D. N.D. N.D. 24.70 N.D. 7.24 N.D.
Min Value 702.26 18.86 34.97 757.60 N.D. N.D. N.D. 21.51 N.D. 5.93 N.D.
Relative Percent Difference (RPD) ±1.99 ±13.81 ±7.88 ±2.52 N.D. N.D. N.D. ±13.81 N.D. ±19.89 N.D.
Average Cannabinoids Per Package 709.30 20.26 36.41 767.27 N.D. N.D. N.D. 23.11 N.D. 6.59 N.D.
Average Cannabinoids Per Serving 35.47 1.01 1.82 38.36 N.D. N.D. N.D. 1.16 N.D. 0.33 N.D.
Max Concentration Per Serving (THC)   Not Applicable
Max Concentration Per Package (THC)   Pass
Relative Percent Difference (RPD)   Pass
Control Study   Yes, MJ1351
Field Duplicate   Pass

N.D. = Not Detected, Min = Minimum, Max = Maximum

RPD is the relative percent difference between increment 1 and increment 2.

RSD is the relative standard deviation between all increments tested.

Total THC and CBD is the calculated sum of CBD or THC and the amount of CBD or THC derived from CBDA or THCA, respectively. These values are calculated by adding a molar correction factor of 0.877 to the CBDA or THCA value.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Terry Rabinowitz Iron laboratories Terry Rabinowitz

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

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IRON Laboratories

Terpene Report by
Mass Spectrometer
Test Certificate #: 129768-001
Client Name, Sample Details

Nakd Farms
Cottage Grove, OR 97424
Sample: Viola - Papaya
License: 060-1007418AD59
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A4010300011621000007505
Metrc Source Pkg#: 1A4010300011621000007467

Test Conditions

Scale: XS205-OR1
Temp: 22.1 °C
Baro Pressure: 1012 hPa
Analyst: HRM
Technician: HRM

Sample ID#: 129768

Lot #: Papaya 1/14/21
Batch #: 129768
Batch Weight (g): 2015
Harvest/Process Date: 01/14/2021
Serving Size (g): 0.05
Date Received: 03/17/2021

Sample #129768
Sample #129768
  • α-Pinene (0.25%)
  • β-Ocimene (0.10%)
  • Camphene (0.05%)
  • Eucalyptol (1,8-Cineol) (0.00%)
  • Sabinene (0.00%)
  • γ-Terpinene (0.04%)
  • Myrcene (0.57%)
  • α-Terpinolene (0.29%)
  • β-Pinene (0.46%)
  • Linalool (0.68%)
  • ∆3-Carene (0.00%)
  • Fenchone (0.00%)
  • α-Terpinene (0.05%)
  • endo-Fenchol (0.23%)
  • α-Ocimene (0.00%)
  • Isopulegol (0.00%)
  • Limonene (0.97%)
  • Geraniol (0.02%)
  • p-Cymene (0.00%)
  • β-Caryophyllene (0.00%)
  • α-Humulene (0.98%)
  • Nerolidol 1 (cis) (0.00%)
  • Nerolidol 2 (trans) (0.05%)
  • Guaiol (1.21%)
  • Caryophyllene Oxide (0.00%)
  • α-Bisabolol (0.42%)
  • α-Phellandrene (0.26%)
  • α-Terpineol (0.15%)
  • Valenence (0.17%)

Total: 6.950%

Predominant Terpenes

1.21%   Guaiol Mild, guaiacwood, tea, rose 0.98%   α-Humulene Woody, oceanic-watery, spicy clove
0.97%   Limonene Citrus, orange, sweet 0.68%   Linalool Citrus, floral, sweet, bois de rose, woody, green, blueberry
0.57%   Myrcene Peppery, spicy balsam 0.46%   β-Pinene Woody, fresh pine, hay

Value in parenthesis indicates percentage of terpene present in the total sample (weight percentage, wt/wt%).
Value in doughnut slice indicates individual terpene abundance with respect to the total terpenes detected.

This sample has not been tested according to OAR 333-007. These results should therefore be used for research and development or quality control purposes only.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Himashi Mead Iron laboratories Himashi Mead

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

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