ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Marijuana Potency Analysis by
High Performance Liquid Chromatography
Testing Accreditation #: 4092-005 Test Certificate #: 129008-001
Client Name, Sample Details

45th Parallel Farms LLC
Dallas, OR 97338
Sample: Northern Wreck Shake
License: 010-100164183CE
Type: Adult Use Flower
Method: FE04U HPLC-UV
Metrc Test Pkg#: 1A4010300000DAD000003800
Metrc Source Pkg#: 1A4010300000DAD000003799
***Water Activity: 0.49
***Moisture: 10.32%
Test Conditions

Prepsheet ID#: ORP210204a
Scale: XS205-OR1
Temp: 21.9 °C
Baro Pressure: 1004 hPa
Analyst: TMR
Technician: TMR
Sample ID#: 129008

Lot #: Northern Wreck 10-13-20
Batch #: 129008
Harvest/Process Date: 10/13/2020
Date Received: 02/02/2021
Test Date: 02/04/2021
Sample #129008
Sample #129008 Sample #129008
Test
Compounds		 THC THCA CBD CBDA CBN CBG CBC THCV* CBDV Total
Cannabinoids*		 Total THC Total CBD Calc Max Total
Cannabinoids*
Amount (%) 1.93 33.85 N/D 0.97 N/D 0.20 N/D N/D N/D 36.95 31.62 0.85 32.67
Amount (mg/g) 19.26 338.54 N/D 9.69 N/D 2.01 N/D N/D N/D 369.5 316.16 8.50 326.67
Amount per Serving (mg) N\D N\D N\D N\D N\D N\D N\D N\D N\D 0.00 Serving Size~ (g): 0.00
LOQ (mg/g) 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5   %Decarb. THC CBD
±%RPD 2.86 2.86 2.50 2.77 3.45 +/-5% 5.83 +/-5% +/-5% 5 0

LOQ = Limit of Quantitation; %RPD = Relative Percent Deviation; %RSD = Relative Standard Deviation; N/D = Not Detected

*Designates values that are not currently included in the accredited scope of Iron Laboratories.

*** Designates tests that use the method FE-45. FE-45 is performed using AOAC 966.02 and 32.004-32.009. FE-45 has relative expanded (k=2) uncertainties of 1.098% for moisture, 1.754% for water activity for unprocessed plant materials, and 13.102% for water activity for infused products. Vitamin E acetate analysis has a relative expanded (k=2) uncertainty of 18.614%.

Total THC and CBD is the calculated sum of THC or CBD and the amount of THC or CBD derived from THCA or CBDA, respectively. These values are calculated by applying a molar correction factor of 0.877 to the THCA or the CBDA value. Calc Max Total Cannabinoids is the sum of Total THC, Total CBD, CBN, CBG, CBC, THCV, and CBDV.

%Decarb. THC and CBD refer to the percentage of THC or CBD relative to THCA or CBDA, respectively.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 1 of 4

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant QC Report
Testing Accreditation #: 4092-005 Test Certificate #: 129008-001
Client Name, Sample Details

45th Parallel Farms LLC
Dallas, OR 97338
Sample: Northern Wreck Shake
License: 010-100164183CE
Type: Adult Use Flower
Method: FE04U HPLC-UV
Metrc Test Pkg#: 1A4010300000DAD000003800
Metrc Source Pkg#: 1A4010300000DAD000003799
***Water Activity: 0.49
***Moisture: 10.32%
Test Conditions

Prepsheet ID#: ORP210204a
Scale: XS205-OR1
Temp: 21.9 °C
Baro Pressure: 1004 hPa
Analyst: TMR
Technician: TMR
Sample ID#: 129008

Lot #: Northern Wreck 10-13-20
Batch #: 129008
Harvest/Process Date: 10/13/2020
Date Received: 02/02/2021
Test Date: 02/04/2021
Sample #129008
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Cannabidivarin (CBDV) N.D. 1 0 0.00 0 0.00 0
Cannabidiolic Acid (CBDA) N.D. 11.56 11.76 101.73 12.09 104.58 2.77
Cannabigerol (CBG) N.D. 1.09 1.44 132.11 1.44 132.11 0.00 HR
Cannabidiol (CBD) N.D. 6.5 6.71 103.23 6.88 105.85 2.50
Δ9-Tetrahydrocannabivarin (THCV) N.D. 1 0 0.00 0 0.00 0
Cannabinol (CBN) N.D. 0.44 0.57 129.55 0.59 134.09 3.45 HR
Δ9-Tetrahydrocannabinol (THC) N.D. 29.39 31.4 106.84 32.31 109.94 2.86
Cannabichromene (CBC) N.D. 0.65 1 153.85 1.06 163.08 5.83 HR
Tetrahydrocannabinolic acid (THCA) N.D. 57.25 59.34 103.65 61.06 106.66 2.86

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 2 of 4

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Pesticide Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-005 Test Certificate #: 129008-001
Client Name, Sample Details

45th Parallel Farms LLC
Dallas, OR 97338
Sample: Northern Wreck Shake
License: 010-100164183CE
Type: Adult Use Flower
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A4010300000DAD000003800
Metrc Source Pkg#: 1A4010300000DAD000003799
Test Conditions

Prepsheet ID#: ORPS210204a
Scale: XS205-OR1
Temp: 22.3 °C
Baro PE: 1017 hPa
Analyst: HRM
Technician: JBS
Sample ID#: 129008

Lot #: Northern Wreck 10-13-20
Batch #: 129008
Harvest/Process Date: 10/13/2020
Date Received: 02/02/2021
Test Date: 02/04/2021
Sample #129008
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
Aldicarb 0.400 0.119 Pass/<LOD Abamectin**** 0.500 0.119 Pass/<LOD
Acephate 0.400 0.119 Pass/<LOD Acequinocyl 2.000 0.239 Pass/<LOD
Acetamiprid 0.200 0.119 Pass/<LOD Azoxystrobin 0.200 0.119 Pass/<LOD
Bifenazate 0.200 0.119 Pass/<LOD Bifenthrin 0.200 0.119 Pass/<LOD
Boscalid 0.400 0.119 Pass/<LOD Carbaryl 0.200 0.119 Pass/<LOD
Carbofuran 0.200 0.119 Pass/<LOD Chlorantraniliprole 0.200 0.119 Pass/<LOD
Chlorfenapyr 1.000 0.478 Pass/<LOD Chlorpyrifos 0.200 0.119 Pass/<LOD
Clofentezine 0.200 0.119 Pass/<LOD Cyfluthrin** 1.000 0.478 Pass/<LOD
Cypermethrin*** 1.000 0.478 Pass/<LOD Daminozide 1.000 0.119 Pass/<LOD
DDVP (Dichlorvos) 1.000 0.239 Pass/<LOD Diazinon 0.200 0.119 Pass/<LOD
Dimethoate 0.200 0.119 Pass/<LOD Ethoprophos 0.200 0.119 Pass/<LOD
Etofenprox 0.400 0.119 Pass/<LOD Etoxazole 0.200 0.119 Pass/<LOD
Fenoxycarb 0.200 0.119 Pass/<LOD Fenpyroximate 0.400 0.119 Pass/<LOD
Fipronil 0.400 0.119 Pass/<LOD Flonicamid 1.000 0.119 Pass/<LOD
Fludioxonil 0.400 0.119 Pass/<LOD Hexythiazox 1.000 0.119 Pass/<LOD
Imazalil 0.200 0.119 Pass/<LOD Imidacloprid 0.400 0.119 Pass/<LOD
Kresoxim Methyl 0.400 0.119 Pass/<LOD Malathion 0.200 0.119 Pass/<LOD
Metalaxyl 0.200 0.119 Pass/<LOD Methiocarb 0.200 0.119 Pass/<LOD
Methomyl 0.400 0.119 Pass/<LOD Methyl Parathion 0.200 0.119 Pass/<LOD
MGK-264‡ 0.200 0.119 Pass/<LOD Myclobutanil 0.000 0.119 Pass/<LOD
Naled 0.500 0.119 Pass/<LOD Oxamyl 1.000 0.119 Pass/<LOD
Paclobutrazol 0.400 0.119 Pass/<LOD Permethrins† 0.200 0.119 Pass/<LOD
Phosmet 0.200 0.119 Pass/<LOD Piperonyl Butoxide 2.000 0.119 Pass/<LOD
Prallethrin 0.200 0.119 Pass/<LOD Propiconazole 0.400 0.119 Pass/<LOD
Propoxur 0.200 0.119 Pass/<LOD Pyrethrins* 1.000 0.119 Pass/<LOD
Pyridaben 0.200 0.119 Pass/<LOD Spinosad***** 0.200 0.119 Pass/<LOD
Spiromesifen 0.200 0.119 Pass/<LOD Spirotetramat 0.200 0.119 Pass/<LOD
Spiroxamine‡ 0.400 0.119 Pass/<LOD Tebuconazole 0.400 0.119 Pass/<LOD
Thiacloprid 0.200 0.119 Pass/<LOD Thiamethoxam 0.200 0.119 Pass/<LOD
Trifloxystrobin 0.200 0.119 Pass/<LOD

* Pyrethrins are reported as the sum of Jasmolin I, Cinerin I, and Pyrethrin I
** Cyfluthrins are reported as the sum of isomers Cyfluthrin I, II, III, and IV
*** Cypermethrins are reported as the sum of isomers Cypermethrin I, II, III, and IV
**** Abamectin is reported as the sum of Avermectin B1a and Avermectin B1b
***** Spinosad is reported as the sum of Spinosyn A and Spinosyn D
† Permethrin and Prallethrin are reported as the sum of cis and trans isomers
‡ MGK-264 and Spiroximine are reported as the sum of isomers I and II
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 2 of 4

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Pesticide QC Report
Testing Accreditation #: 4092-005 Test Certificate #: 129008-001
Client Name, Sample Details

45th Parallel Farms LLC
Dallas, OR 97338
Sample: Northern Wreck Shake
License: 010-100164183CE
Type: Adult Use Flower
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A4010300000DAD000003800
Metrc Source Pkg#: 1A4010300000DAD000003799
Test Conditions

Prepsheet ID#: ORPS210204a
Scale: XS205-OR1
Temp: 22.3 °C
Baro PE: 1017 hPa
Analyst: HRM
Technician: JBS
Sample ID#: 129008

Lot #: Northern Wreck 10-13-20
Batch #: 129008
Harvest/Process Date: 10/13/2020
Date Received: 02/02/2021
Test Date: 02/04/2021
Sample #129008
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS recovery% MSD recovery% Relative Percent Difference (%) QC Flag
Acephate N.D. 1 0.97 0.935 97.00 93.50 3.67
Acequinocyl N.D. 1 0.788 0.49 78.80 49.00 46.64 LR Q
Acetamiprid N.D. 1 1.17 1.21 117.00 121.00 3.36
Aldicarb N.D. 1 1.25 1.23 125.00 123.00 1.61
Avermectin B1a N.D. 0.97 1.25 1.29 128.87 132.99 3.15 HR
Azoxystrobin N.D. 1 1.08 1.12 108.00 112.00 3.64
Bifenazate N.D. 1 1.08 1.07 108.00 107.00 0.93
Bifenthrin N.D. 1 1.16 1.2 116.00 120.00 3.39
Boscalid N.D. 1 0.856 0.884 85.60 88.40 3.22
Carbaryl N.D. 1 1.13 0.987 113.00 98.70 13.51
Carbofuran N.D. 1 1.22 1.21 122.00 121.00 0.82
Chlorantraniliprole N.D. 1 0.901 0.929 90.10 92.90 3.06
Chlorfenapyr N.D. 1 0.781 0.801 78.10 80.10 2.53
Chlorpyriphos N.D. 1 0.99 1.06 99.00 106.00 6.83
Clofentezine N.D. 1 0.989 0.926 98.90 92.60 6.58
Cyfluthrin N.D. 1 1.13 1.43 113.00 143.00 23.44 HRQ
Cypermethrin N.D. 1 0.938 1.77 93.80 177.00 61.45 HRQ
Daminoside N.D. 1 0.362 0.378 36.20 37.80 4.32 LR
Diazanon N.D. 1 6.89 7.13 689.00 713.00 3.42 HR
Dichlorvos N.D. 1 1.27 1.11 127.00 111.00 13.45
Dimethoate N.D. 1 1.1 1.16 110.00 116.00 5.31
Ethoprophos N.D. 1 0.924 0.969 92.40 96.90 4.75
Etofenprox N.D. 1 1.25 1.19 125.00 119.00 4.92
Etoxazole N.D. 1 1.29 1.24 129.00 124.00 3.95
Fenoxycarb N.D. 1 0.853 0.882 85.30 88.20 3.34
Fenpyroximate N.D. 1 1.24 1.25 124.00 125.00 0.80
Fipronil N.D. 1 1.32 1.32 132.00 132.00 0.00 HR
Flonicamid N.D. 1 1.13 1.15 113.00 115.00 1.75
Fludioxonil N.D. 1 1.46 1.43 146.00 143.00 2.08 HR
Hexythiazox N.D. 1 0.542 0.469 54.20 46.90 14.44 LR
Imazalil N.D. 1 0.912 0.923 91.20 92.30 1.20
Imidacloprid N.D. 1 1.17 1.17 117.00 117.00 0.00
Kresoxim-methyl N.D. 1 0.889 0.811 88.90 81.10 9.18
Malathion N.D. 1 0.861 0.851 86.10 85.10 1.17
Metalaxyl N.D. 1 1.02 1.11 102.00 111.00 8.45
Methiocarb N.D. 1 1.12 1.08 112.00 108.00 3.64
Methomyl N.D. 1 0.934 0.944 93.40 94.40 1.06
MGK-264 N.D. 1 0.881 0.911 88.10 91.10 3.35
Myclobutanil N.D. 1 1 1.02 100.00 102.00 1.98
Naled (dibrom) N.D. 1 0.344 0.282 34.40 28.20 19.81 LR
Oxamyl N.D. 1 1.25 1.29 125.00 129.00 3.15
Paclobutrazol N.D. 1 0.941 0.968 94.10 96.80 2.83
Parathion-methyl N.D. 1 1.12 1.06 112.00 106.00 5.50
Permethrins N.D. 1 1.16 1.114 116.00 111.40 4.05
Phosmet N.D. 1 0.882 0.849 88.20 84.90 3.81
Piperonyl butoxide N.D. 1 1.1 1.1 110.00 110.00 0.00
Prallethrin N.D. 1 0.875 0.914 87.50 91.40 4.36
Propiconazole N.D. 1 0.824 0.886 82.40 88.60 7.25
Propoxur N.D. 1 1.21 1.09 121.00 109.00 10.43
Pyrethrin N.D. 0.65 0.546 0.583 84.00 89.69 6.55
Pyridaben N.D. 1 1.11 1.09 111.00 109.00 1.82
SpinosynA N.D. 0.84 0.702 0.691 83.57 82.26 1.58
SpinosynD N.D. 0.16 0.132 0.129 82.50 80.63 2.30
Spiromesifen N.D. 1 0.141 0.141 14.10 14.10 0.00 LR
Spirotetramat N.D. 1 0.851 0.83 85.10 83.00 2.50
Spiroxamine N.D. 1 0.951 0.965 95.10 96.50 1.46
Tebuconazole N.D. 1 0.855 0.851 85.50 85.10 0.47
Thiacloprid N.D. 1 1.05 1.07 105.00 107.00 1.89
Thiamethoxam N.D. 1 0.9 0.955 90.00 95.50 5.93
Trifloxystrobin N.D. 1 1.15 1.13 115.00 113.00 1.75

N.D. = Not Detected

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 30%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (60-120%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 3 of 4
IRON Laboratories

Terpene Report by
Mass Spectrometer
Test Certificate #: 129008-001
Client Name, Sample Details

45th Parallel Farms LLC
Dallas, OR 97338
Sample: Northern Wreck Shake
License: 010-100164183CE
Type: Adult Use Flower
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A4010300000DAD000003800
Metrc Source Pkg#: 1A4010300000DAD000003799

Test Conditions

Scale: XS205-OR1
Temp: 22.1 °C
Baro Pressure: 1012 hPa
Analyst: HRM
Technician: JBS

Sample ID#: 129008

Lot #: Northern Wreck 10-13-20
Batch #: 129008
Harvest/Process Date: 10/13/2020
Date Received: 02/02/2021

Sample #129008
Sample #129008
  • α-Pinene (0.00%)
  • β-Ocimene (0.05%)
  • Camphene (0.00%)
  • Eucalyptol (1,8-Cineol) (0.02%)
  • Sabinene (0.00%)
  • γ-Terpinene (0.00%)
  • Myrcene (0.24%)
  • α-Terpinolene (0.00%)
  • β-Pinene (0.15%)
  • Linalool (0.22%)
  • ∆3-Carene (0.00%)
  • Fenchone (0.00%)
  • α-Terpinene (0.00%)
  • endo-Fenchol (0.02%)
  • α-Ocimene (0.00%)
  • Isopulegol (0.00%)
  • Limonene (0.06%)
  • Geraniol (0.00%)
  • p-Cymene (0.00%)
  • β-Caryophyllene (0.22%)
  • α-Humulene (0.59%)
  • Nerolidol 1 (cis) (0.00%)
  • Nerolidol 2 (trans) (0.06%)
  • Guaiol (0.30%)
  • Caryophyllene Oxide (0.00%)
  • α-Bisabolol (0.35%)
  • α-Phellandrene (0.00%)
  • α-Terpineol (0.02%)
  • Valenence (0.07%)

Total: 2.370%

Predominant Terpenes

0.59%   α-Humulene Woody, oceanic-watery, spicy clove 0.35%   α-Bisabolol Fruity, nutty, coconut
0.30%   Guaiol Mild, guaiacwood, tea, rose 0.24%   Myrcene Peppery, spicy balsam
0.22%   β-Caryophyllene Sweet, woody, spicy, clove 0.22%   Linalool Citrus, floral, sweet, bois de rose, woody, green, blueberry

Value in parenthesis indicates percentage of terpene present in the total sample (weight percentage, wt/wt%).
Value in doughnut slice indicates individual terpene abundance with respect to the total terpenes detected.

This sample has not been tested according to OAR 333-007. These results should therefore be used for research and development or quality control purposes only.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Himashi Mead Iron laboratories Himashi Mead

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 4 of 4