ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Marijuana Potency Analysis by
High Performance Liquid Chromatography

Testing Accreditation #: 4092-005 Test Certificate #: 128636-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Mach 4
License: 030-1009646F7F8
Type: AU Tincture
Method: FE04U HPLC-UV
Metrc Test Pkg#: 1A401030002C949000001400
Metrc Source Pkg#: 1A401030002C949000001336

Test Conditions

Prepsheet ID#: ORP210111b
Scale: XS205-OR1
Temp: 22.8 °C
Baro Pressure: 1007 hPa
Analyst: TMR
Technician: TMR

Sample ID#: 128636

Lot #: Mach 4 #1 1.1.2021
Batch #: 128636
Batch Weight (g): 572
Harvest/Process Date: 01/01/2021
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 01/06/2021
Test Date: 01/11/2021

Sample #128636
Sample #128636 Sample #128636
Test
Compounds
THC THCA CBD CBDA CBN CBG CBC THCV* CBDV Total
Cannabinoids*
Total THC Total CBD Calc Max Total
Cannabinoids*
Amount (%) 8.47 82.47 N/D 1.76 N/D 0.42 N/D N/D N/D 93.11 80.79 1.54 82.75
Amount (mg/g) 84.70 824.66 N/D 17.58 N/D 4.15 N/D N/D N/D 931.09 807.93 15.42 827.50
Amount per Serving (mg) 4.24 41.23 N\D 0.88 N\D 0.21 N\D N\D N\D 46.55 Serving Size~ (g): 0.05
LOQ (mg/g) 2 2 2 2 2 2 2 2 2   %Decarb. THC CBD
±%RPD 7.43 25.33 6.91 5.51 2.42 2.10 4.21 2.70 7.58 9 0

LOQ = Limit of Quantitation; %RPD = Relative Percent Deviation; %RSD = Relative Standard Deviation; N/D = Not Detected

*Designates values that are not currently included in the accredited scope of Iron Laboratories.

*** Designates tests that use the method FE-45. FE-45 is performed using AOAC 966.02 and 32.004-32.009. FE-45 has relative expanded (k=2) uncertainties of 1.098% for moisture, 1.754% for water activity for unprocessed plant materials, and 13.102% for water activity for infused products. Vitamin E acetate analysis has a relative expanded (k=2) uncertainty of 18.614%.

Total THC and CBD is the calculated sum of THC or CBD and the amount of THC or CBD derived from THCA or CBDA, respectively. These values are calculated by applying a molar correction factor of 0.877 to the THCA or the CBDA value. Calc Max Total Cannabinoids is the sum of Total THC, Total CBD, CBN, CBG, CBC, THCV, and CBDV.

%Decarb. THC and CBD refer to the percentage of THC or CBD relative to THCA or CBDA, respectively.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 1 of 12

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant QC Report

Testing Accreditation #: 4092-005 Test Certificate #: 128636-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Mach 4
License: 030-1009646F7F8
Type: AU Tincture
Method: FE04U HPLC-UV
Metrc Test Pkg#: 1A401030002C949000001400
Metrc Source Pkg#: 1A401030002C949000001336

Test Conditions

Prepsheet ID#: ORP210111b
Scale: XS205-OR1
Temp: 22.8 °C
Baro Pressure: 1007 hPa
Analyst: TMR
Technician: TMR

Sample ID#: 128636

Lot #: Mach 4 #1 1.1.2021
Batch #: 128636
Batch Weight (g): 572
Harvest/Process Date: 01/01/2021
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 01/06/2021
Test Date: 01/11/2021

Sample #128636
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Cannabidivarin (CBDV) N.D. 4.92 4.57 92.89 4.93 100.20 7.58
Cannabidiolic Acid (CBDA) N.D. 4.11 3.88 94.40 4.1 99.76 5.51
Cannabigerol (CBG) N.D. 5.23 5.29 101.15 5.18 99.04 2.10
Cannabidiol (CBD) N.D. 5.4 5.03 93.15 5.39 99.81 6.91
Δ9-Tetrahydrocannabivarin (THCV) N.D. 5.13 5.25 102.34 5.11 99.61 2.70
Cannabinol (CBN) N.D. 4.91 5.02 102.24 4.9 99.80 2.42
Δ9-Tetrahydrocannabinol (THC) N.D. 5.99 6.42 107.18 5.96 99.50 7.43
Cannabichromene (CBC) N.D. 5.15 5.34 103.69 5.12 99.42 4.21
Tetrahydrocannabinolic acid (THCA) N.D. 3.82 3.87 101.31 3 78.53 25.33

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 2 of 12

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Marijuana Potency Analysis by
High Performance Liquid Chromatography

Testing Accreditation #: 4092-005 Test Certificate #: 128636-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Mach 4
License: 030-1009646F7F8
Type: AU Tincture
Method: FE04U HPLC-UV
Metrc Test Pkg#: 1A401030002C949000001400
Metrc Source Pkg#: 1A401030002C949000001336

Test Conditions

Prepsheet ID#: ORP210111b
Scale: XS205-OR1
Temp: 22.8 °C
Baro Pressure: 1007 hPa
Analyst: TMR
Technician: TMR

Sample ID#: 128636

Lot #: Mach 4 #1 1.1.2021
Batch #: 128636
Batch Weight (g): 572
Harvest/Process Date: 01/01/2021
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 01/06/2021
Test Date: 01/11/2021

Sample #128636
Sample #128636 Sample #128636
Test
Compounds
THC THCA CBD CBDA CBN CBG CBC THCV* CBDV Total
Cannabinoids*
Total THC Total CBD Calc Max Total
Cannabinoids*
Amount (%) 8.48 84.42 N/D 1.79 N/D 0.43 N/D N/D N/D 95.12 82.52 1.57 84.51
Amount (mg/g) 84.80 844.21 N/D 17.89 N/D 4.28 N/D N/D N/D 951.18 825.17 15.69 845.14
Amount per Serving (mg) 4.24 42.21 N\D 0.89 N\D 0.21 N\D N\D N\D 47.56 Serving Size~ (g): 0.05
LOQ (mg/g) 1.9 1.9 1.9 1.9 1.9 1.9 1.9 1.9 1.9   %Decarb. THC CBD
±%RPD 7.43 25.33 6.91 5.51 2.42 2.10 4.21 2.70 7.58 0 0

LOQ = Limit of Quantitation; %RPD = Relative Percent Deviation; %RSD = Relative Standard Deviation; N/D = Not Detected

*Designates values that are not currently included in the accredited scope of Iron Laboratories.

*** Designates tests that use the method FE-45. FE-45 is performed using AOAC 966.02 and 32.004-32.009. FE-45 has relative expanded (k=2) uncertainties of 1.098% for moisture, 1.754% for water activity for unprocessed plant materials, and 13.102% for water activity for infused products. Vitamin E acetate analysis has a relative expanded (k=2) uncertainty of 18.614%.

Total THC and CBD is the calculated sum of THC or CBD and the amount of THC or CBD derived from THCA or CBDA, respectively. These values are calculated by applying a molar correction factor of 0.877 to the THCA or the CBDA value. Calc Max Total Cannabinoids is the sum of Total THC, Total CBD, CBN, CBG, CBC, THCV, and CBDV.

%Decarb. THC and CBD refer to the percentage of THC or CBD relative to THCA or CBDA, respectively.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 2 of 12

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant QC Report

Testing Accreditation #: 4092-005 Test Certificate #: 128636-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Mach 4
License: 030-1009646F7F8
Type: AU Tincture
Method: FE04U HPLC-UV
Metrc Test Pkg#: 1A401030002C949000001400
Metrc Source Pkg#: 1A401030002C949000001336

Test Conditions

Prepsheet ID#: ORP210111b
Scale: XS205-OR1
Temp: 22.8 °C
Baro Pressure: 1007 hPa
Analyst: TMR
Technician: TMR

Sample ID#: 128636

Lot #: Mach 4 #1 1.1.2021
Batch #: 128636
Batch Weight (g): 572
Harvest/Process Date: 01/01/2021
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 01/06/2021
Test Date: 01/11/2021

Sample #128636
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Cannabidivarin (CBDV) N.D. 4.92 4.57 92.89 4.93 100.20 7.58
Cannabidiolic Acid (CBDA) N.D. 4.11 3.88 94.40 4.1 99.76 5.51
Cannabigerol (CBG) N.D. 5.23 5.29 101.15 5.18 99.04 2.10
Cannabidiol (CBD) N.D. 5.4 5.03 93.15 5.39 99.81 6.91
Δ9-Tetrahydrocannabivarin (THCV) N.D. 5.13 5.25 102.34 5.11 99.61 2.70
Cannabinol (CBN) N.D. 4.91 5.02 102.24 4.9 99.80 2.42
Δ9-Tetrahydrocannabinol (THC) N.D. 5.99 6.42 107.18 5.96 99.50 7.43
Cannabichromene (CBC) N.D. 5.15 5.34 103.69 5.12 99.42 4.21
Tetrahydrocannabinolic acid (THCA) N.D. 3.82 3.87 101.31 3 78.53 25.33

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 3 of 12

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Pesticide Analysis by
Mass Spectrometer

Testing Accreditation #: 4092-005 Test Certificate #: 128636-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Mach 4
License: 030-1009646F7F8
Type: AU Tincture
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A401030002C949000001400
Metrc Source Pkg#: 1A401030002C949000001336

Test Conditions

Prepsheet ID#: ORPS210111b
Scale: XS205-OR1
Temp: 22.2 °C
Baro PE: 1004 hPa
Analyst: HRM
Technician: JBS

Sample ID#: 128636

Lot #: Mach 4 #1 1.1.2021
Batch #: 128636
Batch Weight (g): 572
Harvest/Process Date: 01/01/2021
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 01/06/2021
Test Date: 01/11/2021

Sample #128636
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
Aldicarb 0.400 0.122 Pass/<LOD Abamectin**** 0.500 0.122 Pass/<LOD
Acephate 0.400 0.122 Pass/<LOD Acequinocyl 2.000 0.244 Pass/<LOD
Acetamiprid 0.200 0.122 Pass/<LOD Azoxystrobin 0.200 0.122 Pass/<LOD
Bifenazate 0.200 0.122 Pass/<LOD Bifenthrin 0.200 0.122 Pass/<LOD
Boscalid 0.400 0.122 Pass/<LOD Carbaryl 0.200 0.122 Pass/<LOD
Carbofuran 0.200 0.122 Pass/<LOD Chlorantraniliprole 0.200 0.122 Pass/<LOD
Chlorfenapyr 1.000 0.489 Pass/<LOD Chlorpyrifos 0.200 0.122 Pass/<LOD
Clofentezine 0.200 0.122 Pass/<LOD Cyfluthrin** 1.000 0.489 Pass/<LOD
Cypermethrin*** 1.000 0.489 Pass/<LOD Daminozide 1.000 0.122 Pass/<LOD
DDVP (Dichlorvos) 1.000 0.244 Pass/<LOD Diazinon 0.200 0.122 Pass/<LOD
Dimethoate 0.200 0.122 Pass/<LOD Ethoprophos 0.200 0.122 Pass/<LOD
Etofenprox 0.400 0.122 Pass/<LOD Etoxazole 0.200 0.122 Pass/<LOD
Fenoxycarb 0.200 0.122 Pass/<LOD Fenpyroximate 0.400 0.122 Pass/<LOD
Fipronil 0.400 0.122 Pass/<LOD Flonicamid 1.000 0.122 Pass/<LOD
Fludioxonil 0.400 0.122 Pass/<LOD Hexythiazox 1.000 0.122 Pass/<LOD
Imazalil 0.200 0.122 Pass/<LOD Imidacloprid 0.400 0.122 Pass/<LOD
Kresoxim Methyl 0.400 0.122 Pass/<LOD Malathion 0.200 0.122 Pass/<LOD
Metalaxyl 0.200 0.122 Pass/<LOD Methiocarb 0.200 0.122 Pass/<LOD
Methomyl 0.400 0.122 Pass/<LOD Methyl Parathion 0.200 0.122 Pass/<LOD
MGK-264‡ 0.200 0.122 Pass/<LOD Myclobutanil 0.000 0.122 Pass/<LOD
Naled 0.500 0.122 Pass/<LOD Oxamyl 1.000 0.122 Pass/<LOD
Paclobutrazol 0.400 0.122 Pass/<LOD Permethrins† 0.200 0.122 Pass/<LOD
Phosmet 0.200 0.122 Pass/<LOD Piperonyl Butoxide 2.000 0.122 Pass/<LOD
Prallethrin 0.200 0.122 Pass/<LOD Propiconazole 0.400 0.122 Pass/<LOD
Propoxur 0.200 0.122 Pass/<LOD Pyrethrins* 1.000 0.122 Pass/<LOD
Pyridaben 0.200 0.122 Pass/<LOD Spinosad***** 0.200 0.122 Pass/<LOD
Spiromesifen 0.200 0.122 Pass/<LOD Spirotetramat 0.200 0.122 Pass/<LOD
Spiroxamine‡ 0.400 0.122 Pass/<LOD Tebuconazole 0.400 0.122 Pass/<LOD
Thiacloprid 0.200 0.122 Pass/<LOD Thiamethoxam 0.200 0.122 Pass/<LOD
Trifloxystrobin 0.200 0.122 Pass/<LOD

* Pyrethrins are reported as the sum of Jasmolin I, Cinerin I, and Pyrethrin I
** Cyfluthrins are reported as the sum of isomers Cyfluthrin I, II, III, and IV
*** Cypermethrins are reported as the sum of isomers Cypermethrin I, II, III, and IV
**** Abamectin is reported as the sum of Avermectin B1a and Avermectin B1b
***** Spinosad is reported as the sum of Spinosyn A and Spinosyn D
† Permethrin and Prallethrin are reported as the sum of cis and trans isomers
‡ MGK-264 and Spiroximine are reported as the sum of isomers I and II
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 3 of 12

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Pesticide QC Report

Testing Accreditation #: 4092-005 Test Certificate #: 128636-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Mach 4
License: 030-1009646F7F8
Type: AU Tincture
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A401030002C949000001400
Metrc Source Pkg#: 1A401030002C949000001336

Test Conditions

Prepsheet ID#: ORPS210111b
Scale: XS205-OR1
Temp: 22.2 °C
Baro PE: 1004 hPa
Analyst: HRM
Technician: JBS

Sample ID#: 128636

Lot #: Mach 4 #1 1.1.2021
Batch #: 128636
Batch Weight (g): 572
Harvest/Process Date: 01/01/2021
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 01/06/2021
Test Date: 01/11/2021

Sample #128636
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS recovery% MSD recovery% Relative Percent Difference (%) QC Flag
Acephate N.D. 1 1.04 1.11 104.00 111.00 6.51
Acequinocyl N.D. 1 0.194 0.337 19.40 33.70 53.86 LR Q
Acetamiprid N.D. 1 1.23 1.31 123.00 131.00 6.30 HR
Aldicarb N.D. 1 1.15 1.22 115.00 122.00 5.91
Avermectin B1a N.D. 0.97 1.74 1.6 179.38 164.95 8.38 HR
Azoxystrobin N.D. 1 1.35 1.51 135.00 151.00 11.19 HR
Bifenazate N.D. 1 2.53 2.91 253.00 291.00 13.97 HR
Bifenthrin N.D. 1 0.929 1.45 92.90 145.00 43.80 HRQ
Boscalid N.D. 1 1.07 1.17 107.00 117.00 8.93
Carbaryl N.D. 1 1.17 1.18 117.00 118.00 0.85
Carbofuran N.D. 1 1.35 1.41 135.00 141.00 4.35 HR
Chlorantraniliprole N.D. 1 2.02 2.22 202.00 222.00 9.43 HR
Chlorfenapyr N.D. 1 0.239 0.924 23.90 92.40 117.80 LR Q
Chlorpyriphos N.D. 1 0.774 1.02 77.40 102.00 27.42 Q
Clofentezine N.D. 1 1.12 1.6 112.00 160.00 35.29 HRQ
Cyfluthrin N.D. 1 1.34 1.47 134.00 147.00 9.25 HR
Cypermethrin N.D. 1 1.19 1.49 119.00 149.00 22.39 HRQ
Daminoside N.D. 1 0.645 0.708 64.50 70.80 9.31 LR
Diazanon N.D. 1 7.31 7.56 731.00 756.00 3.36 HR
Dichlorvos N.D. 1 1.96 1.88 196.00 188.00 4.17 HR
Dimethoate N.D. 1 1.3 1.32 130.00 132.00 1.53 HR
Ethoprophos N.D. 1 1.23 1.3 123.00 130.00 5.53
Etofenprox N.D. 1 0.677 0.828 67.70 82.80 20.07 LR Q
Etoxazole N.D. 1 1.18 1.25 118.00 125.00 5.76
Fenoxycarb N.D. 1 1.66 1.88 166.00 188.00 12.43 HR
Fenpyroximate N.D. 1 1.06 1.23 106.00 123.00 14.85
Fipronil N.D. 1 1.25 1.29 125.00 129.00 3.15
Flonicamid N.D. 1 1.37 1.4 137.00 140.00 2.17 HR
Fludioxonil N.D. 1 1.43 1.45 143.00 145.00 1.39 HR
Hexythiazox N.D. 1 0.607 0.766 60.70 76.60 23.16 LR Q
Imazalil N.D. 1 2.26 2.34 226.00 234.00 3.48 HR
Imidacloprid N.D. 1 1.64 1.7 164.00 170.00 3.59 HR
Kresoxim-methyl N.D. 1 2.06 2.16 206.00 216.00 4.74 HR
Malathion N.D. 1 1.37 1.54 137.00 154.00 11.68 HR
Metalaxyl N.D. 1 2.32 2.36 232.00 236.00 1.71 HR
Methiocarb N.D. 1 1.31 1.42 131.00 142.00 8.06 HR
Methomyl N.D. 1 1.72 1.78 172.00 178.00 3.43 HR
MGK-264 N.D. 1 1.22 1.4 122.00 140.00 13.74 HR
Myclobutanil N.D. 1 1.96 2.24 196.00 224.00 13.33 HR
Naled (dibrom) N.D. 1 0.515 0.548 51.50 54.80 6.21 LR
Oxamyl N.D. 1 1.6 1.61 160.00 161.00 0.62 HR
Paclobutrazol N.D. 1 2.51 2.56 251.00 256.00 1.97 HR
Parathion-methyl N.D. 1 1.05 1.16 105.00 116.00 9.95
Permethrins N.D. 1 0.739 0.956 73.90 95.60 25.60 LR Q
Phosmet N.D. 1 1.44 1.72 144.00 172.00 17.72 HR
Piperonyl butoxide N.D. 1 1.01 1.12 101.00 112.00 10.33
Prallethrin N.D. 1 1.8 2.02 180.00 202.00 11.52 HR
Propiconazole N.D. 1 1.14 1.3 114.00 130.00 13.11
Propoxur N.D. 1 1.26 1.38 126.00 138.00 9.09 HR
Pyrethrin N.D. 0.65 0.675 0.897 103.85 138.00 28.24 HRQ
Pyridaben N.D. 1 0.719 0.846 71.90 84.60 16.23
SpinosynA N.D. 0.84 1.36 1.51 161.90 179.76 10.45 HR
SpinosynD N.D. 0.16 0.283 0.314 176.88 196.25 10.39 HR
Spiromesifen N.D. 1 0.202 0.239 20.20 23.90 16.78 LR
Spirotetramat N.D. 1 1.4 1.54 140.00 154.00 9.52 HR
Spiroxamine N.D. 1 1.92 1.99 192.00 199.00 3.58 HR
Tebuconazole N.D. 1 1.77 2.01 177.00 201.00 12.70 HR
Thiacloprid N.D. 1 1.54 1.55 154.00 155.00 0.65 HR
Thiamethoxam N.D. 1 2.09 2.13 209.00 213.00 1.90 HR
Trifloxystrobin N.D. 1 1.21 1.38 121.00 138.00 13.13 HR

N.D. = Not Detected

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 30%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (60-120%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 4 of 12

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Pesticide Analysis by
Mass Spectrometer

Testing Accreditation #: 4092-005 Test Certificate #: 128636-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Mach 4
License: 030-1009646F7F8
Type: AU Tincture
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A401030002C949000001400
Metrc Source Pkg#: 1A401030002C949000001336

Test Conditions

Prepsheet ID#: ORPS210111b
Scale: XS205-OR1
Temp: 22.2 °C
Baro PE: 1004 hPa
Analyst: HRM
Technician: JBS

Sample ID#: 128636

Lot #: Mach 4 #1 1.1.2021
Batch #: 128636
Batch Weight (g): 572
Harvest/Process Date: 01/01/2021
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 01/06/2021
Test Date: 01/11/2021

Sample #128636
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
Aldicarb 0.400 0.120 Pass/<LOD Abamectin**** 0.500 0.120 Pass/<LOD
Acephate 0.400 0.120 Pass/<LOD Acequinocyl 2.000 0.240 Pass/<LOD
Acetamiprid 0.200 0.120 Pass/<LOD Azoxystrobin 0.200 0.120 Pass/<LOD
Bifenazate 0.200 0.120 Pass/<LOD Bifenthrin 0.200 0.120 Pass/<LOD
Boscalid 0.400 0.120 Pass/<LOD Carbaryl 0.200 0.120 Pass/<LOD
Carbofuran 0.200 0.120 Pass/<LOD Chlorantraniliprole 0.200 0.120 Pass/<LOD
Chlorfenapyr 1.000 0.480 Pass/<LOD Chlorpyrifos 0.200 0.120 Pass/<LOD
Clofentezine 0.200 0.120 Pass/<LOD Cyfluthrin** 1.000 0.480 Pass/<LOD
Cypermethrin*** 1.000 0.480 Pass/<LOD Daminozide 1.000 0.120 Pass/<LOD
DDVP (Dichlorvos) 1.000 0.240 Pass/<LOD Diazinon 0.200 0.120 Pass/<LOD
Dimethoate 0.200 0.120 Pass/<LOD Ethoprophos 0.200 0.120 Pass/<LOD
Etofenprox 0.400 0.120 Pass/<LOD Etoxazole 0.200 0.120 Pass/<LOD
Fenoxycarb 0.200 0.120 Pass/<LOD Fenpyroximate 0.400 0.120 Pass/<LOD
Fipronil 0.400 0.120 Pass/<LOD Flonicamid 1.000 0.120 Pass/<LOD
Fludioxonil 0.400 0.120 Pass/<LOD Hexythiazox 1.000 0.120 Pass/<LOD
Imazalil 0.200 0.120 Pass/<LOD Imidacloprid 0.400 0.120 Pass/<LOD
Kresoxim Methyl 0.400 0.120 Pass/<LOD Malathion 0.200 0.120 Pass/<LOD
Metalaxyl 0.200 0.120 Pass/<LOD Methiocarb 0.200 0.120 Pass/<LOD
Methomyl 0.400 0.120 Pass/<LOD Methyl Parathion 0.200 0.120 Pass/<LOD
MGK-264‡ 0.200 0.120 Pass/<LOD Myclobutanil 0.000 0.120 Pass/<LOD
Naled 0.500 0.120 Pass/<LOD Oxamyl 1.000 0.120 Pass/<LOD
Paclobutrazol 0.400 0.120 Pass/<LOD Permethrins† 0.200 0.120 Pass/<LOD
Phosmet 0.200 0.120 Pass/<LOD Piperonyl Butoxide 2.000 0.120 Pass/<LOD
Prallethrin 0.200 0.120 Pass/<LOD Propiconazole 0.400 0.120 Pass/<LOD
Propoxur 0.200 0.120 Pass/<LOD Pyrethrins* 1.000 0.120 Pass/<LOD
Pyridaben 0.200 0.120 Pass/<LOD Spinosad***** 0.200 0.120 Pass/<LOD
Spiromesifen 0.200 0.120 Pass/<LOD Spirotetramat 0.200 0.120 Pass/<LOD
Spiroxamine‡ 0.400 0.120 Pass/<LOD Tebuconazole 0.400 0.120 Pass/<LOD
Thiacloprid 0.200 0.120 Pass/<LOD Thiamethoxam 0.200 0.120 Pass/<LOD
Trifloxystrobin 0.200 0.120 Pass/<LOD

* Pyrethrins are reported as the sum of Jasmolin I, Cinerin I, and Pyrethrin I
** Cyfluthrins are reported as the sum of isomers Cyfluthrin I, II, III, and IV
*** Cypermethrins are reported as the sum of isomers Cypermethrin I, II, III, and IV
**** Abamectin is reported as the sum of Avermectin B1a and Avermectin B1b
***** Spinosad is reported as the sum of Spinosyn A and Spinosyn D
† Permethrin and Prallethrin are reported as the sum of cis and trans isomers
‡ MGK-264 and Spiroximine are reported as the sum of isomers I and II
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 5 of 12

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Pesticide QC Report

Testing Accreditation #: 4092-005 Test Certificate #: 128636-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Mach 4
License: 030-1009646F7F8
Type: AU Tincture
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A401030002C949000001400
Metrc Source Pkg#: 1A401030002C949000001336

Test Conditions

Prepsheet ID#: ORPS210111b
Scale: XS205-OR1
Temp: 22.2 °C
Baro PE: 1004 hPa
Analyst: HRM
Technician: JBS

Sample ID#: 128636

Lot #: Mach 4 #1 1.1.2021
Batch #: 128636
Batch Weight (g): 572
Harvest/Process Date: 01/01/2021
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 01/06/2021
Test Date: 01/11/2021

Sample #128636
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS recovery% MSD recovery% Relative Percent Difference (%) QC Flag
Acephate N.D. 1 1.04 1.11 104.00 111.00 6.51
Acequinocyl N.D. 1 0.194 0.337 19.40 33.70 53.86 LR Q
Acetamiprid N.D. 1 1.23 1.31 123.00 131.00 6.30 HR
Aldicarb N.D. 1 1.15 1.22 115.00 122.00 5.91
Avermectin B1a N.D. 0.97 1.74 1.6 179.38 164.95 8.38 HR
Azoxystrobin N.D. 1 1.35 1.51 135.00 151.00 11.19 HR
Bifenazate N.D. 1 2.53 2.91 253.00 291.00 13.97 HR
Bifenthrin N.D. 1 0.929 1.45 92.90 145.00 43.80 HRQ
Boscalid N.D. 1 1.07 1.17 107.00 117.00 8.93
Carbaryl N.D. 1 1.17 1.18 117.00 118.00 0.85
Carbofuran N.D. 1 1.35 1.41 135.00 141.00 4.35 HR
Chlorantraniliprole N.D. 1 2.02 2.22 202.00 222.00 9.43 HR
Chlorfenapyr N.D. 1 0.239 0.924 23.90 92.40 117.80 LR Q
Chlorpyriphos N.D. 1 0.774 1.02 77.40 102.00 27.42 Q
Clofentezine N.D. 1 1.12 1.6 112.00 160.00 35.29 HRQ
Cyfluthrin N.D. 1 1.34 1.47 134.00 147.00 9.25 HR
Cypermethrin N.D. 1 1.19 1.49 119.00 149.00 22.39 HRQ
Daminoside N.D. 1 0.645 0.708 64.50 70.80 9.31 LR
Diazanon N.D. 1 7.31 7.56 731.00 756.00 3.36 HR
Dichlorvos N.D. 1 1.96 1.88 196.00 188.00 4.17 HR
Dimethoate N.D. 1 1.3 1.32 130.00 132.00 1.53 HR
Ethoprophos N.D. 1 1.23 1.3 123.00 130.00 5.53
Etofenprox N.D. 1 0.677 0.828 67.70 82.80 20.07 LR Q
Etoxazole N.D. 1 1.18 1.25 118.00 125.00 5.76
Fenoxycarb N.D. 1 1.66 1.88 166.00 188.00 12.43 HR
Fenpyroximate N.D. 1 1.06 1.23 106.00 123.00 14.85
Fipronil N.D. 1 1.25 1.29 125.00 129.00 3.15
Flonicamid N.D. 1 1.37 1.4 137.00 140.00 2.17 HR
Fludioxonil N.D. 1 1.43 1.45 143.00 145.00 1.39 HR
Hexythiazox N.D. 1 0.607 0.766 60.70 76.60 23.16 LR Q
Imazalil N.D. 1 2.26 2.34 226.00 234.00 3.48 HR
Imidacloprid N.D. 1 1.64 1.7 164.00 170.00 3.59 HR
Kresoxim-methyl N.D. 1 2.06 2.16 206.00 216.00 4.74 HR
Malathion N.D. 1 1.37 1.54 137.00 154.00 11.68 HR
Metalaxyl N.D. 1 2.32 2.36 232.00 236.00 1.71 HR
Methiocarb N.D. 1 1.31 1.42 131.00 142.00 8.06 HR
Methomyl N.D. 1 1.72 1.78 172.00 178.00 3.43 HR
MGK-264 N.D. 1 1.22 1.4 122.00 140.00 13.74 HR
Myclobutanil N.D. 1 1.96 2.24 196.00 224.00 13.33 HR
Naled (dibrom) N.D. 1 0.515 0.548 51.50 54.80 6.21 LR
Oxamyl N.D. 1 1.6 1.61 160.00 161.00 0.62 HR
Paclobutrazol N.D. 1 2.51 2.56 251.00 256.00 1.97 HR
Parathion-methyl N.D. 1 1.05 1.16 105.00 116.00 9.95
Permethrins N.D. 1 0.739 0.956 73.90 95.60 25.60 LR Q
Phosmet N.D. 1 1.44 1.72 144.00 172.00 17.72 HR
Piperonyl butoxide N.D. 1 1.01 1.12 101.00 112.00 10.33
Prallethrin N.D. 1 1.8 2.02 180.00 202.00 11.52 HR
Propiconazole N.D. 1 1.14 1.3 114.00 130.00 13.11
Propoxur N.D. 1 1.26 1.38 126.00 138.00 9.09 HR
Pyrethrin N.D. 0.65 0.675 0.897 103.85 138.00 28.24 HRQ
Pyridaben N.D. 1 0.719 0.846 71.90 84.60 16.23
SpinosynA N.D. 0.84 1.36 1.51 161.90 179.76 10.45 HR
SpinosynD N.D. 0.16 0.283 0.314 176.88 196.25 10.39 HR
Spiromesifen N.D. 1 0.202 0.239 20.20 23.90 16.78 LR
Spirotetramat N.D. 1 1.4 1.54 140.00 154.00 9.52 HR
Spiroxamine N.D. 1 1.92 1.99 192.00 199.00 3.58 HR
Tebuconazole N.D. 1 1.77 2.01 177.00 201.00 12.70 HR
Thiacloprid N.D. 1 1.54 1.55 154.00 155.00 0.65 HR
Thiamethoxam N.D. 1 2.09 2.13 209.00 213.00 1.90 HR
Trifloxystrobin N.D. 1 1.21 1.38 121.00 138.00 13.13 HR

N.D. = Not Detected

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 30%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (60-120%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 6 of 12

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents Analysis by
Mass Spectrometer

Testing Accreditation #: 4092-005 Test Certificate #: 128636-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Mach 4
License: 030-1009646F7F8
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A401030002C949000001400
Metrc Source Pkg#: 1A401030002C949000001336

Test Conditions

Prepsheet ID#: ORHS210112a
Scale: XS205-OR1
Temp: 19.8 °C
Baro PE: 1007 hPa
Analyst: HRM
Technician: HRM

Sample ID#: 128636

Lot #: Mach 4 #1 1.1.2021
Batch #: 128636
Batch Weight (g): 572
Harvest/Process Date: 01/01/2021
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 01/06/2021
Test Date: 01/12/2021

Sample #128636
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
1,2-Dichloroethane 2 1 Not Tested 1,2-Dimethoxyethane 100 5 Pass/<LOD
1,4-dioxane 380 200 Pass/<LOD 1-Butanol 5,000 100 Pass/<LOD
1-Pentanol 5,000 100 Pass/<LOD 1-Propanol 5,000 100 Pass/<LOD
2,2-Dimethylpropane (Neopentane) 5,000 100 Pass/<LOD 2,2-Dimethylbutane (Hexanes) 290 100 Pass/<LOD
2,3-Dimethylbutane (Hexanes) 290 100 Pass/<LOD 2-Butanol 5,000 100 Pass/<LOD
2-Butanone (MEK) 5,000 50 Pass/<LOD 2-Ethoxyethanol 160 40 Pass/<LOD
2-Methylbutane (Isopentane) 5,000 50 Pass/<LOD 2-Methylpentane (Hexanes) 290 50 Pass/<LOD
2-Methylpropane (Isobutane) 5,000 100 Pass/<LOD 2-propanol (Isopropyl Alcohol) 5,000 50 Pass/<LOD
2-Propanone (Acetone) 5,000 50 Pass/<LOD 3-Methylpentane (Hexanes) 290 50 Pass/<LOD
Acetonitrile 410 100 Pass/<LOD Benzene 2 1 Pass/<LOD
Butane 5,000 100 Pass/2,021 Chloroform 2 1 Pass/<LOD
Cumene 70 50 Pass/<LOD Cyclohexane 3,880 1,000 Pass/<LOD
Dichloromethane 600 50 Pass/<LOD Dimethylsulfoxide (DMSO) 5,000 500 Pass/<LOD
Ethanol 5,000 500 Pass/<LOD Ethyl acetate 5,000 50 Pass/<LOD
Ethyl ether 5,000 500 Pass/<LOD Ethylene glycol 620 310 Pass/<LOD
Ethylene oxide 50 50 Pass/<LOD Heptane 5,000 50 Pass/<LOD
Hexane 290 290 Pass/<LOD Isopropyl acetate 5,000 50 Pass/<LOD
Methanol 3,000 500 Pass/<LOD Naptha 400 100 Not Tested
N,N-Dimethylacetamide 1,090 100 Pass/<LOD N,N-Dimethylformamide (DMF) 880 500 Pass/<LOD
Pentane 5,000 50 Pass/<LOD Petroleum Ether 400 100 Not Tested
Propane 5,000 100 Pass/<LOD Pyridine 200 10 Pass/<LOD
Sulfolane 160 200 Pass/<LOD Tetrahydrofuran (THF) 720 200 Pass/<LOD
Toluene 890 50 Pass/<LOD Trichloroethylene 25 5 Not Tested
Xylenes* 2,170 50 Pass/<LOD

Total Butanes = 2021 ug/g (PASS); Total Pentanes = 0 ug/g (PASS); Total Hexanes = 0 ug/g (PASS)

* Xylenes are reported as the sum of o-xylene, m-xylene, p-xylene, and ethylbenzene
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 7 of 12

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents QC Report

Testing Accreditation #: 4092-005 Test Certificate #: 128636-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Mach 4
License: 030-1009646F7F8
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A401030002C949000001400
Metrc Source Pkg#: 1A401030002C949000001336

Test Conditions

Prepsheet ID#: ORHS210112a
Scale: XS205-OR1
Temp: 19.8 °C
Baro PE: 1007 hPa
Analyst: HRM
Technician: HRM

Sample ID#: 128636

Lot #: Mach 4 #1 1.1.2021
Batch #: 128636
Batch Weight (g): 572
Harvest/Process Date: 01/01/2021
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 01/06/2021
Test Date: 01/12/2021

Sample #128636
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS Recovery (%) MSD Recovery (%) Relative Percent Difference (%) QC Flag
1,2-Dichloroethane N.D. 0 0 0 nan nan
n-Propane N.D. 250 295 294 118.00 117.60 0.34
Isobutane N.D. 250 246 237 98.40 94.80 3.73
Methanol N.D. 250 190 135 76.00 54.00 33.85 LRQ
n-Butane N.D. 250 296 212 118.40 84.80 33.07 Q
2,2-Dimethylpropane N.D. 250 239 249 95.60 99.60 4.10
Ethanol N.D. 250 287 292 114.80 116.80 1.73
Isopentane N.D. 250 259 256 103.60 102.40 1.17
Acetonitrile N.D. 250 208 198 83.20 79.20 4.93
Diethyl ether N.D. 250 352 353 140.80 141.20 0.28 HR
2-propanone N.D. 250 219 201 87.60 80.40 8.57
2-propanol N.D. 250 222 274 88.80 109.60 20.97 Q
n-Pentane N.D. 250 240 244 96.00 97.60 1.65
2,2-Dimethylbutane N.D. 250 244 246 97.60 98.40 0.82
2,3-Dimethylbutane N.D. 250 225 246 90.00 98.40 8.92
Methylene chloride N.D. 250 283 289 113.20 115.60 2.10
2-Methylpentane N.D. 250 215 231 86.00 92.40 7.17
3-Methylpentane N.D. 250 212 220 84.80 88.00 3.70
2-Butanol N.D. 250 296 298 118.40 119.20 0.67
n-Hexane N.D. 250 375 387 150.00 154.80 3.15 HR
Ethyl acetate N.D. 250 289 294 115.60 117.60 1.72
Tetrahydrofuran N.D. 250 313 320 0.00 0.00 0.00
Trichloroethylene N.D. 0 0 0 nan nan
Isopropyl acetate N.D. 250 305 312 0.00 0.00 0.00
Benzene N.D. 250 290 295 116.00 118.00 1.71
Chloroform N.D. 0 0 0 nan nan
Cyclohexane N.D. 250 366 364 146.40 145.60 0.55 HR
Ethylene glycol N.D. 250 324 330 129.60 132.00 1.83 HR
Heptane N.D. 250 379 363 151.60 145.20 4.31 HR
2-Ethoxyethanol N.D. 250 343 276 137.20 110.40 21.65 HRQ
1,4-Dioxane N.D. 250 288 297 115.20 118.80 3.08
Pyridine N.D. 0 0 0 0.00 0.00 0.00
Toluene N.D. 250 286 290 114.40 116.00 1.39
Chlorobenzene N.D. 0 0 0 0.00 0.00 0.00
Ethylbenzene N.D. 250 289 295 115.60 118.00 2.05
m-Xylene/p-Xylene N.D. 500 580 591 116.00 118.20 1.88
o-Xylene N.D. 250 293 297 117.20 118.80 1.36
Cumene N.D. 250 291 293 116.40 117.20 0.68
Ethylene oxide N.D. 250 336 333 134.40 133.20 0.90 HR

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

N.D. = Not Detected

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 8 of 12

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents Analysis by
Mass Spectrometer

Testing Accreditation #: 4092-005 Test Certificate #: 128636-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Mach 4
License: 030-1009646F7F8
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A401030002C949000001400
Metrc Source Pkg#: 1A401030002C949000001336

Test Conditions

Prepsheet ID#: ORHS210112a
Scale: XS205-OR1
Temp: 19.8 °C
Baro PE: 1007 hPa
Analyst: HRM
Technician: HRM

Sample ID#: 128636

Lot #: Mach 4 #1 1.1.2021
Batch #: 128636
Batch Weight (g): 572
Harvest/Process Date: 01/01/2021
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 01/06/2021
Test Date: 01/12/2021

Sample #128636
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
1,2-Dichloroethane 2 1 Not Tested 1,2-Dimethoxyethane 100 5 Pass/<LOD
1,4-dioxane 380 200 Pass/<LOD 1-Butanol 5,000 100 Pass/<LOD
1-Pentanol 5,000 100 Pass/<LOD 1-Propanol 5,000 100 Pass/<LOD
2,2-Dimethylpropane (Neopentane) 5,000 100 Pass/<LOD 2,2-Dimethylbutane (Hexanes) 290 100 Pass/<LOD
2,3-Dimethylbutane (Hexanes) 290 100 Pass/<LOD 2-Butanol 5,000 100 Pass/<LOD
2-Butanone (MEK) 5,000 50 Pass/<LOD 2-Ethoxyethanol 160 40 Pass/<LOD
2-Methylbutane (Isopentane) 5,000 50 Pass/<LOD 2-Methylpentane (Hexanes) 290 50 Pass/<LOD
2-Methylpropane (Isobutane) 5,000 100 Pass/<LOD 2-propanol (Isopropyl Alcohol) 5,000 50 Pass/<LOD
2-Propanone (Acetone) 5,000 50 Pass/<LOD 3-Methylpentane (Hexanes) 290 50 Pass/<LOD
Acetonitrile 410 100 Pass/<LOD Benzene 2 1 Pass/<LOD
Butane 5,000 100 Pass/2,278 Chloroform 2 1 Pass/<LOD
Cumene 70 50 Pass/<LOD Cyclohexane 3,880 1,000 Pass/<LOD
Dichloromethane 600 50 Pass/<LOD Dimethylsulfoxide (DMSO) 5,000 500 Pass/<LOD
Ethanol 5,000 500 Pass/<LOD Ethyl acetate 5,000 50 Pass/<LOD
Ethyl ether 5,000 500 Pass/<LOD Ethylene glycol 620 310 Pass/<LOD
Ethylene oxide 50 50 Pass/<LOD Heptane 5,000 50 Pass/<LOD
Hexane 290 290 Pass/<LOD Isopropyl acetate 5,000 50 Pass/<LOD
Methanol 3,000 500 Pass/<LOD Naptha 400 100 Not Tested
N,N-Dimethylacetamide 1,090 100 Pass/<LOD N,N-Dimethylformamide (DMF) 880 500 Pass/<LOD
Pentane 5,000 50 Pass/<LOD Petroleum Ether 400 100 Not Tested
Propane 5,000 100 Pass/<LOD Pyridine 200 10 Pass/<LOD
Sulfolane 160 200 Pass/<LOD Tetrahydrofuran (THF) 720 200 Pass/<LOD
Toluene 890 50 Pass/<LOD Trichloroethylene 25 5 Not Tested
Xylenes* 2,170 50 Pass/<LOD

Total Butanes = 2278 ug/g (PASS); Total Pentanes = 0 ug/g (PASS); Total Hexanes = 0 ug/g (PASS)

* Xylenes are reported as the sum of o-xylene, m-xylene, p-xylene, and ethylbenzene
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 9 of 12

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents QC Report

Testing Accreditation #: 4092-005 Test Certificate #: 128636-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Mach 4
License: 030-1009646F7F8
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A401030002C949000001400
Metrc Source Pkg#: 1A401030002C949000001336

Test Conditions

Prepsheet ID#: ORHS210112a
Scale: XS205-OR1
Temp: 19.8 °C
Baro PE: 1007 hPa
Analyst: HRM
Technician: HRM

Sample ID#: 128636

Lot #: Mach 4 #1 1.1.2021
Batch #: 128636
Batch Weight (g): 572
Harvest/Process Date: 01/01/2021
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 01/06/2021
Test Date: 01/12/2021

Sample #128636
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS Recovery (%) MSD Recovery (%) Relative Percent Difference (%) QC Flag
1,2-Dichloroethane N.D. 0 0 0 nan nan
n-Propane N.D. 250 295 294 118.00 117.60 0.34
Isobutane N.D. 250 246 237 98.40 94.80 3.73
Methanol N.D. 250 190 135 76.00 54.00 33.85 LRQ
n-Butane N.D. 250 296 212 118.40 84.80 33.07 Q
2,2-Dimethylpropane N.D. 250 239 249 95.60 99.60 4.10
Ethanol N.D. 250 287 292 114.80 116.80 1.73
Isopentane N.D. 250 259 256 103.60 102.40 1.17
Acetonitrile N.D. 250 208 198 83.20 79.20 4.93
Diethyl ether N.D. 250 352 353 140.80 141.20 0.28 HR
2-propanone N.D. 250 219 201 87.60 80.40 8.57
2-propanol N.D. 250 222 274 88.80 109.60 20.97 Q
n-Pentane N.D. 250 240 244 96.00 97.60 1.65
2,2-Dimethylbutane N.D. 250 244 246 97.60 98.40 0.82
2,3-Dimethylbutane N.D. 250 225 246 90.00 98.40 8.92
Methylene chloride N.D. 250 283 289 113.20 115.60 2.10
2-Methylpentane N.D. 250 215 231 86.00 92.40 7.17
3-Methylpentane N.D. 250 212 220 84.80 88.00 3.70
2-Butanol N.D. 250 296 298 118.40 119.20 0.67
n-Hexane N.D. 250 375 387 150.00 154.80 3.15 HR
Ethyl acetate N.D. 250 289 294 115.60 117.60 1.72
Tetrahydrofuran N.D. 250 313 320 0.00 0.00 0.00
Trichloroethylene N.D. 0 0 0 nan nan
Isopropyl acetate N.D. 250 305 312 0.00 0.00 0.00
Benzene N.D. 250 290 295 116.00 118.00 1.71
Chloroform N.D. 0 0 0 nan nan
Cyclohexane N.D. 250 366 364 146.40 145.60 0.55 HR
Ethylene glycol N.D. 250 324 330 129.60 132.00 1.83 HR
Heptane N.D. 250 379 363 151.60 145.20 4.31 HR
2-Ethoxyethanol N.D. 250 343 276 137.20 110.40 21.65 HRQ
1,4-Dioxane N.D. 250 288 297 115.20 118.80 3.08
Pyridine N.D. 0 0 0 0.00 0.00 0.00
Toluene N.D. 250 286 290 114.40 116.00 1.39
Chlorobenzene N.D. 0 0 0 0.00 0.00 0.00
Ethylbenzene N.D. 250 289 295 115.60 118.00 2.05
m-Xylene/p-Xylene N.D. 500 580 591 116.00 118.20 1.88
o-Xylene N.D. 250 293 297 117.20 118.80 1.36
Cumene N.D. 250 291 293 116.40 117.20 0.68
Ethylene oxide N.D. 250 336 333 134.40 133.20 0.90 HR

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

N.D. = Not Detected

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

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ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Homogeneity Report by
High Performance Liquid Chromatography

Testing Accreditation #: 4092-005 Test Certificate #: 128636-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Mach 4
License: 030-1009646F7F8
Type: AU Tincture
Metrc Test Pkg#: 1A401030002C949000001400
Metrc Source Pkg#: 1A401030002C949000001336

Sample ID#: 128636

Lot #: Mach 4 #1 1.1.2021
Batch #: 128636
Batch Weight (g): 572
Harvest/Process Date: 01/01/2021
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 01/06/2021

Sample #128636
Increments Tested (mg/g) TOTAL THC TOTAL CBD THC THCA THCV CBD CBC CBDA CBDV CBG CBN
Increment 1 807.93 15.42 84.70 824.66 N.D. N.D. 1.68 17.58 N.D. 4.15 N.D.
Increment 2 825.35 15.69 84.80 844.41 N.D. N.D. 1.83 17.89 N.D. 4.28 N.D.
Average Value 816.64 15.55 84.75 834.54 N.D. N.D. 1.76 17.74 N.D. 4.22 N.D.
Max Value 825.35 15.69 84.80 844.41 N.D. N.D. 1.83 17.89 N.D. 4.28 N.D.
Min Value 807.93 15.42 84.70 824.66 N.D. N.D. 1.68 17.58 N.D. 4.15 N.D.
Relative Percent Difference (RPD) ±2.13 ±1.75 ±0.12 ±2.37 N.D. N.D. ±8.55 ±1.75 N.D. ±3.08 N.D.
Average Cannabinoids Per Package 816.64 15.55 84.75 834.54 N.D. N.D. 1.76 17.74 N.D. 4.22 N.D.
Average Cannabinoids Per Serving 40.83 0.78 4.24 41.73 N.D. N.D. 0.09 0.89 N.D. 0.21 N.D.
Max Concentration Per Serving (THC)   Pass
Max Concentration Per Package (THC)   Not Applicable
Relative Percent Difference (RPD)   Pass
Control Study   Yes, 554574
Field Duplicate   Pass

N.D. = Not Detected, Min = Minimum, Max = Maximum

RPD is the relative percent difference between increment 1 and increment 2.

RSD is the relative standard deviation between all increments tested.

Total THC and CBD is the calculated sum of CBD or THC and the amount of CBD or THC derived from CBDA or THCA, respectively. These values are calculated by adding a molar correction factor of 0.877 to the CBDA or THCA value.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Terry Rabinowitz Iron laboratories Terry Rabinowitz

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 11 of 12

IRON Laboratories

Terpene Report by
Mass Spectrometer

Test Certificate #: 128636-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Mach 4
License: 030-1009646F7F8
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A401030002C949000001400
Metrc Source Pkg#: 1A401030002C949000001336

Test Conditions

Scale: XS205-OR1
Temp: 19.8 °C
Baro Pressure: 1007 hPa
Analyst: HRM
Technician: HRM

Sample ID#: 128636

Lot #: Mach 4 #1 1.1.2021
Batch #: 128636
Batch Weight (g): 572
Harvest/Process Date: 01/01/2021
Serving Size (g): 0.05
Date Received: 01/06/2021

Sample #128636
Sample #128636
  • α-Pinene (0.07%)
  • β-Ocimene (0.05%)
  • Camphene (0.02%)
  • Eucalyptol (1,8-Cineol) (0.00%)
  • Sabinene (0.00%)
  • γ-Terpinene (0.02%)
  • Myrcene (0.74%)
  • α-Terpinolene (0.11%)
  • β-Pinene (0.56%)
  • Linalool (0.89%)
  • ∆3-Carene (0.00%)
  • Fenchone (0.00%)
  • α-Terpinene (0.02%)
  • endo-Fenchol (0.21%)
  • α-Ocimene (0.00%)
  • Isopulegol (0.00%)
  • Limonene (0.49%)
  • Geraniol (0.02%)
  • p-Cymene (0.00%)
  • β-Caryophyllene (0.16%)
  • α-Humulene (1.17%)
  • Nerolidol 1 (cis) (0.03%)
  • Nerolidol 2 (trans) (0.05%)
  • Guaiol (0.02%)
  • Caryophyllene Oxide (0.29%)
  • α-Bisabolol (0.12%)
  • α-Phellandrene (0.11%)
  • α-Terpineol (0.13%)
  • Valenence (0.00%)

Total: 5.280%

Predominant Terpenes

1.17%   α-Humulene Woody, oceanic-watery, spicy clove 0.89%   Linalool Citrus, floral, sweet, bois de rose, woody, green, blueberry
0.74%   Myrcene Peppery, spicy balsam 0.56%   β-Pinene Woody, fresh pine, hay
0.49%   Limonene Citrus, orange, sweet 0.29%   Caryophyllene Oxide Sweet, fresh, woody, spicy

Value in parenthesis indicates percentage of terpene present in the total sample (weight percentage, wt/wt%).
Value in doughnut slice indicates individual terpene abundance with respect to the total terpenes detected.

This sample has not been tested according to OAR 333-007. These results should therefore be used for research and development or quality control purposes only.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Himashi Mead Iron laboratories Himashi Mead

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 12 of 12