ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Marijuana Potency Analysis by
High Performance Liquid Chromatography
Testing Accreditation #: 4092-005 Test Certificate #: 128332-001
Client Name, Sample Details

45th Parallel Farms LLC
Dallas, OR 97338
Sample: Northern Wreck Shake
License: 010-100164183CE
Type: Adult Use Flower
Method: FE04U HPLC-UV
Metrc Test Pkg#: 1A4010300000DAD000003775
Metrc Source Pkg#: 1A4010300000DAD000003759
***Water Activity: 0.481
***Moisture: 9.96%
Test Conditions

Prepsheet ID#: ORP201221a
Scale: XS205-OR1
Temp: 22.2 °C
Baro Pressure: 1006 hPa
Analyst: TMR
Technician: TMR
Sample ID#: 128332

Lot #: Northern Wreck 10/08/20
Batch #: 128332
Batch Weight (g): 6810
Harvest/Process Date: 10/08/2020
Date Received: 12/18/2020
Test Date: 12/21/2020
Sample #128332
Sample #128332 Sample #128332
Test
Compounds		 THC THCA CBD CBDA CBN CBG CBC THCV* CBDV Total
Cannabinoids*		 Total THC Total CBD Calc Max Total
Cannabinoids*
Amount (%) 1.74 32.25 N/D 1.00 N/D 0.25 N/D N/D N/D 35.24 30.02 0.88 31.15
Amount (mg/g) 17.35 322.48 N/D 10.01 N/D 2.53 N/D N/D N/D 352.37 300.16 8.78 311.47
Amount per Serving (mg) N\D N\D N\D N\D N\D N\D N\D N\D N\D 0.00 Serving Size~ (g): 0.00
LOQ (mg/g) 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5   %Decarb. THC CBD
±%RPD 12.21 8.74 17.27 16.87 10.10 12.40 24.66 +/-5% +/-5% 5 0

LOQ = Limit of Quantitation; %RPD = Relative Percent Deviation; %RSD = Relative Standard Deviation; N/D = Not Detected

*Designates values that are not currently included in the accredited scope of Iron Laboratories.

*** Designates tests that use the method FE-45. FE-45 is performed using AOAC 966.02 and 32.004-32.009. FE-45 has relative expanded (k=2) uncertainties of 1.098% for moisture, 1.754% for water activity for unprocessed plant materials, and 13.102% for water activity for infused products. Vitamin E acetate analysis has a relative expanded (k=2) uncertainty of 18.614%.

Total THC and CBD is the calculated sum of THC or CBD and the amount of THC or CBD derived from THCA or CBDA, respectively. These values are calculated by applying a molar correction factor of 0.877 to the THCA or the CBDA value. Calc Max Total Cannabinoids is the sum of Total THC, Total CBD, CBN, CBG, CBC, THCV, and CBDV.

%Decarb. THC and CBD refer to the percentage of THC or CBD relative to THCA or CBDA, respectively.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 1 of 4

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant QC Report
Testing Accreditation #: 4092-005 Test Certificate #: 128332-001
Client Name, Sample Details

45th Parallel Farms LLC
Dallas, OR 97338
Sample: Northern Wreck Shake
License: 010-100164183CE
Type: Adult Use Flower
Method: FE04U HPLC-UV
Metrc Test Pkg#: 1A4010300000DAD000003775
Metrc Source Pkg#: 1A4010300000DAD000003759
***Water Activity: 0.481
***Moisture: 9.96%
Test Conditions

Prepsheet ID#: ORP201221a
Scale: XS205-OR1
Temp: 22.2 °C
Baro Pressure: 1006 hPa
Analyst: TMR
Technician: TMR
Sample ID#: 128332

Lot #: Northern Wreck 10/08/20
Batch #: 128332
Batch Weight (g): 6810
Harvest/Process Date: 10/08/2020
Date Received: 12/18/2020
Test Date: 12/21/2020
Sample #128332
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Cannabidivarin (CBDV) N.D. 1 0 0.00 0 0.00 0
Cannabidiolic Acid (CBDA) N.D. 11.56 13.37 115.66 11.29 97.66 16.87
Cannabigerol (CBG) N.D. 1.09 1.37 125.69 1.21 111.01 12.40
Cannabidiol (CBD) N.D. 6.5 7.11 109.38 5.98 92.00 17.27
Δ9-Tetrahydrocannabivarin (THCV) N.D. 1 0 0.00 0 0.00 0
Cannabinol (CBN) N.D. 0.44 0.52 118.18 0.47 106.82 10.10
Δ9-Tetrahydrocannabinol (THC) N.D. 29.39 32.68 111.19 28.92 98.40 12.21
Cannabichromene (CBC) N.D. 0.65 0.64 98.46 0.82 126.15 24.66 Q
Tetrahydrocannabinolic acid (THCA) N.D. 57.25 63.98 111.76 58.62 102.39 8.74

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 2 of 4

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Pesticide Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-005 Test Certificate #: 128332-001
Client Name, Sample Details

45th Parallel Farms LLC
Dallas, OR 97338
Sample: Northern Wreck Shake
License: 010-100164183CE
Type: Adult Use Flower
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A4010300000DAD000003775
Metrc Source Pkg#: 1A4010300000DAD000003759
Test Conditions

Prepsheet ID#: ORPS201222a
Scale: XS205-OR1
Temp: 22 °C
Baro PE: 1013 hPa
Analyst: HRM
Technician: JBS
Sample ID#: 128332

Lot #: Northern Wreck 10/08/20
Batch #: 128332
Batch Weight (g): 6810
Harvest/Process Date: 10/08/2020
Date Received: 12/18/2020
Test Date: 12/22/2020
Sample #128332
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
Aldicarb 0.400 0.120 Pass/<LOD Abamectin**** 0.500 0.120 Pass/<LOD
Acephate 0.400 0.120 Pass/<LOD Acequinocyl 2.000 0.241 Pass/<LOD
Acetamiprid 0.200 0.120 Pass/<LOD Azoxystrobin 0.200 0.120 Pass/<LOD
Bifenazate 0.200 0.120 Pass/<LOD Bifenthrin 0.200 0.120 Pass/<LOD
Boscalid 0.400 0.120 Pass/<LOD Carbaryl 0.200 0.120 Pass/<LOD
Carbofuran 0.200 0.120 Pass/<LOD Chlorantraniliprole 0.200 0.120 Pass/<LOD
Chlorfenapyr 1.000 0.481 Pass/<LOD Chlorpyrifos 0.200 0.120 Pass/<LOD
Clofentezine 0.200 0.120 Pass/<LOD Cyfluthrin** 1.000 0.481 Pass/<LOD
Cypermethrin*** 1.000 0.481 Pass/<LOD Daminozide 1.000 0.120 Pass/<LOD
DDVP (Dichlorvos) 1.000 0.241 Pass/<LOD Diazinon 0.200 0.120 Pass/<LOD
Dimethoate 0.200 0.120 Pass/<LOD Ethoprophos 0.200 0.120 Pass/<LOD
Etofenprox 0.400 0.120 Pass/<LOD Etoxazole 0.200 0.120 Pass/<LOD
Fenoxycarb 0.200 0.120 Pass/<LOD Fenpyroximate 0.400 0.120 Pass/<LOD
Fipronil 0.400 0.120 Pass/<LOD Flonicamid 1.000 0.120 Pass/<LOD
Fludioxonil 0.400 0.120 Pass/<LOD Hexythiazox 1.000 0.120 Pass/<LOD
Imazalil 0.200 0.120 Pass/<LOD Imidacloprid 0.400 0.120 Pass/<LOD
Kresoxim Methyl 0.400 0.120 Pass/<LOD Malathion 0.200 0.120 Pass/<LOD
Metalaxyl 0.200 0.120 Pass/<LOD Methiocarb 0.200 0.120 Pass/<LOD
Methomyl 0.400 0.120 Pass/<LOD Methyl Parathion 0.200 0.120 Pass/<LOD
MGK-264‡ 0.200 0.120 Pass/<LOD Myclobutanil 0.000 0.120 Pass/<LOD
Naled 0.500 0.120 Pass/<LOD Oxamyl 1.000 0.120 Pass/<LOD
Paclobutrazol 0.400 0.120 Pass/<LOD Permethrins† 0.200 0.120 Pass/<LOD
Phosmet 0.200 0.120 Pass/<LOD Piperonyl Butoxide 2.000 0.120 Pass/<LOD
Prallethrin 0.200 0.120 Pass/<LOD Propiconazole 0.400 0.120 Pass/<LOD
Propoxur 0.200 0.120 Pass/<LOD Pyrethrins* 1.000 0.120 Pass/<LOD
Pyridaben 0.200 0.120 Pass/<LOD Spinosad***** 0.200 0.120 Pass/<LOD
Spiromesifen 0.200 0.120 Pass/<LOD Spirotetramat 0.200 0.120 Pass/<LOD
Spiroxamine‡ 0.400 0.120 Pass/<LOD Tebuconazole 0.400 0.120 Pass/<LOD
Thiacloprid 0.200 0.120 Pass/<LOD Thiamethoxam 0.200 0.120 Pass/<LOD
Trifloxystrobin 0.200 0.120 Pass/<LOD

* Pyrethrins are reported as the sum of Jasmolin I, Cinerin I, and Pyrethrin I
** Cyfluthrins are reported as the sum of isomers Cyfluthrin I, II, III, and IV
*** Cypermethrins are reported as the sum of isomers Cypermethrin I, II, III, and IV
**** Abamectin is reported as the sum of Avermectin B1a and Avermectin B1b
***** Spinosad is reported as the sum of Spinosyn A and Spinosyn D
† Permethrin and Prallethrin are reported as the sum of cis and trans isomers
‡ MGK-264 and Spiroximine are reported as the sum of isomers I and II
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 2 of 4

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-005
OLCC No. 1002158CD2E

Oregon Compliant Pesticide QC Report
Testing Accreditation #: 4092-005 Test Certificate #: 128332-001
Client Name, Sample Details

45th Parallel Farms LLC
Dallas, OR 97338
Sample: Northern Wreck Shake
License: 010-100164183CE
Type: Adult Use Flower
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A4010300000DAD000003775
Metrc Source Pkg#: 1A4010300000DAD000003759
Test Conditions

Prepsheet ID#: ORPS201222a
Scale: XS205-OR1
Temp: 22 °C
Baro PE: 1013 hPa
Analyst: HRM
Technician: JBS
Sample ID#: 128332

Lot #: Northern Wreck 10/08/20
Batch #: 128332
Batch Weight (g): 6810
Harvest/Process Date: 10/08/2020
Date Received: 12/18/2020
Test Date: 12/22/2020
Sample #128332
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS recovery% MSD recovery% Relative Percent Difference (%) QC Flag
Acephate N.D. 1 1.03 0.913 103.00 91.30 12.04
Acequinocyl N.D. 1 0.856 0.633 85.60 63.30 29.95 LR Q
Acetamiprid N.D. 1 1.18 1.07 118.00 107.00 9.78
Aldicarb N.D. 1 1.2 1.1 120.00 110.00 8.70
Avermectin B1a N.D. 0.97 1.25 1.02 128.87 105.15 20.26 Q
Azoxystrobin N.D. 1 1.03 0.968 103.00 96.80 6.21
Bifenazate N.D. 1 1.01 0.956 101.00 95.60 5.49
Bifenthrin N.D. 1 1.06 1.02 106.00 102.00 3.85
Boscalid N.D. 1 0.919 0.786 91.90 78.60 15.60
Carbaryl N.D. 1 1.09 1.02 109.00 102.00 6.64
Carbofuran N.D. 1 1.23 1.13 123.00 113.00 8.47
Chlorantraniliprole N.D. 1 0.938 0.868 93.80 86.80 7.75
Chlorfenapyr N.D. 1 1.32 0.61 132.00 61.00 73.58 LR Q
Chlorpyriphos N.D. 1 1.04 0.917 104.00 91.70 12.57
Clofentezine N.D. 1 0.838 0.801 83.80 80.10 4.51
Cyfluthrin N.D. 1 1.27 1.04 127.00 104.00 19.91
Cypermethrin N.D. 1 1.29 1.09 129.00 109.00 16.81
Daminoside N.D. 1 0.513 0.421 51.30 42.10 19.70 LR
Diazanon N.D. 1 3.07 2.75 307.00 275.00 11.00 HR
Dichlorvos N.D. 1 1.21 1.11 121.00 111.00 8.62
Dimethoate N.D. 1 1.1 1.02 110.00 102.00 7.55
Ethoprophos N.D. 1 0.929 0.809 92.90 80.90 13.81
Etofenprox N.D. 1 1.17 1.07 117.00 107.00 8.93
Etoxazole N.D. 1 1.24 1.09 124.00 109.00 12.88
Fenoxycarb N.D. 1 0.867 0.777 86.70 77.70 10.95
Fenpyroximate N.D. 1 1.25 1.08 125.00 108.00 14.59
Fipronil N.D. 1 1.28 1.09 128.00 109.00 16.03
Flonicamid N.D. 1 1.16 1.03 116.00 103.00 11.87
Fludioxonil N.D. 1 1.46 1.24 146.00 124.00 16.30 HR
Hexythiazox N.D. 1 0.466 0.473 46.60 47.30 1.49 LR
Imazalil N.D. 1 0.964 0.883 96.40 88.30 8.77
Imidacloprid N.D. 1 1.24 1.02 124.00 102.00 19.47
Kresoxim-methyl N.D. 1 0.844 0.754 84.40 75.40 11.26
Malathion N.D. 1 0.899 0.843 89.90 84.30 6.43
Metalaxyl N.D. 1 1.06 0.958 106.00 95.80 10.11
Methiocarb N.D. 1 1.15 1.08 115.00 108.00 6.28
Methomyl N.D. 1 0.96 0.858 96.00 85.80 11.22
MGK-264 N.D. 1 0.998 0.844 99.80 84.40 16.72
Myclobutanil N.D. 1 1.04 0.91 104.00 91.00 13.33
Naled (dibrom) N.D. 1 0.371 0.375 37.10 37.50 1.07 LR
Oxamyl N.D. 1 1.3 1.17 130.00 117.00 10.53
Paclobutrazol N.D. 1 1 0.878 100.00 87.80 12.99
Parathion-methyl N.D. 1 1.14 1.04 114.00 104.00 9.17
Permethrins N.D. 1 1.14 1.009 114.00 100.90 12.19
Phosmet N.D. 1 0.849 0.78 84.90 78.00 8.47
Piperonyl butoxide N.D. 1 1.1 1 110.00 100.00 9.52
Prallethrin N.D. 1 0.886 0.786 88.60 78.60 11.96
Propiconazole N.D. 1 0.938 0.816 93.80 81.60 13.91
Propoxur N.D. 1 1.15 1.06 115.00 106.00 8.14
Pyrethrin N.D. 0.65 0.5 0.5 76.92 76.92 0.00
Pyridaben N.D. 1 1.08 0.991 108.00 99.10 8.59
SpinosynA N.D. 0.84 0.707 0.648 84.17 77.14 8.71
SpinosynD N.D. 0.16 0.136 0.142 85.00 88.75 4.32
Spiromesifen N.D. 1 0.273 0.261 27.30 26.10 4.49 LR
Spirotetramat N.D. 1 0.947 0.834 94.70 83.40 12.69
Spiroxamine N.D. 1 0.982 0.883 98.20 88.30 10.62
Tebuconazole N.D. 1 0.896 0.789 89.60 78.90 12.70
Thiacloprid N.D. 1 1.09 1.01 109.00 101.00 7.62
Thiamethoxam N.D. 1 0.946 0.868 94.60 86.80 8.60
Trifloxystrobin N.D. 1 1.13 1.01 113.00 101.00 11.21

N.D. = Not Detected

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 30%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (60-120%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 3 of 4
IRON Laboratories

Terpene Report by
Mass Spectrometer
Test Certificate #: 128332-001
Client Name, Sample Details

45th Parallel Farms LLC
Dallas, OR 97338
Sample: Northern Wreck Shake
License: 010-100164183CE
Type: Adult Use Flower
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A4010300000DAD000003775
Metrc Source Pkg#: 1A4010300000DAD000003759

Test Conditions

Scale: XS205-OR1
Temp: 22.1 °C
Baro Pressure: 1012 hPa
Analyst: JBS
Technician: HRM

Sample ID#: 128332

Lot #: Northern Wreck 10/08/20
Batch #: 128332
Batch Weight (g): 6810
Harvest/Process Date: 10/08/2020
Date Received: 12/18/2020

Sample #128332
Sample #128332
  • α-Pinene (0.00%)
  • β-Ocimene (0.05%)
  • Camphene (0.00%)
  • Eucalyptol (1,8-Cineol) (0.02%)
  • Sabinene (0.00%)
  • γ-Terpinene (0.00%)
  • Myrcene (0.24%)
  • α-Terpinolene (0.00%)
  • β-Pinene (0.20%)
  • Linalool (0.32%)
  • ∆3-Carene (0.00%)
  • Fenchone (0.00%)
  • α-Terpinene (0.00%)
  • endo-Fenchol (0.03%)
  • α-Ocimene (0.00%)
  • Isopulegol (0.00%)
  • Limonene (0.10%)
  • Geraniol (0.00%)
  • p-Cymene (0.00%)
  • β-Caryophyllene (0.17%)
  • α-Humulene (0.65%)
  • Nerolidol 1 (cis) (0.00%)
  • Nerolidol 2 (trans) (0.05%)
  • Guaiol (0.22%)
  • Caryophyllene Oxide (0.08%)
  • α-Bisabolol (0.25%)
  • α-Phellandrene (0.02%)
  • α-Terpineol (0.02%)
  • Valenence (0.20%)

Total: 2.620%

Predominant Terpenes

0.65%   α-Humulene Woody, oceanic-watery, spicy clove 0.32%   Linalool Citrus, floral, sweet, bois de rose, woody, green, blueberry
0.25%   α-Bisabolol Fruity, nutty, coconut 0.24%   Myrcene Peppery, spicy balsam
0.22%   Guaiol Mild, guaiacwood, tea, rose 0.20%   Valenence Sweet, citrus, grapefruit, woody, orange

Value in parenthesis indicates percentage of terpene present in the total sample (weight percentage, wt/wt%).
Value in doughnut slice indicates individual terpene abundance with respect to the total terpenes detected.

This sample has not been tested according to OAR 333-007. These results should therefore be used for research and development or quality control purposes only.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Himashi Mead Iron laboratories Himashi Mead

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 4 of 4