Harvest/Process Date: 12/04/2020 Serving Size (g): 1 Date Received: 12/04/2020 Test Date: 12/04/2020 Valid Through: 12/05/2021 Report Issued: 12/07/2020
Test Compounds
THC
THCA
CBD
CBDA
CBN
CBG*
CBC*
THCV*
CBDV*
Total Cannabinoids*
Total THC
Total CBD
Calc Max Total Cannabinoids*
Amount (%)
1.5
25.3
N/D
0.7
0.3
0.2
N/D
N/D
N/D
28.0
23.7
0.6
24.8
Amount (mg/g)
15.3
252.9
N/D
7.0
3.0
1.7
N/D
N/D
N/D
279.9
237.0
6.2
247.9
Amount per Serving (mg)
15.3
252.9
N\D
7.0
3.0
1.7
N\D
N\D
N\D
279.9
Serving Size~ (g):
1.0
LOQ (mg/g)
0.99
0.99
0.99
0.99
0.99
0.99
0.99
0.99
0.99
%Decarb.
THC
CBD
±%RPD
1.60
2.87
3.89
2.01
3.11
2.90
3.14
3.41
2.94
6
0%
LOQ = Limit of Quantitation; %RPD = Relative Percent Deviation; %RSD = Relative Standard Deviation; N/D = Not Detected
*Designates values that are not currently included in the accredited scope of Iron Laboratories.
*** Designates tests that use the method FE-45. FE-45 is performed using AOAC 966.02 and 32.004-32.009. FE-45 has relative expanded (k=2) uncertainties of 1.098% for moisture, 1.754% for water activity for unprocessed plant materials, and 13.102% for water activity for infused products. Vitamin E acetate analysis has a relative expanded (k=2) uncertainty of 18.614%.
Total THC and CBD is the calculated sum of THC or CBD and the amount of THC or CBD derived from THCA or CBDA, respectively. These values are calculated by applying a molar correction factor of 0.877 to the THCA or the CBDA value. Calc Max Total Cannabinoids is the sum of Total THC, Total CBD, CBN, CBG, CBC, THCV, and CBDV.
%Decarb. THC and CBD refer to the percentage of THC or CBD relative to THCA or CBDA, respectively.
This sample has not undergone random sampling and has not been tested for compliant state, batch representative testing. These results should therefore be used for research and development or quality control purposes only. Results apply to the sample as received.
This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Iron Laboratories, LLC is an ISO/IEC 17025:2017 Testing Laboratory laboratory accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802
Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390
Page 1 of 2
ISO/IEC 17025:2017 Accredited
QC Report
Testing Accreditation #: 77802
Test Certificate #: 128045-001
Client Name, Sample Details
Hempress Farms
Walled Lake,
MI
48390 Sample: Blue Sun Type: Flower Method: FE04U HPLC-UV
Harvest/Process Date: 12/04/2020 Serving Size (g): 1 Date Received: 12/04/2020 Test Date: 12/04/2020 Valid Through: 12/05/2021 Report Issued: 12/07/2020
Target Compound Name
Method Blank (μg/g)
LCS Spike (μg/g)
LCS Amount (μg/g)
Percent Recovery (%) LCS
LCS Duplicate Amount (μg/g)
Percent Recovery (%) LCSD
Relative Percent Difference (%)
QC Flag
Cannabidivarin (CBDV)
0
5.74
5.92777
103.27
6.10487
106.36
2.94
Cannabidiolic Acid (CBDA)
0
5.4939
5.72691
104.24
5.84299
106.35
2.01
Cannabigerol (CBG)
0
5.64962
5.87116
103.92
6.04422
106.98
2.90
Cannabidiol (CBD)
0
5.64653
5.84158
103.45
6.0734
107.56
3.89
Δ9-Tetrahydrocannabivarin (THCV)
0
5.68031
5.91336
104.10
6.11841
107.71
3.41
Cannabinol (CBN)
0
5.26182
5.50299
104.58
5.67682
107.89
3.11
Δ9-Tetrahydrocannabinol (THC)
0
6.26104
6.46344
103.23
6.56747
104.89
1.60
Cannabichromene (CBC)
0
5.48605
5.76629
105.11
5.95016
108.46
3.14
Tetrahydrocannabinolic acid (THCA)
0
5.2738
5.48884
104.08
5.64847
107.10
2.87
N.D. = Not Detected
LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.
I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.
Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%
HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.
This sample has not undergone random sampling and has not been tested for compliant state, batch representative testing. These results should therefore be used for research and development or quality control purposes only. Results apply to the sample as received.
This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Iron Laboratories, LLC is an ISO/IEC 17025:2017 Testing Laboratory laboratory accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802
Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390
Page 2 of 2
ISO/IEC 17025:2017 Accredited
Terpene Report by Mass Spectrometer
Testing Accreditation #: 77802
Test Certificate #: 128045-001
Client Name, Sample Details
Hempress Farms
Walled Lake,
MI
48390 Sample: Blue Sun Type: Flower Method: SOP FE-44-MI
Harvest/Process Date: 12/04/2020 Serving Size (g): 1 Date Received: 12/04/2020
α-Pinene (0.18%)
β-Ocimene (0.04%)
Camphene (0.03%)
Eucalyptol (1,8-Cineol) (0.00%)
Sabinene (0.00%)
γ-Terpinene (0.00%)
Myrcene (0.16%)
α-Terpinolene (0.01%)
β-Pinene (0.18%)
Linalool (0.26%)
∆3-Carene (0.00%)
Fenchone (0.00%)
α-Terpinene (0.00%)
endo-Fenchol (0.00%)
α-Ocimene (0.00%)
Isopulegol (0.00%)
Limonene (0.48%)
Geraniol (0.01%)
p-Cymene (0.00%)
β-Caryophyllene (0.19%)
α-Humulene (0.06%)
Nerolidol 1 (cis) (0.00%)
Nerolidol 2 (trans) (0.00%)
Guaiol (0.00%)
Caryophyllene Oxide (0.00%)
α-Bisabolol (0.09%)
α-Phellandrene (0.00%)
α-Terpineol (0.00%)
Valenence (0.00%)
Total: 1.690%
Predominant Terpenes
0.48%
Limonene
Citrus, orange, sweet
0.26%
Linalool
Citrus, floral, sweet, bois de rose, woody, green, blueberry
0.19%
β-Caryophyllene
Sweet, woody, spicy, clove
0.18%
β-Pinene
Woody, fresh pine, hay
0.18%
α-Pinene
Fresh camphor, sweet, pine, earthy, woody
0.16%
Myrcene
Peppery, spicy balsam
Results should be interpreted as qualitative only (present/absent). Quantitative values are only estimations for the purpose of research and development, and are not included in Iron Laboratories accredited scope. Eucalyptol, Sabinene, Fenchone, endo-Fenchol, Caryophyllene Oxide, a-Phellandrene, a-Terpineol, and Valencene are not currently tested for by Iron Laboratories Michigan.
Value in parenthesis indicates percentage of terpene present in the total sample (weight percentage, wt/wt%).
Value in doughnut slice indicates individual terpene abundance with respect to the total terpenes detected.
These results should be used for research and development or quality control purposes only. If applicable, results for caregivers apply to the sample as received.
This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Iron Laboratories, LLC is an ISO/IEC 17025:2017 Testing Laboratory laboratory accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802
Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390