ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Marijuana Potency Analysis by
High Performance Liquid Chromatography

Testing Accreditation #: 4092-004 Test Certificate #: 126653-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Island Zkittlez
License: 030-1009646F7F8
Type: Extract
Method: FE04U HPLC-UV
Metrc Test Pkg#: 1A401030002C949000000768
Metrc Source Pkg#: 1A401030002C949000000761

Test Conditions

Prepsheet ID#: ORP200917A
Scale: XS205-OR1
Temp: 22.3 °C
Baro Pressure: 999.6 hPa
Analyst: HRM
Technician: TMR

Sample ID#: 126653

Lot #: Island Zkittlez 9/15/20
Batch #: 126653
Batch Weight (g): 306
Harvest/Process Date: 09/15/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 09/16/2020
Test Date: 09/17/2020

Sample #126653
Sample #126653 Sample #126653
Test
Compounds
THC THCA CBD CBDA CBN CBG CBC THCV* CBDV Total
Cannabinoids*
Total THC Total CBD Calc Max Total
Cannabinoids*
Amount (%) 4.39 84.94 N/D 5.76 0.35 0.54 N/D N/D N/D 95.98 78.88 5.05 84.83
Amount (mg/g) 43.93 849.38 N/D 57.58 3.50 5.44 N/D N/D N/D 959.83 788.84 50.50 848.28
Amount per Serving (mg) 2.20 42.47 N\D 2.88 0.18 0.27 N\D N\D N\D 47.99 Serving Size~ (g): 0.05
LOQ (mg/g) 1.8 1.8 1.8 1.8 1.8 1.8 1.8 1.8 1.8   %Decarb. THC CBD
±%RPD 12.83 1.58 11.31 12.51 10.80 10.88 4.41 11.58 11.24 5 0

LOQ = Limit of Quantitation; %RPD = Relative Percent Deviation; %RSD = Relative Standard Deviation; N/D = Not Detected

*Designates values that are not currently included in the accredited scope of Iron Laboratories.

*** Designates tests that use the method FE-45. FE-45 is performed using AOAC 966.02 and 32.004-32.009. FE-45 has relative expanded (k=2) uncertainties of 1.098% for moisture, 1.754% for water activity for unprocessed plant materials, and 13.102% for water activity for infused products. Vitamin E acetate analysis has a relative expanded (k=2) uncertainty of 18.614%.

Total THC and CBD is the calculated sum of THC or CBD and the amount of THC or CBD derived from THCA or CBDA, respectively. These values are calculated by applying a molar correction factor of 0.877 to the THCA or the CBDA value. Calc Max Total Cannabinoids is the sum of Total THC, Total CBD, CBN, CBG, CBC, THCV, and CBDV.

%Decarb. THC and CBD refer to the percentage of THC or CBD relative to THCA or CBDA, respectively.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 1 of 8

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant QC Report

Testing Accreditation #: 4092-004 Test Certificate #: 126653-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Island Zkittlez
License: 030-1009646F7F8
Type: Extract
Method: FE04U HPLC-UV
Metrc Test Pkg#: 1A401030002C949000000768
Metrc Source Pkg#: 1A401030002C949000000761

Test Conditions

Prepsheet ID#: ORP200917A
Scale: XS205-OR1
Temp: 22.3 °C
Baro Pressure: 999.6 hPa
Analyst: HRM
Technician: TMR

Sample ID#: 126653

Lot #: Island Zkittlez 9/15/20
Batch #: 126653
Batch Weight (g): 306
Harvest/Process Date: 09/15/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 09/16/2020
Test Date: 09/17/2020

Sample #126653
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Cannabidivarin (CBDV) N.D. 5.5 5.04 91.64 5.64 102.55 11.24
Cannabidiolic Acid (CBDA) N.D. 5.29 4.87 92.06 5.52 104.35 12.51
Cannabigerol (CBG) N.D. 5.46 5.04 92.31 5.62 102.93 10.88
Cannabidiol (CBD) N.D. 5.37 4.92 91.62 5.51 102.61 11.31
Δ9-Tetrahydrocannabivarin (THCV) N.D. 5.43 4.88 89.87 5.48 100.92 11.58
Cannabinol (CBN) N.D. 5.26 4.73 89.92 5.27 100.19 10.80
Δ9-Tetrahydrocannabinol (THC) N.D. 5.23 4.67 89.29 5.31 101.53 12.83
Cannabichromene (CBC) N.D. 5.94 5.33 89.73 5.1 85.86 4.41
Tetrahydrocannabinolic acid (THCA) N.D. 6.25 5.74 91.84 5.65 90.40 1.58

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 2 of 8

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Marijuana Potency Analysis by
High Performance Liquid Chromatography

Testing Accreditation #: 4092-004 Test Certificate #: 126653-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Island Zkittlez
License: 030-1009646F7F8
Type: Extract
Method: FE04U HPLC-UV
Metrc Test Pkg#: 1A401030002C949000000768
Metrc Source Pkg#: 1A401030002C949000000761

Test Conditions

Prepsheet ID#: ORP200917A
Scale: XS205-OR1
Temp: 22.3 °C
Baro Pressure: 999.6 hPa
Analyst: HRM
Technician: TMR

Sample ID#: 126653

Lot #: Island Zkittlez 9/15/20
Batch #: 126653
Batch Weight (g): 306
Harvest/Process Date: 09/15/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 09/16/2020
Test Date: 09/17/2020

Sample #126653
Sample #126653 Sample #126653
Test
Compounds
THC THCA CBD CBDA CBN CBG CBC THCV* CBDV Total
Cannabinoids*
Total THC Total CBD Calc Max Total
Cannabinoids*
Amount (%) 4.26 84.51 N/D 5.76 0.35 0.55 N/D N/D N/D 95.43 78.38 5.05 84.33
Amount (mg/g) 42.58 845.14 N/D 57.56 3.48 5.54 N/D N/D N/D 954.3 783.77 50.48 843.27
Amount per Serving (mg) 2.13 42.26 N\D 2.88 0.17 0.28 N\D N\D N\D 47.72 Serving Size~ (g): 0.05
LOQ (mg/g) 1.9 1.9 1.9 1.9 1.9 1.9 1.9 1.9 1.9   %Decarb. THC CBD
±%RPD 12.83 1.58 11.31 12.51 10.80 10.88 4.41 11.58 11.24 0 0

LOQ = Limit of Quantitation; %RPD = Relative Percent Deviation; %RSD = Relative Standard Deviation; N/D = Not Detected

*Designates values that are not currently included in the accredited scope of Iron Laboratories.

*** Designates tests that use the method FE-45. FE-45 is performed using AOAC 966.02 and 32.004-32.009. FE-45 has relative expanded (k=2) uncertainties of 1.098% for moisture, 1.754% for water activity for unprocessed plant materials, and 13.102% for water activity for infused products. Vitamin E acetate analysis has a relative expanded (k=2) uncertainty of 18.614%.

Total THC and CBD is the calculated sum of THC or CBD and the amount of THC or CBD derived from THCA or CBDA, respectively. These values are calculated by applying a molar correction factor of 0.877 to the THCA or the CBDA value. Calc Max Total Cannabinoids is the sum of Total THC, Total CBD, CBN, CBG, CBC, THCV, and CBDV.

%Decarb. THC and CBD refer to the percentage of THC or CBD relative to THCA or CBDA, respectively.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 2 of 8

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant QC Report

Testing Accreditation #: 4092-004 Test Certificate #: 126653-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Island Zkittlez
License: 030-1009646F7F8
Type: Extract
Method: FE04U HPLC-UV
Metrc Test Pkg#: 1A401030002C949000000768
Metrc Source Pkg#: 1A401030002C949000000761

Test Conditions

Prepsheet ID#: ORP200917A
Scale: XS205-OR1
Temp: 22.3 °C
Baro Pressure: 999.6 hPa
Analyst: HRM
Technician: TMR

Sample ID#: 126653

Lot #: Island Zkittlez 9/15/20
Batch #: 126653
Batch Weight (g): 306
Harvest/Process Date: 09/15/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 09/16/2020
Test Date: 09/17/2020

Sample #126653
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Cannabidivarin (CBDV) N.D. 5.5 5.04 91.64 5.64 102.55 11.24
Cannabidiolic Acid (CBDA) N.D. 5.29 4.87 92.06 5.52 104.35 12.51
Cannabigerol (CBG) N.D. 5.46 5.04 92.31 5.62 102.93 10.88
Cannabidiol (CBD) N.D. 5.37 4.92 91.62 5.51 102.61 11.31
Δ9-Tetrahydrocannabivarin (THCV) N.D. 5.43 4.88 89.87 5.48 100.92 11.58
Cannabinol (CBN) N.D. 5.26 4.73 89.92 5.27 100.19 10.80
Δ9-Tetrahydrocannabinol (THC) N.D. 5.23 4.67 89.29 5.31 101.53 12.83
Cannabichromene (CBC) N.D. 5.94 5.33 89.73 5.1 85.86 4.41
Tetrahydrocannabinolic acid (THCA) N.D. 6.25 5.74 91.84 5.65 90.40 1.58

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 3 of 8

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents Analysis by
Mass Spectrometer

Testing Accreditation #: 4092-004 Test Certificate #: 126653-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Island Zkittlez
License: 030-1009646F7F8
Type: Extract
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A401030002C949000000768
Metrc Source Pkg#: 1A401030002C949000000761

Test Conditions

Prepsheet ID#: ORHS200920a
Scale: XS205-OR1
Temp: 19.2 °C
Baro PE: 998.9 hPa
Analyst: HRM
Technician: HRM

Sample ID#: 126653

Lot #: Island Zkittlez 9/15/20
Batch #: 126653
Batch Weight (g): 306
Harvest/Process Date: 09/15/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 09/16/2020
Test Date: 09/20/2020

Sample #126653
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
1,2-Dichloroethane 2 1 Not Tested 1,2-Dimethoxyethane 100 5 Pass/<LOD
1,4-dioxane 380 200 Pass/<LOD 1-Butanol 5,000 100 Pass/<LOD
1-Pentanol 5,000 100 Pass/<LOD 1-Propanol 5,000 100 Pass/<LOD
2,2-Dimethylpropane (Neopentane) 5,000 100 Pass/<LOD 2,2-Dimethylbutane (Hexanes) 290 100 Pass/<LOD
2,3-Dimethylbutane (Hexanes) 290 100 Pass/<LOD 2-Butanol 5,000 100 Pass/<LOD
2-Butanone (MEK) 5,000 50 Pass/<LOD 2-Ethoxyethanol 160 40 Pass/<LOD
2-Methylbutane (Isopentane) 5,000 50 Pass/<LOD 2-Methylpentane (Hexanes) 290 50 Pass/<LOD
2-Methylpropane (Isobutane) 5,000 100 Pass/<LOD 2-propanol (Isopropyl Alcohol) 5,000 50 Pass/139
2-Propanone (Acetone) 5,000 50 Pass/75 3-Methylpentane (Hexanes) 290 50 Pass/<LOD
Acetonitrile 410 100 Pass/<LOD Benzene 2 1 Pass/<LOD
Butane 5,000 100 Pass/144 Chloroform 2 1 Pass/<LOD
Cumene 70 50 Pass/<LOD Cyclohexane 3,880 1,000 Pass/<LOD
Dichloromethane 600 50 Pass/<LOD Dimethylsulfoxide (DMSO) 5,000 500 Pass/<LOD
Ethanol 5,000 500 Pass/<LOD Ethyl acetate 5,000 50 Pass/<LOD
Ethyl ether 5,000 500 Pass/<LOD Ethylene glycol 620 310 Pass/<LOD
Ethylene oxide 50 50 Pass/<LOD Heptane 5,000 50 Pass/<LOD
Hexane 290 290 Pass/<LOD Isopropyl acetate 5,000 50 Pass/<LOD
Methanol 3,000 500 Pass/<LOD Naptha 400 100 Not Tested
N,N-Dimethylacetamide 1,090 100 Pass/<LOD N,N-Dimethylformamide (DMF) 880 500 Pass/<LOD
Pentane 5,000 50 Pass/<LOD Petroleum Ether 400 100 Not Tested
Propane 5,000 100 Pass/<LOD Pyridine 200 10 Pass/<LOD
Sulfolane 160 200 Pass/<LOD Tetrahydrofuran (THF) 720 200 Pass/<LOD
Toluene 890 50 Pass/<LOD Trichloroethylene 25 5 Not Tested
Xylenes* 2,170 50 Pass/<LOD

Total Butanes = 144 ug/g (PASS); Total Pentanes = 0 ug/g (PASS); Total Hexanes = 0 ug/g (PASS)

* Xylenes are reported as the sum of o-xylene, m-xylene, p-xylene, and ethylbenzene
MRL - Maximum Residue Limit; LOD - Limit of Detection

This sample has not been tested according to OAR 333-007. These results should therefore be used for research and development or quality control purposes only.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 3 of 8

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents QC Report

Testing Accreditation #: 4092-004 Test Certificate #: 126653-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Island Zkittlez
License: 030-1009646F7F8
Type: Extract
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A401030002C949000000768
Metrc Source Pkg#: 1A401030002C949000000761

Test Conditions

Prepsheet ID#: ORHS200920a
Scale: XS205-OR1
Temp: 19.2 °C
Baro PE: 998.9 hPa
Analyst: HRM
Technician: HRM

Sample ID#: 126653

Lot #: Island Zkittlez 9/15/20
Batch #: 126653
Batch Weight (g): 306
Harvest/Process Date: 09/15/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 09/16/2020
Test Date: 09/20/2020

Sample #126653
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS Recovery (%) MSD Recovery (%) Relative Percent Difference (%) QC Flag
1,2-Dichloroethane N.D. 0 0 0 nan nan
n-Propane N.D. 250 0 25 0.00 10.00 200.00 LRQ
Isobutane N.D. 250 18 26 7.20 10.40 36.36 LRQ
Methanol N.D. 250 183 211 73.20 84.40 14.21
n-Butane N.D. 250 26 33 10.40 13.20 23.73 LRQ
2,2-Dimethylpropane N.D. 250 32 46 12.80 18.40 35.90 LRQ
Ethanol N.D. 250 146 193 58.40 77.20 27.73 LRQ
Isopentane N.D. 250 49 70 19.60 28.00 35.29 LRQ
Acetonitrile N.D. 250 107 154 42.80 61.60 36.02 LRQ
Diethyl ether N.D. 250 86 113 34.40 45.20 27.14 LRQ
2-propanone N.D. 250 106 186 42.40 74.40 54.79 LRQ
2-propanol N.D. 250 132 183 52.80 73.20 32.38 LRQ
n-Pentane N.D. 250 34 -33 13.60 -13.20 13.00 LRQ
2,2-Dimethylbutane N.D. 250 70 97 28.00 38.80 32.34 LRQ
2,3-Dimethylbutane N.D. 250 69 101 27.60 40.40 37.65 LRQ
Methylene chloride N.D. 250 120 166 48.00 66.40 32.17 LRQ
2-Methylpentane N.D. 250 71 106 28.40 42.40 39.55 LRQ
3-Methylpentane N.D. 250 80 108 32.00 43.20 29.79 LRQ
2-Butanol N.D. 250 124 182 49.60 72.80 37.91 LRQ
n-Hexane N.D. 250 82 107 32.80 42.80 26.46 LRQ
Ethyl acetate N.D. 250 119 172 47.60 68.80 36.43 LRQ
Tetrahydrofuran N.D. 250 117 165 0.00 0.00 0.00 LRQ
Trichloroethylene N.D. 0 0 0 nan nan
Isopropyl acetate N.D. 250 122 172 0.00 0.00 0.00 LRQ
Benzene N.D. 250 130 177 52.00 70.80 30.62 LRQ
Chloroform N.D. 0 0 0 nan nan
Cyclohexane N.D. 250 102 138 40.80 55.20 30.00 LRQ
Ethylene glycol N.D. 250 144 202 57.60 80.80 33.53 LRQ
Heptane N.D. 250 104 128 41.60 51.20 20.69 LRQ
2-Ethoxyethanol N.D. 250 144 219 57.60 87.60 41.32 LRQ
1,4-Dioxane N.D. 250 135 189 54.00 75.60 33.33 LRQ
Pyridine N.D. 0 0 0 0.00 0.00 0.00
Toluene N.D. 250 123 176 49.20 70.40 35.45 LRQ
Chlorobenzene N.D. 0 0 0 0.00 0.00 0.00
Ethylbenzene N.D. 250 130 184 52.00 73.60 34.39 LRQ
m-Xylene/p-Xylene N.D. 500 262 373 52.40 74.60 34.96 LRQ
o-Xylene N.D. 250 133 186 53.20 74.40 33.23 LRQ
Cumene N.D. 250 137 190 54.80 76.00 32.42 LRQ
Ethylene oxide N.D. 250 92 106 36.80 42.40 14.14 LRLR

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

N.D. = Not Detected

This sample has not been tested according to OAR 333-007. These results should therefore be used for research and development or quality control purposes only.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 4 of 8

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents Analysis by
Mass Spectrometer

Testing Accreditation #: 4092-004 Test Certificate #: 126653-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Island Zkittlez
License: 030-1009646F7F8
Type: Extract
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A401030002C949000000768
Metrc Source Pkg#: 1A401030002C949000000761

Test Conditions

Prepsheet ID#: ORHS200920a
Scale: XS205-OR1
Temp: 19.2 °C
Baro PE: 998.9 hPa
Analyst: HRM
Technician: HRM

Sample ID#: 126653

Lot #: Island Zkittlez 9/15/20
Batch #: 126653
Batch Weight (g): 306
Harvest/Process Date: 09/15/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 09/16/2020
Test Date: 09/20/2020

Sample #126653
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
1,2-Dichloroethane 2 1 Not Tested 1,2-Dimethoxyethane 100 5 Pass/<LOD
1,4-dioxane 380 200 Pass/<LOD 1-Butanol 5,000 100 Pass/<LOD
1-Pentanol 5,000 100 Pass/<LOD 1-Propanol 5,000 100 Pass/<LOD
2,2-Dimethylpropane (Neopentane) 5,000 100 Pass/<LOD 2,2-Dimethylbutane (Hexanes) 290 100 Pass/<LOD
2,3-Dimethylbutane (Hexanes) 290 100 Pass/<LOD 2-Butanol 5,000 100 Pass/<LOD
2-Butanone (MEK) 5,000 50 Pass/<LOD 2-Ethoxyethanol 160 40 Pass/<LOD
2-Methylbutane (Isopentane) 5,000 50 Pass/<LOD 2-Methylpentane (Hexanes) 290 50 Pass/<LOD
2-Methylpropane (Isobutane) 5,000 100 Pass/<LOD 2-propanol (Isopropyl Alcohol) 5,000 50 Pass/125
2-Propanone (Acetone) 5,000 50 Pass/60 3-Methylpentane (Hexanes) 290 50 Pass/<LOD
Acetonitrile 410 100 Pass/<LOD Benzene 2 1 Pass/<LOD
Butane 5,000 100 Pass/120 Chloroform 2 1 Pass/<LOD
Cumene 70 50 Pass/<LOD Cyclohexane 3,880 1,000 Pass/<LOD
Dichloromethane 600 50 Pass/<LOD Dimethylsulfoxide (DMSO) 5,000 500 Pass/<LOD
Ethanol 5,000 500 Pass/<LOD Ethyl acetate 5,000 50 Pass/<LOD
Ethyl ether 5,000 500 Pass/<LOD Ethylene glycol 620 310 Pass/<LOD
Ethylene oxide 50 50 Pass/<LOD Heptane 5,000 50 Pass/<LOD
Hexane 290 290 Pass/<LOD Isopropyl acetate 5,000 50 Pass/<LOD
Methanol 3,000 500 Pass/<LOD Naptha 400 100 Not Tested
N,N-Dimethylacetamide 1,090 100 Pass/<LOD N,N-Dimethylformamide (DMF) 880 500 Pass/<LOD
Pentane 5,000 50 Pass/<LOD Petroleum Ether 400 100 Not Tested
Propane 5,000 100 Pass/<LOD Pyridine 200 10 Pass/<LOD
Sulfolane 160 200 Pass/<LOD Tetrahydrofuran (THF) 720 200 Pass/<LOD
Toluene 890 50 Pass/<LOD Trichloroethylene 25 5 Not Tested
Xylenes* 2,170 50 Pass/<LOD

Total Butanes = 120 ug/g (PASS); Total Pentanes = 0 ug/g (PASS); Total Hexanes = 0 ug/g (PASS)

* Xylenes are reported as the sum of o-xylene, m-xylene, p-xylene, and ethylbenzene
MRL - Maximum Residue Limit; LOD - Limit of Detection

This sample has not been tested according to OAR 333-007. These results should therefore be used for research and development or quality control purposes only.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 5 of 8

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents QC Report

Testing Accreditation #: 4092-004 Test Certificate #: 126653-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Island Zkittlez
License: 030-1009646F7F8
Type: Extract
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A401030002C949000000768
Metrc Source Pkg#: 1A401030002C949000000761

Test Conditions

Prepsheet ID#: ORHS200920a
Scale: XS205-OR1
Temp: 19.2 °C
Baro PE: 998.9 hPa
Analyst: HRM
Technician: HRM

Sample ID#: 126653

Lot #: Island Zkittlez 9/15/20
Batch #: 126653
Batch Weight (g): 306
Harvest/Process Date: 09/15/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 09/16/2020
Test Date: 09/20/2020

Sample #126653
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS Recovery (%) MSD Recovery (%) Relative Percent Difference (%) QC Flag
1,2-Dichloroethane N.D. 0 0 0 nan nan
n-Propane N.D. 250 0 25 0.00 10.00 200.00 LRQ
Isobutane N.D. 250 18 26 7.20 10.40 36.36 LRQ
Methanol N.D. 250 183 211 73.20 84.40 14.21
n-Butane N.D. 250 26 33 10.40 13.20 23.73 LRQ
2,2-Dimethylpropane N.D. 250 32 46 12.80 18.40 35.90 LRQ
Ethanol N.D. 250 146 193 58.40 77.20 27.73 LRQ
Isopentane N.D. 250 49 70 19.60 28.00 35.29 LRQ
Acetonitrile N.D. 250 107 154 42.80 61.60 36.02 LRQ
Diethyl ether N.D. 250 86 113 34.40 45.20 27.14 LRQ
2-propanone N.D. 250 106 186 42.40 74.40 54.79 LRQ
2-propanol N.D. 250 132 183 52.80 73.20 32.38 LRQ
n-Pentane N.D. 250 34 -33 13.60 -13.20 13.00 LRQ
2,2-Dimethylbutane N.D. 250 70 97 28.00 38.80 32.34 LRQ
2,3-Dimethylbutane N.D. 250 69 101 27.60 40.40 37.65 LRQ
Methylene chloride N.D. 250 120 166 48.00 66.40 32.17 LRQ
2-Methylpentane N.D. 250 71 106 28.40 42.40 39.55 LRQ
3-Methylpentane N.D. 250 80 108 32.00 43.20 29.79 LRQ
2-Butanol N.D. 250 124 182 49.60 72.80 37.91 LRQ
n-Hexane N.D. 250 82 107 32.80 42.80 26.46 LRQ
Ethyl acetate N.D. 250 119 172 47.60 68.80 36.43 LRQ
Tetrahydrofuran N.D. 250 117 165 0.00 0.00 0.00 LRQ
Trichloroethylene N.D. 0 0 0 nan nan
Isopropyl acetate N.D. 250 122 172 0.00 0.00 0.00 LRQ
Benzene N.D. 250 130 177 52.00 70.80 30.62 LRQ
Chloroform N.D. 0 0 0 nan nan
Cyclohexane N.D. 250 102 138 40.80 55.20 30.00 LRQ
Ethylene glycol N.D. 250 144 202 57.60 80.80 33.53 LRQ
Heptane N.D. 250 104 128 41.60 51.20 20.69 LRQ
2-Ethoxyethanol N.D. 250 144 219 57.60 87.60 41.32 LRQ
1,4-Dioxane N.D. 250 135 189 54.00 75.60 33.33 LRQ
Pyridine N.D. 0 0 0 0.00 0.00 0.00
Toluene N.D. 250 123 176 49.20 70.40 35.45 LRQ
Chlorobenzene N.D. 0 0 0 0.00 0.00 0.00
Ethylbenzene N.D. 250 130 184 52.00 73.60 34.39 LRQ
m-Xylene/p-Xylene N.D. 500 262 373 52.40 74.60 34.96 LRQ
o-Xylene N.D. 250 133 186 53.20 74.40 33.23 LRQ
Cumene N.D. 250 137 190 54.80 76.00 32.42 LRQ
Ethylene oxide N.D. 250 92 106 36.80 42.40 14.14 LRLR

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

N.D. = Not Detected

This sample has not been tested according to OAR 333-007. These results should therefore be used for research and development or quality control purposes only.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

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ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Homogeneity Report by
High Performance Liquid Chromatography

Testing Accreditation #: 4092-004 Test Certificate #: 126653-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Island Zkittlez
License: 030-1009646F7F8
Type: Extract
Metrc Test Pkg#: 1A401030002C949000000768
Metrc Source Pkg#: 1A401030002C949000000761

Sample ID#: 126653

Lot #: Island Zkittlez 9/15/20
Batch #: 126653
Batch Weight (g): 306
Harvest/Process Date: 09/15/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 09/16/2020

Sample #126653
Increments Tested (mg/g) TOTAL THC TOTAL CBD THC THCA THCV CBD CBC CBDA CBDV CBG CBN
Increment 1 788.84 50.50 43.93 849.38 N.D. N.D. N.D. 57.58 N.D. 5.44 3.50
Increment 2 783.77 50.48 42.58 845.14 N.D. N.D. N.D. 57.56 N.D. 5.54 3.48
Average Value 786.30 50.49 43.26 847.26 N.D. N.D. N.D. 57.57 N.D. 5.49 3.49
Max Value 788.84 50.50 43.93 849.38 N.D. N.D. N.D. 57.58 N.D. 5.54 3.50
Min Value 783.77 50.48 42.58 845.14 N.D. N.D. N.D. 57.56 N.D. 5.44 3.48
Relative Percent Difference (RPD) ±0.64 ±0.03 ±3.12 ±0.50 N.D. N.D. N.D. ±0.03 N.D. ±1.82 ±0.57
Average Cannabinoids Per Package 786.30 50.49 43.26 847.26 N.D. N.D. N.D. 57.57 N.D. 5.49 3.49
Average Cannabinoids Per Serving 39.32 2.52 2.16 42.36 N.D. N.D. N.D. 2.88 N.D. 0.27 0.17
Max Concentration Per Serving (THC)   Pass
Max Concentration Per Package (THC)   Not Applicable
Relative Percent Difference (RPD)   Pass
Control Study   Yes, MJ1957
Field Duplicate   Pass

N.D. = Not Detected, Min = Minimum, Max = Maximum

RPD is the relative percent difference between increment 1 and increment 2.

RSD is the relative standard deviation between all increments tested.

Total THC and CBD is the calculated sum of CBD or THC and the amount of CBD or THC derived from CBDA or THCA, respectively. These values are calculated by adding a molar correction factor of 0.877 to the CBDA or THCA value.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

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IRON Laboratories

Terpene Report by
Mass Spectrometer

Test Certificate #: 126653-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Island Zkittlez
License: 030-1009646F7F8
Type: Extract
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A401030002C949000000768
Metrc Source Pkg#: 1A401030002C949000000761

Test Conditions

Scale: XS205-OR1
Temp: 19.2 °C
Baro Pressure: 998.9 hPa
Analyst: HRM
Technician: HRM

Sample ID#: 126653

Lot #: Island Zkittlez 9/15/20
Batch #: 126653
Batch Weight (g): 306
Harvest/Process Date: 09/15/2020
Serving Size (g): 0.05
Date Received: 09/16/2020

Sample #126653
Sample #126653
  • α-Pinene (0.11%)
  • β-Ocimene (0.00%)
  • Camphene (0.02%)
  • Eucalyptol (1,8-Cineol) (0.00%)
  • Sabinene (0.00%)
  • γ-Terpinene (0.20%)
  • Myrcene (0.29%)
  • α-Terpinolene (1.89%)
  • β-Pinene (0.12%)
  • Linalool (0.29%)
  • ∆3-Carene (0.05%)
  • Fenchone (0.00%)
  • α-Terpinene (0.21%)
  • endo-Fenchol (0.21%)
  • α-Ocimene (0.00%)
  • Isopulegol (0.00%)
  • Limonene (0.26%)
  • Geraniol (0.00%)
  • p-Cymene (0.00%)
  • β-Caryophyllene (0.00%)
  • α-Humulene (0.69%)
  • Nerolidol 1 (cis) (0.00%)
  • Nerolidol 2 (trans) (0.03%)
  • Guaiol (0.00%)
  • Caryophyllene Oxide (0.00%)
  • α-Bisabolol (0.19%)
  • α-Phellandrene (0.92%)
  • α-Terpineol (0.46%)
  • Valenence (0.60%)

Total: 6.540%

Predominant Terpenes

1.89%   α-Terpinolene Fresh wood, sweet, pine, citrus 0.92%   α-Phellandrene Citrus, green, black pepper
0.69%   α-Humulene Woody, oceanic-watery, spicy clove 0.60%   Valenence Sweet, citrus, grapefruit, woody, orange
0.46%   α-Terpineol Pine, woody, lemon, lime, citrus, floral 0.29%   Myrcene Peppery, spicy balsam

Value in parenthesis indicates percentage of terpene present in the total sample (weight percentage, wt/wt%).
Value in doughnut slice indicates individual terpene abundance with respect to the total terpenes detected.

This sample has not been tested according to OAR 333-007. These results should therefore be used for research and development or quality control purposes only.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Joseph Rutowski Iron laboratories Joseph Rutowski

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 8 of 8