ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Marijuana Potency Analysis by
High Performance Liquid Chromatography
Testing Accreditation #: 4092-004 Test Certificate #: 126108-001
Client Name, Sample Details

45th Parallel Farms LLC
Dallas, OR 97338
Sample: Holy Grail
License: 010-100164183CE
Type: Adult Use Flower
Method: FE04U HPLC-UV
Metrc Test Pkg#: 1A4010300017891000000489
Metrc Source Pkg#: 1A4010300017891000000532
***Water Activity: 0.579
***Moisture: 12.66%
Test Conditions

Prepsheet ID#: ORP200824a
Scale: XS205-OR1
Temp: 21.6 °C
Baro Pressure: 1005 hPa
Analyst: HRM
Technician: TMR
Sample ID#: 126108

Lot #: Holy Grail 8/5/20
Batch #: 126108
Batch Weight (g): 6810
Harvest/Process Date: 08/05/2020
Date Received: 08/20/2020
Test Date: 08/24/2020
Sample #126108
Sample #126108 Sample #126108
Test
Compounds		 THC THCA CBD CBDA CBN CBG CBC THCV* CBDV Total
Cannabinoids*		 Total THC Total CBD Calc Max Total
Cannabinoids*
Amount (%) 0.96 21.99 N/D 0.55 0.11 0.18 0.10 N/D N/D 23.89 20.24 0.48 21.12
Amount (mg/g) 9.60 219.87 N/D 5.47 1.13 1.82 0.97 N/D N/D 238.86 202.43 4.80 211.15
Amount per Serving (mg) N\D N\D N\D N\D N\D N\D N\D N\D N\D 0.00 Serving Size~ (g): 0.00
LOQ (mg/g) 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5   %Decarb. THC CBD
±%RPD +/-5% 9.31 +/-5% 13.13 8.33 2.54 5.00 +/-5% +/-5% 4 0

LOQ = Limit of Quantitation; %RPD = Relative Percent Deviation; %RSD = Relative Standard Deviation; N/D = Not Detected

*Designates values that are not currently included in the accredited scope of Iron Laboratories.

*** Designates tests that use the method FE-45. FE-45 is performed using AOAC 966.02 and 32.004-32.009. FE-45 has relative expanded (k=2) uncertainties of 1.098% for moisture, 1.754% for water activity for unprocessed plant materials, and 13.102% for water activity for infused products. Vitamin E acetate analysis has a relative expanded (k=2) uncertainty of 18.614%.

Total THC and CBD is the calculated sum of THC or CBD and the amount of THC or CBD derived from THCA or CBDA, respectively. These values are calculated by applying a molar correction factor of 0.877 to the THCA or the CBDA value. Calc Max Total Cannabinoids is the sum of Total THC, Total CBD, CBN, CBG, CBC, THCV, and CBDV.

%Decarb. THC and CBD refer to the percentage of THC or CBD relative to THCA or CBDA, respectively.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 1 of 4

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant QC Report
Testing Accreditation #: 4092-004 Test Certificate #: 126108-001
Client Name, Sample Details

45th Parallel Farms LLC
Dallas, OR 97338
Sample: Holy Grail
License: 010-100164183CE
Type: Adult Use Flower
Method: FE04U HPLC-UV
Metrc Test Pkg#: 1A4010300017891000000489
Metrc Source Pkg#: 1A4010300017891000000532
***Water Activity: 0.579
***Moisture: 12.66%
Test Conditions

Prepsheet ID#: ORP200824a
Scale: XS205-OR1
Temp: 21.6 °C
Baro Pressure: 1005 hPa
Analyst: HRM
Technician: TMR
Sample ID#: 126108

Lot #: Holy Grail 8/5/20
Batch #: 126108
Batch Weight (g): 6810
Harvest/Process Date: 08/05/2020
Date Received: 08/20/2020
Test Date: 08/24/2020
Sample #126108
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Cannabidivarin (CBDV) N.D. 1 0 0.00 0 0.00 0
Cannabidiolic Acid (CBDA) N.D. 11.33 11.12 98.15 9.75 86.05 13.13
Cannabigerol (CBG) N.D. 1.78 1.99 111.80 1.94 108.99 2.54
Cannabidiol (CBD) N.D. 1 0 0.00 0 0.00 0
Δ9-Tetrahydrocannabivarin (THCV) N.D. 1 0 0.00 0 0.00 0
Cannabinol (CBN) N.D. 0.42 0.69 164.29 0.75 178.57 8.33 HR
Δ9-Tetrahydrocannabinol (THC) 1 0.00 0.00 0
Cannabichromene (CBC) N.D. 0.64 0.82 128.13 0.78 121.88 5.00
Tetrahydrocannabinolic acid (THCA) N.D. 150.95 145.87 96.63 132.89 88.04 9.31

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 2 of 4

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Pesticide Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-004 Test Certificate #: 126108-001
Client Name, Sample Details

45th Parallel Farms LLC
Dallas, OR 97338
Sample: Holy Grail
License: 010-100164183CE
Type: Adult Use Flower
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A4010300017891000000489
Metrc Source Pkg#: 1A4010300017891000000532
Test Conditions

Prepsheet ID#: ORPS200814a
Scale: 1129293203
Temp: 20.7 °C
Baro PE: 1005 hPa
Analyst: HRM/EDT
Technician: HRM/EDT
Sample ID#: 126108

Lot #: Holy Grail 8/5/20
Batch #: 126108
Batch Weight (g): 6810
Harvest/Process Date: 08/05/2020
Date Received: 08/20/2020
Test Date: 08/24/2020
Sample #126108
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
Aldicarb 0.400 0.125 Pass/<LOD Abamectin**** 0.500 0.125 Pass/<LOD
Acephate 0.400 0.125 Pass/<LOD Acequinocyl 2.000 0.249 Pass/<LOD
Acetamiprid 0.200 0.125 Pass/<LOD Azoxystrobin 0.200 0.125 Pass/<LOD
Bifenazate 0.200 0.125 Pass/<LOD Bifenthrin 0.200 0.125 Pass/<LOD
Boscalid 0.400 0.125 Pass/<LOD Carbaryl 0.200 0.125 Pass/<LOD
Carbofuran 0.200 0.125 Pass/<LOD Chlorantraniliprole 0.200 0.125 Pass/<LOD
Chlorfenapyr 1.000 0.498 Pass/<LOD Chlorpyrifos 0.200 0.125 Pass/<LOD
Clofentezine 0.200 0.125 Pass/<LOD Cyfluthrin** 1.000 0.498 Pass/<LOD
Cypermethrin*** 1.000 0.498 Pass/<LOD Daminozide 1.000 0.125 Pass/<LOD
DDVP (Dichlorvos) 1.000 0.249 Pass/<LOD Diazinon 0.200 0.125 Pass/<LOD
Dimethoate 0.200 0.125 Pass/<LOD Ethoprophos 0.200 0.125 Pass/<LOD
Etofenprox 0.400 0.125 Pass/<LOD Etoxazole 0.200 0.125 Pass/<LOD
Fenoxycarb 0.200 0.125 Pass/<LOD Fenpyroximate 0.400 0.125 Pass/<LOD
Fipronil 0.400 0.125 Pass/<LOD Flonicamid 1.000 0.125 Pass/<LOD
Fludioxonil 0.400 0.125 Pass/<LOD Hexythiazox 1.000 0.125 Pass/<LOD
Imazalil 0.200 0.125 Pass/<LOD Imidacloprid 0.400 0.125 Pass/<LOD
Kresoxim Methyl 0.400 0.125 Pass/<LOD Malathion 0.200 0.125 Pass/<LOD
Metalaxyl 0.200 0.125 Pass/<LOD Methiocarb 0.200 0.125 Pass/<LOD
Methomyl 0.400 0.125 Pass/<LOD Methyl Parathion 0.200 0.125 Pass/<LOD
MGK-264‡ 0.200 0.125 Pass/<LOD Myclobutanil 0.000 0.125 Pass/<LOD
Naled 0.500 0.125 Pass/<LOD Oxamyl 1.000 0.125 Pass/<LOD
Paclobutrazol 0.400 0.125 Pass/<LOD Permethrins† 0.200 0.125 Pass/<LOD
Phosmet 0.200 0.125 Pass/<LOD Piperonyl Butoxide 2.000 0.125 Pass/<LOD
Prallethrin 0.200 0.125 Pass/<LOD Propiconazole 0.400 0.125 Pass/<LOD
Propoxur 0.200 0.125 Pass/<LOD Pyrethrins* 1.000 0.125 Pass/<LOD
Pyridaben 0.200 0.125 Pass/<LOD Spinosad***** 0.200 0.125 Pass/<LOD
Spiromesifen 0.200 0.125 Pass/<LOD Spirotetramat 0.200 0.125 Pass/<LOD
Spiroxamine‡ 0.400 0.125 Pass/<LOD Tebuconazole 0.400 0.125 Pass/<LOD
Thiacloprid 0.200 0.125 Pass/<LOD Thiamethoxam 0.200 0.125 Pass/<LOD
Trifloxystrobin 0.200 0.125 Pass/<LOD

* Pyrethrins are reported as the sum of Jasmolin I, Cinerin I, and Pyrethrin I
** Cyfluthrins are reported as the sum of isomers Cyfluthrin I, II, III, and IV
*** Cypermethrins are reported as the sum of isomers Cypermethrin I, II, III, and IV
**** Abamectin is reported as the sum of Avermectin B1a and Avermectin B1b
***** Spinosad is reported as the sum of Spinosyn A and Spinosyn D
† Permethrin and Prallethrin are reported as the sum of cis and trans isomers
‡ MGK-264 and Spiroximine are reported as the sum of isomers I and II
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 2 of 4

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Pesticide QC Report
Testing Accreditation #: 4092-004 Test Certificate #: 126108-001
Client Name, Sample Details

45th Parallel Farms LLC
Dallas, OR 97338
Sample: Holy Grail
License: 010-100164183CE
Type: Adult Use Flower
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A4010300017891000000489
Metrc Source Pkg#: 1A4010300017891000000532
Test Conditions

Prepsheet ID#: ORPS200814a
Scale: 1129293203
Temp: 20.7 °C
Baro PE: 1005 hPa
Analyst: HRM/EDT
Technician: HRM/EDT
Sample ID#: 126108

Lot #: Holy Grail 8/5/20
Batch #: 126108
Batch Weight (g): 6810
Harvest/Process Date: 08/05/2020
Date Received: 08/20/2020
Test Date: 08/24/2020
Sample #126108
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS recovery% MSD recovery% Relative Percent Difference (%) QC Flag
Acephate N.D. 1 0.917 0.932 91.70 93.20 1.62
Acequinocyl N.D. 1 0.576 0.512 57.60 51.20 11.76 LR
Acetamiprid N.D. 1 1.03 1.03 103.00 103.00 0.00
Aldicarb N.D. 1 1.01 1.04 101.00 104.00 2.93
Avermectin B1a N.D. 0.97 1.09 1.12 112.37 115.46 2.71
Azoxystrobin N.D. 1 0.905 0.923 90.50 92.30 1.97
Bifenazate N.D. 1 0.881 0.841 88.10 84.10 4.65
Bifenthrin N.D. 1 1.14 1.14 114.00 114.00 0.00
Boscalid N.D. 1 0.984 0.966 98.40 96.60 1.85
Carbaryl N.D. 1 0.976 0.996 97.60 99.60 2.03
Carbofuran N.D. 1 1.04 1.03 104.00 103.00 0.97
Chlorantraniliprole N.D. 1 1.02 1.04 102.00 104.00 1.94
Chlorfenapyr N.D. 1 0.934 0.984 93.40 98.40 5.21
Chlorpyriphos N.D. 1 0.76 1.01 76.00 101.00 28.25 Q
Clofentezine N.D. 1 0.739 0.827 73.90 82.70 11.24
Cyfluthrin N.D. 1 1.54 1.69 154.00 169.00 9.29 HR
Cypermethrin N.D. 1 No Peak No Peak 0.00 0.00
Daminoside N.D. 1 0.173 0.299 17.30 29.90 53.39 LR Q
Diazanon N.D. 1 0.938 0.935 93.80 93.50 0.32
Dichlorvos N.D. 1 0.841 0.928 84.10 92.80 9.84
Dimethoate N.D. 1 0.985 1 98.50 100.00 1.51
Ethoprophos N.D. 1 0.821 0.836 82.10 83.60 1.81
Etofenprox N.D. 1 1.11 1.13 111.00 113.00 1.79
Etoxazole N.D. 1 1.26 1.15 126.00 115.00 9.13
Fenoxycarb N.D. 1 0.998 1.01 99.80 101.00 1.20
Fenpyroximate N.D. 1 1.19 1.18 119.00 118.00 0.84
Fipronil N.D. 1 1.04 1.05 104.00 105.00 0.96
Flonicamid N.D. 1 1.02 1.03 102.00 103.00 0.98
Fludioxonil N.D. 1 1.17 1.14 117.00 114.00 2.60
Hexythiazox N.D. 1 0.312 0.459 31.20 45.90 38.13 LR Q
Imazalil N.D. 1 0.942 1.01 94.20 101.00 6.97
Imidacloprid N.D. 1 1.2 1.12 120.00 112.00 6.90
Kresoxim-methyl N.D. 1 0.88 0.859 88.00 85.90 2.42
Malathion N.D. 1 0.976 0.972 97.60 97.20 0.41
Metalaxyl N.D. 1 1.06 1.04 106.00 104.00 1.90
Methiocarb N.D. 1 1.04 1.01 104.00 101.00 2.93
Methomyl N.D. 1 0.988 0.992 98.80 99.20 0.40
MGK-264 N.D. 1 1 0.979 100.00 97.90 2.12
Myclobutanil N.D. 1 1.02 1.02 102.00 102.00 0.00
Naled (dibrom) N.D. 1 0.309 0.302 30.90 30.20 2.29 LR
Oxamyl N.D. 1 1.06 1.09 106.00 109.00 2.79
Paclobutrazol N.D. 1 1.05 1.03 105.00 103.00 1.92
Parathion-methyl N.D. 1 1.06 1.05 106.00 105.00 0.95
Permethrins N.D. 1 0.851 1.123 85.10 112.30 27.56 Q
Phosmet N.D. 1 0.927 0.933 92.70 93.30 0.65
Piperonyl butoxide N.D. 1 1.14 1.16 114.00 116.00 1.74
Prallethrin N.D. 1 1.01 1.03 101.00 103.00 1.96
Propiconazole N.D. 1 1.02 1.05 102.00 105.00 2.90
Propoxur N.D. 1 0.926 0.96 92.60 96.00 3.61
Pyrethrin N.D. 0.65 0.665 0.63 102.31 96.92 5.41
Pyridaben N.D. 1 1.1 1.1 110.00 110.00 0.00
SpinosynA N.D. 0.84 0.757 0.813 90.12 96.79 7.13
SpinosynD N.D. 0.16 0.106 0.108 66.25 67.50 1.87 LR
Spiromesifen N.D. 1 0.0925 0.0876 9.25 8.76 5.44 LR
Spirotetramat N.D. 1 0.913 0.958 91.30 95.80 4.81
Spiroxamine N.D. 1 0.941 0.976 94.10 97.60 3.65
Tebuconazole N.D. 1 0.949 0.955 94.90 95.50 0.63
Thiacloprid N.D. 1 1.01 1.04 101.00 104.00 2.93
Thiamethoxam N.D. 1 1.04 1.05 104.00 105.00 0.96
Trifloxystrobin N.D. 1 1.18 1.18 118.00 118.00 0.00

N.D. = Not Detected

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 30%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (60-120%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 3 of 4
IRON Laboratories

Terpene Report by
Mass Spectrometer
Test Certificate #: 126108-001
Client Name, Sample Details

45th Parallel Farms LLC
Dallas, OR 97338
Sample: Holy Grail
License: 010-100164183CE
Type: Adult Use Flower
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A4010300017891000000489
Metrc Source Pkg#: 1A4010300017891000000532

Test Conditions

Scale: XS205-OR1
Temp: 19.2 °C
Baro Pressure: 1002.2 hPa
Analyst: HRM
Technician: HRM

Sample ID#: 126108

Lot #: Holy Grail 8/5/20
Batch #: 126108
Batch Weight (g): 6810
Harvest/Process Date: 08/05/2020
Date Received: 08/20/2020

Sample #126108
Sample #126108
  • α-Pinene (0.00%)
  • β-Ocimene (0.05%)
  • Camphene (0.00%)
  • Eucalyptol (1,8-Cineol) (0.00%)
  • Sabinene (0.00%)
  • γ-Terpinene (0.00%)
  • Myrcene (0.22%)
  • α-Terpinolene (0.00%)
  • β-Pinene (0.30%)
  • Linalool (0.23%)
  • ∆3-Carene (0.00%)
  • Fenchone (0.00%)
  • α-Terpinene (0.00%)
  • endo-Fenchol (0.04%)
  • α-Ocimene (0.00%)
  • Isopulegol (0.00%)
  • Limonene (0.14%)
  • Geraniol (0.00%)
  • p-Cymene (0.00%)
  • β-Caryophyllene (0.00%)
  • α-Humulene (0.31%)
  • Nerolidol 1 (cis) (0.00%)
  • Nerolidol 2 (trans) (0.02%)
  • Guaiol (0.16%)
  • Caryophyllene Oxide (0.00%)
  • α-Bisabolol (0.05%)
  • α-Phellandrene (0.00%)
  • α-Terpineol (0.10%)
  • Valenence (0.28%)

Total: 1.900%

Predominant Terpenes

0.31%   α-Humulene Woody, oceanic-watery, spicy clove 0.30%   β-Pinene Woody, fresh pine, hay
0.28%   Valenence Sweet, citrus, grapefruit, woody, orange 0.23%   Linalool Citrus, floral, sweet, bois de rose, woody, green, blueberry
0.22%   Myrcene Peppery, spicy balsam 0.16%   Guaiol Mild, guaiacwood, tea, rose

Value in parenthesis indicates percentage of terpene present in the total sample (weight percentage, wt/wt%).
Value in doughnut slice indicates individual terpene abundance with respect to the total terpenes detected.

This sample has not been tested according to OAR 333-007. These results should therefore be used for research and development or quality control purposes only.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Himashi Mead Iron laboratories Himashi Mead

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 4 of 4