ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Marijuana Potency Analysis by
High Performance Liquid Chromatography
Testing Accreditation #: 4092-004 Test Certificate #: 125292-001
Client Name, Sample Details

Oregon Grow Group
Florence, OR 97439
Sample: Tangerine Breath
License: 020-1011919EEBA
Type: Adult Use Flower
Method: FE04U HPLC-UV
Metrc Test Pkg#: 1A40103000223A9000000148
Metrc Source Pkg#: 1A40103000223A9000000145
***Water Activity: 0.537
***Moisture: 11.67%
Test Conditions

Prepsheet ID#: ORP200714a
Scale: XS205-OR1
Temp: 21.7 °C
Baro Pressure: 1002 hPa
Analyst: HRM
Technician: TMR
Sample ID#: 125292

Lot #: 6-10-20 Tangerine Breath
Batch #: 125292
Batch Weight (g): 1417.9
Harvest/Process Date: 06/10/2020
Serving Size (g): 1
Date Received: 07/09/2020
Test Date: 07/14/2020
Sample #125292
Sample #125292 Sample #125292
Test
Compounds		 THC THCA CBD CBDA CBN CBG CBC THCV* CBDV Total
Cannabinoids*		 Total THC Total CBD Calc Max Total
Cannabinoids*
Amount (%) 1.55 22.57 N/D 0.53 N/D 0.10 0.14 N/D N/D 24.89 21.34 0.46 22.04
Amount (mg/g) 15.45 225.68 N/D 5.26 N/D 1.04 1.42 N/D N/D 248.85 213.37 4.61 220.44
Amount per Serving (mg) 15.45 225.68 N\D 5.26 N\D 1.04 1.42 N\D N\D 248.85 Serving Size~ (g): 1.00
LOQ (mg/g) 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5   %Decarb. THC CBD
±%RPD 8.14 4.32 +/-5% 4.50 3.43 10.94 5.22 +/-5% +/-5% 6 0

LOQ = Limit of Quantitation; %RPD = Relative Percent Deviation; %RSD = Relative Standard Deviation; N/D = Not Detected

*Designates values that are not currently included in the accredited scope of Iron Laboratories.

*** Designates tests that use the method FE-45. FE-45 is performed using AOAC 966.02 and 32.004-32.009. FE-45 has relative expanded (k=2) uncertainties of 1.098% for moisture, 1.754% for water activity for unprocessed plant materials, and 13.102% for water activity for infused products. Vitamin E acetate analysis has a relative expanded (k=2) uncertainty of 18.614%.

Total THC and CBD is the calculated sum of THC or CBD and the amount of THC or CBD derived from THCA or CBDA, respectively. These values are calculated by applying a molar correction factor of 0.877 to the THCA or the CBDA value. Calc Max Total Cannabinoids is the sum of Total THC, Total CBD, CBN, CBG, CBC, THCV, and CBDV.

%Decarb. THC and CBD refer to the percentage of THC or CBD relative to THCA or CBDA, respectively.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 1 of 4

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant QC Report
Testing Accreditation #: 4092-004 Test Certificate #: 125292-001
Client Name, Sample Details

Oregon Grow Group
Florence, OR 97439
Sample: Tangerine Breath
License: 020-1011919EEBA
Type: Adult Use Flower
Method: FE04U HPLC-UV
Metrc Test Pkg#: 1A40103000223A9000000148
Metrc Source Pkg#: 1A40103000223A9000000145
***Water Activity: 0.537
***Moisture: 11.67%
Test Conditions

Prepsheet ID#: ORP200714a
Scale: XS205-OR1
Temp: 21.7 °C
Baro Pressure: 1002 hPa
Analyst: HRM
Technician: TMR
Sample ID#: 125292

Lot #: 6-10-20 Tangerine Breath
Batch #: 125292
Batch Weight (g): 1417.9
Harvest/Process Date: 06/10/2020
Serving Size (g): 1
Date Received: 07/09/2020
Test Date: 07/14/2020
Sample #125292
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Cannabidivarin (CBDV) N.D. 1 0 0.00 0 0.00 0
Cannabidiolic Acid (CBDA) N.D. 13.24 10.91 82.40 10.43 78.78 4.50
Cannabigerol (CBG) N.D. 1.57 1.35 85.99 1.21 77.07 10.94
Cannabidiol (CBD) N.D. 1 0 0.00 0 0.00 0
Δ9-Tetrahydrocannabivarin (THCV) N.D. 1 0 0.00 0 0.00 0
Cannabinol (CBN) N.D. 0.97 0.89 91.75 0.86 88.66 3.43
Δ9-Tetrahydrocannabinol (THC) N.D. 34.51 30.82 89.31 28.41 82.32 8.14
Cannabichromene (CBC) N.D. 1.1 0.59 53.64 0.56 50.91 5.22
Tetrahydrocannabinolic acid (THCA) N.D. 175.96 150.14 85.33 143.79 81.72 4.32

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 2 of 4

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Pesticide Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-004 Test Certificate #: 125292-001
Client Name, Sample Details

Oregon Grow Group
Florence, OR 97439
Sample: Tangerine Breath
License: 020-1011919EEBA
Type: Adult Use Flower
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A40103000223A9000000148
Metrc Source Pkg#: 1A40103000223A9000000145
Test Conditions

Prepsheet ID#: ORPS200714a
Scale: 1129293203
Temp: 21.7 °C
Baro PE: 1001 hPa
Analyst: HRM/EDT
Technician: HRM/EDT
Sample ID#: 125292

Lot #: 6-10-20 Tangerine Breath
Batch #: 125292
Batch Weight (g): 1417.9
Harvest/Process Date: 06/10/2020
Serving Size (g): 1
Date Received: 07/09/2020
Test Date: 07/14/2020
Sample #125292
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
Aldicarb 0.400 0.118 Pass/<LOD Abamectin**** 0.500 0.118 Pass/<LOD
Acephate 0.400 0.118 Pass/<LOD Acequinocyl 2.000 0.237 Pass/<LOD
Acetamiprid 0.200 0.118 Pass/<LOD Azoxystrobin 0.200 0.118 Pass/<LOD
Bifenazate 0.200 0.118 Pass/<LOD Bifenthrin 0.200 0.118 Pass/<LOD
Boscalid 0.400 0.118 Pass/<LOD Carbaryl 0.200 0.118 Pass/<LOD
Carbofuran 0.200 0.118 Pass/<LOD Chlorantraniliprole 0.200 0.118 Pass/<LOD
Chlorfenapyr 1.000 0.474 Pass/<LOD Chlorpyrifos 0.200 0.118 Pass/<LOD
Clofentezine 0.200 0.118 Pass/<LOD Cyfluthrin** 1.000 0.474 Pass/<LOD
Cypermethrin*** 1.000 0.474 Pass/<LOD Daminozide 1.000 0.118 Pass/<LOD
DDVP (Dichlorvos) 1.000 0.237 Pass/<LOD Diazinon 0.200 0.118 Pass/<LOD
Dimethoate 0.200 0.118 Pass/<LOD Ethoprophos 0.200 0.118 Pass/<LOD
Etofenprox 0.400 0.118 Pass/<LOD Etoxazole 0.200 0.118 Pass/<LOD
Fenoxycarb 0.200 0.118 Pass/<LOD Fenpyroximate 0.400 0.118 Pass/<LOD
Fipronil 0.400 0.118 Pass/<LOD Flonicamid 1.000 0.118 Pass/<LOD
Fludioxonil 0.400 0.118 Pass/<LOD Hexythiazox 1.000 0.118 Pass/<LOD
Imazalil 0.200 0.118 Pass/<LOD Imidacloprid 0.400 0.118 Pass/<LOD
Kresoxim Methyl 0.400 0.118 Pass/<LOD Malathion 0.200 0.118 Pass/<LOD
Metalaxyl 0.200 0.118 Pass/<LOD Methiocarb 0.200 0.118 Pass/<LOD
Methomyl 0.400 0.118 Pass/<LOD Methyl Parathion 0.200 0.118 Pass/<LOD
MGK-264‡ 0.200 0.118 Pass/<LOD Myclobutanil 0.000 0.118 Pass/<LOD
Naled 0.500 0.118 Pass/<LOD Oxamyl 1.000 0.118 Pass/<LOD
Paclobutrazol 0.400 0.118 Pass/<LOD Permethrins† 0.200 0.118 Pass/<LOD
Phosmet 0.200 0.118 Pass/<LOD Piperonyl Butoxide 2.000 0.118 Pass/<LOD
Prallethrin 0.200 0.118 Pass/<LOD Propiconazole 0.400 0.118 Pass/<LOD
Propoxur 0.200 0.118 Pass/<LOD Pyrethrins* 1.000 0.118 Pass/<LOD
Pyridaben 0.200 0.118 Pass/<LOD Spinosad***** 0.200 0.118 Pass/<LOD
Spiromesifen 0.200 0.118 Pass/<LOD Spirotetramat 0.200 0.118 Pass/<LOD
Spiroxamine‡ 0.400 0.118 Pass/<LOD Tebuconazole 0.400 0.118 Pass/<LOD
Thiacloprid 0.200 0.118 Pass/<LOD Thiamethoxam 0.200 0.118 Pass/<LOD
Trifloxystrobin 0.200 0.118 Pass/<LOD

* Pyrethrins are reported as the sum of Jasmolin I, Cinerin I, and Pyrethrin I
** Cyfluthrins are reported as the sum of isomers Cyfluthrin I, II, III, and IV
*** Cypermethrins are reported as the sum of isomers Cypermethrin I, II, III, and IV
**** Abamectin is reported as the sum of Avermectin B1a and Avermectin B1b
***** Spinosad is reported as the sum of Spinosyn A and Spinosyn D
† Permethrin and Prallethrin are reported as the sum of cis and trans isomers
‡ MGK-264 and Spiroximine are reported as the sum of isomers I and II
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 2 of 4

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Pesticide QC Report
Testing Accreditation #: 4092-004 Test Certificate #: 125292-001
Client Name, Sample Details

Oregon Grow Group
Florence, OR 97439
Sample: Tangerine Breath
License: 020-1011919EEBA
Type: Adult Use Flower
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A40103000223A9000000148
Metrc Source Pkg#: 1A40103000223A9000000145
Test Conditions

Prepsheet ID#: ORPS200714a
Scale: 1129293203
Temp: 21.7 °C
Baro PE: 1001 hPa
Analyst: HRM/EDT
Technician: HRM/EDT
Sample ID#: 125292

Lot #: 6-10-20 Tangerine Breath
Batch #: 125292
Batch Weight (g): 1417.9
Harvest/Process Date: 06/10/2020
Serving Size (g): 1
Date Received: 07/09/2020
Test Date: 07/14/2020
Sample #125292
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS recovery% MSD recovery% Relative Percent Difference (%) QC Flag
Acephate N.D. 1 1.01 1.03 101.00 103.00 1.96
Acequinocyl N.D. 1 0.84 0.74 84.00 74.00 12.66
Acetamiprid N.D. 1 1.05 1.12 105.00 112.00 6.45
Aldicarb N.D. 1 1.05 1.09 105.00 109.00 3.74
Avermectin B1a N.D. 0.97 1.12 1.12 115.46 115.46 0.00
Azoxystrobin N.D. 1 0.95 0.968 95.00 96.80 1.88
Bifenazate N.D. 1 0.503 0.478 50.30 47.80 5.10 LR
Bifenthrin N.D. 1 1.08 1.13 108.00 113.00 4.52
Boscalid N.D. 1 0.93 0.941 93.00 94.10 1.18
Carbaryl N.D. 1 1.08 1.08 108.00 108.00 0.00
Carbofuran N.D. 1 1.15 1.17 115.00 117.00 1.72
Chlorantraniliprole N.D. 1 0.949 0.933 94.90 93.30 1.70
Chlorfenapyr N.D. 1 0.96 0.802 96.00 80.20 17.93
Chlorpyriphos N.D. 1 1.03 1.05 103.00 105.00 1.92
Clofentezine N.D. 1 0.81 0.805 81.00 80.50 0.62
Cyfluthrin N.D. 1 1.1 0.979 110.00 97.90 11.64
Cypermethrin N.D. 1 0.994 1.03 99.40 103.00 3.56
Daminoside N.D. 1 0.426 0.481 42.60 48.10 12.13 LR
Diazanon N.D. 1 0.895 0.889 89.50 88.90 0.67
Dichlorvos N.D. 1 1.18 1.08 118.00 108.00 8.85
Dimethoate N.D. 1 1.03 1.05 103.00 105.00 1.92
Ethoprophos N.D. 1 0.877 0.879 87.70 87.90 0.23
Etofenprox N.D. 1 1.1 1.06 110.00 106.00 3.70
Etoxazole N.D. 1 1.11 1.19 111.00 119.00 6.96
Fenoxycarb N.D. 1 0.892 0.926 89.20 92.60 3.74
Fenpyroximate N.D. 1 1.18 1.15 118.00 115.00 2.58
Fipronil N.D. 1 1.1 1.11 110.00 111.00 0.90
Flonicamid N.D. 1 1.04 1.1 104.00 110.00 5.61
Fludioxonil N.D. 1 1.15 1.19 115.00 119.00 3.42
Hexythiazox N.D. 1 1.06 0.795 106.00 79.50 28.57 Q
Imazalil N.D. 1 0.922 0.963 92.20 96.30 4.35
Imidacloprid N.D. 1 1.05 1.11 105.00 111.00 5.56
Kresoxim-methyl N.D. 1 0.907 0.908 90.70 90.80 0.11
Malathion N.D. 1 0.973 0.894 97.30 89.40 8.46
Metalaxyl N.D. 1 0.965 0.968 96.50 96.80 0.31
Methiocarb N.D. 1 1.03 1.03 103.00 103.00 0.00
Methomyl N.D. 1 0.963 0.982 96.30 98.20 1.95
MGK-264 N.D. 1 1.07 1.03 107.00 103.00 3.81
Myclobutanil N.D. 1 0.998 0.983 99.80 98.30 1.51
Naled (dibrom) N.D. 1 0.562 0.556 56.20 55.60 1.07 LR
Oxamyl N.D. 1 1.15 1.2 115.00 120.00 4.26
Paclobutrazol N.D. 1 0.973 0.988 97.30 98.80 1.53
Parathion-methyl N.D. 1 1.07 1.12 107.00 112.00 4.57
Permethrins N.D. 1 1.014 1.018 101.40 101.80 0.39
Phosmet N.D. 1 0.935 0.921 93.50 92.10 1.51
Piperonyl butoxide N.D. 1 1.16 1.19 116.00 119.00 2.55
Prallethrin N.D. 1 1 1.01 100.00 101.00 1.00
Propiconazole N.D. 1 0.993 0.996 99.30 99.60 0.30
Propoxur N.D. 1 1.12 1.1 112.00 110.00 1.80
Pyrethrin N.D. 0.65 0.511 0.511 78.62 78.62 0.00
Pyridaben N.D. 1 1.11 1.08 111.00 108.00 2.74
SpinosynA N.D. 0.84 0.847 0.719 100.83 85.60 16.35
SpinosynD N.D. 0.16 0.175 0.173 109.38 108.13 1.15
Spiromesifen N.D. 1 0.287 0.3 28.70 30.00 4.43 LR
Spirotetramat N.D. 1 0.899 0.895 89.90 89.50 0.45
Spiroxamine N.D. 1 0.977 1.04 97.70 104.00 6.25
Tebuconazole N.D. 1 0.921 0.907 92.10 90.70 1.53
Thiacloprid N.D. 1 1.05 1.08 105.00 108.00 2.82
Thiamethoxam N.D. 1 0.947 0.973 94.70 97.30 2.71
Trifloxystrobin N.D. 1 1.03 1.04 103.00 104.00 0.97

N.D. = Not Detected

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 30%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (60-120%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 3 of 4
IRON Laboratories

Terpene Report by
Mass Spectrometer
Test Certificate #: 125292-001
Client Name, Sample Details

Oregon Grow Group
Florence, OR 97439
Sample: Tangerine Breath
License: 020-1011919EEBA
Type: Adult Use Flower
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A40103000223A9000000148
Metrc Source Pkg#: 1A40103000223A9000000145

Test Conditions

Scale: XS205-OR1
Temp: 19.9 °C
Baro Pressure: 1003 hPa
Analyst: HRM
Technician: HRM

Sample ID#: 125292

Lot #: 6-10-20 Tangerine Breath
Batch #: 125292
Batch Weight (g): 1417.9
Harvest/Process Date: 06/10/2020
Serving Size (g): 1
Date Received: 07/09/2020

Sample #125292
Sample #125292
  • α-Pinene (0.04%)
  • β-Ocimene (0.05%)
  • Camphene (0.00%)
  • Eucalyptol (1,8-Cineol) (0.00%)
  • Sabinene (0.00%)
  • γ-Terpinene (0.00%)
  • Myrcene (0.04%)
  • α-Terpinolene (0.02%)
  • β-Pinene (0.06%)
  • Linalool (0.13%)
  • ∆3-Carene (0.00%)
  • Fenchone (0.00%)
  • α-Terpinene (0.00%)
  • endo-Fenchol (0.00%)
  • α-Ocimene (0.00%)
  • Isopulegol (0.00%)
  • Limonene (0.16%)
  • Geraniol (0.00%)
  • p-Cymene (0.00%)
  • β-Caryophyllene (0.72%)
  • α-Humulene (0.32%)
  • Nerolidol 1 (cis) (0.00%)
  • Nerolidol 2 (trans) (0.02%)
  • Guaiol (0.00%)
  • Caryophyllene Oxide (0.02%)
  • α-Bisabolol (0.14%)
  • α-Phellandrene (0.00%)
  • α-Terpineol (0.18%)
  • Valenence (0.00%)

Total: 1.900%

Predominant Terpenes

0.72%   β-Caryophyllene Sweet, woody, spicy, clove 0.32%   α-Humulene Woody, oceanic-watery, spicy clove
0.18%   α-Terpineol Pine, woody, lemon, lime, citrus, floral 0.16%   Limonene Citrus, orange, sweet
0.14%   α-Bisabolol Fruity, nutty, coconut 0.13%   Linalool Citrus, floral, sweet, bois de rose, woody, green, blueberry

Value in parenthesis indicates percentage of terpene present in the total sample (weight percentage, wt/wt%).
Value in doughnut slice indicates individual terpene abundance with respect to the total terpenes detected.

This sample has not been tested according to OAR 333-007. These results should therefore be used for research and development or quality control purposes only.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 4 of 4