ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Marijuana Potency Analysis by
High Performance Liquid Chromatography

Testing Accreditation #: 4092-004 Test Certificate #: 125191-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Fermented Fruit
License: 030-1009646F7F8
Type: AU Tincture
Method: FE04U HPLC-UV
Metrc Test Pkg#: 1A401030002C949000000451
Metrc Source Pkg#: 1A401030002C949000000448

Test Conditions

Prepsheet ID#: ORP200706a
Scale: XS205-OR1
Temp: 21.8 °C
Baro Pressure: 1003 hPa
Analyst: HRM
Technician: tmr

Sample ID#: 125191

Lot #: Fermented Fruit 7.01.20 #1
Batch #: 125191
Batch Weight (g): 155.1
Harvest/Process Date: 07/01/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 07/01/2020
Test Date: 07/06/2020

Sample #125191
Sample #125191 Sample #125191
Test
Compounds
THC THCA CBD CBDA CBN CBG CBC THCV* CBDV Total
Cannabinoids*
Total THC Total CBD Calc Max Total
Cannabinoids*
Amount (%) 5.29 82.64 N/D 1.46 0.67 0.39 0.29 N/D N/D 90.73 77.77 1.28 80.39
Amount (mg/g) 52.94 826.36 N/D 14.55 6.67 3.92 2.90 N/D N/D 907.34 777.66 12.76 803.91
Amount per Serving (mg) 2.65 41.32 N\D 0.73 0.33 0.20 0.15 N\D N\D 45.37 Serving Size~ (g): 0.05
LOQ (mg/g) 2.2 2.2 2.2 2.2 2.2 2.2 2.2 2.2 2.2   %Decarb. THC CBD
±%RPD 18.92 18.32 18.31 17.54 17.88 18.75 17.88 18.35 17.78 6 0

LOQ = Limit of Quantitation; %RPD = Relative Percent Deviation; %RSD = Relative Standard Deviation; N/D = Not Detected

*Designates values that are not currently included in the accredited scope of Iron Laboratories.

*** Designates tests that use the method FE-45. FE-45 is performed using AOAC 966.02 and 32.004-32.009. FE-45 has relative expanded (k=2) uncertainties of 1.098% for moisture, 1.754% for water activity for unprocessed plant materials, and 13.102% for water activity for infused products. Vitamin E acetate analysis has a relative expanded (k=2) uncertainty of 18.614%.

Total THC and CBD is the calculated sum of THC or CBD and the amount of THC or CBD derived from THCA or CBDA, respectively. These values are calculated by applying a molar correction factor of 0.877 to the THCA or the CBDA value. Calc Max Total Cannabinoids is the sum of Total THC, Total CBD, CBN, CBG, CBC, THCV, and CBDV.

%Decarb. THC and CBD refer to the percentage of THC or CBD relative to THCA or CBDA, respectively.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 1 of 11

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant QC Report

Testing Accreditation #: 4092-004 Test Certificate #: 125191-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Fermented Fruit
License: 030-1009646F7F8
Type: AU Tincture
Method: FE04U HPLC-UV
Metrc Test Pkg#: 1A401030002C949000000451
Metrc Source Pkg#: 1A401030002C949000000448

Test Conditions

Prepsheet ID#: ORP200706a
Scale: XS205-OR1
Temp: 21.8 °C
Baro Pressure: 1003 hPa
Analyst: HRM
Technician: tmr

Sample ID#: 125191

Lot #: Fermented Fruit 7.01.20 #1
Batch #: 125191
Batch Weight (g): 155.1
Harvest/Process Date: 07/01/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 07/01/2020
Test Date: 07/06/2020

Sample #125191
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Cannabidivarin (CBDV) N.D. 6.7 5.33 79.55 6.37 95.07 17.78
Cannabidiolic Acid (CBDA) N.D. 6.17 4.94 80.06 5.89 95.46 17.54
Cannabigerol (CBG) N.D. 6.74 5.22 77.45 6.3 93.47 18.75
Cannabidiol (CBD) N.D. 6.47 5.16 79.75 6.2 95.83 18.31
Δ9-Tetrahydrocannabivarin (THCV) N.D. 6.38 4.95 77.59 5.95 93.26 18.35
Cannabinol (CBN) N.D. 6.39 4.99 78.09 5.97 93.43 17.88
Δ9-Tetrahydrocannabinol (THC) N.D. 6.4 4.93 77.03 5.96 93.13 18.92
Cannabichromene (CBC) N.D. 6.98 5.45 78.08 6.52 93.41 17.88
Tetrahydrocannabinolic acid (THCA) N.D. 6.16 4.86 78.90 5.84 94.81 18.32

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 2 of 11

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Pesticide Analysis by
Mass Spectrometer

Testing Accreditation #: 4092-004 Test Certificate #: 125191-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Fermented Fruit
License: 030-1009646F7F8
Type: AU Tincture
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A401030002C949000000451
Metrc Source Pkg#: 1A401030002C949000000448

Test Conditions

Prepsheet ID#: ORPS200701a
Scale: 1129293203
Temp: 21.3 °C
Baro PE: 1001 hPa
Analyst: HRM/EDT
Technician: HRM/EDT

Sample ID#: 125191

Lot #: Fermented Fruit 7.01.20 #1
Batch #: 125191
Batch Weight (g): 155.1
Harvest/Process Date: 07/01/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 07/01/2020
Test Date: 07/01/2020

Sample #125191
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
Aldicarb 0.400 0.122 Pass/<LOD Abamectin**** 0.500 0.122 Pass/<LOD
Acephate 0.400 0.122 Pass/<LOD Acequinocyl 2.000 0.244 Pass/<LOD
Acetamiprid 0.200 0.122 Pass/<LOD Azoxystrobin 0.200 0.122 Pass/<LOD
Bifenazate 0.200 0.122 Pass/<LOD Bifenthrin 0.200 0.122 Pass/<LOD
Boscalid 0.400 0.122 Pass/<LOD Carbaryl 0.200 0.122 Pass/<LOD
Carbofuran 0.200 0.122 Pass/<LOD Chlorantraniliprole 0.200 0.122 Pass/<LOD
Chlorfenapyr 1.000 0.487 Pass/<LOD Chlorpyrifos 0.200 0.122 Pass/<LOD
Clofentezine 0.200 0.122 Pass/<LOD Cyfluthrin** 1.000 0.487 Pass/<LOD
Cypermethrin*** 1.000 0.487 Pass/<LOD Daminozide 1.000 0.122 Pass/<LOD
DDVP (Dichlorvos) 1.000 0.244 Pass/<LOD Diazinon 0.200 0.122 Pass/<LOD
Dimethoate 0.200 0.122 Pass/<LOD Ethoprophos 0.200 0.122 Pass/<LOD
Etofenprox 0.400 0.122 Pass/<LOD Etoxazole 0.200 0.122 Pass/<LOD
Fenoxycarb 0.200 0.122 Pass/<LOD Fenpyroximate 0.400 0.122 Pass/<LOD
Fipronil 0.400 0.122 Pass/<LOD Flonicamid 1.000 0.122 Pass/<LOD
Fludioxonil 0.400 0.122 Pass/<LOD Hexythiazox 1.000 0.122 Pass/<LOD
Imazalil 0.200 0.122 Pass/<LOD Imidacloprid 0.400 0.122 Pass/<LOD
Kresoxim Methyl 0.400 0.122 Pass/<LOD Malathion 0.200 0.122 Pass/<LOD
Metalaxyl 0.200 0.122 Pass/<LOD Methiocarb 0.200 0.122 Pass/<LOD
Methomyl 0.400 0.122 Pass/<LOD Methyl Parathion 0.200 0.122 Pass/<LOD
MGK-264‡ 0.200 0.122 Pass/<LOD Myclobutanil 0.000 0.122 Pass/<LOD
Naled 0.500 0.122 Pass/<LOD Oxamyl 1.000 0.122 Pass/<LOD
Paclobutrazol 0.400 0.122 Pass/<LOD Permethrins† 0.200 0.122 Pass/<LOD
Phosmet 0.200 0.122 Pass/<LOD Piperonyl Butoxide 2.000 0.122 Pass/0.279
Prallethrin 0.200 0.122 Pass/<LOD Propiconazole 0.400 0.122 Pass/<LOD
Propoxur 0.200 0.122 Pass/<LOD Pyrethrins* 1.000 0.122 Pass/<LOD
Pyridaben 0.200 0.122 Pass/<LOD Spinosad***** 0.200 0.122 Pass/<LOD
Spiromesifen 0.200 0.122 Pass/<LOD Spirotetramat 0.200 0.122 Pass/<LOD
Spiroxamine‡ 0.400 0.122 Pass/<LOD Tebuconazole 0.400 0.122 Pass/<LOD
Thiacloprid 0.200 0.122 Pass/<LOD Thiamethoxam 0.200 0.122 Pass/<LOD
Trifloxystrobin 0.200 0.122 Pass/<LOD

* Pyrethrins are reported as the sum of Jasmolin I, Cinerin I, and Pyrethrin I
** Cyfluthrins are reported as the sum of isomers Cyfluthrin I, II, III, and IV
*** Cypermethrins are reported as the sum of isomers Cypermethrin I, II, III, and IV
**** Abamectin is reported as the sum of Avermectin B1a and Avermectin B1b
***** Spinosad is reported as the sum of Spinosyn A and Spinosyn D
† Permethrin and Prallethrin are reported as the sum of cis and trans isomers
‡ MGK-264 and Spiroximine are reported as the sum of isomers I and II
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 2 of 11

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Pesticide QC Report

Testing Accreditation #: 4092-004 Test Certificate #: 125191-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Fermented Fruit
License: 030-1009646F7F8
Type: AU Tincture
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A401030002C949000000451
Metrc Source Pkg#: 1A401030002C949000000448

Test Conditions

Prepsheet ID#: ORPS200701a
Scale: 1129293203
Temp: 21.3 °C
Baro PE: 1001 hPa
Analyst: HRM/EDT
Technician: HRM/EDT

Sample ID#: 125191

Lot #: Fermented Fruit 7.01.20 #1
Batch #: 125191
Batch Weight (g): 155.1
Harvest/Process Date: 07/01/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 07/01/2020
Test Date: 07/01/2020

Sample #125191
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS recovery% MSD recovery% Relative Percent Difference (%) QC Flag
Acephate N.D. 1 0.996 1.06 99.60 106.00 6.23
Acequinocyl N.D. 1 0.321 0.455 32.10 45.50 34.54 LR Q
Acetamiprid N.D. 1 1.16 1.23 116.00 123.00 5.86
Aldicarb N.D. 1 0.998 1.03 99.80 103.00 3.16
Avermectin B1a N.D. 0.97 1.39 1.3 143.30 134.02 6.69
Azoxystrobin N.D. 1 1.11 1.2 111.00 120.00 7.79
Bifenazate N.D. 1 0.474 0.361 47.40 36.10 27.07 LR Q
Bifenthrin N.D. 1 0.935 1.13 93.50 113.00 18.89
Boscalid N.D. 1 1.22 1.2 122.00 120.00 1.65
Carbaryl N.D. 1 1.1 1.17 110.00 117.00 6.17
Carbofuran N.D. 1 1.26 1.3 126.00 130.00 3.13
Chlorantraniliprole N.D. 1 1.51 1.64 151.00 164.00 8.25 HR
Chlorfenapyr N.D. 1 0.639 0.702 63.90 70.20 9.40 LR
Chlorpyriphos N.D. 1 0.944 1.05 94.40 105.00 10.63
Clofentezine N.D. 1 1.23 1.24 123.00 124.00 0.81
Cyfluthrin N.D. 1 1.51 1.54 151.00 154.00 1.97 HR
Cypermethrin N.D. 1 1.33 1.33 133.00 133.00 0.00
Daminoside N.D. 1 0.642 0.59 64.20 59.00 8.44 LR
Diazanon N.D. 1 1.41 1.46 141.00 146.00 3.48
Dichlorvos N.D. 1 1.04 1.15 104.00 115.00 10.05
Dimethoate N.D. 1 1.13 1.16 113.00 116.00 2.62
Ethoprophos N.D. 1 1.1 1.12 110.00 112.00 1.80
Etofenprox N.D. 1 0.862 0.943 86.20 94.30 8.98
Etoxazole N.D. 1 1.13 1.17 113.00 117.00 3.48
Fenoxycarb N.D. 1 1.48 1.46 148.00 146.00 1.36
Fenpyroximate N.D. 1 1.12 1.24 112.00 124.00 10.17
Fipronil N.D. 1 0.972 0.989 97.20 98.90 1.73
Flonicamid N.D. 1 1.28 1.26 128.00 126.00 1.57
Fludioxonil N.D. 1 0.966 0.943 96.60 94.30 2.41
Hexythiazox N.D. 1 0.766 0.903 76.60 90.30 16.42
Imazalil N.D. 1 1.58 0.885 158.00 88.50 56.39 HR Q
Imidacloprid N.D. 1 1.41 1.37 141.00 137.00 2.88
Kresoxim-methyl N.D. 1 1.62 1.79 162.00 179.00 9.97 HR
Malathion N.D. 1 1.36 1.36 136.00 136.00 0.00
Metalaxyl N.D. 1 1.73 1.7 173.00 170.00 1.75
Methiocarb N.D. 1 1.12 1.2 112.00 120.00 6.90
Methomyl N.D. 1 1.28 1.24 128.00 124.00 3.17
MGK-264 N.D. 1 1.17 1.16 117.00 116.00 0.86
Myclobutanil N.D. 1 1.62 1.71 162.00 171.00 5.41 HR
Naled (dibrom) N.D. 1 0.597 0.691 59.70 69.10 14.60 LR
Oxamyl N.D. 1 1.21 1.26 121.00 126.00 4.05
Paclobutrazol N.D. 1 2.01 1.76 201.00 176.00 13.26 HR
Parathion-methyl N.D. 1 1.09 1.2 109.00 120.00 9.61
Permethrins N.D. 1 0.85 0.979 85.00 97.90 14.11 Q
Phosmet N.D. 1 1.41 1.42 141.00 142.00 0.71 HR
Piperonyl butoxide N.D. 1 1.07 1.24 107.00 124.00 14.72
Prallethrin N.D. 1 1.65 1.64 165.00 164.00 0.61 HR
Propiconazole N.D. 1 1.42 1.48 142.00 148.00 4.14
Propoxur N.D. 1 1.09 1.31 109.00 131.00 18.33
Pyrethrin N.D. 0.65 0.846 0.911 130.15 140.15 7.40
Pyridaben N.D. 1 0.948 0.991 94.80 99.10 4.44
SpinosynA N.D. 0.84 1.23 1.29 146.43 153.57 4.76
SpinosynD N.D. 0.16 0.272 0.283 170.00 176.88 3.96 HR
Spiromesifen N.D. 1 0.294 0.279 29.40 27.90 5.24 LR
Spirotetramat N.D. 1 1.56 1.65 156.00 165.00 5.61 HR
Spiroxamine N.D. 1 1.52 1.55 152.00 155.00 1.95
Tebuconazole N.D. 1 1.6 1.85 160.00 185.00 14.49 HR
Thiacloprid N.D. 1 1.36 1.4 136.00 140.00 2.90
Thiamethoxam N.D. 1 1.73 1.61 173.00 161.00 7.19 HR
Trifloxystrobin N.D. 1 1.18 1.22 118.00 122.00 3.33

N.D. = Not Detected

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 30%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (60-120%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 3 of 11

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Pesticide Analysis by
Mass Spectrometer

Testing Accreditation #: 4092-004 Test Certificate #: 125191-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Fermented Fruit
License: 030-1009646F7F8
Type: AU Tincture
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A401030002C949000000451
Metrc Source Pkg#: 1A401030002C949000000448

Test Conditions

Prepsheet ID#: ORPS200701a
Scale: 1129293203
Temp: 21.3 °C
Baro PE: 1001 hPa
Analyst: HRM/EDT
Technician: HRM/EDT

Sample ID#: 125191

Lot #: Fermented Fruit 7.01.20 #1
Batch #: 125191
Batch Weight (g): 155.1
Harvest/Process Date: 07/01/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 07/01/2020
Test Date: 07/01/2020

Sample #125191
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
Aldicarb 0.400 0.122 Pass/<LOD Abamectin**** 0.500 0.122 Pass/<LOD
Acephate 0.400 0.122 Pass/<LOD Acequinocyl 2.000 0.244 Pass/<LOD
Acetamiprid 0.200 0.122 Pass/<LOD Azoxystrobin 0.200 0.122 Pass/<LOD
Bifenazate 0.200 0.122 Pass/<LOD Bifenthrin 0.200 0.122 Pass/<LOD
Boscalid 0.400 0.122 Pass/<LOD Carbaryl 0.200 0.122 Pass/<LOD
Carbofuran 0.200 0.122 Pass/<LOD Chlorantraniliprole 0.200 0.122 Pass/<LOD
Chlorfenapyr 1.000 0.487 Pass/<LOD Chlorpyrifos 0.200 0.122 Pass/<LOD
Clofentezine 0.200 0.122 Pass/<LOD Cyfluthrin** 1.000 0.487 Pass/<LOD
Cypermethrin*** 1.000 0.487 Pass/<LOD Daminozide 1.000 0.122 Pass/<LOD
DDVP (Dichlorvos) 1.000 0.244 Pass/<LOD Diazinon 0.200 0.122 Pass/<LOD
Dimethoate 0.200 0.122 Pass/<LOD Ethoprophos 0.200 0.122 Pass/<LOD
Etofenprox 0.400 0.122 Pass/<LOD Etoxazole 0.200 0.122 Pass/<LOD
Fenoxycarb 0.200 0.122 Pass/<LOD Fenpyroximate 0.400 0.122 Pass/<LOD
Fipronil 0.400 0.122 Pass/<LOD Flonicamid 1.000 0.122 Pass/<LOD
Fludioxonil 0.400 0.122 Pass/<LOD Hexythiazox 1.000 0.122 Pass/<LOD
Imazalil 0.200 0.122 Pass/<LOD Imidacloprid 0.400 0.122 Pass/<LOD
Kresoxim Methyl 0.400 0.122 Pass/<LOD Malathion 0.200 0.122 Pass/<LOD
Metalaxyl 0.200 0.122 Pass/<LOD Methiocarb 0.200 0.122 Pass/<LOD
Methomyl 0.400 0.122 Pass/<LOD Methyl Parathion 0.200 0.122 Pass/<LOD
MGK-264‡ 0.200 0.122 Pass/<LOD Myclobutanil 0.000 0.122 Pass/<LOD
Naled 0.500 0.122 Pass/<LOD Oxamyl 1.000 0.122 Pass/<LOD
Paclobutrazol 0.400 0.122 Pass/<LOD Permethrins† 0.200 0.122 Pass/<LOD
Phosmet 0.200 0.122 Pass/<LOD Piperonyl Butoxide 2.000 0.122 Pass/0.254
Prallethrin 0.200 0.122 Pass/<LOD Propiconazole 0.400 0.122 Pass/<LOD
Propoxur 0.200 0.122 Pass/<LOD Pyrethrins* 1.000 0.122 Pass/<LOD
Pyridaben 0.200 0.122 Pass/<LOD Spinosad***** 0.200 0.122 Pass/<LOD
Spiromesifen 0.200 0.122 Pass/<LOD Spirotetramat 0.200 0.122 Pass/<LOD
Spiroxamine‡ 0.400 0.122 Pass/<LOD Tebuconazole 0.400 0.122 Pass/<LOD
Thiacloprid 0.200 0.122 Pass/<LOD Thiamethoxam 0.200 0.122 Pass/<LOD
Trifloxystrobin 0.200 0.122 Pass/<LOD

* Pyrethrins are reported as the sum of Jasmolin I, Cinerin I, and Pyrethrin I
** Cyfluthrins are reported as the sum of isomers Cyfluthrin I, II, III, and IV
*** Cypermethrins are reported as the sum of isomers Cypermethrin I, II, III, and IV
**** Abamectin is reported as the sum of Avermectin B1a and Avermectin B1b
***** Spinosad is reported as the sum of Spinosyn A and Spinosyn D
† Permethrin and Prallethrin are reported as the sum of cis and trans isomers
‡ MGK-264 and Spiroximine are reported as the sum of isomers I and II
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 4 of 11

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Pesticide QC Report

Testing Accreditation #: 4092-004 Test Certificate #: 125191-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Fermented Fruit
License: 030-1009646F7F8
Type: AU Tincture
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A401030002C949000000451
Metrc Source Pkg#: 1A401030002C949000000448

Test Conditions

Prepsheet ID#: ORPS200701a
Scale: 1129293203
Temp: 21.3 °C
Baro PE: 1001 hPa
Analyst: HRM/EDT
Technician: HRM/EDT

Sample ID#: 125191

Lot #: Fermented Fruit 7.01.20 #1
Batch #: 125191
Batch Weight (g): 155.1
Harvest/Process Date: 07/01/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 07/01/2020
Test Date: 07/01/2020

Sample #125191
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS recovery% MSD recovery% Relative Percent Difference (%) QC Flag
Acephate N.D. 1 0.996 1.06 99.60 106.00 6.23
Acequinocyl N.D. 1 0.321 0.455 32.10 45.50 34.54 LR Q
Acetamiprid N.D. 1 1.16 1.23 116.00 123.00 5.86
Aldicarb N.D. 1 0.998 1.03 99.80 103.00 3.16
Avermectin B1a N.D. 0.97 1.39 1.3 143.30 134.02 6.69
Azoxystrobin N.D. 1 1.11 1.2 111.00 120.00 7.79
Bifenazate N.D. 1 0.474 0.361 47.40 36.10 27.07 LR Q
Bifenthrin N.D. 1 0.935 1.13 93.50 113.00 18.89
Boscalid N.D. 1 1.22 1.2 122.00 120.00 1.65
Carbaryl N.D. 1 1.1 1.17 110.00 117.00 6.17
Carbofuran N.D. 1 1.26 1.3 126.00 130.00 3.13
Chlorantraniliprole N.D. 1 1.51 1.64 151.00 164.00 8.25 HR
Chlorfenapyr N.D. 1 0.639 0.702 63.90 70.20 9.40 LR
Chlorpyriphos N.D. 1 0.944 1.05 94.40 105.00 10.63
Clofentezine N.D. 1 1.23 1.24 123.00 124.00 0.81
Cyfluthrin N.D. 1 1.51 1.54 151.00 154.00 1.97 HR
Cypermethrin N.D. 1 1.33 1.33 133.00 133.00 0.00
Daminoside N.D. 1 0.642 0.59 64.20 59.00 8.44 LR
Diazanon N.D. 1 1.41 1.46 141.00 146.00 3.48
Dichlorvos N.D. 1 1.04 1.15 104.00 115.00 10.05
Dimethoate N.D. 1 1.13 1.16 113.00 116.00 2.62
Ethoprophos N.D. 1 1.1 1.12 110.00 112.00 1.80
Etofenprox N.D. 1 0.862 0.943 86.20 94.30 8.98
Etoxazole N.D. 1 1.13 1.17 113.00 117.00 3.48
Fenoxycarb N.D. 1 1.48 1.46 148.00 146.00 1.36
Fenpyroximate N.D. 1 1.12 1.24 112.00 124.00 10.17
Fipronil N.D. 1 0.972 0.989 97.20 98.90 1.73
Flonicamid N.D. 1 1.28 1.26 128.00 126.00 1.57
Fludioxonil N.D. 1 0.966 0.943 96.60 94.30 2.41
Hexythiazox N.D. 1 0.766 0.903 76.60 90.30 16.42
Imazalil N.D. 1 1.58 0.885 158.00 88.50 56.39 HR Q
Imidacloprid N.D. 1 1.41 1.37 141.00 137.00 2.88
Kresoxim-methyl N.D. 1 1.62 1.79 162.00 179.00 9.97 HR
Malathion N.D. 1 1.36 1.36 136.00 136.00 0.00
Metalaxyl N.D. 1 1.73 1.7 173.00 170.00 1.75
Methiocarb N.D. 1 1.12 1.2 112.00 120.00 6.90
Methomyl N.D. 1 1.28 1.24 128.00 124.00 3.17
MGK-264 N.D. 1 1.17 1.16 117.00 116.00 0.86
Myclobutanil N.D. 1 1.62 1.71 162.00 171.00 5.41 HR
Naled (dibrom) N.D. 1 0.597 0.691 59.70 69.10 14.60 LR
Oxamyl N.D. 1 1.21 1.26 121.00 126.00 4.05
Paclobutrazol N.D. 1 2.01 1.76 201.00 176.00 13.26 HR
Parathion-methyl N.D. 1 1.09 1.2 109.00 120.00 9.61
Permethrins N.D. 1 0.85 0.979 85.00 97.90 14.11 Q
Phosmet N.D. 1 1.41 1.42 141.00 142.00 0.71 HR
Piperonyl butoxide N.D. 1 1.07 1.24 107.00 124.00 14.72
Prallethrin N.D. 1 1.65 1.64 165.00 164.00 0.61 HR
Propiconazole N.D. 1 1.42 1.48 142.00 148.00 4.14
Propoxur N.D. 1 1.09 1.31 109.00 131.00 18.33
Pyrethrin N.D. 0.65 0.846 0.911 130.15 140.15 7.40
Pyridaben N.D. 1 0.948 0.991 94.80 99.10 4.44
SpinosynA N.D. 0.84 1.23 1.29 146.43 153.57 4.76
SpinosynD N.D. 0.16 0.272 0.283 170.00 176.88 3.96 HR
Spiromesifen N.D. 1 0.294 0.279 29.40 27.90 5.24 LR
Spirotetramat N.D. 1 1.56 1.65 156.00 165.00 5.61 HR
Spiroxamine N.D. 1 1.52 1.55 152.00 155.00 1.95
Tebuconazole N.D. 1 1.6 1.85 160.00 185.00 14.49 HR
Thiacloprid N.D. 1 1.36 1.4 136.00 140.00 2.90
Thiamethoxam N.D. 1 1.73 1.61 173.00 161.00 7.19 HR
Trifloxystrobin N.D. 1 1.18 1.22 118.00 122.00 3.33

N.D. = Not Detected

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 30%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (60-120%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 5 of 11

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents Analysis by
Mass Spectrometer

Testing Accreditation #: 4092-004 Test Certificate #: 125191-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Fermented Fruit
License: 030-1009646F7F8
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A401030002C949000000451
Metrc Source Pkg#: 1A401030002C949000000448

Test Conditions

Prepsheet ID#: ORHS200701a
Scale: XS205-OR1
Temp: 21.2 °C
Baro PE: 1009 hPa
Analyst: HRM
Technician: HRM

Sample ID#: 125191

Lot #: Fermented Fruit 7.01.20 #1
Batch #: 125191
Batch Weight (g): 155.1
Harvest/Process Date: 07/01/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 07/01/2020
Test Date: 07/01/2020

Sample #125191
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
1,2-Dichloroethane 2 1 Pass/<LOD 1,2-Dimethoxyethane 100 5 Pass/<LOD
1,4-dioxane 380 200 Pass/<LOD 1-Butanol 5,000 100 Pass/<LOD
1-Pentanol 5,000 100 Pass/<LOD 1-Propanol 5,000 100 Pass/<LOD
2,2-Dimethylpropane (Neopentane) 5,000 100 Pass/<LOD 2,2-Dimethylbutane (Hexanes) 290 100 Pass/<LOD
2,3-Dimethylbutane (Hexanes) 290 100 Pass/<LOD 2-Butanol 5,000 100 Pass/<LOD
2-Butanone (MEK) 5,000 50 Pass/<LOD 2-Ethoxyethanol 160 40 Pass/<LOD
2-Methylbutane (Isopentane) 5,000 50 Pass/<LOD 2-Methylpentane (Hexanes) 290 50 Pass/<LOD
2-Methylpropane (Isobutane) 5,000 100 Pass/<LOD 2-propanol (Isopropyl Alcohol) 5,000 50 Pass/96
2-Propanone (Acetone) 5,000 50 Pass/<LOD 3-Methylpentane (Hexanes) 290 50 Pass/<LOD
Acetonitrile 410 100 Pass/<LOD Benzene 2 1 Pass/<LOD
Butane 5,000 100 Pass/<LOD Chloroform 2 1 Pass/<LOD
Cumene 70 50 Pass/<LOD Cyclohexane 3,880 1,000 Pass/<LOD
Dichloromethane 600 50 Pass/<LOD Dimethylsulfoxide (DMSO) 5,000 500 Pass/<LOD
Ethanol 5,000 500 Pass/<LOD Ethyl acetate 5,000 50 Pass/<LOD
Ethyl ether 5,000 500 Pass/<LOD Ethylene glycol 620 310 Pass/<LOD
Ethylene oxide 50 50 Pass/<LOD Heptane 5,000 50 Pass/<LOD
Hexane 290 290 Pass/<LOD Isopropyl acetate 5,000 50 Pass/<LOD
Methanol 3,000 500 Pass/<LOD Naptha 400 100 Pass/<LOD
N,N-Dimethylacetamide 1,090 100 Pass/<LOD N,N-Dimethylformamide (DMF) 880 500 Pass/<LOD
Pentane 5,000 50 Pass/<LOD Petroleum Ether 400 100 Pass/<LOD
Propane 5,000 100 Pass/<LOD Pyridine 200 10 Pass/<LOD
Sulfolane 160 200 Pass/<LOD Tetrahydrofuran (THF) 720 200 Pass/<LOD
Toluene 890 50 Pass/<LOD Trichloroethylene 25 5 Pass/<LOD
Xylenes* 2,170 50 Pass/<LOD

Total Butanes = 64 ug/g (PASS); Total Pentanes = 0 ug/g (PASS); Total Hexanes = 0 ug/g (PASS)

* Xylenes are reported as the sum of o-xylene, m-xylene, p-xylene, and ethylbenzene
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 6 of 11

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents QC Report

Testing Accreditation #: 4092-004 Test Certificate #: 125191-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Fermented Fruit
License: 030-1009646F7F8
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A401030002C949000000451
Metrc Source Pkg#: 1A401030002C949000000448

Test Conditions

Prepsheet ID#: ORHS200701a
Scale: XS205-OR1
Temp: 21.2 °C
Baro PE: 1009 hPa
Analyst: HRM
Technician: HRM

Sample ID#: 125191

Lot #: Fermented Fruit 7.01.20 #1
Batch #: 125191
Batch Weight (g): 155.1
Harvest/Process Date: 07/01/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 07/01/2020
Test Date: 07/01/2020

Sample #125191
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS Recovery (%) MSD Recovery (%) Relative Percent Difference (%) QC Flag
1,2-Dichloroethane N.D. 0 0 0 nan nan
n-Propane N.D. 250 47 51 18.80 20.40 8.16 LR
Isobutane N.D. 250 77 79 30.80 31.60 2.56 LR
Methanol N.D. 250 119 130 47.60 52.00 8.84 LR
n-Butane N.D. 250 89 89 35.60 35.60 0.00 LR
2,2-Dimethylpropane N.D. 250 104 104 41.60 41.60 0.00 LR
Ethanol N.D. 250 154 160 61.60 64.00 3.82 LR
Isopentane N.D. 250 122 125 48.80 50.00 2.43 LR
Acetonitrile N.D. 250 168 190 67.20 76.00 12.29 LR
Diethyl ether N.D. 250 146 150 58.40 60.00 2.70 LR
2-propanone N.D. 250 151 151 60.40 60.40 0.00 LR
2-propanol N.D. 250 177 184 70.80 73.60 3.88
n-Pentane N.D. 250 101 61 40.40 24.40 49.38 LRQ
2,2-Dimethylbutane N.D. 250 135 136 54.00 54.40 0.74 LR
2,3-Dimethylbutane N.D. 250 134 142 53.60 56.80 5.80 LR
Methylene chloride N.D. 250 163 168 65.20 67.20 3.02 LR
2-Methylpentane N.D. 250 133 140 53.20 56.00 5.13 LR
3-Methylpentane N.D. 250 142 146 56.80 58.40 2.78 LR
2-Butanol N.D. 250 174 179 69.60 71.60 2.83 LR
n-Hexane N.D. 250 140 137 56.00 54.80 2.17 LR
Ethyl acetate N.D. 250 165 172 66.00 68.80 4.15 LR
Tetrahydrofuran N.D. 250 159 165 0.00 0.00 0.00 LR
Trichloroethylene N.D. 0 0 0 nan nan
Isopropyl acetate N.D. 250 167 169 0.00 0.00 0.00 LR
Benzene N.D. 250 181 186 72.40 74.40 2.72
Chloroform N.D. 0 0 0 nan nan
Cyclohexane N.D. 250 154 154 61.60 61.60 0.00 LR
Ethylene glycol N.D. 250 196 218 78.40 87.20 10.63
Heptane N.D. 250 190 174 76.00 69.60 8.79 LR
2-Ethoxyethanol N.D. 250 183 192 73.20 76.80 4.80
1,4-Dioxane N.D. 250 187 198 74.80 79.20 5.71
Pyridine N.D. 0 0 0 0.00 0.00 0.00
Toluene N.D. 250 179 186 71.60 74.40 3.84
Chlorobenzene N.D. 0 0 0 0.00 0.00 0.00
Ethylbenzene N.D. 250 179 185 71.60 74.00 3.30
m-Xylene/p-Xylene N.D. 500 358 368 71.60 73.60 2.75
o-Xylene N.D. 250 181 183 72.40 73.20 1.10
Cumene N.D. 250 190 194 76.00 77.60 2.08
Ethylene oxide N.D. 250 132 132 52.80 52.80 0.00 LR

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

N.D. = Not Detected

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 7 of 11

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents Analysis by
Mass Spectrometer

Testing Accreditation #: 4092-004 Test Certificate #: 125191-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Fermented Fruit
License: 030-1009646F7F8
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A401030002C949000000451
Metrc Source Pkg#: 1A401030002C949000000448

Test Conditions

Prepsheet ID#: ORHS200701a
Scale: XS205-OR1
Temp: 21.2 °C
Baro PE: 1009 hPa
Analyst: HRM
Technician: HRM

Sample ID#: 125191

Lot #: Fermented Fruit 7.01.20 #1
Batch #: 125191
Batch Weight (g): 155.1
Harvest/Process Date: 07/01/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 07/01/2020
Test Date: 07/01/2020

Sample #125191
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
1,2-Dichloroethane 2 1 Pass/<LOD 1,2-Dimethoxyethane 100 5 Pass/<LOD
1,4-dioxane 380 200 Pass/<LOD 1-Butanol 5,000 100 Pass/<LOD
1-Pentanol 5,000 100 Pass/<LOD 1-Propanol 5,000 100 Pass/<LOD
2,2-Dimethylpropane (Neopentane) 5,000 100 Pass/<LOD 2,2-Dimethylbutane (Hexanes) 290 100 Pass/<LOD
2,3-Dimethylbutane (Hexanes) 290 100 Pass/<LOD 2-Butanol 5,000 100 Pass/<LOD
2-Butanone (MEK) 5,000 50 Pass/<LOD 2-Ethoxyethanol 160 40 Pass/<LOD
2-Methylbutane (Isopentane) 5,000 50 Pass/<LOD 2-Methylpentane (Hexanes) 290 50 Pass/<LOD
2-Methylpropane (Isobutane) 5,000 100 Pass/<LOD 2-propanol (Isopropyl Alcohol) 5,000 50 Pass/72
2-Propanone (Acetone) 5,000 50 Pass/<LOD 3-Methylpentane (Hexanes) 290 50 Pass/<LOD
Acetonitrile 410 100 Pass/<LOD Benzene 2 1 Pass/<LOD
Butane 5,000 100 Pass/<LOD Chloroform 2 1 Pass/<LOD
Cumene 70 50 Pass/<LOD Cyclohexane 3,880 1,000 Pass/<LOD
Dichloromethane 600 50 Pass/<LOD Dimethylsulfoxide (DMSO) 5,000 500 Pass/<LOD
Ethanol 5,000 500 Pass/<LOD Ethyl acetate 5,000 50 Pass/<LOD
Ethyl ether 5,000 500 Pass/<LOD Ethylene glycol 620 310 Pass/<LOD
Ethylene oxide 50 50 Pass/<LOD Heptane 5,000 50 Pass/<LOD
Hexane 290 290 Pass/<LOD Isopropyl acetate 5,000 50 Pass/<LOD
Methanol 3,000 500 Pass/<LOD Naptha 400 100 Pass/<LOD
N,N-Dimethylacetamide 1,090 100 Pass/<LOD N,N-Dimethylformamide (DMF) 880 500 Pass/<LOD
Pentane 5,000 50 Pass/<LOD Petroleum Ether 400 100 Pass/<LOD
Propane 5,000 100 Pass/<LOD Pyridine 200 10 Pass/<LOD
Sulfolane 160 200 Pass/<LOD Tetrahydrofuran (THF) 720 200 Pass/<LOD
Toluene 890 50 Pass/<LOD Trichloroethylene 25 5 Pass/<LOD
Xylenes* 2,170 50 Pass/<LOD

Total Butanes = 74 ug/g (PASS); Total Pentanes = 0 ug/g (PASS); Total Hexanes = 0 ug/g (PASS)

* Xylenes are reported as the sum of o-xylene, m-xylene, p-xylene, and ethylbenzene
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 8 of 11

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents QC Report

Testing Accreditation #: 4092-004 Test Certificate #: 125191-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Fermented Fruit
License: 030-1009646F7F8
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A401030002C949000000451
Metrc Source Pkg#: 1A401030002C949000000448

Test Conditions

Prepsheet ID#: ORHS200701a
Scale: XS205-OR1
Temp: 21.2 °C
Baro PE: 1009 hPa
Analyst: HRM
Technician: HRM

Sample ID#: 125191

Lot #: Fermented Fruit 7.01.20 #1
Batch #: 125191
Batch Weight (g): 155.1
Harvest/Process Date: 07/01/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 07/01/2020
Test Date: 07/01/2020

Sample #125191
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS Recovery (%) MSD Recovery (%) Relative Percent Difference (%) QC Flag
1,2-Dichloroethane N.D. 0 0 0 nan nan
n-Propane N.D. 250 47 51 18.80 20.40 8.16 LR
Isobutane N.D. 250 77 79 30.80 31.60 2.56 LR
Methanol N.D. 250 119 130 47.60 52.00 8.84 LR
n-Butane N.D. 250 89 89 35.60 35.60 0.00 LR
2,2-Dimethylpropane N.D. 250 104 104 41.60 41.60 0.00 LR
Ethanol N.D. 250 154 160 61.60 64.00 3.82 LR
Isopentane N.D. 250 122 125 48.80 50.00 2.43 LR
Acetonitrile N.D. 250 168 190 67.20 76.00 12.29 LR
Diethyl ether N.D. 250 146 150 58.40 60.00 2.70 LR
2-propanone N.D. 250 151 151 60.40 60.40 0.00 LR
2-propanol N.D. 250 177 184 70.80 73.60 3.88
n-Pentane N.D. 250 101 61 40.40 24.40 49.38 LRQ
2,2-Dimethylbutane N.D. 250 135 136 54.00 54.40 0.74 LR
2,3-Dimethylbutane N.D. 250 134 142 53.60 56.80 5.80 LR
Methylene chloride N.D. 250 163 168 65.20 67.20 3.02 LR
2-Methylpentane N.D. 250 133 140 53.20 56.00 5.13 LR
3-Methylpentane N.D. 250 142 146 56.80 58.40 2.78 LR
2-Butanol N.D. 250 174 179 69.60 71.60 2.83 LR
n-Hexane N.D. 250 140 137 56.00 54.80 2.17 LR
Ethyl acetate N.D. 250 165 172 66.00 68.80 4.15 LR
Tetrahydrofuran N.D. 250 159 165 0.00 0.00 0.00 LR
Trichloroethylene N.D. 0 0 0 nan nan
Isopropyl acetate N.D. 250 167 169 0.00 0.00 0.00 LR
Benzene N.D. 250 181 186 72.40 74.40 2.72
Chloroform N.D. 0 0 0 nan nan
Cyclohexane N.D. 250 154 154 61.60 61.60 0.00 LR
Ethylene glycol N.D. 250 196 218 78.40 87.20 10.63
Heptane N.D. 250 190 174 76.00 69.60 8.79 LR
2-Ethoxyethanol N.D. 250 183 192 73.20 76.80 4.80
1,4-Dioxane N.D. 250 187 198 74.80 79.20 5.71
Pyridine N.D. 0 0 0 0.00 0.00 0.00
Toluene N.D. 250 179 186 71.60 74.40 3.84
Chlorobenzene N.D. 0 0 0 0.00 0.00 0.00
Ethylbenzene N.D. 250 179 185 71.60 74.00 3.30
m-Xylene/p-Xylene N.D. 500 358 368 71.60 73.60 2.75
o-Xylene N.D. 250 181 183 72.40 73.20 1.10
Cumene N.D. 250 190 194 76.00 77.60 2.08
Ethylene oxide N.D. 250 132 132 52.80 52.80 0.00 LR

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

N.D. = Not Detected

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 9 of 11

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Homogeneity Report by
High Performance Liquid Chromatography

Testing Accreditation #: 4092-004 Test Certificate #: 125191-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Fermented Fruit
License: 030-1009646F7F8
Type: AU Tincture
Metrc Test Pkg#: 1A401030002C949000000451
Metrc Source Pkg#: 1A401030002C949000000448

Sample ID#: 125191

Lot #: Fermented Fruit 7.01.20 #1
Batch #: 125191
Batch Weight (g): 155.1
Harvest/Process Date: 07/01/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 07/01/2020

Sample #125191
Increments Tested (mg/g) TOTAL THC TOTAL CBD THC THCA THCV CBD CBC CBDA CBDV CBG CBN
Increment 1 799.66 12.24 49.81 855.02 N.D. N.D. 2.70 13.96 N.D. 3.80 6.81
Increment 2 755.65 13.28 56.08 797.69 N.D. N.D. 3.09 15.14 N.D. 4.03 6.53
Average Value 777.66 12.76 52.95 826.36 N.D. N.D. 2.90 14.55 N.D. 3.92 6.67
Max Value 799.66 13.28 56.08 855.02 N.D. N.D. 3.09 15.14 N.D. 4.03 6.81
Min Value 755.65 12.24 49.81 797.69 N.D. N.D. 2.70 13.96 N.D. 3.80 6.53
Relative Percent Difference (RPD) ±5.66 ±8.11 ±11.84 ±6.94 N.D. N.D. ±13.47 ±8.11 N.D. ±5.87 ±4.20
Average Cannabinoids Per Package 777.66 12.76 52.95 826.36 N.D. N.D. 2.90 14.55 N.D. 3.92 6.67
Average Cannabinoids Per Serving 38.88 0.64 2.65 41.32 N.D. N.D. 0.14 0.73 N.D. 0.20 0.33
Max Concentration Per Serving (THC)   Pass
Max Concentration Per Package (THC)   Pass
Relative Percent Difference (RPD)   Pass
Control Study   Yes, MJ1957
Field Duplicate   Pass

N.D. = Not Detected, Min = Minimum, Max = Maximum

RPD is the relative percent difference between increment 1 and increment 2.

RSD is the relative standard deviation between all increments tested.

Total THC and CBD is the calculated sum of CBD or THC and the amount of CBD or THC derived from CBDA or THCA, respectively. These values are calculated by adding a molar correction factor of 0.877 to the CBDA or THCA value.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

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IRON Laboratories

Terpene Report by
Mass Spectrometer

Test Certificate #: 125191-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Fermented Fruit
License: 030-1009646F7F8
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A401030002C949000000451
Metrc Source Pkg#: 1A401030002C949000000448

Test Conditions

Scale: XS205-OR1
Temp: 21.2 °C
Baro Pressure: 1009 hPa
Analyst: HRM
Technician: HRM

Sample ID#: 125191

Lot #: Fermented Fruit 7.01.20 #1
Batch #: 125191
Batch Weight (g): 155.1
Harvest/Process Date: 07/01/2020
Serving Size (g): 0.05
Date Received: 07/01/2020

Sample #125191
Sample #125191
  • α-Pinene (0.09%)
  • β-Ocimene (0.03%)
  • Camphene (0.03%)
  • Eucalyptol (1,8-Cineol) (0.00%)
  • Sabinene (0.00%)
  • γ-Terpinene (0.00%)
  • Myrcene (0.26%)
  • α-Terpinolene (0.05%)
  • β-Pinene (0.33%)
  • Linalool (0.28%)
  • ∆3-Carene (0.00%)
  • Fenchone (0.00%)
  • α-Terpinene (0.00%)
  • endo-Fenchol (0.00%)
  • α-Ocimene (0.00%)
  • Isopulegol (0.00%)
  • Limonene (0.48%)
  • Geraniol (0.00%)
  • p-Cymene (0.00%)
  • β-Caryophyllene (1.26%)
  • α-Humulene (0.57%)
  • Nerolidol 1 (cis) (0.00%)
  • Nerolidol 2 (trans) (0.07%)
  • Guaiol (0.00%)
  • Caryophyllene Oxide (0.08%)
  • α-Bisabolol (0.08%)
  • α-Phellandrene (0.00%)
  • α-Terpineol (0.42%)
  • Valenence (0.00%)

Total: 4.030%

Predominant Terpenes

1.26%   β-Caryophyllene Sweet, woody, spicy, clove 0.57%   α-Humulene Woody, oceanic-watery, spicy clove
0.48%   Limonene Citrus, orange, sweet 0.42%   α-Terpineol Pine, woody, lemon, lime, citrus, floral
0.33%   β-Pinene Woody, fresh pine, hay 0.28%   Linalool Citrus, floral, sweet, bois de rose, woody, green, blueberry

Value in parenthesis indicates percentage of terpene present in the total sample (weight percentage, wt/wt%).
Value in doughnut slice indicates individual terpene abundance with respect to the total terpenes detected.

This sample has not been tested according to OAR 333-007. These results should therefore be used for research and development or quality control purposes only.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Joseph Rutowski Iron laboratories Joseph Rutowski

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 11 of 11