ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Marijuana Potency Analysis by
High Performance Liquid Chromatography
Testing Accreditation #: 4092-004 Test Certificate #: 125069-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Zherbet Gelato Rope
License: 030-1009646F7F8
Type: AU Tincture
Method: FE04U HPLC-UV
Metrc Test Pkg#: 1A401030002C94900000429
Metrc Source Pkg#: 1A401030002C94900000418
Test Conditions

Prepsheet ID#: ORP200629a
Scale: XS205-OR1
Temp: 21.8 °C
Baro Pressure: 1003 hPa
Analyst: HRM
Technician: TMR
Sample ID#: 125069

Lot #: Zherbet Gelato Rope 6/24/20 #1
Batch #: 125069
Batch Weight (g): 160.5
Harvest/Process Date: 06/24/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 06/25/2020
Test Date: 06/29/2020
Sample #125069
Sample #125069 Sample #125069
Test
Compounds		 THC THCA CBD CBDA CBN CBG CBC THCV* CBDV Total
Cannabinoids*		 Total THC Total CBD Calc Max Total
Cannabinoids*
Amount (%) 4.47 82.76 N/D 2.78 N/D 0.73 0.31 N/D N/D 91.06 77.05 2.44 80.53
Amount (mg/g) 44.66 827.62 N/D 27.83 N/D 7.34 3.10 N/D N/D 910.55 770.48 24.41 805.33
Amount per Serving (mg) 2.23 41.38 N\D 1.39 N\D 0.37 0.16 N\D N\D 45.53 Serving Size~ (g): 0.05
LOQ (mg/g) 1.8 1.8 1.8 1.8 1.8 1.8 1.8 1.8 1.8   %Decarb. THC CBD
±%RPD 2.54 3.60 2.07 1.95 2.83 1.37 1.61 2.90 0.83 5 0

LOQ = Limit of Quantitation; %RPD = Relative Percent Deviation; %RSD = Relative Standard Deviation; N/D = Not Detected

*Designates values that are not currently included in the accredited scope of Iron Laboratories.

*** Designates tests that use the method FE-45. FE-45 is performed using AOAC 966.02 and 32.004-32.009. FE-45 has relative expanded (k=2) uncertainties of 1.098% for moisture, 1.754% for water activity for unprocessed plant materials, and 13.102% for water activity for infused products. Vitamin E acetate analysis has a relative expanded (k=2) uncertainty of 18.614%.

Total THC and CBD is the calculated sum of THC or CBD and the amount of THC or CBD derived from THCA or CBDA, respectively. These values are calculated by applying a molar correction factor of 0.877 to the THCA or the CBDA value. Calc Max Total Cannabinoids is the sum of Total THC, Total CBD, CBN, CBG, CBC, THCV, and CBDV.

%Decarb. THC and CBD refer to the percentage of THC or CBD relative to THCA or CBDA, respectively.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 1 of 11

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant QC Report
Testing Accreditation #: 4092-004 Test Certificate #: 125069-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Zherbet Gelato Rope
License: 030-1009646F7F8
Type: AU Tincture
Method: FE04U HPLC-UV
Metrc Test Pkg#: 1A401030002C94900000429
Metrc Source Pkg#: 1A401030002C94900000418
Test Conditions

Prepsheet ID#: ORP200629a
Scale: XS205-OR1
Temp: 21.8 °C
Baro Pressure: 1003 hPa
Analyst: HRM
Technician: TMR
Sample ID#: 125069

Lot #: Zherbet Gelato Rope 6/24/20 #1
Batch #: 125069
Batch Weight (g): 160.5
Harvest/Process Date: 06/24/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 06/25/2020
Test Date: 06/29/2020
Sample #125069
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Cannabidivarin (CBDV) N.D. 5.97 5.97 100.00 6.02 100.84 0.83
Cannabidiolic Acid (CBDA) N.D. 5.7 5.59 98.07 5.7 100.00 1.95
Cannabigerol (CBG) N.D. 6.02 5.81 96.51 5.89 97.84 1.37
Cannabidiol (CBD) N.D. 5.81 5.73 98.62 5.85 100.69 2.07
Δ9-Tetrahydrocannabivarin (THCV) N.D. 5.68 5.43 95.60 5.59 98.42 2.90
Cannabinol (CBN) N.D. 5.8 5.57 96.03 5.73 98.79 2.83
Δ9-Tetrahydrocannabinol (THC) N.D. 5.73 5.44 94.94 5.58 97.38 2.54
Cannabichromene (CBC) N.D. 6.28 6.15 97.93 6.25 99.52 1.61
Tetrahydrocannabinolic acid (THCA) N.D. 5.75 5.45 94.78 5.65 98.26 3.60

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 2 of 11

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Pesticide Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-004 Test Certificate #: 125069-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Zherbet Gelato Rope
License: 030-1009646F7F8
Type: AU Tincture
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A401030002C94900000429
Metrc Source Pkg#: 1A401030002C94900000418
Test Conditions

Prepsheet ID#: ORPS200626b
Scale: 1129293203
Temp: 20.7 °C
Baro PE: 998.7 hPa
Analyst: HRM/EDT
Technician: HRM/EDT
Sample ID#: 125069

Lot #: Zherbet Gelato Rope 6/24/20 #1
Batch #: 125069
Batch Weight (g): 160.5
Harvest/Process Date: 06/24/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 06/25/2020
Test Date: 06/26/2020
Sample #125069
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
Aldicarb 0.400 0.120 Pass/<LOD Abamectin**** 0.500 0.120 Pass/<LOD
Acephate 0.400 0.120 Pass/<LOD Acequinocyl 2.000 0.240 Pass/<LOD
Acetamiprid 0.200 0.120 Pass/<LOD Azoxystrobin 0.200 0.120 Pass/<LOD
Bifenazate 0.200 0.120 Pass/<LOD Bifenthrin 0.200 0.120 Pass/<LOD
Boscalid 0.400 0.120 Pass/<LOD Carbaryl 0.200 0.120 Pass/<LOD
Carbofuran 0.200 0.120 Pass/<LOD Chlorantraniliprole 0.200 0.120 Pass/<LOD
Chlorfenapyr 1.000 0.480 Pass/<LOD Chlorpyrifos 0.200 0.120 Pass/<LOD
Clofentezine 0.200 0.120 Pass/<LOD Cyfluthrin** 1.000 0.480 Pass/<LOD
Cypermethrin*** 1.000 0.480 Pass/<LOD Daminozide 1.000 0.120 Pass/<LOD
DDVP (Dichlorvos) 1.000 0.240 Pass/<LOD Diazinon 0.200 0.120 Pass/<LOD
Dimethoate 0.200 0.120 Pass/<LOD Ethoprophos 0.200 0.120 Pass/<LOD
Etofenprox 0.400 0.120 Pass/<LOD Etoxazole 0.200 0.120 Pass/<LOD
Fenoxycarb 0.200 0.120 Pass/<LOD Fenpyroximate 0.400 0.120 Pass/<LOD
Fipronil 0.400 0.120 Pass/<LOD Flonicamid 1.000 0.120 Pass/<LOD
Fludioxonil 0.400 0.120 Pass/<LOD Hexythiazox 1.000 0.120 Pass/<LOD
Imazalil 0.200 0.120 Pass/<LOD Imidacloprid 0.400 0.120 Pass/<LOD
Kresoxim Methyl 0.400 0.120 Pass/<LOD Malathion 0.200 0.120 Pass/<LOD
Metalaxyl 0.200 0.120 Pass/<LOD Methiocarb 0.200 0.120 Pass/<LOD
Methomyl 0.400 0.120 Pass/<LOD Methyl Parathion 0.200 0.120 Pass/<LOD
MGK-264‡ 0.200 0.120 Pass/<LOD Myclobutanil 0.000 0.120 Pass/<LOD
Naled 0.500 0.120 Pass/<LOD Oxamyl 1.000 0.120 Pass/<LOD
Paclobutrazol 0.400 0.120 Pass/<LOD Permethrins† 0.200 0.120 Pass/<LOD
Phosmet 0.200 0.120 Pass/<LOD Piperonyl Butoxide 2.000 0.120 Pass/<LOD
Prallethrin 0.200 0.120 Pass/<LOD Propiconazole 0.400 0.120 Pass/<LOD
Propoxur 0.200 0.120 Pass/<LOD Pyrethrins* 1.000 0.120 Pass/<LOD
Pyridaben 0.200 0.120 Pass/<LOD Spinosad***** 0.200 0.120 Pass/<LOD
Spiromesifen 0.200 0.120 Pass/<LOD Spirotetramat 0.200 0.120 Pass/<LOD
Spiroxamine‡ 0.400 0.120 Pass/<LOD Tebuconazole 0.400 0.120 Pass/<LOD
Thiacloprid 0.200 0.120 Pass/<LOD Thiamethoxam 0.200 0.120 Pass/<LOD
Trifloxystrobin 0.200 0.120 Pass/<LOD

* Pyrethrins are reported as the sum of Jasmolin I, Cinerin I, and Pyrethrin I
** Cyfluthrins are reported as the sum of isomers Cyfluthrin I, II, III, and IV
*** Cypermethrins are reported as the sum of isomers Cypermethrin I, II, III, and IV
**** Abamectin is reported as the sum of Avermectin B1a and Avermectin B1b
***** Spinosad is reported as the sum of Spinosyn A and Spinosyn D
† Permethrin and Prallethrin are reported as the sum of cis and trans isomers
‡ MGK-264 and Spiroximine are reported as the sum of isomers I and II
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 2 of 11

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Pesticide QC Report
Testing Accreditation #: 4092-004 Test Certificate #: 125069-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Zherbet Gelato Rope
License: 030-1009646F7F8
Type: AU Tincture
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A401030002C94900000429
Metrc Source Pkg#: 1A401030002C94900000418
Test Conditions

Prepsheet ID#: ORPS200626b
Scale: 1129293203
Temp: 20.7 °C
Baro PE: 998.7 hPa
Analyst: HRM/EDT
Technician: HRM/EDT
Sample ID#: 125069

Lot #: Zherbet Gelato Rope 6/24/20 #1
Batch #: 125069
Batch Weight (g): 160.5
Harvest/Process Date: 06/24/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 06/25/2020
Test Date: 06/26/2020
Sample #125069
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS recovery% MSD recovery% Relative Percent Difference (%) QC Flag
Acephate N.D. 1 0.974 0.952 97.40 95.20 2.28
Acequinocyl N.D. 1 0.26 0.345 26.00 34.50 28.10 LR Q
Acetamiprid N.D. 1 1 0.978 100.00 97.80 2.22
Aldicarb N.D. 1 0.922 0.912 92.20 91.20 1.09
Avermectin B1a N.D. 0.97 1.2 1.06 123.71 109.28 12.39
Azoxystrobin N.D. 1 0.972 0.978 97.20 97.80 0.62
Bifenazate N.D. 1 0.347 0.198 34.70 19.80 54.68 LR Q
Bifenthrin N.D. 1 0.783 0.785 78.30 78.50 0.26
Boscalid N.D. 1 1.05 0.993 105.00 99.30 5.58
Carbaryl N.D. 1 1.03 1.06 103.00 106.00 2.87
Carbofuran N.D. 1 1.07 1.08 107.00 108.00 0.93
Chlorantraniliprole N.D. 1 1.48 1.49 148.00 149.00 0.67 HR
Chlorfenapyr N.D. 1 0.756 0.689 75.60 68.90 9.27 LR
Chlorpyriphos N.D. 1 0.871 0.898 87.10 89.80 3.05
Clofentezine N.D. 1 0.963 1.01 96.30 101.00 4.76
Cyfluthrin N.D. 1 0.964 0.999 96.40 99.90 3.57
Cypermethrin N.D. 1 0.902 0.914 90.20 91.40 1.32
Daminoside N.D. 1 0.732 0.554 73.20 55.40 27.68 LR Q
Diazanon N.D. 1 1.31 1.31 131.00 131.00 0.00 HR
Dichlorvos N.D. 1 0.852 0.858 85.20 85.80 0.70
Dimethoate N.D. 1 0.914 0.872 91.40 87.20 4.70
Ethoprophos N.D. 1 0.852 0.845 85.20 84.50 0.82
Etofenprox N.D. 1 0.718 0.72 71.80 72.00 0.28
Etoxazole N.D. 1 1.05 1.03 105.00 103.00 1.92
Fenoxycarb N.D. 1 1.28 1.3 128.00 130.00 1.55
Fenpyroximate N.D. 1 0.882 0.909 88.20 90.90 3.02
Fipronil N.D. 1 1.05 0.999 105.00 99.90 4.98
Flonicamid N.D. 1 0.945 0.942 94.50 94.20 0.32
Fludioxonil N.D. 1 1.02 0.998 102.00 99.80 2.18
Hexythiazox N.D. 1 0.645 0.681 64.50 68.10 5.43 LR
Imazalil N.D. 1 0.9 1.39 90.00 139.00 42.79 HRQ
Imidacloprid N.D. 1 1.03 1.06 103.00 106.00 2.87
Kresoxim-methyl N.D. 1 1.49 1.54 149.00 154.00 3.30 HR
Malathion N.D. 1 1.18 1.2 118.00 120.00 1.68
Metalaxyl N.D. 1 1.5 1.51 150.00 151.00 0.66 HR
Methiocarb N.D. 1 0.903 0.94 90.30 94.00 4.02
Methomyl N.D. 1 1.19 1.15 119.00 115.00 3.42
MGK-264 N.D. 1 0.885 0.927 88.50 92.70 4.64
Myclobutanil N.D. 1 1.31 1.41 131.00 141.00 7.35 HR
Naled (dibrom) N.D. 1 0.521 0.543 52.10 54.30 4.14 LR
Oxamyl N.D. 1 0.975 0.98 97.50 98.00 0.51
Paclobutrazol N.D. 1 1.66 1.67 166.00 167.00 0.60 HR
Parathion-methyl N.D. 1 0.955 0.94 95.50 94.00 1.58
Permethrins N.D. 1 0.666 0.709 66.60 70.90 6.25
Phosmet N.D. 1 1.19 1.23 119.00 123.00 3.31
Piperonyl butoxide N.D. 1 1.04 1.07 104.00 107.00 2.84
Prallethrin N.D. 1 1.36 1.33 136.00 133.00 2.23 HR
Propiconazole N.D. 1 1.09 1.11 109.00 111.00 1.82
Propoxur N.D. 1 1.16 1.16 116.00 116.00 0.00
Pyrethrin N.D. 0.65 0.673 0.702 103.54 108.00 4.22
Pyridaben N.D. 1 0.786 0.787 78.60 78.70 0.13
SpinosynA N.D. 0.84 1.09 1.08 129.76 128.57 0.92
SpinosynD N.D. 0.16 0.206 0.213 128.75 133.13 3.34 HR
Spiromesifen N.D. 1 0.27 0.269 27.00 26.90 0.37 LR
Spirotetramat N.D. 1 1.22 1.26 122.00 126.00 3.23
Spiroxamine N.D. 1 1.39 1.39 139.00 139.00 0.00 HR
Tebuconazole N.D. 1 1.39 1.48 139.00 148.00 6.27 HR
Thiacloprid N.D. 1 1.03 1.03 103.00 103.00 0.00
Thiamethoxam N.D. 1 1.49 1.44 149.00 144.00 3.41 HR
Trifloxystrobin N.D. 1 0.971 0.97 97.10 97.00 0.10

N.D. = Not Detected

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 30%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (60-120%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 3 of 11

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Pesticide Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-004 Test Certificate #: 125069-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Zherbet Gelato Rope
License: 030-1009646F7F8
Type: AU Tincture
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A401030002C94900000429
Metrc Source Pkg#: 1A401030002C94900000418
Test Conditions

Prepsheet ID#: ORPS200626b
Scale: 1129293203
Temp: 20.7 °C
Baro PE: 998.7 hPa
Analyst: HRM/EDT
Technician: HRM/EDT
Sample ID#: 125069

Lot #: Zherbet Gelato Rope 6/24/20 #1
Batch #: 125069
Batch Weight (g): 160.5
Harvest/Process Date: 06/24/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 06/25/2020
Test Date: 06/26/2020
Sample #125069
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
Aldicarb 0.400 0.123 Pass/<LOD Abamectin**** 0.500 0.123 Pass/<LOD
Acephate 0.400 0.123 Pass/<LOD Acequinocyl 2.000 0.246 Pass/<LOD
Acetamiprid 0.200 0.123 Pass/<LOD Azoxystrobin 0.200 0.123 Pass/<LOD
Bifenazate 0.200 0.123 Pass/<LOD Bifenthrin 0.200 0.123 Pass/<LOD
Boscalid 0.400 0.123 Pass/<LOD Carbaryl 0.200 0.123 Pass/<LOD
Carbofuran 0.200 0.123 Pass/<LOD Chlorantraniliprole 0.200 0.123 Pass/<LOD
Chlorfenapyr 1.000 0.492 Pass/<LOD Chlorpyrifos 0.200 0.123 Pass/<LOD
Clofentezine 0.200 0.123 Pass/<LOD Cyfluthrin** 1.000 0.492 Pass/<LOD
Cypermethrin*** 1.000 0.492 Pass/<LOD Daminozide 1.000 0.123 Pass/<LOD
DDVP (Dichlorvos) 1.000 0.246 Pass/<LOD Diazinon 0.200 0.123 Pass/<LOD
Dimethoate 0.200 0.123 Pass/<LOD Ethoprophos 0.200 0.123 Pass/<LOD
Etofenprox 0.400 0.123 Pass/<LOD Etoxazole 0.200 0.123 Pass/<LOD
Fenoxycarb 0.200 0.123 Pass/<LOD Fenpyroximate 0.400 0.123 Pass/<LOD
Fipronil 0.400 0.123 Pass/<LOD Flonicamid 1.000 0.123 Pass/<LOD
Fludioxonil 0.400 0.123 Pass/<LOD Hexythiazox 1.000 0.123 Pass/<LOD
Imazalil 0.200 0.123 Pass/<LOD Imidacloprid 0.400 0.123 Pass/<LOD
Kresoxim Methyl 0.400 0.123 Pass/<LOD Malathion 0.200 0.123 Pass/<LOD
Metalaxyl 0.200 0.123 Pass/<LOD Methiocarb 0.200 0.123 Pass/<LOD
Methomyl 0.400 0.123 Pass/<LOD Methyl Parathion 0.200 0.123 Pass/<LOD
MGK-264‡ 0.200 0.123 Pass/<LOD Myclobutanil 0.000 0.123 Pass/<LOD
Naled 0.500 0.123 Pass/<LOD Oxamyl 1.000 0.123 Pass/<LOD
Paclobutrazol 0.400 0.123 Pass/<LOD Permethrins† 0.200 0.123 Pass/<LOD
Phosmet 0.200 0.123 Pass/<LOD Piperonyl Butoxide 2.000 0.123 Pass/<LOD
Prallethrin 0.200 0.123 Pass/<LOD Propiconazole 0.400 0.123 Pass/<LOD
Propoxur 0.200 0.123 Pass/<LOD Pyrethrins* 1.000 0.123 Pass/<LOD
Pyridaben 0.200 0.123 Pass/<LOD Spinosad***** 0.200 0.123 Pass/<LOD
Spiromesifen 0.200 0.123 Pass/<LOD Spirotetramat 0.200 0.123 Pass/<LOD
Spiroxamine‡ 0.400 0.123 Pass/<LOD Tebuconazole 0.400 0.123 Pass/<LOD
Thiacloprid 0.200 0.123 Pass/<LOD Thiamethoxam 0.200 0.123 Pass/<LOD
Trifloxystrobin 0.200 0.123 Pass/<LOD

* Pyrethrins are reported as the sum of Jasmolin I, Cinerin I, and Pyrethrin I
** Cyfluthrins are reported as the sum of isomers Cyfluthrin I, II, III, and IV
*** Cypermethrins are reported as the sum of isomers Cypermethrin I, II, III, and IV
**** Abamectin is reported as the sum of Avermectin B1a and Avermectin B1b
***** Spinosad is reported as the sum of Spinosyn A and Spinosyn D
† Permethrin and Prallethrin are reported as the sum of cis and trans isomers
‡ MGK-264 and Spiroximine are reported as the sum of isomers I and II
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 4 of 11

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Pesticide QC Report
Testing Accreditation #: 4092-004 Test Certificate #: 125069-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Zherbet Gelato Rope
License: 030-1009646F7F8
Type: AU Tincture
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A401030002C94900000429
Metrc Source Pkg#: 1A401030002C94900000418
Test Conditions

Prepsheet ID#: ORPS200626b
Scale: 1129293203
Temp: 20.7 °C
Baro PE: 998.7 hPa
Analyst: HRM/EDT
Technician: HRM/EDT
Sample ID#: 125069

Lot #: Zherbet Gelato Rope 6/24/20 #1
Batch #: 125069
Batch Weight (g): 160.5
Harvest/Process Date: 06/24/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 06/25/2020
Test Date: 06/26/2020
Sample #125069
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS recovery% MSD recovery% Relative Percent Difference (%) QC Flag
Acephate N.D. 1 0.974 0.952 97.40 95.20 2.28
Acequinocyl N.D. 1 0.26 0.345 26.00 34.50 28.10 LR Q
Acetamiprid N.D. 1 1 0.978 100.00 97.80 2.22
Aldicarb N.D. 1 0.922 0.912 92.20 91.20 1.09
Avermectin B1a N.D. 0.97 1.2 1.06 123.71 109.28 12.39
Azoxystrobin N.D. 1 0.972 0.978 97.20 97.80 0.62
Bifenazate N.D. 1 0.347 0.198 34.70 19.80 54.68 LR Q
Bifenthrin N.D. 1 0.783 0.785 78.30 78.50 0.26
Boscalid N.D. 1 1.05 0.993 105.00 99.30 5.58
Carbaryl N.D. 1 1.03 1.06 103.00 106.00 2.87
Carbofuran N.D. 1 1.07 1.08 107.00 108.00 0.93
Chlorantraniliprole N.D. 1 1.48 1.49 148.00 149.00 0.67 HR
Chlorfenapyr N.D. 1 0.756 0.689 75.60 68.90 9.27 LR
Chlorpyriphos N.D. 1 0.871 0.898 87.10 89.80 3.05
Clofentezine N.D. 1 0.963 1.01 96.30 101.00 4.76
Cyfluthrin N.D. 1 0.964 0.999 96.40 99.90 3.57
Cypermethrin N.D. 1 0.902 0.914 90.20 91.40 1.32
Daminoside N.D. 1 0.732 0.554 73.20 55.40 27.68 LR Q
Diazanon N.D. 1 1.31 1.31 131.00 131.00 0.00 HR
Dichlorvos N.D. 1 0.852 0.858 85.20 85.80 0.70
Dimethoate N.D. 1 0.914 0.872 91.40 87.20 4.70
Ethoprophos N.D. 1 0.852 0.845 85.20 84.50 0.82
Etofenprox N.D. 1 0.718 0.72 71.80 72.00 0.28
Etoxazole N.D. 1 1.05 1.03 105.00 103.00 1.92
Fenoxycarb N.D. 1 1.28 1.3 128.00 130.00 1.55
Fenpyroximate N.D. 1 0.882 0.909 88.20 90.90 3.02
Fipronil N.D. 1 1.05 0.999 105.00 99.90 4.98
Flonicamid N.D. 1 0.945 0.942 94.50 94.20 0.32
Fludioxonil N.D. 1 1.02 0.998 102.00 99.80 2.18
Hexythiazox N.D. 1 0.645 0.681 64.50 68.10 5.43 LR
Imazalil N.D. 1 0.9 1.39 90.00 139.00 42.79 HRQ
Imidacloprid N.D. 1 1.03 1.06 103.00 106.00 2.87
Kresoxim-methyl N.D. 1 1.49 1.54 149.00 154.00 3.30 HR
Malathion N.D. 1 1.18 1.2 118.00 120.00 1.68
Metalaxyl N.D. 1 1.5 1.51 150.00 151.00 0.66 HR
Methiocarb N.D. 1 0.903 0.94 90.30 94.00 4.02
Methomyl N.D. 1 1.19 1.15 119.00 115.00 3.42
MGK-264 N.D. 1 0.885 0.927 88.50 92.70 4.64
Myclobutanil N.D. 1 1.31 1.41 131.00 141.00 7.35 HR
Naled (dibrom) N.D. 1 0.521 0.543 52.10 54.30 4.14 LR
Oxamyl N.D. 1 0.975 0.98 97.50 98.00 0.51
Paclobutrazol N.D. 1 1.66 1.67 166.00 167.00 0.60 HR
Parathion-methyl N.D. 1 0.955 0.94 95.50 94.00 1.58
Permethrins N.D. 1 0.666 0.709 66.60 70.90 6.25
Phosmet N.D. 1 1.19 1.23 119.00 123.00 3.31
Piperonyl butoxide N.D. 1 1.04 1.07 104.00 107.00 2.84
Prallethrin N.D. 1 1.36 1.33 136.00 133.00 2.23 HR
Propiconazole N.D. 1 1.09 1.11 109.00 111.00 1.82
Propoxur N.D. 1 1.16 1.16 116.00 116.00 0.00
Pyrethrin N.D. 0.65 0.673 0.702 103.54 108.00 4.22
Pyridaben N.D. 1 0.786 0.787 78.60 78.70 0.13
SpinosynA N.D. 0.84 1.09 1.08 129.76 128.57 0.92
SpinosynD N.D. 0.16 0.206 0.213 128.75 133.13 3.34 HR
Spiromesifen N.D. 1 0.27 0.269 27.00 26.90 0.37 LR
Spirotetramat N.D. 1 1.22 1.26 122.00 126.00 3.23
Spiroxamine N.D. 1 1.39 1.39 139.00 139.00 0.00 HR
Tebuconazole N.D. 1 1.39 1.48 139.00 148.00 6.27 HR
Thiacloprid N.D. 1 1.03 1.03 103.00 103.00 0.00
Thiamethoxam N.D. 1 1.49 1.44 149.00 144.00 3.41 HR
Trifloxystrobin N.D. 1 0.971 0.97 97.10 97.00 0.10

N.D. = Not Detected

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 30%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (60-120%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 5 of 11

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-004 Test Certificate #: 125069-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Zherbet Gelato Rope
License: 030-1009646F7F8
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A401030002C94900000429
Metrc Source Pkg#: 1A401030002C94900000418
Test Conditions

Prepsheet ID#: ORHS200629a
Scale: XS205-OR1
Temp: 22.1 °C
Baro PE: 1012 hPa
Analyst: HRM
Technician: HRM
Sample ID#: 125069

Lot #: Zherbet Gelato Rope 6/24/20 #1
Batch #: 125069
Batch Weight (g): 160.5
Harvest/Process Date: 06/24/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 06/25/2020
Test Date: 06/29/2020
Sample #125069
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
1,2-Dichloroethane 2 1 Pass/<LOD 1,2-Dimethoxyethane 100 5 Pass/<LOD
1,4-dioxane 380 200 Pass/<LOD 1-Butanol 5,000 100 Pass/<LOD
1-Pentanol 5,000 100 Pass/<LOD 1-Propanol 5,000 100 Pass/<LOD
2,2-Dimethylpropane (Neopentane) 5,000 100 Pass/<LOD 2,2-Dimethylbutane (Hexanes) 290 100 Pass/<LOD
2,3-Dimethylbutane (Hexanes) 290 100 Pass/<LOD 2-Butanol 5,000 100 Pass/<LOD
2-Butanone (MEK) 5,000 50 Pass/<LOD 2-Ethoxyethanol 160 40 Pass/<LOD
2-Methylbutane (Isopentane) 5,000 50 Pass/<LOD 2-Methylpentane (Hexanes) 290 50 Pass/<LOD
2-Methylpropane (Isobutane) 5,000 100 Pass/<LOD 2-propanol (Isopropyl Alcohol) 5,000 50 Pass/180
2-Propanone (Acetone) 5,000 50 Pass/<LOD 3-Methylpentane (Hexanes) 290 50 Pass/<LOD
Acetonitrile 410 100 Pass/<LOD Benzene 2 1 Pass/<LOD
Butane 5,000 100 Pass/318 Chloroform 2 1 Pass/<LOD
Cumene 70 50 Pass/<LOD Cyclohexane 3,880 1,000 Pass/<LOD
Dichloromethane 600 50 Pass/<LOD Dimethylsulfoxide (DMSO) 5,000 500 Pass/<LOD
Ethanol 5,000 500 Pass/<LOD Ethyl acetate 5,000 50 Pass/<LOD
Ethyl ether 5,000 500 Pass/<LOD Ethylene glycol 620 310 Pass/<LOD
Ethylene oxide 50 50 Pass/<LOD Heptane 5,000 50 Pass/<LOD
Hexane 290 290 Pass/<LOD Isopropyl acetate 5,000 50 Pass/<LOD
Methanol 3,000 500 Pass/<LOD Naptha 400 100 Pass/<LOD
N,N-Dimethylacetamide 1,090 100 Pass/<LOD N,N-Dimethylformamide (DMF) 880 500 Pass/<LOD
Pentane 5,000 50 Pass/<LOD Petroleum Ether 400 100 Pass/<LOD
Propane 5,000 100 Pass/<LOD Pyridine 200 10 Pass/<LOD
Sulfolane 160 200 Pass/<LOD Tetrahydrofuran (THF) 720 200 Pass/<LOD
Toluene 890 50 Pass/<LOD Trichloroethylene 25 5 Pass/<LOD
Xylenes* 2,170 50 Pass/<LOD

Total Butanes = 318 ug/g (PASS); Total Pentanes = 0 ug/g (PASS); Total Hexanes = 0 ug/g (PASS)

* Xylenes are reported as the sum of o-xylene, m-xylene, p-xylene, and ethylbenzene
MRL - Maximum Residue Limit; LOD - Limit of Detection

This sample has not been tested according to OAR 333-007. These results should therefore be used for research and development or quality control purposes only.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 6 of 11

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents QC Report
Testing Accreditation #: 4092-004 Test Certificate #: 125069-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Zherbet Gelato Rope
License: 030-1009646F7F8
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A401030002C94900000429
Metrc Source Pkg#: 1A401030002C94900000418
Test Conditions

Prepsheet ID#: ORHS200629a
Scale: XS205-OR1
Temp: 22.1 °C
Baro PE: 1012 hPa
Analyst: HRM
Technician: HRM
Sample ID#: 125069

Lot #: Zherbet Gelato Rope 6/24/20 #1
Batch #: 125069
Batch Weight (g): 160.5
Harvest/Process Date: 06/24/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 06/25/2020
Test Date: 06/29/2020
Sample #125069
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS Recovery (%) MSD Recovery (%) Relative Percent Difference (%) QC Flag
1,2-Dichloroethane N.D. 0 0 0 nan nan
n-Propane N.D. 250 69 56 27.60 22.40 20.80 LR
Isobutane N.D. 250 106 88 42.40 35.20 18.56 LR
Methanol N.D. 250 102 55 40.80 22.00 59.87 LRQ
n-Butane N.D. 250 117 95 46.80 38.00 20.75 LRQ
2,2-Dimethylpropane N.D. 250 135 119 54.00 47.60 12.60 LR
Ethanol N.D. 250 183 157 73.20 62.80 15.29 LR
Isopentane N.D. 250 153 130 61.20 52.00 16.25 LR
Acetonitrile N.D. 250 155 137 62.00 54.80 12.33 LR
Diethyl ether N.D. 250 162 138 64.80 55.20 16.00 LR
2-propanone N.D. 250 187 167 74.80 66.80 11.30 LR
2-propanol N.D. 250 201 179 80.40 71.60 11.58
n-Pentane N.D. 250 44 0 17.60 0.00 200.00 LRQ
2,2-Dimethylbutane N.D. 250 163 143 65.20 57.20 13.07 LR
2,3-Dimethylbutane N.D. 250 168 131 67.20 52.40 24.75 LRQ
Methylene chloride N.D. 250 180 160 72.00 64.00 11.76 LR
2-Methylpentane N.D. 250 164 151 65.60 60.40 8.25 LR
3-Methylpentane N.D. 250 167 152 66.80 60.80 9.40 LR
2-Butanol N.D. 250 198 186 79.20 74.40 6.25
n-Hexane N.D. 250 155 140 62.00 56.00 10.17 LR
Ethyl acetate N.D. 250 181 167 72.40 66.80 8.05 LR
Tetrahydrofuran N.D. 250 188 170 0.00 0.00 0.00 LR
Trichloroethylene N.D. 0 0 0 nan nan
Isopropyl acetate N.D. 250 191 185 0.00 0.00 0.00
Benzene N.D. 250 204 194 81.60 77.60 5.03
Chloroform N.D. 0 0 0 nan nan
Cyclohexane N.D. 250 180 166 72.00 66.40 8.09 LR
Ethylene glycol N.D. 250 208 203 83.20 81.20 2.43
Heptane N.D. 250 180 164 72.00 65.60 9.30 LR
2-Ethoxyethanol N.D. 250 189 205 75.60 82.00 8.12
1,4-Dioxane N.D. 250 213 210 85.20 84.00 1.42
Pyridine N.D. 0 0 0 0.00 0.00 0.00
Toluene N.D. 250 199 203 79.60 81.20 1.99
Chlorobenzene N.D. 0 0 0 0.00 0.00 0.00
Ethylbenzene N.D. 250 204 213 81.60 85.20 4.32
m-Xylene/p-Xylene N.D. 500 408 426 81.60 85.20 4.32
o-Xylene N.D. 250 204 215 81.60 86.00 5.25
Cumene N.D. 250 217 230 86.80 92.00 5.82
Ethylene oxide N.D. 250 144 111 57.60 44.40 25.88 LRQ

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

N.D. = Not Detected

This sample has not been tested according to OAR 333-007. These results should therefore be used for research and development or quality control purposes only.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 7 of 11

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-004 Test Certificate #: 125069-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Zherbet Gelato Rope
License: 030-1009646F7F8
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A401030002C94900000429
Metrc Source Pkg#: 1A401030002C94900000418
Test Conditions

Prepsheet ID#: ORHS200629a
Scale: XS205-OR1
Temp: 22.1 °C
Baro PE: 1012 hPa
Analyst: HRM
Technician: HRM
Sample ID#: 125069

Lot #: Zherbet Gelato Rope 6/24/20 #1
Batch #: 125069
Batch Weight (g): 160.5
Harvest/Process Date: 06/24/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 06/25/2020
Test Date: 06/29/2020
Sample #125069
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
1,2-Dichloroethane 2 1 Pass/<LOD 1,2-Dimethoxyethane 100 5 Pass/<LOD
1,4-dioxane 380 200 Pass/<LOD 1-Butanol 5,000 100 Pass/<LOD
1-Pentanol 5,000 100 Pass/<LOD 1-Propanol 5,000 100 Pass/<LOD
2,2-Dimethylpropane (Neopentane) 5,000 100 Pass/<LOD 2,2-Dimethylbutane (Hexanes) 290 100 Pass/<LOD
2,3-Dimethylbutane (Hexanes) 290 100 Pass/<LOD 2-Butanol 5,000 100 Pass/<LOD
2-Butanone (MEK) 5,000 50 Pass/<LOD 2-Ethoxyethanol 160 40 Pass/<LOD
2-Methylbutane (Isopentane) 5,000 50 Pass/<LOD 2-Methylpentane (Hexanes) 290 50 Pass/<LOD
2-Methylpropane (Isobutane) 5,000 100 Pass/<LOD 2-propanol (Isopropyl Alcohol) 5,000 50 Pass/142
2-Propanone (Acetone) 5,000 50 Pass/<LOD 3-Methylpentane (Hexanes) 290 50 Pass/<LOD
Acetonitrile 410 100 Pass/<LOD Benzene 2 1 Pass/<LOD
Butane 5,000 100 Pass/186 Chloroform 2 1 Pass/<LOD
Cumene 70 50 Pass/<LOD Cyclohexane 3,880 1,000 Pass/<LOD
Dichloromethane 600 50 Pass/<LOD Dimethylsulfoxide (DMSO) 5,000 500 Pass/<LOD
Ethanol 5,000 500 Pass/<LOD Ethyl acetate 5,000 50 Pass/<LOD
Ethyl ether 5,000 500 Pass/<LOD Ethylene glycol 620 310 Pass/<LOD
Ethylene oxide 50 50 Pass/<LOD Heptane 5,000 50 Pass/<LOD
Hexane 290 290 Pass/<LOD Isopropyl acetate 5,000 50 Pass/<LOD
Methanol 3,000 500 Pass/<LOD Naptha 400 100 Pass/<LOD
N,N-Dimethylacetamide 1,090 100 Pass/<LOD N,N-Dimethylformamide (DMF) 880 500 Pass/<LOD
Pentane 5,000 50 Pass/<LOD Petroleum Ether 400 100 Pass/<LOD
Propane 5,000 100 Pass/<LOD Pyridine 200 10 Pass/<LOD
Sulfolane 160 200 Pass/<LOD Tetrahydrofuran (THF) 720 200 Pass/<LOD
Toluene 890 50 Pass/<LOD Trichloroethylene 25 5 Pass/<LOD
Xylenes* 2,170 50 Pass/<LOD

Total Butanes = 186 ug/g (PASS); Total Pentanes = 0 ug/g (PASS); Total Hexanes = 0 ug/g (PASS)

* Xylenes are reported as the sum of o-xylene, m-xylene, p-xylene, and ethylbenzene
MRL - Maximum Residue Limit; LOD - Limit of Detection

This sample has not been tested according to OAR 333-007. These results should therefore be used for research and development or quality control purposes only.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 8 of 11

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents QC Report
Testing Accreditation #: 4092-004 Test Certificate #: 125069-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Zherbet Gelato Rope
License: 030-1009646F7F8
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A401030002C94900000429
Metrc Source Pkg#: 1A401030002C94900000418
Test Conditions

Prepsheet ID#: ORHS200629a
Scale: XS205-OR1
Temp: 22.1 °C
Baro PE: 1012 hPa
Analyst: HRM
Technician: HRM
Sample ID#: 125069

Lot #: Zherbet Gelato Rope 6/24/20 #1
Batch #: 125069
Batch Weight (g): 160.5
Harvest/Process Date: 06/24/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 06/25/2020
Test Date: 06/29/2020
Sample #125069
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS Recovery (%) MSD Recovery (%) Relative Percent Difference (%) QC Flag
1,2-Dichloroethane N.D. 0 0 0 nan nan
n-Propane N.D. 250 69 56 27.60 22.40 20.80 LR
Isobutane N.D. 250 106 88 42.40 35.20 18.56 LR
Methanol N.D. 250 102 55 40.80 22.00 59.87 LRQ
n-Butane N.D. 250 117 95 46.80 38.00 20.75 LRQ
2,2-Dimethylpropane N.D. 250 135 119 54.00 47.60 12.60 LR
Ethanol N.D. 250 183 157 73.20 62.80 15.29 LR
Isopentane N.D. 250 153 130 61.20 52.00 16.25 LR
Acetonitrile N.D. 250 155 137 62.00 54.80 12.33 LR
Diethyl ether N.D. 250 162 138 64.80 55.20 16.00 LR
2-propanone N.D. 250 187 167 74.80 66.80 11.30 LR
2-propanol N.D. 250 201 179 80.40 71.60 11.58
n-Pentane N.D. 250 44 0 17.60 0.00 200.00 LRQ
2,2-Dimethylbutane N.D. 250 163 143 65.20 57.20 13.07 LR
2,3-Dimethylbutane N.D. 250 168 131 67.20 52.40 24.75 LRQ
Methylene chloride N.D. 250 180 160 72.00 64.00 11.76 LR
2-Methylpentane N.D. 250 164 151 65.60 60.40 8.25 LR
3-Methylpentane N.D. 250 167 152 66.80 60.80 9.40 LR
2-Butanol N.D. 250 198 186 79.20 74.40 6.25
n-Hexane N.D. 250 155 140 62.00 56.00 10.17 LR
Ethyl acetate N.D. 250 181 167 72.40 66.80 8.05 LR
Tetrahydrofuran N.D. 250 188 170 0.00 0.00 0.00 LR
Trichloroethylene N.D. 0 0 0 nan nan
Isopropyl acetate N.D. 250 191 185 0.00 0.00 0.00
Benzene N.D. 250 204 194 81.60 77.60 5.03
Chloroform N.D. 0 0 0 nan nan
Cyclohexane N.D. 250 180 166 72.00 66.40 8.09 LR
Ethylene glycol N.D. 250 208 203 83.20 81.20 2.43
Heptane N.D. 250 180 164 72.00 65.60 9.30 LR
2-Ethoxyethanol N.D. 250 189 205 75.60 82.00 8.12
1,4-Dioxane N.D. 250 213 210 85.20 84.00 1.42
Pyridine N.D. 0 0 0 0.00 0.00 0.00
Toluene N.D. 250 199 203 79.60 81.20 1.99
Chlorobenzene N.D. 0 0 0 0.00 0.00 0.00
Ethylbenzene N.D. 250 204 213 81.60 85.20 4.32
m-Xylene/p-Xylene N.D. 500 408 426 81.60 85.20 4.32
o-Xylene N.D. 250 204 215 81.60 86.00 5.25
Cumene N.D. 250 217 230 86.80 92.00 5.82
Ethylene oxide N.D. 250 144 111 57.60 44.40 25.88 LRQ

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

N.D. = Not Detected

This sample has not been tested according to OAR 333-007. These results should therefore be used for research and development or quality control purposes only.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 9 of 11

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Homogeneity Report by
High Performance Liquid Chromatography
Testing Accreditation #: 4092-004 Test Certificate #: 125069-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Zherbet Gelato Rope
License: 030-1009646F7F8
Type: AU Tincture
Metrc Test Pkg#: 1A401030002C94900000429
Metrc Source Pkg#: 1A401030002C94900000418
Sample ID#: 125069

Lot #: Zherbet Gelato Rope 6/24/20 #1
Batch #: 125069
Batch Weight (g): 160.5
Harvest/Process Date: 06/24/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 06/25/2020
Sample #125069
Increments Tested (mg/g) TOTAL THC TOTAL CBD THC THCA THCV CBD CBC CBDA CBDV CBG CBN
Increment 1 775.32 24.71 45.06 832.68 N.D. N.D. 3.11 28.17 N.D. 7.46 N.D.
Increment 2 765.65 24.11 44.27 822.55 N.D. N.D. 3.09 27.49 N.D. 7.22 N.D.
Average Value 770.48 24.41 44.67 827.62 N.D. N.D. 3.10 27.83 N.D. 7.34 N.D.
Max Value 775.32 24.71 45.06 832.68 N.D. N.D. 3.11 28.17 N.D. 7.46 N.D.
Min Value 765.65 24.11 44.27 822.55 N.D. N.D. 3.09 27.49 N.D. 7.22 N.D.
Relative Percent Difference (RPD) ±1.26 ±2.44 ±1.77 ±1.22 N.D. N.D. ±0.65 ±2.44 N.D. ±3.27 N.D.
Average Cannabinoids Per Package 770.48 24.41 44.67 827.62 N.D. N.D. 3.10 27.83 N.D. 7.34 N.D.
Average Cannabinoids Per Serving 38.52 1.22 2.23 41.38 N.D. N.D. 0.16 1.39 N.D. 0.37 N.D.
Max Concentration Per Serving (THC)   Pass
Max Concentration Per Package (THC)   Pass
Relative Percent Difference (RPD)   Pass
Control Study   Yes, MJ1957
Field Duplicate   Pass

N.D. = Not Detected, Min = Minimum, Max = Maximum

RPD is the relative percent difference between increment 1 and increment 2.

RSD is the relative standard deviation between all increments tested.

Total THC and CBD is the calculated sum of CBD or THC and the amount of CBD or THC derived from CBDA or THCA, respectively. These values are calculated by adding a molar correction factor of 0.877 to the CBDA or THCA value.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

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IRON Laboratories

Terpene Report by
Mass Spectrometer
Test Certificate #: 125069-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Zherbet Gelato Rope
License: 030-1009646F7F8
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A401030002C94900000429
Metrc Source Pkg#: 1A401030002C94900000418

Test Conditions

Scale: XS205-OR1
Temp: 22.1 °C
Baro Pressure: 1012 hPa
Analyst: HRM
Technician: HRM

Sample ID#: 125069

Lot #: Zherbet Gelato Rope 6/24/20 #1
Batch #: 125069
Batch Weight (g): 160.5
Harvest/Process Date: 06/24/2020
Serving Size (g): 0.05
Date Received: 06/25/2020

Sample #125069
Sample #125069
  • α-Pinene (0.24%)
  • β-Ocimene (0.10%)
  • Camphene (0.05%)
  • Eucalyptol (1,8-Cineol) (0.00%)
  • Sabinene (0.00%)
  • γ-Terpinene (0.03%)
  • Myrcene (0.21%)
  • α-Terpinolene (0.10%)
  • β-Pinene (0.29%)
  • Linalool (0.27%)
  • ∆3-Carene (0.00%)
  • Fenchone (0.00%)
  • α-Terpinene (0.03%)
  • endo-Fenchol (0.00%)
  • α-Ocimene (0.00%)
  • Isopulegol (0.00%)
  • Limonene (0.55%)
  • Geraniol (0.00%)
  • p-Cymene (0.00%)
  • β-Caryophyllene (1.66%)
  • α-Humulene (0.67%)
  • Nerolidol 1 (cis) (0.00%)
  • Nerolidol 2 (trans) (0.02%)
  • Guaiol (0.00%)
  • Caryophyllene Oxide (0.00%)
  • α-Bisabolol (0.09%)
  • α-Phellandrene (0.00%)
  • α-Terpineol (0.36%)
  • Valenence (0.00%)

Total: 4.670%

Predominant Terpenes

1.66%   β-Caryophyllene Sweet, woody, spicy, clove 0.67%   α-Humulene Woody, oceanic-watery, spicy clove
0.55%   Limonene Citrus, orange, sweet 0.36%   α-Terpineol Pine, woody, lemon, lime, citrus, floral
0.29%   β-Pinene Woody, fresh pine, hay 0.27%   Linalool Citrus, floral, sweet, bois de rose, woody, green, blueberry

Value in parenthesis indicates percentage of terpene present in the total sample (weight percentage, wt/wt%).
Value in doughnut slice indicates individual terpene abundance with respect to the total terpenes detected.

This sample has not been tested according to OAR 333-007. These results should therefore be used for research and development or quality control purposes only.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 11 of 11