IRON LaboratoriesPJLA

ISO/IEC 17025:2005 Accredited

Marihuana Potency Analysis by
High Performance Liquid Chromatography
Testing Accreditation #: 77802 Test Certificate #: 125047-001
Client Name, Sample Details

Kelly Young
Central Lake, MI 49622
Sample: Cartridge
Type: Concentrate
Method: FE04U HPLC-UV
Test Conditions

Prepsheet ID#: MIP200625
Scale: XS205-MI2
Temp: 22 °C
Baro Pressure: 972.4 hPa
Analyst: KEB
Technician: ANJ
Sample ID#: 125047

Harvest/Process Date: 06/25/2020
Serving Size (g): 1
Date Received: 06/25/2020
Test Date: 06/25/2020
Valid Through: 06/26/2021
Report Issued: 06/26/2020
Sample #125047
Sample #125047 Sample #125047
Test
Compounds		 THC THCA CBD CBDA CBN CBG* CBC* THCV* CBDV* Total
Cannabinoids*		 Total THC Total CBD Calc Max Total
Cannabinoids*
Amount (%) 63.3 N/D N/D N/D N/D 0.9 1.0 N/D N/D 65.1 63.3 0.0 65.1
Amount (mg/g) 632.5 N/D N/D N/D N/D 8.9 9.8 N/D N/D 651.2 632.5 0.0 651.2
Amount per Serving (mg) 632.5 N\D N\D N\D N\D 8.9 9.8 N\D N\D 651.2 Serving Size~ (g): 1.0
LOQ (mg/g) 2.88 2.88 2.88 2.88 2.88 2.88 2.88 2.88 2.88   %Decarb. THC CBD
±%RPD 3.07 3.09 1.49 2.47 3.76 0.70 1.49 0.50 2.16 100% N/A

Sample tested for potency and vitamin E acetate. Sample does not contain vitamin E acetate over 100 ug/g (PASS).

LOQ = Limit of Quantitation; %RPD = Relative Percent Deviation; %RSD = Relative Standard Deviation; N/D = Not Detected

*Designates values that are not currently included in the accredited scope of Iron Laboratories.

*** Designates tests that use the method FE-45. FE-45 is performed using AOAC 966.02 and 32.004-32.009. FE-45 has relative expanded (k=2) uncertainties of 1.098% for moisture, 1.754% for water activity for unprocessed plant materials, and 13.102% for water activity for infused products. Vitamin E acetate analysis has a relative expanded (k=2) uncertainty of 18.614%.

Total THC and CBD is the calculated sum of THC or CBD and the amount of THC or CBD derived from THCA or CBDA, respectively. These values are calculated by applying a molar correction factor of 0.877 to the THCA or the CBDA value. Calc Max Total Cannabinoids is the sum of Total THC, Total CBD, CBN, CBG, CBC, THCV, and CBDV.

%Decarb. THC and CBD refer to the percentage of THC or CBD relative to THCA or CBDA, respectively.

This sample has not undergone random sampling and has not been tested for compliant state, batch representative testing. These results should therefore be used for research and development or quality control purposes only. Results apply to the sample as received.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
KEB - LM Iron laboratories KEB - LM

Iron Laboratories, LLC is an ISO/IEC 17025:2005 Testing Laboratory laboratory, accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 1 of 6

IRON LaboratoriesPJLA

ISO/IEC 17025:2005 Accredited

QC Report
Testing Accreditation #: 77802 Test Certificate #: 125047-001
Client Name, Sample Details

Kelly Young
Central Lake, MI 49622
Sample: Cartridge
Type: Concentrate
Method: FE04U HPLC-UV
Test Conditions

Prepsheet ID#: MIP200625
Scale: XS205-MI2
Temp: 22 °C
Baro Pressure: 972.4 hPa
Analyst: KEB
Technician: ANJ
Sample ID#: 125047

Harvest/Process Date: 06/25/2020
Serving Size (g): 1
Date Received: 06/25/2020
Test Date: 06/25/2020
Valid Through: 06/26/2021
Report Issued: 06/26/2020
Sample #125047
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Cannabidivarin (CBDV) 0 5.91368 6.05725 102.43 6.18955 104.66 2.16
Cannabidiolic Acid (CBDA) 0 5.43127 5.49698 101.21 5.63442 103.74 2.47
Cannabigerol (CBG) 0 5.85366 5.96031 101.82 6.00212 102.54 0.70
Cannabidiol (CBD) 0 5.76012 5.91865 102.75 5.83114 101.23 1.49
Δ9-Tetrahydrocannabivarin (THCV) 0 6.10678 6.26723 102.63 6.2359 102.11 0.50
Cannabinol (CBN) 0 5.80855 5.94924 102.42 6.17732 106.35 3.76
Δ9-Tetrahydrocannabinol (THC) 0 5.74023 5.89653 102.72 6.08023 105.92 3.07
Cannabichromene (CBC) 0 6.03125 6.1365 101.75 6.22862 103.27 1.49
Tetrahydrocannabinolic acid (THCA) 0 5.27835 5.39893 102.28 5.56834 105.49 3.09

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

This sample has not undergone random sampling and has not been tested for compliant state, batch representative testing. These results should therefore be used for research and development or quality control purposes only. Results apply to the sample as received.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
KEB - LM Iron laboratories KEB - LM

Iron Laboratories, LLC is an ISO/IEC 17025:2005 Testing Laboratory laboratory, accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 2 of 6

IRON LaboratoriesPJLA

ISO/IEC 17025:2005 Accredited

Pesticide Analysis by
Mass Spectrometer
Testing Accreditation #: 77802 Test Certificate #: 125047-001
Client Name, Sample Details

Kelly Young
Central Lake, MI 49622
Sample: Cartridge
Type: Concentrate
Method: FE-52 (EN 15662 & AOAC 2007.01)
Test Conditions

Prepsheet ID#: MIPS200626a
Scale: XS205-MI2
Temp: 22.1 °C
Baro PE: 977.9 hPa
Analyst: JRT
Technician: ANJ
Sample ID#: 125047

Harvest/Process Date: 06/25/2020
Serving Size (g): 1
Date Received: 06/25/2020
Test Date: 06/26/2020
Valid Through: 06/26/2021
Report Issued: 06/29/2020
Sample #125047
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
Aldicarb 0.400 0.125 Pass/<LOD Abamectin**** 0.500 0.125 Pass/<LOD
Acephate 0.400 0.125 Pass/<LOD Acequinocyl 2.000 0.250 Pass/<LOD
Acetamiprid 0.200 0.125 Pass/<LOD Azoxystrobin 0.200 0.125 Pass/<LOD
Bifenazate 0.200 0.125 Pass/<LOD Bifenthrin 0.200 0.125 Pass/<LOD
Boscalid 0.400 0.125 Pass/<LOD Carbaryl 0.200 0.125 Pass/<LOD
Carbofuran 0.200 0.125 Pass/<LOD Chlorantraniliprole 0.200 0.125 Pass/<LOD
Chlorfenapyr 1.000 0.500 Pass/<LOD Chlorpyrifos 0.200 0.125 Pass/<LOD
Clofentezine 0.200 0.125 Pass/<LOD Cyfluthrin** 1.000 0.500 Pass/<LOD
Cypermethrin*** 1.000 0.500 Pass/<LOD Daminozide 1.000 0.500 Pass/<LOD
DDVP (Dichlorvos) 1.000 0.250 Pass/<LOD Diazinon 0.200 0.125 Pass/<LOD
Dimethoate 0.200 0.125 Pass/<LOD Ethoprophos 0.200 0.125 Pass/<LOD
Etofenprox 0.400 0.125 Pass/<LOD Etoxazole 0.200 0.125 Pass/<LOD
Fenoxycarb 0.200 0.125 Pass/<LOD Fenpyroximate 0.400 0.125 Pass/<LOD
Fipronil 0.400 0.125 Pass/<LOD Flonicamid 1.000 0.125 Pass/<LOD
Fludioxonil 0.400 0.125 Pass/<LOD Hexythiazox 1.000 0.125 Pass/<LOD
Imazalil 0.200 0.125 Pass/<LOD Imidacloprid 0.400 0.125 Pass/<LOD
Kresoxim Methyl 0.400 0.125 Pass/<LOD Malathion 0.200 0.125 Pass/<LOD
Metalaxyl 0.200 0.125 Pass/<LOD Methiocarb 0.200 0.125 Pass/<LOD
Methomyl 0.400 0.125 Pass/<LOD Methyl Parathion 0.200 0.125 Pass/<LOD
MGK-264‡ 0.200 0.125 Pass/<LOD Myclobutanil 0.200 0.125 Pass/<LOD
Naled 0.500 0.125 Pass/<LOD Oxamyl 1.000 0.125 Pass/<LOD
Paclobutrazol 0.400 0.125 Pass/<LOD Permethrins† 0.200 0.125 Pass/<LOD
Phosmet 0.200 0.125 Pass/<LOD Piperonyl Butoxide 100.000 1.900 Pass/<LOD
Prallethrin 0.200 0.125 Pass/<LOD Propiconazole 0.400 0.125 Pass/<LOD
Propoxur 0.200 0.125 Pass/<LOD Pyrethrins* 1.000 0.125 Pass/<LOD
Pyridaben 0.200 0.125 Pass/<LOD Spinosad***** 0.200 0.125 Pass/<LOD
Spiromesifen 0.200 0.125 Pass/<LOD Spirotetramat 0.200 0.125 Pass/<LOD
Spiroxamine‡ 0.400 0.125 Pass/<LOD Tebuconazole 0.400 0.125 Pass/<LOD
Thiacloprid 0.200 0.125 Pass/<LOD Thiamethoxam 0.200 0.125 Pass/<LOD
Trifloxystrobin 0.200 0.125 Pass/<LOD

* Pyrethrins are reported as the sum of Jasmolin I, Cinerin I, and Pyrethrin I
** Cyfluthrins are reported as the sum of isomers Cyfluthrin I, II, III, and IV
*** Cypermethrins are reported as the sum of isomers Cypermethrin I, II, III, and IV
**** Abamectin is reported as the sum of Avermectin B1a and Avermectin B1b
***** Spinosad is reported as the sum of Spinosyn A and Spinosyn D
† Permethrin and Prallethrin are reported as the sum of cis and trans isomers
‡ MGK-264 and Spiroximine are reported as the sum of isomers I and II
MRL - Maximum Residue Limit; LOD - Limit of Detection

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
KEB - LM Iron laboratories KEB - LM

Iron Laboratories, LLC is an ISO/IEC 17025:2005 Testing Laboratory laboratory, accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 2 of 6

IRON LaboratoriesPJLA

ISO/IEC 17025:2005 Accredited

Pesticide QC Report
Testing Accreditation #: 77802 Test Certificate #: 125047-001
Client Name, Sample Details

Kelly Young
Central Lake, MI 49622
Sample: Cartridge
Type: Concentrate
Method: FE-52 (EN 15662 & AOAC 2007.01)
Test Conditions

Prepsheet ID#: MIPS200626a
Scale: XS205-MI2
Temp: 22.1 °C
Baro PE: 977.9 hPa
Analyst: JRT
Technician: ANJ
Sample ID#: 125047

Harvest/Process Date: 06/25/2020
Serving Size (g): 1
Date Received: 06/25/2020
Test Date: 06/26/2020
Valid Through: 06/26/2021
Report Issued: 06/29/2020
Sample #125047
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS recovery% MSD recovery% Relative Percent Difference (%) QC Flag
Acephate N.D. 1 0.909 0.997 90.90 99.70 9.23
Acequinocyl N.D. 1 0.345 0.503 34.50 50.30 37.26 LRQ
Acetamiprid N.D. 1 0.805 0.91 80.50 91.00 12.24
Aldicarb N.D. 1 0.861 0.874 86.10 87.40 1.50
Avermectin B1a N.D. 0.97 0.583 0.624 60.10 64.33 6.79
Azoxystrobin N.D. 1 0.935 0.972 93.50 97.20 3.88
Bifenazate N.D. 1 0.428 0.304 42.80 30.40 33.88 LRQ
Bifenthrin N.D. 1 0.566 0.588 56.60 58.80 3.81 LR
Boscalid N.D. 1 0.619 0.691 61.90 69.10 10.99
Carbaryl N.D. 1 0.842 0.884 84.20 88.40 4.87
Carbofuran N.D. 1 0.94 0.934 94.00 93.40 0.64
Chlorantraniliprole N.D. 1 0.812 0.914 81.20 91.40 11.82
Chlorfenapyr N.D. 1 0.847 0.799 84.70 79.90 5.83
Chlorpyriphos N.D. 1 0.674 0.747 67.40 74.70 10.27
Clofentezine N.D. 1 0.635 0.708 63.50 70.80 10.87
Cyfluthrin N.D. 1 0.604 0.664 60.40 66.40 9.46
Cypermethrin N.D. 1 0.651 0.706 65.10 70.60 8.11
Daminoside N.D. 1 0.228 0.247 22.80 24.70 8.00 LR
Diazanon N.D. 1 0.896 0.923 89.60 92.30 2.97
Dichlorvos N.D. 1 0.608 0.762 60.80 76.20 22.48
Dimethoate N.D. 1 0.868 0.903 86.80 90.30 3.95
Ethoprophos N.D. 1 0.915 0.993 91.50 99.30 8.18
Etofenprox N.D. 1 0.74 0.761 74.00 76.10 2.80
Etoxazole N.D. 1 1.1 1.04 110.00 104.00 5.61
Fenoxycarb N.D. 1 0.687 0.735 68.70 73.50 6.75
Fenpyroximate N.D. 1 0.868 0.926 86.80 92.60 6.47
Fipronil N.D. 1 0.989 1 98.90 100.00 1.11
Flonicamid N.D. 1 0.54 0.677 54.00 67.70 22.51 LR
Fludioxonil N.D. 1 0.978 0.979 97.80 97.90 0.10
Hexythiazox N.D. 1 0.475 0.573 47.50 57.30 18.70 LR
Imazalil N.D. 1 0.95 1.02 95.00 102.00 7.11
Imidacloprid N.D. 1 0.604 0.684 60.40 68.40 12.42
Kresoxim-methyl N.D. 1 1.01 1.02 101.00 102.00 0.99
Malathion N.D. 1 1.09 1.15 109.00 115.00 5.36
Metalaxyl N.D. 1 1.09 0.981 109.00 98.10 10.53
Methiocarb N.D. 1 0.739 0.873 73.90 87.30 16.63
Methomyl N.D. 1 0.943 0.898 94.30 89.80 4.89
MGK-264 N.D. 1 0.803 0.818 80.30 81.80 1.85
Myclobutanil N.D. 1 0.708 0.792 70.80 79.20 11.20
Naled (dibrom) N.D. 1 0.305 0.412 30.50 41.20 29.85 LR
Oxamyl N.D. 1 1.05 1.07 105.00 107.00 1.89
Paclobutrazol N.D. 1 0.856 0.979 85.60 97.90 13.41
Parathion-methyl N.D. 1 0.937 1.03 93.70 103.00 9.46
Permethrins N.D. 1 0.606 0.638 60.60 63.80 5.14
Phosmet N.D. 1 0.821 0.771 82.10 77.10 6.28
Piperonyl butoxide N.D. 1 1.06 1.31 106.00 131.00 21.10 HR
Prallethrin N.D. 1 0.754 0.822 75.40 82.20 8.63
Propiconazole N.D. 1 0.805 0.825 80.50 82.50 2.45
Propoxur N.D. 1 0.939 0.996 93.90 99.60 5.89
Pyrethrin N.D. 0.65 0.489 0.534 75.23 82.15 8.80
Pyridaben N.D. 1 0.801 0.848 80.10 84.80 5.70
SpinosynA N.D. 0.84 0.814 0.829 96.90 98.69 1.83
SpinosynD N.D. 0.16 0.165 0.172 103.13 107.50 4.15
Spiromesifen N.D. 1 0.31 0.263 31.00 26.30 16.40 LR
Spirotetramat N.D. 1 0.918 0.991 91.80 99.10 7.65
Spiroxamine N.D. 1 0.966 0.949 96.60 94.90 1.78
Tebuconazole N.D. 1 0.905 1.04 90.50 104.00 13.88
Thiacloprid N.D. 1 0.779 0.843 77.90 84.30 7.89
Thiamethoxam N.D. 1 0.663 0.735 66.30 73.50 10.30
Trifloxystrobin N.D. 1 0.974 0.95 97.40 95.00 2.49

N.D. = Not Detected

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 30%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (60-120%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
KEB - LM Iron laboratories KEB - LM

Iron Laboratories, LLC is an ISO/IEC 17025:2005 Testing Laboratory laboratory, accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 3 of 6

IRON LaboratoriesPJLA

ISO/IEC 17025:2005 Accredited

Residual Solvents Analysis by
Mass Spectrometer
Testing Accreditation #: 77802 Test Certificate #: 125047-001
Client Name, Sample Details

Kelly Young
Central Lake, MI 49622
Sample: Cartridge
Type: Concentrate
Method: SOP FE-44-MI
Test Conditions

Prepsheet ID#: MIHS200624b
Scale: XS205-MI2
Temp: 22.4 °C
Baro PE: 976.5 hPa
Analyst: JRT
Technician: JRT
Sample ID#: 125047

Harvest/Process Date: 06/25/2020
Serving Size (g): 1
Date Received: 06/25/2020
Test Date: 06/24/2020
Valid Through: 06/24/2021
Report Issued: 06/26/2020
Sample #125047
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
1,2-Dichloroethane 2 1 Pass/<LOD 1,2-Dimethoxyethane 5,000 250 Not Tested
1,4-dioxane 5,000 25 Not Tested 1-Butanol 5,000 250 Not Tested
1-Pentanol 5,000 250 Not Tested 1-Propanol 5,000 250 Not Tested
2,2-Dimethylpropane (Neopentane) 750 25 Pass/<LOD 2,2-Dimethylbutane (Hexanes) 50 25 Pass/<LOD
2,3-Dimethylbutane (Hexanes) 50 25 Pass/<LOD 2-Butanol 5,000 25 Not Tested
2-Butanone (MEK) 5,000 250 Not Tested 2-Ethoxyethanol 5,000 25 Not Tested
2-Methylbutane (Isopentane) 750 25 Pass/<LOD 2-Methylpentane (Hexanes) 50 25 Pass/<LOD
2-Methylpropane (Isobutane) 800 25 Pass/<LOD 2-propanol (Isopropyl Alcohol) 500 25 Pass/<LOD
2-Propanone (Acetone) 750 25 Pass/<LOD 3-Methylpentane (Hexanes) 50 25 Pass/<LOD
Acetonitrile 60 30 Pass/<LOD Benzene 1 1 Pass/<LOD
Butane 800 25 Pass/<LOD Chloroform 2 2 Pass/<LOD
Cumene 5,000 25 Not Tested Cyclohexane 50 25 Not Tested
Dichloromethane 125 25 Pass/<LOD Dimethylsulfoxide (DMSO) 5,000 250 Not Tested
Ethanol 1,000 50 Pass/<LOD Ethyl acetate 400 25 Pass/<LOD
Ethyl ether 500 25 Pass/<LOD Ethylene glycol 5,000 25 Not Tested
Ethylene oxide 5 3 Pass/<LOD Heptane 500 25 Pass/<LOD
Hexane 50 25 Pass/<LOD Isopropyl acetate 5,000 25 Not Tested
Methanol 250 125 Pass/<LOD Naptha 400 100 Pass/<LOD
N,N-Dimethylacetamide 5,000 250 Not Tested N,N-Dimethylformamide (DMF) 5,000 250 Not Tested
Pentane 750 25 Pass/<LOD Petroleum Ether 400 100 Pass/<LOD
Propane 2,100 25 Pass/<LOD Pyridine 5,000 250 Not Tested
Sulfolane 5,000 25 Not Tested Tetrahydrofuran (THF) 5,000 25 Not Tested
Toluene 150 25 Pass/<LOD Trichloroethylene 25 25 Pass/<LOD
Xylenes* 150 25 Pass/<LOD

Total Butanes = 0 ug/g (PASS); Total Pentanes = 0 ug/g (PASS); Total Hexanes = 0 ug/g (PASS)

* Xylenes are reported as the sum of o-xylene, m-xylene, p-xylene, and ethylbenzene
MRL - Maximum Residue Limit; LOD - Limit of Detection

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
KEB - LM Iron laboratories KEB - LM

Iron Laboratories, LLC is an ISO/IEC 17025:2005 Testing Laboratory laboratory, accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 4 of 6

IRON LaboratoriesPJLA

ISO/IEC 17025:2005 Accredited

Residual Solvents QC Report
Testing Accreditation #: 77802 Test Certificate #: 125047-001
Client Name, Sample Details

Kelly Young
Central Lake, MI 49622
Sample: Cartridge
Type: Concentrate
Method: SOP FE-44-MI
Test Conditions

Prepsheet ID#: MIHS200624b
Scale: XS205-MI2
Temp: 22.4 °C
Baro PE: 976.5 hPa
Analyst: JRT
Technician: JRT
Sample ID#: 125047

Harvest/Process Date: 06/25/2020
Serving Size (g): 1
Date Received: 06/25/2020
Test Date: 06/24/2020
Valid Through: 06/24/2021
Report Issued: 06/26/2020
Sample #125047
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS Recovery (%) MSD Recovery (%) Relative Percent Difference (%) QC Flag
1,2-Dichloroethane N.D. 25 26 26 104.00 104.00 0.00
n-Propane N.D. 250 200 191 80.00 76.40 4.60
Isobutane N.D. 250 236 226 94.40 90.40 4.33
Methanol N.D. 250 242 233 96.80 93.20 3.79
n-Butane N.D. 250 254 238 101.60 95.20 6.50
2,2-Dimethylpropane N.D. 250 250 243 100.00 97.20 2.84
Ethanol N.D. 250 236 235 94.40 94.00 0.42
Isopentane N.D. 250 262 251 104.80 100.40 4.29
Acetonitrile N.D. 250 248 244 99.20 97.60 1.63
Diethyl ether N.D. 250 257 251 102.80 100.40 2.36
2-propanone N.D. 250 272 269 108.80 107.60 1.11
2-propanol N.D. 250 253 253 101.20 101.20 0.00
n-Pentane N.D. 250 262 259 104.80 103.60 1.15
2,2-Dimethylbutane N.D. 250 277 255 110.80 102.00 8.27
2,3-Dimethylbutane N.D. 250 253 252 101.20 100.80 0.40
Methylene chloride N.D. 250 253 250 101.20 100.00 1.19
2-Methylpentane N.D. 250 263 254 105.20 101.60 3.48
3-Methylpentane N.D. 250 265 255 106.00 102.00 3.85
2-Butanol N.D. 0 0 0 0.00 0.00 0.00
n-Hexane N.D. 250 264 252 105.60 100.80 4.65
Ethyl acetate N.D. 250 253 249 101.20 99.60 1.59
Tetrahydrofuran N.D. 0 0 0 0.00 0.00 0.00
Trichloroethylene N.D. 25 28 27 112.00 108.00 3.64
Isopropyl acetate N.D. 0 0 0 0.00 0.00 0.00
Benzene N.D. 25 27 27 108.00 108.00 0.00
Chloroform N.D. 25 26 25 104.00 100.00 3.92
Cyclohexane N.D. 0 0 0 0.00 0.00 0.00
Ethylene glycol N.D. 0 0 0 0.00 0.00 0.00
Heptane N.D. 250 262 250 104.80 100.00 4.69
2-Ethoxyethanol N.D. 0 0 0 0.00 0.00 0.00
1,4-Dioxane N.D. 0 0 0 0.00 0.00 0.00
Pyridine N.D. 0 0 0 0.00 0.00 0.00
Toluene N.D. 250 274 266 109.60 106.40 2.96
Chlorobenzene N.D. 0 0 0 0.00 0.00 0.00
Ethylbenzene N.D. 0 0 0 0.00 0.00 0.00
m-Xylene/p-Xylene N.D. 125 144 138 115.20 110.40 4.26
o-Xylene N.D. 125 153 146 122.40 116.80 4.68
Cumene N.D. 0 0 0 0.00 0.00 0.00
Ethylene oxide N.D. 25 26 26 104.00 104.00 0.00

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

N.D. = Not Detected

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
KEB - LM Iron laboratories KEB - LM

Iron Laboratories, LLC is an ISO/IEC 17025:2005 Testing Laboratory laboratory, accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

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IRON LaboratoriesPJLA

ISO/IEC 17025:2005 Accredited

Heavy Metals Analysis
Testing Accreditation #: 77802 Test Certificate #: 125047-001
Client Name, Sample Details

Kelly Young
Central Lake, MI 49622
Sample: Cartridge
Type: Concentrate
Method: FE60 ICPMS-MI
Test Conditions

Prepsheet ID#: MIICP200625cMK
Temp: 22.9 °C
Baro PE: 978.8 hPa
Analyst: TAC
Technician: MK
Sample ID#: 125047

Harvest/Process Date: 06/25/2020
Serving Size (g): 1
Date Received: 06/25/2020
Test Date: 06/25/2020
Valid Through: 06/25/2021
Report Issued: 07/02/2020
Sample #125047
Sample #125047 Sample #125047
Test Compound MRL (PPM) LOD (PPM) Status (PPM)
Arsenic 0.4 0.1 Pass/<LOD
Copper 0 1.5 Not Tested
Cadmium 0.4 0.1 Pass/<LOD
Chromium 1.2 0.3 Pass/<LOD
Lead 1 0.25 Pass/<LOD
Mercury 0.2 0.05 Pass/<LOD
Nickel 1 0.25 Pass/0.298

MRL - Maximum Residue Limit; LOD - Limit of Detection

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
MEH QM Iron laboratories MEH QM

Iron Laboratories, LLC is an ISO/IEC 17025:2005 Testing Laboratory laboratory, accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

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IRON LaboratoriesPJLA

ISO/IEC 17025:2005 Accredited

QC Report
Testing Accreditation #: 77802 Test Certificate #: 125047-001
Client Name, Sample Details

Kelly Young
Central Lake, MI 49622
Sample: Cartridge
Type: Concentrate
Method: FE60 ICPMS-MI
Test Conditions

Prepsheet ID#: MIICP200625cMK
Temp: 22.9 °C
Baro PE: 978.8 hPa
Analyst: TAC
Technician: MK
Sample ID#: 125047

Harvest/Process Date: 06/25/2020
Serving Size (g): 1
Date Received: 06/25/2020
Test Date: 06/25/2020
Valid Through: 06/25/2021
Report Issued: 07/02/2020
Sample #125047
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD QC Flag
Arsenic N/D 0.160 0.143 89.38 0.120 75.00
Cadmium N/D 0.160 0.161 100.63 0.134 83.75
Chromium N/D 0.480 0.552 115.00 0.441 91.88
Copper N/D 2.400 2.500 104.17 2.140 89.17
Lead N/D 0.400 0.367 91.75 0.326 81.50
Mercury N/D 0.080 0.081 101.25 0.071 88.75
Nickel N/D 0.400 0.633 158.25 0.535 133.75 HR

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
MEH QM Iron laboratories MEH QM

Iron Laboratories, LLC is an ISO/IEC 17025:2005 Testing Laboratory laboratory, accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

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