ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Marijuana Potency Analysis by
High Performance Liquid Chromatography
Testing Accreditation #: 4092-004 Test Certificate #: 124468-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Mach 4
License: 030-1009646F7F8
Type: AU Tincture
Method: FE04U HPLC-UV
Metrc Test Pkg#: 1A401030002C949000000239
Metrc Source Pkg#: 1A401030002C949000000235
Test Conditions

Prepsheet ID#: ORP200605C
Scale: XS205-OR1
Temp: 22.1 °C
Baro Pressure: 1002 hPa
Analyst: HRM
Technician: TMR
Sample ID#: 124468

Lot #: Mach 4 6/2/20 #1
Batch #: 124468
Batch Weight (g): 812.7
Harvest/Process Date: 06/02/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 06/03/2020
Test Date: 06/05/2020
Sample #124468
Sample #124468 Sample #124468
Test
Compounds		 THC THCA CBD CBDA CBN CBG CBC THCV* CBDV Total
Cannabinoids*		 Total THC Total CBD Calc Max Total
Cannabinoids*
Amount (%) 9.93 73.08 N/D 1.96 0.28 0.52 0.22 N/D N/D 85.98 74.02 1.72 76.75
Amount (mg/g) 99.26 730.83 N/D 19.57 2.78 5.16 2.24 N/D N/D 859.84 740.20 17.16 767.54
Amount per Serving (mg) 4.96 36.54 N\D 0.98 0.14 0.26 0.11 N\D N\D 42.99 Serving Size~ (g): 0.05
LOQ (mg/g) 1.8 1.8 1.8 1.8 1.8 1.8 1.8 1.8 1.8   %Decarb. THC CBD
±%RPD 1.14 2.89 3.61 3.49 3.32 3.37 5.05 3.42 3.74 12 0

LOQ = Limit of Quantitation; %RPD = Relative Percent Deviation; %RSD = Relative Standard Deviation; N/D = Not Detected

*Designates values that are not currently included in the accredited scope of Iron Laboratories.

*** Designates tests that use the method FE-45. FE-45 is performed using AOAC 966.02 and 32.004-32.009. FE-45 has relative expanded (k=2) uncertainties of 1.098% for moisture, 1.754% for water activity for unprocessed plant materials, and 13.102% for water activity for infused products. Vitamin E acetate analysis has a relative expanded (k=2) uncertainty of 18.614%.

Total THC and CBD is the calculated sum of THC or CBD and the amount of THC or CBD derived from THCA or CBDA, respectively. These values are calculated by applying a molar correction factor of 0.877 to the THCA or the CBDA value. Calc Max Total Cannabinoids is the sum of Total THC, Total CBD, CBN, CBG, CBC, THCV, and CBDV.

%Decarb. THC and CBD refer to the percentage of THC or CBD relative to THCA or CBDA, respectively.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 1 of 11

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant QC Report
Testing Accreditation #: 4092-004 Test Certificate #: 124468-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Mach 4
License: 030-1009646F7F8
Type: AU Tincture
Method: FE04U HPLC-UV
Metrc Test Pkg#: 1A401030002C949000000239
Metrc Source Pkg#: 1A401030002C949000000235
Test Conditions

Prepsheet ID#: ORP200605C
Scale: XS205-OR1
Temp: 22.1 °C
Baro Pressure: 1002 hPa
Analyst: HRM
Technician: TMR
Sample ID#: 124468

Lot #: Mach 4 6/2/20 #1
Batch #: 124468
Batch Weight (g): 812.7
Harvest/Process Date: 06/02/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 06/03/2020
Test Date: 06/05/2020
Sample #124468
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Cannabidivarin (CBDV) N.D. 5.41 5.99 110.72 5.77 106.65 3.74
Cannabidiolic Acid (CBDA) N.D. 5.21 5.83 111.90 5.63 108.06 3.49
Cannabigerol (CBG) N.D. 5.4 6.03 111.67 5.83 107.96 3.37
Cannabidiol (CBD) N.D. 5.51 6.2 112.52 5.98 108.53 3.61
Δ9-Tetrahydrocannabivarin (THCV) N.D. 5.4 5.94 110.00 5.74 106.30 3.42
Cannabinol (CBN) N.D. 5.28 5.82 110.23 5.63 106.63 3.32
Δ9-Tetrahydrocannabinol (THC) N.D. 5.57 6.15 110.41 6.08 109.16 1.14
Cannabichromene (CBC) N.D. 6.35 6.9 108.66 6.56 103.31 5.05
Tetrahydrocannabinolic acid (THCA) N.D. 5.13 5.62 109.55 5.46 106.43 2.89

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 2 of 11

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Pesticide Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-004 Test Certificate #: 124468-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Mach 4
License: 030-1009646F7F8
Type: AU Tincture
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A401030002C949000000239
Metrc Source Pkg#: 1A401030002C949000000235
Test Conditions

Prepsheet ID#: ORPS200604a
Scale: 1129293203
Temp: 21.4 °C
Baro PE: 999.3 hPa
Analyst: JER
Technician: HRM/EDT
Sample ID#: 124468

Lot #: Mach 4 6/2/20 #1
Batch #: 124468
Batch Weight (g): 812.7
Harvest/Process Date: 06/02/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 06/03/2020
Test Date: 06/05/2020
Sample #124468
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
Aldicarb 0.400 0.122 Pass/<LOD Abamectin**** 0.500 0.122 Pass/<LOD
Acephate 0.400 0.122 Pass/<LOD Acequinocyl 2.000 0.244 Pass/<LOD
Acetamiprid 0.200 0.122 Pass/<LOD Azoxystrobin 0.200 0.122 Pass/<LOD
Bifenazate 0.200 0.122 Pass/<LOD Bifenthrin 0.200 0.122 Pass/<LOD
Boscalid 0.400 0.122 Pass/<LOD Carbaryl 0.200 0.122 Pass/<LOD
Carbofuran 0.200 0.122 Pass/<LOD Chlorantraniliprole 0.200 0.122 Pass/<LOD
Chlorfenapyr 1.000 0.489 Pass/<LOD Chlorpyrifos 0.200 0.122 Pass/<LOD
Clofentezine 0.200 0.122 Pass/<LOD Cyfluthrin** 1.000 0.489 Pass/<LOD
Cypermethrin*** 1.000 0.489 Pass/<LOD Daminozide 1.000 0.122 Pass/<LOD
DDVP (Dichlorvos) 1.000 0.244 Pass/<LOD Diazinon 0.200 0.122 Pass/<LOD
Dimethoate 0.200 0.122 Pass/<LOD Ethoprophos 0.200 0.122 Pass/<LOD
Etofenprox 0.400 0.122 Pass/<LOD Etoxazole 0.200 0.122 Pass/<LOD
Fenoxycarb 0.200 0.122 Pass/<LOD Fenpyroximate 0.400 0.122 Pass/<LOD
Fipronil 0.400 0.122 Pass/<LOD Flonicamid 1.000 0.122 Pass/<LOD
Fludioxonil 0.400 0.122 Pass/<LOD Hexythiazox 1.000 0.122 Pass/<LOD
Imazalil 0.200 0.122 Pass/<LOD Imidacloprid 0.400 0.122 Pass/<LOD
Kresoxim Methyl 0.400 0.122 Pass/<LOD Malathion 0.200 0.122 Pass/<LOD
Metalaxyl 0.200 0.122 Pass/<LOD Methiocarb 0.200 0.122 Pass/<LOD
Methomyl 0.400 0.122 Pass/<LOD Methyl Parathion 0.200 0.122 Pass/<LOD
MGK-264‡ 0.200 0.122 Pass/<LOD Myclobutanil 0.000 0.122 Pass/<LOD
Naled 0.500 0.122 Pass/<LOD Oxamyl 1.000 0.122 Pass/<LOD
Paclobutrazol 0.400 0.122 Pass/<LOD Permethrins† 0.200 0.122 Pass/<LOD
Phosmet 0.200 0.122 Pass/<LOD Piperonyl Butoxide 2.000 0.122 Pass/<LOD
Prallethrin 0.200 0.122 Pass/<LOD Propiconazole 0.400 0.122 Pass/<LOD
Propoxur 0.200 0.122 Pass/<LOD Pyrethrins* 1.000 0.122 Pass/<LOD
Pyridaben 0.200 0.122 Pass/<LOD Spinosad***** 0.200 0.122 Pass/<LOD
Spiromesifen 0.200 0.122 Pass/<LOD Spirotetramat 0.200 0.122 Pass/<LOD
Spiroxamine‡ 0.400 0.122 Pass/<LOD Tebuconazole 0.400 0.122 Pass/<LOD
Thiacloprid 0.200 0.122 Pass/<LOD Thiamethoxam 0.200 0.122 Pass/<LOD
Trifloxystrobin 0.200 0.122 Pass/<LOD

* Pyrethrins are reported as the sum of Jasmolin I, Cinerin I, and Pyrethrin I
** Cyfluthrins are reported as the sum of isomers Cyfluthrin I, II, III, and IV
*** Cypermethrins are reported as the sum of isomers Cypermethrin I, II, III, and IV
**** Abamectin is reported as the sum of Avermectin B1a and Avermectin B1b
***** Spinosad is reported as the sum of Spinosyn A and Spinosyn D
† Permethrin and Prallethrin are reported as the sum of cis and trans isomers
‡ MGK-264 and Spiroximine are reported as the sum of isomers I and II
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 2 of 11

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Pesticide QC Report
Testing Accreditation #: 4092-004 Test Certificate #: 124468-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Mach 4
License: 030-1009646F7F8
Type: AU Tincture
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A401030002C949000000239
Metrc Source Pkg#: 1A401030002C949000000235
Test Conditions

Prepsheet ID#: ORPS200604a
Scale: 1129293203
Temp: 21.4 °C
Baro PE: 999.3 hPa
Analyst: JER
Technician: HRM/EDT
Sample ID#: 124468

Lot #: Mach 4 6/2/20 #1
Batch #: 124468
Batch Weight (g): 812.7
Harvest/Process Date: 06/02/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 06/03/2020
Test Date: 06/05/2020
Sample #124468
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS recovery% MSD recovery% Relative Percent Difference (%) QC Flag
Acephate N.D. 1 1.02 1 102.00 100.00 1.98
Acequinocyl N.D. 1 0.368 0.463 36.80 46.30 22.86 LRQ
Acetamiprid N.D. 1 0.902 0.952 90.20 95.20 5.39
Aldicarb N.D. 1 0.921 0.915 92.10 91.50 0.65
Avermectin B1a N.D. 0.97 1.4 1.4 144.33 144.33 0.00 HR
Azoxystrobin N.D. 1 0.91 0.946 91.00 94.60 3.88
Bifenazate N.D. 1 0.565 0.548 56.50 54.80 3.05 LR
Bifenthrin N.D. 1 0.689 0.666 68.90 66.60 3.39 LR
Boscalid N.D. 1 1 1.22 100.00 122.00 19.82
Carbaryl N.D. 1 1.15 1.12 115.00 112.00 2.64
Carbofuran N.D. 1 0.789 0.853 78.90 85.30 7.80
Chlorantraniliprole N.D. 1 1.09 1.38 109.00 138.00 23.48 HRQ
Chlorfenapyr N.D. 1 0.845 0.985 84.50 98.50 15.30
Chlorpyriphos N.D. 1 0.863 0.883 86.30 88.30 2.29
Clofentezine N.D. 1 0.944 1.08 94.40 108.00 13.44
Cyfluthrin N.D. 1 0.855 1.1 85.50 110.00 25.06 Q
Cypermethrin N.D. 1 0.861 0.914 86.10 91.40 5.97
Daminoside N.D. 1 1.41 1.36 141.00 136.00 3.61 HR
Diazanon N.D. 1 1.26 1.24 126.00 124.00 1.60
Dichlorvos N.D. 1 0.92 0.894 92.00 89.40 2.87
Dimethoate N.D. 1 0.736 0.735 73.60 73.50 0.14
Ethoprophos N.D. 1 0.712 0.756 71.20 75.60 5.99
Etofenprox N.D. 1 0.722 0.736 72.20 73.60 1.92
Etoxazole N.D. 1 0.974 0.94 97.40 94.00 3.55
Fenoxycarb N.D. 1 1.1 1.23 110.00 123.00 11.16
Fenpyroximate N.D. 1 0.837 0.794 83.70 79.40 5.27
Fipronil N.D. 1 1.21 1.13 121.00 113.00 6.84
Flonicamid N.D. 1 0.794 0.816 79.40 81.60 2.73
Fludioxonil N.D. 1 1.12 1.04 112.00 104.00 7.41
Hexythiazox N.D. 1 0.614 0.754 61.40 75.40 20.47 LRQ
Imazalil N.D. 1 1.28 1.23 128.00 123.00 3.98
Imidacloprid N.D. 1 0.906 0.867 90.60 86.70 4.40
Kresoxim-methyl N.D. 1 1.46 1.54 146.00 154.00 5.33 HR
Malathion N.D. 1 1.14 1.07 114.00 107.00 6.33
Metalaxyl N.D. 1 1.1 1.08 110.00 108.00 1.83
Methiocarb N.D. 1 0.763 0.838 76.30 83.80 9.37
Methomyl N.D. 1 1.17 1.15 117.00 115.00 1.72
MGK-264 N.D. 1 0.799 0.86 79.90 86.00 7.35
Myclobutanil N.D. 1 0.967 1.17 96.70 117.00 19.00
Naled (dibrom) N.D. 1 0.601 0.604 60.10 60.40 0.50 LR
Oxamyl N.D. 1 0.842 0.841 84.20 84.10 0.12
Paclobutrazol N.D. 1 1.26 1.38 126.00 138.00 9.09 HR
Parathion-methyl N.D. 1 1.13 0.901 113.00 90.10 22.55 Q
Permethrins N.D. 1 0.608 0.661 60.80 66.10 8.35 LR
Phosmet N.D. 1 1.19 1.27 119.00 127.00 6.50
Piperonyl butoxide N.D. 1 1.05 1.11 105.00 111.00 5.56
Prallethrin N.D. 1 1.21 1.26 121.00 126.00 4.05
Propiconazole N.D. 1 1.08 1.1 108.00 110.00 1.83
Propoxur N.D. 1 0.974 1.04 97.40 104.00 6.55
Pyrethrin N.D. 0.65 0.737 0.752 113.38 115.69 2.01
Pyridaben N.D. 1 0.775 0.709 77.50 70.90 8.89
SpinosynA N.D. 0.84 1.15 1.16 136.90 138.10 0.87 HR
SpinosynD N.D. 0.16 0.205 0.207 128.13 129.38 0.97
Spiromesifen N.D. 1 0.285 0.291 28.50 29.10 2.08 LR
Spirotetramat N.D. 1 1.21 1.23 121.00 123.00 1.64
Spiroxamine N.D. 1 1.37 1.27 137.00 127.00 7.58 HR
Tebuconazole N.D. 1 1.18 1.36 118.00 136.00 14.17 HR
Thiacloprid N.D. 1 0.917 0.927 91.70 92.70 1.08
Thiamethoxam N.D. 1 1.15 1.11 115.00 111.00 3.54
Trifloxystrobin N.D. 1 0.942 0.932 94.20 93.20 1.07

N.D. = Not Detected

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 30%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (60-120%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 3 of 11

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Pesticide Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-004 Test Certificate #: 124468-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Mach 4
License: 030-1009646F7F8
Type: AU Tincture
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A401030002C949000000239
Metrc Source Pkg#: 1A401030002C949000000235
Test Conditions

Prepsheet ID#: ORPS200604a
Scale: 1129293203
Temp: 21.4 °C
Baro PE: 999.3 hPa
Analyst: JER
Technician: HRM/EDT
Sample ID#: 124468

Lot #: Mach 4 6/2/20 #1
Batch #: 124468
Batch Weight (g): 812.7
Harvest/Process Date: 06/02/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 06/03/2020
Test Date: 06/05/2020
Sample #124468
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
Aldicarb 0.400 0.124 Pass/<LOD Abamectin**** 0.500 0.124 Pass/<LOD
Acephate 0.400 0.124 Pass/<LOD Acequinocyl 2.000 0.248 Pass/<LOD
Acetamiprid 0.200 0.124 Pass/<LOD Azoxystrobin 0.200 0.124 Pass/<LOD
Bifenazate 0.200 0.124 Pass/<LOD Bifenthrin 0.200 0.124 Pass/<LOD
Boscalid 0.400 0.124 Pass/<LOD Carbaryl 0.200 0.124 Pass/<LOD
Carbofuran 0.200 0.124 Pass/<LOD Chlorantraniliprole 0.200 0.124 Pass/<LOD
Chlorfenapyr 1.000 0.496 Pass/<LOD Chlorpyrifos 0.200 0.124 Pass/<LOD
Clofentezine 0.200 0.124 Pass/<LOD Cyfluthrin** 1.000 0.496 Pass/<LOD
Cypermethrin*** 1.000 0.496 Pass/<LOD Daminozide 1.000 0.124 Pass/<LOD
DDVP (Dichlorvos) 1.000 0.248 Pass/<LOD Diazinon 0.200 0.124 Pass/<LOD
Dimethoate 0.200 0.124 Pass/<LOD Ethoprophos 0.200 0.124 Pass/<LOD
Etofenprox 0.400 0.124 Pass/<LOD Etoxazole 0.200 0.124 Pass/<LOD
Fenoxycarb 0.200 0.124 Pass/<LOD Fenpyroximate 0.400 0.124 Pass/<LOD
Fipronil 0.400 0.124 Pass/<LOD Flonicamid 1.000 0.124 Pass/<LOD
Fludioxonil 0.400 0.124 Pass/<LOD Hexythiazox 1.000 0.124 Pass/<LOD
Imazalil 0.200 0.124 Pass/<LOD Imidacloprid 0.400 0.124 Pass/<LOD
Kresoxim Methyl 0.400 0.124 Pass/<LOD Malathion 0.200 0.124 Pass/<LOD
Metalaxyl 0.200 0.124 Pass/<LOD Methiocarb 0.200 0.124 Pass/<LOD
Methomyl 0.400 0.124 Pass/<LOD Methyl Parathion 0.200 0.124 Pass/<LOD
MGK-264‡ 0.200 0.124 Pass/<LOD Myclobutanil 0.000 0.124 Pass/<LOD
Naled 0.500 0.124 Pass/<LOD Oxamyl 1.000 0.124 Pass/<LOD
Paclobutrazol 0.400 0.124 Pass/<LOD Permethrins† 0.200 0.124 Pass/<LOD
Phosmet 0.200 0.124 Pass/<LOD Piperonyl Butoxide 2.000 0.124 Pass/<LOD
Prallethrin 0.200 0.124 Pass/<LOD Propiconazole 0.400 0.124 Pass/<LOD
Propoxur 0.200 0.124 Pass/<LOD Pyrethrins* 1.000 0.124 Pass/<LOD
Pyridaben 0.200 0.124 Pass/<LOD Spinosad***** 0.200 0.124 Pass/<LOD
Spiromesifen 0.200 0.124 Pass/<LOD Spirotetramat 0.200 0.124 Pass/<LOD
Spiroxamine‡ 0.400 0.124 Pass/<LOD Tebuconazole 0.400 0.124 Pass/<LOD
Thiacloprid 0.200 0.124 Pass/<LOD Thiamethoxam 0.200 0.124 Pass/<LOD
Trifloxystrobin 0.200 0.124 Pass/<LOD

* Pyrethrins are reported as the sum of Jasmolin I, Cinerin I, and Pyrethrin I
** Cyfluthrins are reported as the sum of isomers Cyfluthrin I, II, III, and IV
*** Cypermethrins are reported as the sum of isomers Cypermethrin I, II, III, and IV
**** Abamectin is reported as the sum of Avermectin B1a and Avermectin B1b
***** Spinosad is reported as the sum of Spinosyn A and Spinosyn D
† Permethrin and Prallethrin are reported as the sum of cis and trans isomers
‡ MGK-264 and Spiroximine are reported as the sum of isomers I and II
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 4 of 11

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Pesticide QC Report
Testing Accreditation #: 4092-004 Test Certificate #: 124468-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Mach 4
License: 030-1009646F7F8
Type: AU Tincture
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A401030002C949000000239
Metrc Source Pkg#: 1A401030002C949000000235
Test Conditions

Prepsheet ID#: ORPS200604a
Scale: 1129293203
Temp: 21.4 °C
Baro PE: 999.3 hPa
Analyst: JER
Technician: HRM/EDT
Sample ID#: 124468

Lot #: Mach 4 6/2/20 #1
Batch #: 124468
Batch Weight (g): 812.7
Harvest/Process Date: 06/02/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 06/03/2020
Test Date: 06/05/2020
Sample #124468
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS recovery% MSD recovery% Relative Percent Difference (%) QC Flag
Acephate N.D. 1 1.02 1 102.00 100.00 1.98
Acequinocyl N.D. 1 0.368 0.463 36.80 46.30 22.86 LRQ
Acetamiprid N.D. 1 0.902 0.952 90.20 95.20 5.39
Aldicarb N.D. 1 0.921 0.915 92.10 91.50 0.65
Avermectin B1a N.D. 0.97 1.4 1.4 144.33 144.33 0.00 HR
Azoxystrobin N.D. 1 0.91 0.946 91.00 94.60 3.88
Bifenazate N.D. 1 0.565 0.548 56.50 54.80 3.05 LR
Bifenthrin N.D. 1 0.689 0.666 68.90 66.60 3.39 LR
Boscalid N.D. 1 1 1.22 100.00 122.00 19.82
Carbaryl N.D. 1 1.15 1.12 115.00 112.00 2.64
Carbofuran N.D. 1 0.789 0.853 78.90 85.30 7.80
Chlorantraniliprole N.D. 1 1.09 1.38 109.00 138.00 23.48 HRQ
Chlorfenapyr N.D. 1 0.845 0.985 84.50 98.50 15.30
Chlorpyriphos N.D. 1 0.863 0.883 86.30 88.30 2.29
Clofentezine N.D. 1 0.944 1.08 94.40 108.00 13.44
Cyfluthrin N.D. 1 0.855 1.1 85.50 110.00 25.06 Q
Cypermethrin N.D. 1 0.861 0.914 86.10 91.40 5.97
Daminoside N.D. 1 1.41 1.36 141.00 136.00 3.61 HR
Diazanon N.D. 1 1.26 1.24 126.00 124.00 1.60
Dichlorvos N.D. 1 0.92 0.894 92.00 89.40 2.87
Dimethoate N.D. 1 0.736 0.735 73.60 73.50 0.14
Ethoprophos N.D. 1 0.712 0.756 71.20 75.60 5.99
Etofenprox N.D. 1 0.722 0.736 72.20 73.60 1.92
Etoxazole N.D. 1 0.974 0.94 97.40 94.00 3.55
Fenoxycarb N.D. 1 1.1 1.23 110.00 123.00 11.16
Fenpyroximate N.D. 1 0.837 0.794 83.70 79.40 5.27
Fipronil N.D. 1 1.21 1.13 121.00 113.00 6.84
Flonicamid N.D. 1 0.794 0.816 79.40 81.60 2.73
Fludioxonil N.D. 1 1.12 1.04 112.00 104.00 7.41
Hexythiazox N.D. 1 0.614 0.754 61.40 75.40 20.47 LRQ
Imazalil N.D. 1 1.28 1.23 128.00 123.00 3.98
Imidacloprid N.D. 1 0.906 0.867 90.60 86.70 4.40
Kresoxim-methyl N.D. 1 1.46 1.54 146.00 154.00 5.33 HR
Malathion N.D. 1 1.14 1.07 114.00 107.00 6.33
Metalaxyl N.D. 1 1.1 1.08 110.00 108.00 1.83
Methiocarb N.D. 1 0.763 0.838 76.30 83.80 9.37
Methomyl N.D. 1 1.17 1.15 117.00 115.00 1.72
MGK-264 N.D. 1 0.799 0.86 79.90 86.00 7.35
Myclobutanil N.D. 1 0.967 1.17 96.70 117.00 19.00
Naled (dibrom) N.D. 1 0.601 0.604 60.10 60.40 0.50 LR
Oxamyl N.D. 1 0.842 0.841 84.20 84.10 0.12
Paclobutrazol N.D. 1 1.26 1.38 126.00 138.00 9.09 HR
Parathion-methyl N.D. 1 1.13 0.901 113.00 90.10 22.55 Q
Permethrins N.D. 1 0.608 0.661 60.80 66.10 8.35 LR
Phosmet N.D. 1 1.19 1.27 119.00 127.00 6.50
Piperonyl butoxide N.D. 1 1.05 1.11 105.00 111.00 5.56
Prallethrin N.D. 1 1.21 1.26 121.00 126.00 4.05
Propiconazole N.D. 1 1.08 1.1 108.00 110.00 1.83
Propoxur N.D. 1 0.974 1.04 97.40 104.00 6.55
Pyrethrin N.D. 0.65 0.737 0.752 113.38 115.69 2.01
Pyridaben N.D. 1 0.775 0.709 77.50 70.90 8.89
SpinosynA N.D. 0.84 1.15 1.16 136.90 138.10 0.87 HR
SpinosynD N.D. 0.16 0.205 0.207 128.13 129.38 0.97
Spiromesifen N.D. 1 0.285 0.291 28.50 29.10 2.08 LR
Spirotetramat N.D. 1 1.21 1.23 121.00 123.00 1.64
Spiroxamine N.D. 1 1.37 1.27 137.00 127.00 7.58 HR
Tebuconazole N.D. 1 1.18 1.36 118.00 136.00 14.17 HR
Thiacloprid N.D. 1 0.917 0.927 91.70 92.70 1.08
Thiamethoxam N.D. 1 1.15 1.11 115.00 111.00 3.54
Trifloxystrobin N.D. 1 0.942 0.932 94.20 93.20 1.07

N.D. = Not Detected

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 30%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (60-120%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 5 of 11

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-004 Test Certificate #: 124468-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Mach 4
License: 030-1009646F7F8
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A401030002C949000000239
Metrc Source Pkg#: 1A401030002C949000000235
Test Conditions

Prepsheet ID#: ORHS200604a
Scale: XS205-OR1
Temp: 21.3 °C
Baro PE: 997.6 hPa
Analyst: HRM
Technician: HRM
Sample ID#: 124468

Lot #: Mach 4 6/2/20 #1
Batch #: 124468
Batch Weight (g): 812.7
Harvest/Process Date: 06/02/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 06/03/2020
Test Date: 06/04/2020
Sample #124468
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
1,2-Dichloroethane 2 1 Pass/<LOD 1,2-Dimethoxyethane 100 5 Pass/<LOD
1,4-dioxane 380 200 Pass/<LOD 1-Butanol 5,000 100 Pass/<LOD
1-Pentanol 5,000 100 Pass/<LOD 1-Propanol 5,000 100 Pass/<LOD
2,2-Dimethylpropane (Neopentane) 5,000 100 Pass/<LOD 2,2-Dimethylbutane (Hexanes) 290 100 Pass/<LOD
2,3-Dimethylbutane (Hexanes) 290 100 Pass/<LOD 2-Butanol 5,000 100 Pass/<LOD
2-Butanone (MEK) 5,000 50 Pass/<LOD 2-Ethoxyethanol 160 40 Pass/<LOD
2-Methylbutane (Isopentane) 5,000 50 Pass/<LOD 2-Methylpentane (Hexanes) 290 50 Pass/<LOD
2-Methylpropane (Isobutane) 5,000 100 Pass/<LOD 2-propanol (Isopropyl Alcohol) 5,000 50 Pass/<LOD
2-Propanone (Acetone) 5,000 50 Pass/<LOD 3-Methylpentane (Hexanes) 290 50 Pass/<LOD
Acetonitrile 410 100 Pass/<LOD Benzene 2 1 Pass/<LOD
Butane 5,000 100 Pass/<LOD Chloroform 2 1 Pass/<LOD
Cumene 70 50 Pass/<LOD Cyclohexane 3,880 1,000 Pass/<LOD
Dichloromethane 600 50 Pass/<LOD Dimethylsulfoxide (DMSO) 5,000 500 Pass/<LOD
Ethanol 5,000 500 Pass/<LOD Ethyl acetate 5,000 50 Pass/<LOD
Ethyl ether 5,000 500 Pass/<LOD Ethylene glycol 620 310 Pass/<LOD
Ethylene oxide 50 50 Pass/<LOD Heptane 5,000 50 Pass/<LOD
Hexane 290 290 Pass/<LOD Isopropyl acetate 5,000 50 Pass/<LOD
Methanol 3,000 500 Pass/<LOD Naptha 400 100 Pass/<LOD
N,N-Dimethylacetamide 1,090 100 Pass/<LOD N,N-Dimethylformamide (DMF) 880 500 Pass/<LOD
Pentane 5,000 50 Pass/<LOD Petroleum Ether 400 100 Pass/<LOD
Propane 5,000 100 Pass/<LOD Pyridine 200 10 Pass/<LOD
Sulfolane 160 200 Pass/<LOD Tetrahydrofuran (THF) 720 200 Pass/<LOD
Toluene 890 50 Pass/<LOD Trichloroethylene 25 5 Pass/<LOD
Xylenes* 2,170 50 Pass/<LOD

Total Butanes = 0 ug/g (PASS); Total Pentanes = 0 ug/g (PASS); Total Hexanes = 0 ug/g (PASS)

* Xylenes are reported as the sum of o-xylene, m-xylene, p-xylene, and ethylbenzene
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 6 of 11

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents QC Report
Testing Accreditation #: 4092-004 Test Certificate #: 124468-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Mach 4
License: 030-1009646F7F8
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A401030002C949000000239
Metrc Source Pkg#: 1A401030002C949000000235
Test Conditions

Prepsheet ID#: ORHS200604a
Scale: XS205-OR1
Temp: 21.3 °C
Baro PE: 997.6 hPa
Analyst: HRM
Technician: HRM
Sample ID#: 124468

Lot #: Mach 4 6/2/20 #1
Batch #: 124468
Batch Weight (g): 812.7
Harvest/Process Date: 06/02/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 06/03/2020
Test Date: 06/04/2020
Sample #124468
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS Recovery (%) MSD Recovery (%) Relative Percent Difference (%) QC Flag
1,2-Dichloroethane N.D. 0 0 0 nan nan
n-Propane N.D. 250 155 179 62.00 71.60 14.37 LR
Isobutane N.D. 250 165 176 66.00 70.40 6.45 LR
Methanol N.D. 250 177 179 70.80 71.60 1.12
n-Butane N.D. 250 176 177 70.40 70.80 0.57
2,2-Dimethylpropane N.D. 250 101 151 40.40 60.40 39.68 LRQ
Ethanol N.D. 250 189 214 75.60 85.60 12.41
Isopentane N.D. 250 114 200 45.60 80.00 54.78 LRQ
Acetonitrile N.D. 250 209 212 83.60 84.80 1.43
Diethyl ether N.D. 250 193 204 77.20 81.60 5.54
2-propanone N.D. 250 231 221 92.40 88.40 4.42
2-propanol N.D. 250 196 233 78.40 93.20 17.25
n-Pentane 87.38 250 54 -33 21.60 -13.20 828.57 LRQ
2,2-Dimethylbutane N.D. 250 129 128 51.60 51.20 0.78 LR
2,3-Dimethylbutane N.D. 250 198 252 79.20 100.80 24.00 Q
Methylene chloride N.D. 250 170 166 68.00 66.40 2.38 LR
2-Methylpentane N.D. 250 134 132 53.60 52.80 1.50 LR
3-Methylpentane N.D. 250 137 140 54.80 56.00 2.17 LR
2-Butanol N.D. 250 216 239 86.40 95.60 10.11
n-Hexane N.D. 250 156 169 62.40 67.60 8.00 LR
Ethyl acetate N.D. 250 184 192 73.60 76.80 4.26
Tetrahydrofuran N.D. 250 171 177 0.00 0.00 0.00 LR
Trichloroethylene N.D. 0 0 0 nan nan
Isopropyl acetate N.D. 250 182 183 0.00 0.00 0.00
Benzene N.D. 250 181 185 72.40 74.00 2.19
Chloroform N.D. 0 0 0 nan nan
Cyclohexane N.D. 250 154 152 61.60 60.80 1.31 LR
Ethylene glycol N.D. 250 203 190 81.20 76.00 6.62
Heptane N.D. 250 148 150 59.20 60.00 1.34 LR
2-Ethoxyethanol N.D. 250 224 229 89.60 91.60 2.21
1,4-Dioxane N.D. 250 180 183 72.00 73.20 1.65
Pyridine N.D. 0 0 0 0.00 0.00 0.00
Toluene N.D. 250 179 185 71.60 74.00 3.30
Chlorobenzene N.D. 0 0 0 0.00 0.00 0.00
Ethylbenzene N.D. 250 181 213 72.40 85.20 16.24
m-Xylene/p-Xylene N.D. 500 453 470 90.60 94.00 3.68
o-Xylene N.D. 250 221 202 88.40 80.80 8.98
Cumene N.D. 250 185 185 74.00 74.00 0.00
Ethylene oxide N.D. 250 176 176 70.40 70.40 0.00

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

N.D. = Not Detected

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 7 of 11

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-004 Test Certificate #: 124468-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Mach 4
License: 030-1009646F7F8
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A401030002C949000000239
Metrc Source Pkg#: 1A401030002C949000000235
Test Conditions

Prepsheet ID#: ORHS200604a
Scale: XS205-OR1
Temp: 21.3 °C
Baro PE: 997.6 hPa
Analyst: HRM
Technician: HRM
Sample ID#: 124468

Lot #: Mach 4 6/2/20 #1
Batch #: 124468
Batch Weight (g): 812.7
Harvest/Process Date: 06/02/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 06/03/2020
Test Date: 06/04/2020
Sample #124468
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
1,2-Dichloroethane 2 1 Pass/<LOD 1,2-Dimethoxyethane 100 5 Pass/<LOD
1,4-dioxane 380 200 Pass/<LOD 1-Butanol 5,000 100 Pass/<LOD
1-Pentanol 5,000 100 Pass/<LOD 1-Propanol 5,000 100 Pass/<LOD
2,2-Dimethylpropane (Neopentane) 5,000 100 Pass/<LOD 2,2-Dimethylbutane (Hexanes) 290 100 Pass/<LOD
2,3-Dimethylbutane (Hexanes) 290 100 Pass/<LOD 2-Butanol 5,000 100 Pass/<LOD
2-Butanone (MEK) 5,000 50 Pass/<LOD 2-Ethoxyethanol 160 40 Pass/<LOD
2-Methylbutane (Isopentane) 5,000 50 Pass/<LOD 2-Methylpentane (Hexanes) 290 50 Pass/<LOD
2-Methylpropane (Isobutane) 5,000 100 Pass/<LOD 2-propanol (Isopropyl Alcohol) 5,000 50 Pass/50
2-Propanone (Acetone) 5,000 50 Pass/<LOD 3-Methylpentane (Hexanes) 290 50 Pass/<LOD
Acetonitrile 410 100 Pass/<LOD Benzene 2 1 Pass/<LOD
Butane 5,000 100 Pass/<LOD Chloroform 2 1 Pass/<LOD
Cumene 70 50 Pass/<LOD Cyclohexane 3,880 1,000 Pass/<LOD
Dichloromethane 600 50 Pass/<LOD Dimethylsulfoxide (DMSO) 5,000 500 Pass/<LOD
Ethanol 5,000 500 Pass/<LOD Ethyl acetate 5,000 50 Pass/<LOD
Ethyl ether 5,000 500 Pass/<LOD Ethylene glycol 620 310 Pass/<LOD
Ethylene oxide 50 50 Pass/<LOD Heptane 5,000 50 Pass/<LOD
Hexane 290 290 Pass/<LOD Isopropyl acetate 5,000 50 Pass/<LOD
Methanol 3,000 500 Pass/<LOD Naptha 400 100 Pass/<LOD
N,N-Dimethylacetamide 1,090 100 Pass/<LOD N,N-Dimethylformamide (DMF) 880 500 Pass/<LOD
Pentane 5,000 50 Pass/<LOD Petroleum Ether 400 100 Pass/<LOD
Propane 5,000 100 Pass/<LOD Pyridine 200 10 Pass/<LOD
Sulfolane 160 200 Pass/<LOD Tetrahydrofuran (THF) 720 200 Pass/<LOD
Toluene 890 50 Pass/<LOD Trichloroethylene 25 5 Pass/<LOD
Xylenes* 2,170 50 Pass/<LOD

Total Butanes = 0 ug/g (PASS); Total Pentanes = 0 ug/g (PASS); Total Hexanes = 0 ug/g (PASS)

* Xylenes are reported as the sum of o-xylene, m-xylene, p-xylene, and ethylbenzene
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 8 of 11

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents QC Report
Testing Accreditation #: 4092-004 Test Certificate #: 124468-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Mach 4
License: 030-1009646F7F8
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A401030002C949000000239
Metrc Source Pkg#: 1A401030002C949000000235
Test Conditions

Prepsheet ID#: ORHS200604a
Scale: XS205-OR1
Temp: 21.3 °C
Baro PE: 997.6 hPa
Analyst: HRM
Technician: HRM
Sample ID#: 124468

Lot #: Mach 4 6/2/20 #1
Batch #: 124468
Batch Weight (g): 812.7
Harvest/Process Date: 06/02/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 06/03/2020
Test Date: 06/04/2020
Sample #124468
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS Recovery (%) MSD Recovery (%) Relative Percent Difference (%) QC Flag
1,2-Dichloroethane N.D. 0 0 0 nan nan
n-Propane N.D. 250 155 179 62.00 71.60 14.37 LR
Isobutane N.D. 250 165 176 66.00 70.40 6.45 LR
Methanol N.D. 250 177 179 70.80 71.60 1.12
n-Butane N.D. 250 176 177 70.40 70.80 0.57
2,2-Dimethylpropane N.D. 250 101 151 40.40 60.40 39.68 LRQ
Ethanol N.D. 250 189 214 75.60 85.60 12.41
Isopentane N.D. 250 114 200 45.60 80.00 54.78 LRQ
Acetonitrile N.D. 250 209 212 83.60 84.80 1.43
Diethyl ether N.D. 250 193 204 77.20 81.60 5.54
2-propanone N.D. 250 231 221 92.40 88.40 4.42
2-propanol N.D. 250 196 233 78.40 93.20 17.25
n-Pentane 87.38 250 54 -33 21.60 -13.20 828.57 LRQ
2,2-Dimethylbutane N.D. 250 129 128 51.60 51.20 0.78 LR
2,3-Dimethylbutane N.D. 250 198 252 79.20 100.80 24.00 Q
Methylene chloride N.D. 250 170 166 68.00 66.40 2.38 LR
2-Methylpentane N.D. 250 134 132 53.60 52.80 1.50 LR
3-Methylpentane N.D. 250 137 140 54.80 56.00 2.17 LR
2-Butanol N.D. 250 216 239 86.40 95.60 10.11
n-Hexane N.D. 250 156 169 62.40 67.60 8.00 LR
Ethyl acetate N.D. 250 184 192 73.60 76.80 4.26
Tetrahydrofuran N.D. 250 171 177 0.00 0.00 0.00 LR
Trichloroethylene N.D. 0 0 0 nan nan
Isopropyl acetate N.D. 250 182 183 0.00 0.00 0.00
Benzene N.D. 250 181 185 72.40 74.00 2.19
Chloroform N.D. 0 0 0 nan nan
Cyclohexane N.D. 250 154 152 61.60 60.80 1.31 LR
Ethylene glycol N.D. 250 203 190 81.20 76.00 6.62
Heptane N.D. 250 148 150 59.20 60.00 1.34 LR
2-Ethoxyethanol N.D. 250 224 229 89.60 91.60 2.21
1,4-Dioxane N.D. 250 180 183 72.00 73.20 1.65
Pyridine N.D. 0 0 0 0.00 0.00 0.00
Toluene N.D. 250 179 185 71.60 74.00 3.30
Chlorobenzene N.D. 0 0 0 0.00 0.00 0.00
Ethylbenzene N.D. 250 181 213 72.40 85.20 16.24
m-Xylene/p-Xylene N.D. 500 453 470 90.60 94.00 3.68
o-Xylene N.D. 250 221 202 88.40 80.80 8.98
Cumene N.D. 250 185 185 74.00 74.00 0.00
Ethylene oxide N.D. 250 176 176 70.40 70.40 0.00

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

N.D. = Not Detected

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 9 of 11

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Homogeneity Report by
High Performance Liquid Chromatography
Testing Accreditation #: 4092-004 Test Certificate #: 124468-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Mach 4
License: 030-1009646F7F8
Type: AU Tincture
Metrc Test Pkg#: 1A401030002C949000000239
Metrc Source Pkg#: 1A401030002C949000000235
Sample ID#: 124468

Lot #: Mach 4 6/2/20 #1
Batch #: 124468
Batch Weight (g): 812.7
Harvest/Process Date: 06/02/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 06/03/2020
Sample #124468
Increments Tested (mg/g) TOTAL THC TOTAL CBD THC THCA THCV CBD CBC CBDA CBDV CBG CBN
Increment 1 701.56 16.75 97.25 689.07 N.D. N.D. 2.16 19.10 N.D. 4.74 2.63
Increment 2 778.84 17.58 101.28 772.59 N.D. N.D. 2.31 20.04 N.D. 5.57 2.93
Average Value 740.20 17.16 99.27 730.83 N.D. N.D. 2.24 19.57 N.D. 5.16 2.78
Max Value 778.84 17.58 101.28 772.59 N.D. N.D. 2.31 20.04 N.D. 5.57 2.93
Min Value 701.56 16.75 97.25 689.07 N.D. N.D. 2.16 19.10 N.D. 4.74 2.63
Relative Percent Difference (RPD) ±10.44 ±4.80 ±4.06 ±11.43 N.D. N.D. ±6.71 ±4.80 N.D. ±16.10 ±10.79
Average Cannabinoids Per Package 740.20 17.16 99.27 730.83 N.D. N.D. 2.24 19.57 N.D. 5.16 2.78
Average Cannabinoids Per Serving 37.01 0.86 4.96 36.54 N.D. N.D. 0.11 0.98 N.D. 0.26 0.14
Max Concentration Per Serving (THC)   Pass
Max Concentration Per Package (THC)   Pass
Relative Percent Difference (RPD)   Pass
Control Study   Yes, MJ1957
Field Duplicate   Pass

N.D. = Not Detected, Min = Minimum, Max = Maximum

RPD is the relative percent difference between increment 1 and increment 2.

RSD is the relative standard deviation between all increments tested.

Total THC and CBD is the calculated sum of CBD or THC and the amount of CBD or THC derived from CBDA or THCA, respectively. These values are calculated by adding a molar correction factor of 0.877 to the CBDA or THCA value.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

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IRON Laboratories

Terpene Report by
Mass Spectrometer
Test Certificate #: 124468-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Mach 4
License: 030-1009646F7F8
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A401030002C949000000239
Metrc Source Pkg#: 1A401030002C949000000235

Test Conditions

Scale: XS205-OR1
Temp: 21.3 °C
Baro Pressure: 997.6 hPa
Analyst: HRM
Technician: HRM

Sample ID#: 124468

Lot #: Mach 4 6/2/20 #1
Batch #: 124468
Batch Weight (g): 812.7
Harvest/Process Date: 06/02/2020
Serving Size (g): 0.05
Date Received: 06/03/2020

Sample #124468
Sample #124468
  • α-Pinene (0.04%)
  • β-Ocimene (0.07%)
  • Camphene (0.00%)
  • Eucalyptol (1,8-Cineol) (0.00%)
  • Sabinene (0.00%)
  • γ-Terpinene (0.00%)
  • Myrcene (0.41%)
  • α-Terpinolene (0.51%)
  • β-Pinene (0.48%)
  • Linalool (0.47%)
  • ∆3-Carene (0.00%)
  • Fenchone (0.00%)
  • α-Terpinene (0.03%)
  • endo-Fenchol (0.00%)
  • α-Ocimene (0.00%)
  • Isopulegol (0.00%)
  • Limonene (0.35%)
  • Geraniol (0.03%)
  • p-Cymene (0.00%)
  • β-Caryophyllene (1.45%)
  • α-Humulene (0.73%)
  • Nerolidol 1 (cis) (0.00%)
  • Nerolidol 2 (trans) (0.03%)
  • Guaiol (0.00%)
  • Caryophyllene Oxide (0.08%)
  • α-Bisabolol (0.05%)
  • α-Phellandrene (0.24%)
  • α-Terpineol (0.10%)
  • Valenence (0.00%)

Total: 5.070%

Predominant Terpenes

1.45%   β-Caryophyllene Sweet, woody, spicy, clove 0.73%   α-Humulene Woody, oceanic-watery, spicy clove
0.51%   α-Terpinolene Fresh wood, sweet, pine, citrus 0.48%   β-Pinene Woody, fresh pine, hay
0.47%   Linalool Citrus, floral, sweet, bois de rose, woody, green, blueberry 0.41%   Myrcene Peppery, spicy balsam

Value in parenthesis indicates percentage of terpene present in the total sample (weight percentage, wt/wt%).
Value in doughnut slice indicates individual terpene abundance with respect to the total terpenes detected.

This sample has not been tested according to OAR 333-007. These results should therefore be used for research and development or quality control purposes only.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 11 of 11