ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Marijuana Potency Analysis by
High Performance Liquid Chromatography

Testing Accreditation #: 4092-004 Test Certificate #: 124369-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Terpee Slurpee
License: 030-1009646F7F8
Type: Extract
Method: FE04U HPLC-UV
Metrc Test Pkg#: 1A401030002C949000000174
Metrc Source Pkg#: 1A401030002C949000000166

Test Conditions

Prepsheet ID#: ORP200601B
Scale: XS205-OR1
Temp: 22.2 °C
Baro Pressure: 1005 hPa
Analyst: HRM
Technician: TMR

Sample ID#: 124369

Lot #: Terpee Slurpee 5/29/20 #1
Batch #: 124369
Batch Weight (g): 1135.5
Harvest/Process Date: 05/29/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 05/29/2020
Test Date: 06/01/2020

Sample #124369
Sample #124369 Sample #124369
Test
Compounds
THC THCA CBD CBDA CBN CBG CBC THCV* CBDV Total
Cannabinoids*
Total THC Total CBD Calc Max Total
Cannabinoids*
Amount (%) 4.05 78.30 N/D 1.29 0.36 0.41 N/D N/D N/D 84.41 72.72 1.13 74.62
Amount (mg/g) 40.51 782.98 N/D 12.89 3.61 4.07 N/D N/D N/D 844.06 727.18 11.30 746.16
Amount per Serving (mg) 2.03 39.15 N\D 0.64 0.18 0.20 N\D N\D N\D 42.20 Serving Size~ (g): 0.05
LOQ (mg/g) 1.7 1.7 1.7 1.7 1.7 1.7 1.7 1.7 1.7   %Decarb. THC CBD
±%RPD 5.26 3.66 2.36 2.85 4.06 2.23 7.20 1.80 3.37 5 0

LOQ = Limit of Quantitation; %RPD = Relative Percent Deviation; %RSD = Relative Standard Deviation; N/D = Not Detected

*Designates values that are not currently included in the accredited scope of Iron Laboratories.

*** Designates tests that use the method FE-45. FE-45 is performed using AOAC 966.02 and 32.004-32.009. FE-45 has relative expanded (k=2) uncertainties of 1.098% for moisture, 1.754% for water activity for unprocessed plant materials, and 13.102% for water activity for infused products. Vitamin E acetate analysis has a relative expanded (k=2) uncertainty of 18.614%.

Total THC and CBD is the calculated sum of THC or CBD and the amount of THC or CBD derived from THCA or CBDA, respectively. These values are calculated by applying a molar correction factor of 0.877 to the THCA or the CBDA value. Calc Max Total Cannabinoids is the sum of Total THC, Total CBD, CBN, CBG, CBC, THCV, and CBDV.

%Decarb. THC and CBD refer to the percentage of THC or CBD relative to THCA or CBDA, respectively.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 1 of 11

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant QC Report

Testing Accreditation #: 4092-004 Test Certificate #: 124369-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Terpee Slurpee
License: 030-1009646F7F8
Type: Extract
Method: FE04U HPLC-UV
Metrc Test Pkg#: 1A401030002C949000000174
Metrc Source Pkg#: 1A401030002C949000000166

Test Conditions

Prepsheet ID#: ORP200601B
Scale: XS205-OR1
Temp: 22.2 °C
Baro Pressure: 1005 hPa
Analyst: HRM
Technician: TMR

Sample ID#: 124369

Lot #: Terpee Slurpee 5/29/20 #1
Batch #: 124369
Batch Weight (g): 1135.5
Harvest/Process Date: 05/29/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 05/29/2020
Test Date: 06/01/2020

Sample #124369
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Cannabidivarin (CBDV) N.D. 5.55 5.55 100.00 5.74 103.42 3.37
Cannabidiolic Acid (CBDA) N.D. 5.41 5.54 102.40 5.7 105.36 2.85
Cannabigerol (CBG) N.D. 5.65 5.77 102.12 5.9 104.42 2.23
Cannabidiol (CBD) N.D. 5.75 5.86 101.91 6 104.35 2.36
Δ9-Tetrahydrocannabivarin (THCV) N.D. 5.55 5.5 99.10 5.6 100.90 1.80
Cannabinol (CBN) N.D. 5.41 5.31 98.15 5.53 102.22 4.06
Δ9-Tetrahydrocannabinol (THC) N.D. 5.82 5.55 95.36 5.85 100.52 5.26
Cannabichromene (CBC) N.D. 7.64 6.76 88.48 6.29 82.33 7.20
Tetrahydrocannabinolic acid (THCA) N.D. 5.21 5.09 97.70 5.28 101.34 3.66

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 2 of 11

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Pesticide Analysis by
Mass Spectrometer

Testing Accreditation #: 4092-004 Test Certificate #: 124369-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Terpee Slurpee
License: 030-1009646F7F8
Type: Extract
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A401030002C949000000174
Metrc Source Pkg#: 1A401030002C949000000166

Test Conditions

Prepsheet ID#: ORPS200601a
Scale: 1129293203
Temp: 20.9 °C
Baro PE: 1010 hPa
Analyst: HRM
Technician: HRM/EDT

Sample ID#: 124369

Lot #: Terpee Slurpee 5/29/20 #1
Batch #: 124369
Batch Weight (g): 1135.5
Harvest/Process Date: 05/29/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 05/29/2020
Test Date: 06/01/2020

Sample #124369
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
Aldicarb 0.400 0.123 Pass/<LOD Abamectin**** 0.500 0.123 Pass/<LOD
Acephate 0.400 0.123 Pass/<LOD Acequinocyl 2.000 0.246 Pass/<LOD
Acetamiprid 0.200 0.123 Pass/<LOD Azoxystrobin 0.200 0.123 Pass/<LOD
Bifenazate 0.200 0.123 Pass/<LOD Bifenthrin 0.200 0.123 Pass/<LOD
Boscalid 0.400 0.123 Pass/<LOD Carbaryl 0.200 0.123 Pass/<LOD
Carbofuran 0.200 0.123 Pass/<LOD Chlorantraniliprole 0.200 0.123 Pass/<LOD
Chlorfenapyr 1.000 0.493 Pass/<LOD Chlorpyrifos 0.200 0.123 Pass/<LOD
Clofentezine 0.200 0.123 Pass/<LOD Cyfluthrin** 1.000 0.493 Pass/<LOD
Cypermethrin*** 1.000 0.493 Pass/<LOD Daminozide 1.000 0.123 Pass/<LOD
DDVP (Dichlorvos) 1.000 0.246 Pass/<LOD Diazinon 0.200 0.123 Pass/<LOD
Dimethoate 0.200 0.123 Pass/<LOD Ethoprophos 0.200 0.123 Pass/<LOD
Etofenprox 0.400 0.123 Pass/<LOD Etoxazole 0.200 0.123 Pass/<LOD
Fenoxycarb 0.200 0.123 Pass/<LOD Fenpyroximate 0.400 0.123 Pass/<LOD
Fipronil 0.400 0.123 Pass/<LOD Flonicamid 1.000 0.123 Pass/<LOD
Fludioxonil 0.400 0.123 Pass/<LOD Hexythiazox 1.000 0.123 Pass/<LOD
Imazalil 0.200 0.123 Pass/<LOD Imidacloprid 0.400 0.123 Pass/<LOD
Kresoxim Methyl 0.400 0.123 Pass/<LOD Malathion 0.200 0.123 Pass/<LOD
Metalaxyl 0.200 0.123 Pass/<LOD Methiocarb 0.200 0.123 Pass/<LOD
Methomyl 0.400 0.123 Pass/<LOD Methyl Parathion 0.200 0.123 Pass/<LOD
MGK-264‡ 0.200 0.123 Pass/<LOD Myclobutanil 0.000 0.123 Pass/<LOD
Naled 0.500 0.123 Pass/<LOD Oxamyl 1.000 0.123 Pass/<LOD
Paclobutrazol 0.400 0.123 Pass/<LOD Permethrins† 0.200 0.123 Pass/<LOD
Phosmet 0.200 0.123 Pass/<LOD Piperonyl Butoxide 2.000 0.123 Pass/<LOD
Prallethrin 0.200 0.123 Pass/<LOD Propiconazole 0.400 0.123 Pass/<LOD
Propoxur 0.200 0.123 Pass/<LOD Pyrethrins* 1.000 0.123 Pass/<LOD
Pyridaben 0.200 0.123 Pass/<LOD Spinosad***** 0.200 0.123 Pass/<LOD
Spiromesifen 0.200 0.123 Pass/<LOD Spirotetramat 0.200 0.123 Pass/<LOD
Spiroxamine‡ 0.400 0.123 Pass/<LOD Tebuconazole 0.400 0.123 Pass/<LOD
Thiacloprid 0.200 0.123 Pass/<LOD Thiamethoxam 0.200 0.123 Pass/<LOD
Trifloxystrobin 0.200 0.123 Pass/<LOD

* Pyrethrins are reported as the sum of Jasmolin I, Cinerin I, and Pyrethrin I
** Cyfluthrins are reported as the sum of isomers Cyfluthrin I, II, III, and IV
*** Cypermethrins are reported as the sum of isomers Cypermethrin I, II, III, and IV
**** Abamectin is reported as the sum of Avermectin B1a and Avermectin B1b
***** Spinosad is reported as the sum of Spinosyn A and Spinosyn D
† Permethrin and Prallethrin are reported as the sum of cis and trans isomers
‡ MGK-264 and Spiroximine are reported as the sum of isomers I and II
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 2 of 11

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Pesticide QC Report

Testing Accreditation #: 4092-004 Test Certificate #: 124369-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Terpee Slurpee
License: 030-1009646F7F8
Type: Extract
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A401030002C949000000174
Metrc Source Pkg#: 1A401030002C949000000166

Test Conditions

Prepsheet ID#: ORPS200601a
Scale: 1129293203
Temp: 20.9 °C
Baro PE: 1010 hPa
Analyst: HRM
Technician: HRM/EDT

Sample ID#: 124369

Lot #: Terpee Slurpee 5/29/20 #1
Batch #: 124369
Batch Weight (g): 1135.5
Harvest/Process Date: 05/29/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 05/29/2020
Test Date: 06/01/2020

Sample #124369
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS recovery% MSD recovery% Relative Percent Difference (%) QC Flag
Acephate N.D. 1 1.12 0.99 112.00 99.00 12.32
Acequinocyl N.D. 1 0.404 0.576 40.40 57.60 35.10 LR LR Q
Acetamiprid N.D. 1 0.953 0.893 95.30 89.30 6.50
Aldicarb N.D. 1 0.83 0.785 83.00 78.50 5.57
Avermectin B1a N.D. 0.97 1.43 1.07 147.42 110.31 28.80 HR Q
Azoxystrobin N.D. 1 0.97 0.923 97.00 92.30 4.97
Bifenazate N.D. 1 0.534 0.449 53.40 44.90 17.29 LR
Bifenthrin N.D. 1 0.734 0.798 73.40 79.80 8.36
Boscalid N.D. 1 1.01 0.936 101.00 93.60 7.61
Carbaryl N.D. 1 1.18 0.85 118.00 85.00 32.51 Q
Carbofuran N.D. 1 0.947 0.94 94.70 94.00 0.74
Chlorantraniliprole N.D. 1 1.38 1.25 138.00 125.00 9.89 HR
Chlorfenapyr N.D. 1 0.586 0.835 58.60 83.50 35.05 LR Q
Chlorpyriphos N.D. 1 0.73 0.876 73.00 87.60 18.18
Clofentezine N.D. 1 0.54 0.0224 54.00 2.24 184.07 LRQ
Cyfluthrin N.D. 1 0.888 0.991 88.80 99.10 10.96
Cypermethrin N.D. 1 0.841 1.08 84.10 108.00 24.88 Q
Daminoside N.D. 1 2.17 1.74 217.00 174.00 21.99 HRQ
Diazanon N.D. 1 1.33 1.27 133.00 127.00 4.62 HR
Dichlorvos N.D. 1 0.977 0.746 97.70 74.60 26.81 Q
Dimethoate N.D. 1 0.901 0.809 90.10 80.90 10.76
Ethoprophos N.D. 1 0.863 0.921 86.30 92.10 6.50
Etofenprox N.D. 1 0.859 0.816 85.90 81.60 5.13
Etoxazole N.D. 1 0.997 0.966 99.70 96.60 3.16
Fenoxycarb N.D. 1 1.18 1.18 118.00 118.00 0.00
Fenpyroximate N.D. 1 1.03 0.974 103.00 97.40 5.59
Fipronil N.D. 1 0.998 1.02 99.80 102.00 2.18
Flonicamid N.D. 1 0.941 0.883 94.10 88.30 6.36
Fludioxonil N.D. 1 0.923 0.923 92.30 92.30 0.00
Hexythiazox N.D. 1 0.618 0.748 61.80 74.80 19.03 LR
Imazalil N.D. 1 1.36 1.07 136.00 107.00 23.87 HR Q
Imidacloprid N.D. 1 0.946 0.956 94.60 95.60 1.05
Kresoxim-methyl N.D. 1 1.39 1.32 139.00 132.00 5.17 HR
Malathion N.D. 1 0.941 1.16 94.10 116.00 20.85 Q
Metalaxyl N.D. 1 1.17 1.26 117.00 126.00 7.41
Methiocarb N.D. 1 0.947 0.862 94.70 86.20 9.40
Methomyl N.D. 1 1.06 1.07 106.00 107.00 0.94
MGK-264 N.D. 1 0.641 0.846 64.10 84.60 27.57 LR Q
Myclobutanil N.D. 1 1.26 1.25 126.00 125.00 0.80
Naled (dibrom) N.D. 1 0.603 0.551 60.30 55.10 9.01 LR
Oxamyl N.D. 1 0.971 0.839 97.10 83.90 14.59
Paclobutrazol N.D. 1 1.49 1.3 149.00 130.00 13.62 HR
Parathion-methyl N.D. 1 0.919 1.02 91.90 102.00 10.42
Permethrins N.D. 1 0.687 0.792 68.70 79.20 14.20 LR Q
Phosmet N.D. 1 1.09 1.17 109.00 117.00 7.08
Piperonyl butoxide N.D. 1 1.18 0.918 118.00 91.80 24.98 Q
Prallethrin N.D. 1 1.02 1.11 102.00 111.00 8.45
Propiconazole N.D. 1 1.24 1.08 124.00 108.00 13.79
Propoxur N.D. 1 0.977 0.854 97.70 85.40 13.44
Pyrethrin N.D. 0.65 0.634 0.704 97.54 108.31 10.46
Pyridaben N.D. 1 0.841 0.852 84.10 85.20 1.30
SpinosynA N.D. 0.84 0.961 0.885 114.40 105.36 8.23
SpinosynD N.D. 0.16 0.157 0.18 98.13 112.50 13.65
Spiromesifen N.D. 1 0.303 0.358 30.30 35.80 16.64 LR
Spirotetramat N.D. 1 1.45 1.13 145.00 113.00 24.81 HR Q
Spiroxamine N.D. 1 1.31 1.2 131.00 120.00 8.76 HR
Tebuconazole N.D. 1 1.58 1.39 158.00 139.00 12.79 HR
Thiacloprid N.D. 1 1.06 1.06 106.00 106.00 0.00
Thiamethoxam N.D. 1 1.29 1.19 129.00 119.00 8.06
Trifloxystrobin N.D. 1 1.02 0.973 102.00 97.30 4.72

N.D. = Not Detected

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 30%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (60-120%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 3 of 11

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Pesticide Analysis by
Mass Spectrometer

Testing Accreditation #: 4092-004 Test Certificate #: 124369-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Terpee Slurpee
License: 030-1009646F7F8
Type: Extract
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A401030002C949000000174
Metrc Source Pkg#: 1A401030002C949000000166

Test Conditions

Prepsheet ID#: ORPS200601a
Scale: 1129293203
Temp: 20.9 °C
Baro PE: 1010 hPa
Analyst: HRM
Technician: HRM/EDT

Sample ID#: 124369

Lot #: Terpee Slurpee 5/29/20 #1
Batch #: 124369
Batch Weight (g): 1135.5
Harvest/Process Date: 05/29/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 05/29/2020
Test Date: 06/01/2020

Sample #124369
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
Aldicarb 0.400 0.126 Pass/<LOD Abamectin**** 0.500 0.126 Pass/<LOD
Acephate 0.400 0.126 Pass/<LOD Acequinocyl 2.000 0.252 Pass/<LOD
Acetamiprid 0.200 0.126 Pass/<LOD Azoxystrobin 0.200 0.126 Pass/<LOD
Bifenazate 0.200 0.126 Pass/<LOD Bifenthrin 0.200 0.126 Pass/<LOD
Boscalid 0.400 0.126 Pass/<LOD Carbaryl 0.200 0.126 Pass/<LOD
Carbofuran 0.200 0.126 Pass/<LOD Chlorantraniliprole 0.200 0.126 Pass/<LOD
Chlorfenapyr 1.000 0.503 Pass/<LOD Chlorpyrifos 0.200 0.126 Pass/<LOD
Clofentezine 0.200 0.126 Pass/<LOD Cyfluthrin** 1.000 0.503 Pass/<LOD
Cypermethrin*** 1.000 0.503 Pass/<LOD Daminozide 1.000 0.126 Pass/<LOD
DDVP (Dichlorvos) 1.000 0.252 Pass/<LOD Diazinon 0.200 0.126 Pass/<LOD
Dimethoate 0.200 0.126 Pass/<LOD Ethoprophos 0.200 0.126 Pass/<LOD
Etofenprox 0.400 0.126 Pass/<LOD Etoxazole 0.200 0.126 Pass/<LOD
Fenoxycarb 0.200 0.126 Pass/<LOD Fenpyroximate 0.400 0.126 Pass/<LOD
Fipronil 0.400 0.126 Pass/<LOD Flonicamid 1.000 0.126 Pass/<LOD
Fludioxonil 0.400 0.126 Pass/<LOD Hexythiazox 1.000 0.126 Pass/<LOD
Imazalil 0.200 0.126 Pass/<LOD Imidacloprid 0.400 0.126 Pass/<LOD
Kresoxim Methyl 0.400 0.126 Pass/<LOD Malathion 0.200 0.126 Pass/<LOD
Metalaxyl 0.200 0.126 Pass/<LOD Methiocarb 0.200 0.126 Pass/<LOD
Methomyl 0.400 0.126 Pass/<LOD Methyl Parathion 0.200 0.126 Pass/<LOD
MGK-264‡ 0.200 0.126 Pass/<LOD Myclobutanil 0.000 0.126 Pass/<LOD
Naled 0.500 0.126 Pass/<LOD Oxamyl 1.000 0.126 Pass/<LOD
Paclobutrazol 0.400 0.126 Pass/<LOD Permethrins† 0.200 0.126 Pass/<LOD
Phosmet 0.200 0.126 Pass/<LOD Piperonyl Butoxide 2.000 0.126 Pass/<LOD
Prallethrin 0.200 0.126 Pass/<LOD Propiconazole 0.400 0.126 Pass/<LOD
Propoxur 0.200 0.126 Pass/<LOD Pyrethrins* 1.000 0.126 Pass/<LOD
Pyridaben 0.200 0.126 Pass/<LOD Spinosad***** 0.200 0.126 Pass/<LOD
Spiromesifen 0.200 0.126 Pass/<LOD Spirotetramat 0.200 0.126 Pass/<LOD
Spiroxamine‡ 0.400 0.126 Pass/<LOD Tebuconazole 0.400 0.126 Pass/<LOD
Thiacloprid 0.200 0.126 Pass/<LOD Thiamethoxam 0.200 0.126 Pass/<LOD
Trifloxystrobin 0.200 0.126 Pass/<LOD

* Pyrethrins are reported as the sum of Jasmolin I, Cinerin I, and Pyrethrin I
** Cyfluthrins are reported as the sum of isomers Cyfluthrin I, II, III, and IV
*** Cypermethrins are reported as the sum of isomers Cypermethrin I, II, III, and IV
**** Abamectin is reported as the sum of Avermectin B1a and Avermectin B1b
***** Spinosad is reported as the sum of Spinosyn A and Spinosyn D
† Permethrin and Prallethrin are reported as the sum of cis and trans isomers
‡ MGK-264 and Spiroximine are reported as the sum of isomers I and II
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 4 of 11

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Pesticide QC Report

Testing Accreditation #: 4092-004 Test Certificate #: 124369-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Terpee Slurpee
License: 030-1009646F7F8
Type: Extract
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A401030002C949000000174
Metrc Source Pkg#: 1A401030002C949000000166

Test Conditions

Prepsheet ID#: ORPS200601a
Scale: 1129293203
Temp: 20.9 °C
Baro PE: 1010 hPa
Analyst: HRM
Technician: HRM/EDT

Sample ID#: 124369

Lot #: Terpee Slurpee 5/29/20 #1
Batch #: 124369
Batch Weight (g): 1135.5
Harvest/Process Date: 05/29/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 05/29/2020
Test Date: 06/01/2020

Sample #124369
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS recovery% MSD recovery% Relative Percent Difference (%) QC Flag
Acephate N.D. 1 1.12 0.99 112.00 99.00 12.32
Acequinocyl N.D. 1 0.404 0.576 40.40 57.60 35.10 LR LR Q
Acetamiprid N.D. 1 0.953 0.893 95.30 89.30 6.50
Aldicarb N.D. 1 0.83 0.785 83.00 78.50 5.57
Avermectin B1a N.D. 0.97 1.43 1.07 147.42 110.31 28.80 HR Q
Azoxystrobin N.D. 1 0.97 0.923 97.00 92.30 4.97
Bifenazate N.D. 1 0.534 0.449 53.40 44.90 17.29 LR
Bifenthrin N.D. 1 0.734 0.798 73.40 79.80 8.36
Boscalid N.D. 1 1.01 0.936 101.00 93.60 7.61
Carbaryl N.D. 1 1.18 0.85 118.00 85.00 32.51 Q
Carbofuran N.D. 1 0.947 0.94 94.70 94.00 0.74
Chlorantraniliprole N.D. 1 1.38 1.25 138.00 125.00 9.89 HR
Chlorfenapyr N.D. 1 0.586 0.835 58.60 83.50 35.05 LR Q
Chlorpyriphos N.D. 1 0.73 0.876 73.00 87.60 18.18
Clofentezine N.D. 1 0.54 0.0224 54.00 2.24 184.07 LRQ
Cyfluthrin N.D. 1 0.888 0.991 88.80 99.10 10.96
Cypermethrin N.D. 1 0.841 1.08 84.10 108.00 24.88 Q
Daminoside N.D. 1 2.17 1.74 217.00 174.00 21.99 HRQ
Diazanon N.D. 1 1.33 1.27 133.00 127.00 4.62 HR
Dichlorvos N.D. 1 0.977 0.746 97.70 74.60 26.81 Q
Dimethoate N.D. 1 0.901 0.809 90.10 80.90 10.76
Ethoprophos N.D. 1 0.863 0.921 86.30 92.10 6.50
Etofenprox N.D. 1 0.859 0.816 85.90 81.60 5.13
Etoxazole N.D. 1 0.997 0.966 99.70 96.60 3.16
Fenoxycarb N.D. 1 1.18 1.18 118.00 118.00 0.00
Fenpyroximate N.D. 1 1.03 0.974 103.00 97.40 5.59
Fipronil N.D. 1 0.998 1.02 99.80 102.00 2.18
Flonicamid N.D. 1 0.941 0.883 94.10 88.30 6.36
Fludioxonil N.D. 1 0.923 0.923 92.30 92.30 0.00
Hexythiazox N.D. 1 0.618 0.748 61.80 74.80 19.03 LR
Imazalil N.D. 1 1.36 1.07 136.00 107.00 23.87 HR Q
Imidacloprid N.D. 1 0.946 0.956 94.60 95.60 1.05
Kresoxim-methyl N.D. 1 1.39 1.32 139.00 132.00 5.17 HR
Malathion N.D. 1 0.941 1.16 94.10 116.00 20.85 Q
Metalaxyl N.D. 1 1.17 1.26 117.00 126.00 7.41
Methiocarb N.D. 1 0.947 0.862 94.70 86.20 9.40
Methomyl N.D. 1 1.06 1.07 106.00 107.00 0.94
MGK-264 N.D. 1 0.641 0.846 64.10 84.60 27.57 LR Q
Myclobutanil N.D. 1 1.26 1.25 126.00 125.00 0.80
Naled (dibrom) N.D. 1 0.603 0.551 60.30 55.10 9.01 LR
Oxamyl N.D. 1 0.971 0.839 97.10 83.90 14.59
Paclobutrazol N.D. 1 1.49 1.3 149.00 130.00 13.62 HR
Parathion-methyl N.D. 1 0.919 1.02 91.90 102.00 10.42
Permethrins N.D. 1 0.687 0.792 68.70 79.20 14.20 LR Q
Phosmet N.D. 1 1.09 1.17 109.00 117.00 7.08
Piperonyl butoxide N.D. 1 1.18 0.918 118.00 91.80 24.98 Q
Prallethrin N.D. 1 1.02 1.11 102.00 111.00 8.45
Propiconazole N.D. 1 1.24 1.08 124.00 108.00 13.79
Propoxur N.D. 1 0.977 0.854 97.70 85.40 13.44
Pyrethrin N.D. 0.65 0.634 0.704 97.54 108.31 10.46
Pyridaben N.D. 1 0.841 0.852 84.10 85.20 1.30
SpinosynA N.D. 0.84 0.961 0.885 114.40 105.36 8.23
SpinosynD N.D. 0.16 0.157 0.18 98.13 112.50 13.65
Spiromesifen N.D. 1 0.303 0.358 30.30 35.80 16.64 LR
Spirotetramat N.D. 1 1.45 1.13 145.00 113.00 24.81 HR Q
Spiroxamine N.D. 1 1.31 1.2 131.00 120.00 8.76 HR
Tebuconazole N.D. 1 1.58 1.39 158.00 139.00 12.79 HR
Thiacloprid N.D. 1 1.06 1.06 106.00 106.00 0.00
Thiamethoxam N.D. 1 1.29 1.19 129.00 119.00 8.06
Trifloxystrobin N.D. 1 1.02 0.973 102.00 97.30 4.72

N.D. = Not Detected

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 30%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (60-120%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 5 of 11

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents Analysis by
Mass Spectrometer

Testing Accreditation #: 4092-004 Test Certificate #: 124369-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Terpee Slurpee
License: 030-1009646F7F8
Type: Extract
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A401030002C949000000174
Metrc Source Pkg#: 1A401030002C949000000166

Test Conditions

Prepsheet ID#: ORHS200602a
Scale: XS205-OR1
Temp: 22.1 °C
Baro PE: 1012 hPa
Analyst: HRM
Technician: HRM

Sample ID#: 124369

Lot #: Terpee Slurpee 5/29/20 #1
Batch #: 124369
Batch Weight (g): 1135.5
Harvest/Process Date: 05/29/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 05/29/2020
Test Date: 03/02/2020

Sample #124369
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
1,2-Dichloroethane 2 1 Pass/<LOD 1,2-Dimethoxyethane 100 5 Pass/<LOD
1,4-dioxane 380 200 Pass/<LOD 1-Butanol 5,000 100 Pass/<LOD
1-Pentanol 5,000 100 Pass/<LOD 1-Propanol 5,000 100 Pass/<LOD
2,2-Dimethylpropane (Neopentane) 5,000 100 Pass/<LOD 2,2-Dimethylbutane (Hexanes) 290 100 Pass/<LOD
2,3-Dimethylbutane (Hexanes) 290 100 Pass/<LOD 2-Butanol 5,000 100 Pass/<LOD
2-Butanone (MEK) 5,000 50 Pass/<LOD 2-Ethoxyethanol 160 40 Pass/<LOD
2-Methylbutane (Isopentane) 5,000 50 Pass/<LOD 2-Methylpentane (Hexanes) 290 50 Pass/<LOD
2-Methylpropane (Isobutane) 5,000 100 Pass/<LOD 2-propanol (Isopropyl Alcohol) 5,000 50 Pass/51
2-Propanone (Acetone) 5,000 50 Pass/<LOD 3-Methylpentane (Hexanes) 290 50 Pass/<LOD
Acetonitrile 410 100 Pass/<LOD Benzene 2 1 Pass/<LOD
Butane 5,000 100 Pass/<LOD Chloroform 2 1 Pass/<LOD
Cumene 70 50 Pass/<LOD Cyclohexane 3,880 1,000 Pass/<LOD
Dichloromethane 600 50 Pass/<LOD Dimethylsulfoxide (DMSO) 5,000 500 Pass/<LOD
Ethanol 5,000 500 Pass/<LOD Ethyl acetate 5,000 50 Pass/<LOD
Ethyl ether 5,000 500 Pass/<LOD Ethylene glycol 620 310 Pass/<LOD
Ethylene oxide 50 50 Pass/<LOD Heptane 5,000 50 Pass/<LOD
Hexane 290 290 Pass/<LOD Isopropyl acetate 5,000 50 Pass/<LOD
Methanol 3,000 500 Pass/<LOD Naptha 400 100 Pass/<LOD
N,N-Dimethylacetamide 1,090 100 Pass/<LOD N,N-Dimethylformamide (DMF) 880 500 Pass/<LOD
Pentane 5,000 50 Pass/<LOD Petroleum Ether 400 100 Pass/<LOD
Propane 5,000 100 Pass/<LOD Pyridine 200 10 Pass/<LOD
Sulfolane 160 200 Pass/<LOD Tetrahydrofuran (THF) 720 200 Pass/<LOD
Toluene 890 50 Pass/<LOD Trichloroethylene 25 5 Pass/<LOD
Xylenes* 2,170 50 Pass/<LOD

Total Butanes = 56 ug/g (PASS); Total Pentanes = 0 ug/g (PASS); Total Hexanes = 0 ug/g (PASS)

* Xylenes are reported as the sum of o-xylene, m-xylene, p-xylene, and ethylbenzene
MRL - Maximum Residue Limit; LOD - Limit of Detection

This sample has not been tested according to OAR 333-007. These results should therefore be used for research and development or quality control purposes only.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 6 of 11

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents QC Report

Testing Accreditation #: 4092-004 Test Certificate #: 124369-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Terpee Slurpee
License: 030-1009646F7F8
Type: Extract
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A401030002C949000000174
Metrc Source Pkg#: 1A401030002C949000000166

Test Conditions

Prepsheet ID#: ORHS200602a
Scale: XS205-OR1
Temp: 22.1 °C
Baro PE: 1012 hPa
Analyst: HRM
Technician: HRM

Sample ID#: 124369

Lot #: Terpee Slurpee 5/29/20 #1
Batch #: 124369
Batch Weight (g): 1135.5
Harvest/Process Date: 05/29/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 05/29/2020
Test Date: 03/02/2020

Sample #124369
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS Recovery (%) MSD Recovery (%) Relative Percent Difference (%) QC Flag
1,2-Dichloroethane N.D. 0 0 0 nan nan
n-Propane N.D. 250 67 66 26.80 26.40 1.50 LR
Isobutane N.D. 250 97 96 38.80 38.40 1.04 LR
Methanol N.D. 250 168 154 67.20 61.60 8.70 LR
n-Butane N.D. 250 106 108 42.40 43.20 1.87 LR
2,2-Dimethylpropane N.D. 250 118 115 47.20 46.00 2.58 LR
Ethanol N.D. 250 180 178 72.00 71.20 1.12
Isopentane N.D. 250 130 130 52.00 52.00 0.00 LR
Acetonitrile N.D. 250 188 183 75.20 73.20 2.70
Diethyl ether N.D. 250 158 178 63.20 71.20 11.90 LR
2-propanone N.D. 250 183 175 73.20 70.00 4.47 LR
2-propanol N.D. 250 158 184 63.20 73.60 15.20 LR
n-Pentane N.D. 250 216 9 86.40 3.60 184.00 LRQ
2,2-Dimethylbutane N.D. 250 142 141 56.80 56.40 0.71 LR
2,3-Dimethylbutane N.D. 250 147 144 58.80 57.60 2.06 LR
Methylene chloride N.D. 250 168 171 67.20 68.40 1.77 LR
2-Methylpentane N.D. 250 149 144 59.60 57.60 3.41 LR
3-Methylpentane N.D. 250 149 147 59.60 58.80 1.35 LR
2-Butanol N.D. 250 226 224 90.40 89.60 0.89
n-Hexane N.D. 250 178 168 71.20 67.20 5.78 LR
Ethyl acetate N.D. 250 188 188 75.20 75.20 0.00
Tetrahydrofuran N.D. 250 183 177 0.00 0.00 0.00
Trichloroethylene N.D. 0 0 0 nan nan
Isopropyl acetate N.D. 250 176 175 0.00 0.00 0.00 LR
Benzene N.D. 250 185 177 74.00 70.80 4.42
Chloroform N.D. 0 0 0 nan nan
Cyclohexane N.D. 250 158 154 63.20 61.60 2.56 LR
Ethylene glycol N.D. 250 223 217 89.20 86.80 2.73
Heptane N.D. 250 165 149 66.00 59.60 10.19 LR
2-Ethoxyethanol N.D. 250 213 222 85.20 88.80 4.14
1,4-Dioxane N.D. 250 188 182 75.20 72.80 3.24
Pyridine N.D. 0 0 0 0.00 0.00 0.00
Toluene N.D. 250 184 179 73.60 71.60 2.75
Chlorobenzene N.D. 0 0 0 0.00 0.00 0.00
Ethylbenzene N.D. 250 189 180 75.60 72.00 4.88
m-Xylene/p-Xylene N.D. 500 380 359 76.00 71.80 5.68
o-Xylene N.D. 250 188 174 75.20 69.60 7.73 LR
Cumene N.D. 250 191 187 76.40 74.80 2.12
Ethylene oxide N.D. 250 176 171 70.40 68.40 2.88 LR

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

N.D. = Not Detected

This sample has not been tested according to OAR 333-007. These results should therefore be used for research and development or quality control purposes only.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 7 of 11

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents Analysis by
Mass Spectrometer

Testing Accreditation #: 4092-004 Test Certificate #: 124369-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Terpee Slurpee
License: 030-1009646F7F8
Type: Extract
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A401030002C949000000174
Metrc Source Pkg#: 1A401030002C949000000166

Test Conditions

Prepsheet ID#: ORHS200602a
Scale: XS205-OR1
Temp: 22.1 °C
Baro PE: 1012 hPa
Analyst: HRM
Technician: HRM

Sample ID#: 124369

Lot #: Terpee Slurpee 5/29/20 #1
Batch #: 124369
Batch Weight (g): 1135.5
Harvest/Process Date: 05/29/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 05/29/2020
Test Date: 03/02/2020

Sample #124369
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
1,2-Dichloroethane 2 1 Pass/<LOD 1,2-Dimethoxyethane 100 5 Pass/<LOD
1,4-dioxane 380 200 Pass/<LOD 1-Butanol 5,000 100 Pass/<LOD
1-Pentanol 5,000 100 Pass/<LOD 1-Propanol 5,000 100 Pass/<LOD
2,2-Dimethylpropane (Neopentane) 5,000 100 Pass/<LOD 2,2-Dimethylbutane (Hexanes) 290 100 Pass/<LOD
2,3-Dimethylbutane (Hexanes) 290 100 Pass/<LOD 2-Butanol 5,000 100 Pass/<LOD
2-Butanone (MEK) 5,000 50 Pass/<LOD 2-Ethoxyethanol 160 40 Pass/<LOD
2-Methylbutane (Isopentane) 5,000 50 Pass/<LOD 2-Methylpentane (Hexanes) 290 50 Pass/<LOD
2-Methylpropane (Isobutane) 5,000 100 Pass/<LOD 2-propanol (Isopropyl Alcohol) 5,000 50 Pass/<LOD
2-Propanone (Acetone) 5,000 50 Pass/<LOD 3-Methylpentane (Hexanes) 290 50 Pass/<LOD
Acetonitrile 410 100 Pass/<LOD Benzene 2 1 Pass/<LOD
Butane 5,000 100 Pass/<LOD Chloroform 2 1 Pass/<LOD
Cumene 70 50 Pass/<LOD Cyclohexane 3,880 1,000 Pass/<LOD
Dichloromethane 600 50 Pass/<LOD Dimethylsulfoxide (DMSO) 5,000 500 Pass/<LOD
Ethanol 5,000 500 Pass/<LOD Ethyl acetate 5,000 50 Pass/<LOD
Ethyl ether 5,000 500 Pass/<LOD Ethylene glycol 620 310 Pass/<LOD
Ethylene oxide 50 50 Pass/<LOD Heptane 5,000 50 Pass/<LOD
Hexane 290 290 Pass/<LOD Isopropyl acetate 5,000 50 Pass/<LOD
Methanol 3,000 500 Pass/<LOD Naptha 400 100 Pass/<LOD
N,N-Dimethylacetamide 1,090 100 Pass/<LOD N,N-Dimethylformamide (DMF) 880 500 Pass/<LOD
Pentane 5,000 50 Pass/<LOD Petroleum Ether 400 100 Pass/<LOD
Propane 5,000 100 Pass/<LOD Pyridine 200 10 Pass/<LOD
Sulfolane 160 200 Pass/<LOD Tetrahydrofuran (THF) 720 200 Pass/<LOD
Toluene 890 50 Pass/<LOD Trichloroethylene 25 5 Pass/<LOD
Xylenes* 2,170 50 Pass/<LOD

Total Butanes = 66 ug/g (PASS); Total Pentanes = 0 ug/g (PASS); Total Hexanes = 0 ug/g (PASS)

* Xylenes are reported as the sum of o-xylene, m-xylene, p-xylene, and ethylbenzene
MRL - Maximum Residue Limit; LOD - Limit of Detection

This sample has not been tested according to OAR 333-007. These results should therefore be used for research and development or quality control purposes only.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 8 of 11

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents QC Report

Testing Accreditation #: 4092-004 Test Certificate #: 124369-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Terpee Slurpee
License: 030-1009646F7F8
Type: Extract
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A401030002C949000000174
Metrc Source Pkg#: 1A401030002C949000000166

Test Conditions

Prepsheet ID#: ORHS200602a
Scale: XS205-OR1
Temp: 22.1 °C
Baro PE: 1012 hPa
Analyst: HRM
Technician: HRM

Sample ID#: 124369

Lot #: Terpee Slurpee 5/29/20 #1
Batch #: 124369
Batch Weight (g): 1135.5
Harvest/Process Date: 05/29/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 05/29/2020
Test Date: 03/02/2020

Sample #124369
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS Recovery (%) MSD Recovery (%) Relative Percent Difference (%) QC Flag
1,2-Dichloroethane N.D. 0 0 0 nan nan
n-Propane N.D. 250 67 66 26.80 26.40 1.50 LR
Isobutane N.D. 250 97 96 38.80 38.40 1.04 LR
Methanol N.D. 250 168 154 67.20 61.60 8.70 LR
n-Butane N.D. 250 106 108 42.40 43.20 1.87 LR
2,2-Dimethylpropane N.D. 250 118 115 47.20 46.00 2.58 LR
Ethanol N.D. 250 180 178 72.00 71.20 1.12
Isopentane N.D. 250 130 130 52.00 52.00 0.00 LR
Acetonitrile N.D. 250 188 183 75.20 73.20 2.70
Diethyl ether N.D. 250 158 178 63.20 71.20 11.90 LR
2-propanone N.D. 250 183 175 73.20 70.00 4.47 LR
2-propanol N.D. 250 158 184 63.20 73.60 15.20 LR
n-Pentane N.D. 250 216 9 86.40 3.60 184.00 LRQ
2,2-Dimethylbutane N.D. 250 142 141 56.80 56.40 0.71 LR
2,3-Dimethylbutane N.D. 250 147 144 58.80 57.60 2.06 LR
Methylene chloride N.D. 250 168 171 67.20 68.40 1.77 LR
2-Methylpentane N.D. 250 149 144 59.60 57.60 3.41 LR
3-Methylpentane N.D. 250 149 147 59.60 58.80 1.35 LR
2-Butanol N.D. 250 226 224 90.40 89.60 0.89
n-Hexane N.D. 250 178 168 71.20 67.20 5.78 LR
Ethyl acetate N.D. 250 188 188 75.20 75.20 0.00
Tetrahydrofuran N.D. 250 183 177 0.00 0.00 0.00
Trichloroethylene N.D. 0 0 0 nan nan
Isopropyl acetate N.D. 250 176 175 0.00 0.00 0.00 LR
Benzene N.D. 250 185 177 74.00 70.80 4.42
Chloroform N.D. 0 0 0 nan nan
Cyclohexane N.D. 250 158 154 63.20 61.60 2.56 LR
Ethylene glycol N.D. 250 223 217 89.20 86.80 2.73
Heptane N.D. 250 165 149 66.00 59.60 10.19 LR
2-Ethoxyethanol N.D. 250 213 222 85.20 88.80 4.14
1,4-Dioxane N.D. 250 188 182 75.20 72.80 3.24
Pyridine N.D. 0 0 0 0.00 0.00 0.00
Toluene N.D. 250 184 179 73.60 71.60 2.75
Chlorobenzene N.D. 0 0 0 0.00 0.00 0.00
Ethylbenzene N.D. 250 189 180 75.60 72.00 4.88
m-Xylene/p-Xylene N.D. 500 380 359 76.00 71.80 5.68
o-Xylene N.D. 250 188 174 75.20 69.60 7.73 LR
Cumene N.D. 250 191 187 76.40 74.80 2.12
Ethylene oxide N.D. 250 176 171 70.40 68.40 2.88 LR

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

N.D. = Not Detected

This sample has not been tested according to OAR 333-007. These results should therefore be used for research and development or quality control purposes only.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 9 of 11

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Homogeneity Report by
High Performance Liquid Chromatography

Testing Accreditation #: 4092-004 Test Certificate #: 124369-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Terpee Slurpee
License: 030-1009646F7F8
Type: Extract
Metrc Test Pkg#: 1A401030002C949000000174
Metrc Source Pkg#: 1A401030002C949000000166

Sample ID#: 124369

Lot #: Terpee Slurpee 5/29/20 #1
Batch #: 124369
Batch Weight (g): 1135.5
Harvest/Process Date: 05/29/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 05/29/2020

Sample #124369
Increments Tested (mg/g) TOTAL THC TOTAL CBD THC THCA THCV CBD CBC CBDA CBDV CBG CBN
Increment 1 737.97 12.43 40.67 795.10 N.D. N.D. N.D. 14.17 N.D. 4.45 3.64
Increment 2 716.39 10.18 40.35 770.86 N.D. N.D. N.D. 11.61 N.D. 3.69 3.58
Average Value 727.18 11.30 40.51 782.98 N.D. N.D. N.D. 12.89 N.D. 4.07 3.61
Max Value 737.97 12.43 40.67 795.10 N.D. N.D. N.D. 14.17 N.D. 4.45 3.64
Min Value 716.39 10.18 40.35 770.86 N.D. N.D. N.D. 11.61 N.D. 3.69 3.58
Relative Percent Difference (RPD) ±2.97 ±19.86 ±0.79 ±3.10 N.D. N.D. N.D. ±19.86 N.D. ±18.67 ±1.66
Average Cannabinoids Per Package 727.18 11.30 40.51 782.98 N.D. N.D. N.D. 12.89 N.D. 4.07 3.61
Average Cannabinoids Per Serving 36.36 0.57 2.03 39.15 N.D. N.D. N.D. 0.64 N.D. 0.20 0.18
Max Concentration Per Serving (THC)   Pass
Max Concentration Per Package (THC)   Not Applicable
Relative Percent Difference (RPD)   Pass
Control Study   Yes, MJ1957
Field Duplicate   Pass

N.D. = Not Detected, Min = Minimum, Max = Maximum

RPD is the relative percent difference between increment 1 and increment 2.

RSD is the relative standard deviation between all increments tested.

Total THC and CBD is the calculated sum of CBD or THC and the amount of CBD or THC derived from CBDA or THCA, respectively. These values are calculated by adding a molar correction factor of 0.877 to the CBDA or THCA value.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

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IRON Laboratories

Terpene Report by
Mass Spectrometer

Test Certificate #: 124369-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Terpee Slurpee
License: 030-1009646F7F8
Type: Extract
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A401030002C949000000174
Metrc Source Pkg#: 1A401030002C949000000166

Test Conditions

Scale: XS205-OR1
Temp: 22.1 °C
Baro Pressure: 1012 hPa
Analyst: HRM
Technician: HRM

Sample ID#: 124369

Lot #: Terpee Slurpee 5/29/20 #1
Batch #: 124369
Batch Weight (g): 1135.5
Harvest/Process Date: 05/29/2020
Serving Size (g): 0.05
Date Received: 05/29/2020

Sample #124369
Sample #124369
  • α-Pinene (0.14%)
  • β-Ocimene (0.47%)
  • Camphene (0.00%)
  • Eucalyptol (1,8-Cineol) (0.00%)
  • Sabinene (0.00%)
  • γ-Terpinene (0.22%)
  • Myrcene (0.31%)
  • α-Terpinolene (2.57%)
  • β-Pinene (0.38%)
  • Linalool (0.18%)
  • ∆3-Carene (0.11%)
  • Fenchone (0.00%)
  • α-Terpinene (0.38%)
  • endo-Fenchol (0.00%)
  • α-Ocimene (0.00%)
  • Isopulegol (0.00%)
  • Limonene (0.29%)
  • Geraniol (0.00%)
  • p-Cymene (0.00%)
  • β-Caryophyllene (0.99%)
  • α-Humulene (0.40%)
  • Nerolidol 1 (cis) (0.00%)
  • Nerolidol 2 (trans) (0.02%)
  • Guaiol (0.00%)
  • Caryophyllene Oxide (0.02%)
  • α-Bisabolol (0.07%)
  • α-Phellandrene (2.81%)
  • α-Terpineol (0.12%)
  • Valenence (0.00%)

Total: 9.480%

Predominant Terpenes

2.81%   α-Phellandrene Citrus, green, black pepper 2.57%   α-Terpinolene Fresh wood, sweet, pine, citrus
0.99%   β-Caryophyllene Sweet, woody, spicy, clove 0.47%   β-Ocimene Citrus, tropical, woody, green
0.40%   α-Humulene Woody, oceanic-watery, spicy clove 0.38%   α-Terpinene Woody, lemon, citrus

Value in parenthesis indicates percentage of terpene present in the total sample (weight percentage, wt/wt%).
Value in doughnut slice indicates individual terpene abundance with respect to the total terpenes detected.

This sample has not been tested according to OAR 333-007. These results should therefore be used for research and development or quality control purposes only.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Joseph Rutowski Iron laboratories Joseph Rutowski

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 11 of 11