IRON LaboratoriesPJLA

ISO/IEC 17025:2005 Accredited

Marihuana Potency Analysis by
High Performance Liquid Chromatography
Testing Accreditation #: 77802 Test Certificate #: 124085-001
Client Name, Sample Details

Dan Mcglinchey
Dearborn Heights, MI 48427
Sample: Control
License: 238805-265124
Type: Flower
Method: FE04U HPLC-UV
Test Conditions

Prepsheet ID#: MIP200518
Scale: XS205-MI2
Temp: 23.9 °C
Baro Pressure: 973.6 hPa
Analyst: KEB
Technician: ANJ
Sample ID#: 124085

Harvest/Process Date: 05/19/2020
Serving Size (g): 1
Date Received: 05/19/2020
Test Date: 05/18/2020
Valid Through: 05/19/2021
Report Issued: 05/19/2020
Sample #124085
Sample #124085 Sample #124085
Test
Compounds		 THC THCA CBD CBDA CBN CBG* CBC* THCV* CBDV* Total
Cannabinoids*		 Total THC Total CBD Calc Max Total
Cannabinoids*
Amount (%) 2.9 22.4 N/D 0.4 N/D 0.1 0.2 N/D N/D 25.9 22.5 0.3 23.1
Amount (mg/g) 28.6 224.0 N/D 3.9 N/D 1.2 1.5 N/D N/D 259.2 225.0 3.4 231.2
Amount per Serving (mg) 28.6 224.0 N\D 3.9 N\D 1.2 1.5 N\D N\D 259.2 Serving Size~ (g): 1.0
LOQ (mg/g) 0.96 0.96 0.96 0.96 0.96 0.96 0.96 0.96 0.96   %Decarb. THC CBD
±%RPD 10.72 1.83 0.11 0.37 1.07 0.65 2.41 0.03 0.55 11 0%

LOQ = Limit of Quantitation; %RPD = Relative Percent Deviation; %RSD = Relative Standard Deviation; N/D = Not Detected

*Designates values that are not currently included in the accredited scope of Iron Laboratories.

*** Designates tests that use the method FE-45. FE-45 is performed using AOAC 966.02 and 32.004-32.009. FE-45 has relative expanded (k=2) uncertainties of 1.098% for moisture, 1.754% for water activity for unprocessed plant materials, and 13.102% for water activity for infused products. Vitamin E acetate analysis has a relative expanded (k=2) uncertainty of 18.614%.

Total THC and CBD is the calculated sum of THC or CBD and the amount of THC or CBD derived from THCA or CBDA, respectively. These values are calculated by applying a molar correction factor of 0.877 to the THCA or the CBDA value. Calc Max Total Cannabinoids is the sum of Total THC, Total CBD, CBN, CBG, CBC, THCV, and CBDV.

%Decarb. THC and CBD refer to the percentage of THC or CBD relative to THCA or CBDA, respectively.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
JRT LM Iron laboratories JRT LM

Iron Laboratories, LLC is an ISO/IEC 17025:2005 Testing Laboratory laboratory, accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 1 of 4

IRON LaboratoriesPJLA

ISO/IEC 17025:2005 Accredited

QC Report
Testing Accreditation #: 77802 Test Certificate #: 124085-001
Client Name, Sample Details

Dan Mcglinchey
Dearborn Heights, MI 48427
Sample: Control
License: 238805-265124
Type: Flower
Method: FE04U HPLC-UV
Test Conditions

Prepsheet ID#: MIP200518
Scale: XS205-MI2
Temp: 23.9 °C
Baro Pressure: 973.6 hPa
Analyst: KEB
Technician: ANJ
Sample ID#: 124085

Harvest/Process Date: 05/19/2020
Serving Size (g): 1
Date Received: 05/19/2020
Test Date: 05/18/2020
Valid Through: 05/19/2021
Report Issued: 05/19/2020
Sample #124085
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Cannabidivarin (CBDV) 0 6.05448 6.08691 100.54 6.05349 99.98 0.55
Cannabidiolic Acid (CBDA) 0 5.52083 5.52571 100.09 5.50539 99.72 0.37
Cannabigerol (CBG) 0 5.85611 5.8621 100.10 5.82398 99.45 0.65
Cannabidiol (CBD) 0 5.66229 5.75455 101.63 5.74798 101.51 0.11
Δ9-Tetrahydrocannabivarin (THCV) 0 5.93703 5.99239 100.93 5.99085 100.91 0.03
Cannabinol (CBN) 0 5.88299 5.89275 100.17 5.8301 99.10 1.07
Δ9-Tetrahydrocannabinol (THC) 0 5.96846 6.24264 104.59 5.60775 93.96 10.72
Cannabichromene (CBC) 0 5.71101 5.78806 101.35 5.6505 98.94 2.41
Tetrahydrocannabinolic acid (THCA) 0 5.18872 5.27343 101.63 5.17782 99.79 1.83

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
JRT LM Iron laboratories JRT LM

Iron Laboratories, LLC is an ISO/IEC 17025:2005 Testing Laboratory laboratory, accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 2 of 4
IRON Laboratories

Terpene Report by
Mass Spectrometer
Test Certificate #: 124085-001
Client Name, Sample Details

Dan Mcglinchey
Dearborn Heights, MI 48427
Sample: Control
License: 238805-265124
Type: Flower
Method: SOP FE-44-OR3

Test Conditions

Scale: AG204-MI1
Temp: 23.3 °C
Baro Pressure: 978 hPa
Analyst: JRT
Technician: TAC/JRT

Sample ID#: 124085

Harvest/Process Date: 05/19/2020
Serving Size (g): 1
Date Received: 05/19/2020

Sample #124085
Sample #124085
  • α-Pinene (0.01%)
  • β-Ocimene (0.00%)
  • Camphene (0.00%)
  • Eucalyptol (1,8-Cineol) (0.00%)
  • Sabinene (0.00%)
  • γ-Terpinene (0.00%)
  • Myrcene (0.01%)
  • α-Terpinolene (0.00%)
  • β-Pinene (0.01%)
  • Linalool (0.05%)
  • ∆3-Carene (0.00%)
  • Fenchone (0.00%)
  • α-Terpinene (0.00%)
  • endo-Fenchol (0.00%)
  • α-Ocimene (0.00%)
  • Isopulegol (0.00%)
  • Limonene (0.05%)
  • Geraniol (0.00%)
  • p-Cymene (0.00%)
  • β-Caryophyllene (0.78%)
  • α-Humulene (0.21%)
  • Nerolidol 1 (cis) (0.00%)
  • Nerolidol 2 (trans) (0.00%)
  • Guaiol (0.00%)
  • Caryophyllene Oxide (0.00%)
  • α-Bisabolol (0.12%)
  • α-Phellandrene (0.00%)
  • α-Terpineol (0.00%)
  • Valenence (0.00%)

Total: 1.240%

Predominant Terpenes

0.78%   β-Caryophyllene Sweet, woody, spicy, clove 0.21%   α-Humulene Woody, oceanic-watery, spicy clove
0.12%   α-Bisabolol Fruity, nutty, coconut 0.05%   Limonene Citrus, orange, sweet
0.05%   Linalool Citrus, floral, sweet, bois de rose, woody, green, blueberry 0.01%   α-Pinene Fresh camphor, sweet, pine, earthy, woody

Value in parenthesis indicates percentage of terpene present in the total sample (weight percentage, wt/wt%).
Value in doughnut slice indicates individual terpene abundance with respect to the total terpenes detected.

This sample has not undergone random sampling and has not been tested for compliant state, batch representative testing. These results should therefore be used for research and development or quality control purposes only. Results apply to the sample as received.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
JRT LM Iron laboratories JRT LM

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 2 of 4

IRON LaboratoriesPJLA

ISO/IEC 17025:2005 Accredited

Microbiology Analysis
Testing Accreditation #: 77802 Test Certificate #: 124085-001
Client Name, Sample Details

Dan Mcglinchey
Dearborn Heights, MI 48427
Sample: Control
License: 238805-265124
Type: Flower
Test Conditions

Scale: PB303-MI1
Temp: 24 °C
Baro Pressure: 983.5 hPa
Analyst: BCN/ARH(Plating)/BCN/ACR(PCR)
Technician: ARH
Sample ID#: 124085

Harvest/Process Date: 05/19/2020
Serving Size (g): 1
Date Received: 05/19/2020
Test Date: 05/17/2020
Valid Through: 05/17/2021
Report Issued: 05/19/2020
Sample #124085
Test Method MCFU (CFU/g) LOD (CFU/g) Status (CFU/g)
Total Aerobic Not Tested N/A 0 Not Tested
Yeast & Mold FE-37 (Plating enumeration) 10,001 1,000 Pass/<LOD
Bile-tolerant gram-negative bacteria Not Tested N/A 0 Not Tested
Total Coliforms FE-37 (Plating enumeration) 1,001 100 Pass/<LOD
E. Coli FE-62 (PCR) 1 10 Pass/Not Present
Salmonella FE-62 (PCR) 1 10 Pass/Not Present
Aspergillus spp. FE-62 (PCR) 1 10 Pass/Not Present

E. coli test screens exclusively for Shiga toxin-producing E. coli. TNTC values for yeast and mold are >150,000 CFU/g. TNTC values for total coliforms are >15,000 CFU/g. Total coiforms positive control had a low recovery of 69.3%.

TNTC = Too Numerous To Count. Maximum Colony Forming Units (MCFU) represents the minimum value that a test would need to achieve in order to be considered a failed result (if applicable). LOD is the Limit of Detection for the method. CFU/g = Colony Forming Units per gram. Aspergillus spp. consists of A. flavus, A. fumigatus, A. niger, and A. terreus.

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
MEH QM Iron laboratories MEH QM

Iron Laboratories, LLC is an ISO/IEC 17025:2005 Testing Laboratory laboratory, accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 3 of 4

IRON LaboratoriesPJLA

ISO/IEC 17025:2005 Accredited

Bio Analysis by
Microscopic Visual Inspection
Testing Accreditation #: 77802 Test Certificate #: 124085-001
Client Name, Sample Details

Dan Mcglinchey
Dearborn Heights, MI 48427
Sample: Control
License: 238805-265124
Type: Flower
Method: FE02 Microscope Dissection
Test Conditions

Analyst: ARH
Technician: ARH
Sample ID#: 124085

Harvest/Process Date: 05/19/2020
Serving Size (g): 1
Date Received: 05/19/2020
Test Date: 05/16/2020
Valid Through: 05/16/2021
Report Issued: 05/18/2020
Sample #124085
Sample #124085 Sample #124085
Severity Rating
Mold and Mildew 0 Pass
Mites (not Russet) 0 Pass
Russet Mites 0 Pass
Thrips 0 Pass
Aphids 0 Pass
Other Pests 0 Pass
Other Organic Matter 0 Pass
Inorganic Matter 0 Pass
Total Organic Foreign Matter <2% Pass
Inorganic Foreign Matter 0% Pass
Stem Material <5% Pass
Severity Rating Key
Correlating %FM ≤2% FM >2% FM
Severity Rating 0 None 1 Mild 2 Moderate 3 Severe Units
Mold and Mildew <2 2 3 4+ Locations/g
Mites (not russet) <1 1-5 6-10 11+ Amount/g
Russet Mites <1 1-10 11-50 51+ Amount/g
Thrips <1 1-3 4-5 6+ Amount/g
Aphids <1 1 2-4 5+ Amount/g
Other Pests <1 1-5 6-10 11+ Amount/g
Other Organic Matter <1 1-5 6-10 11+ Amount/g
Inorganic Matter 0 — — >0 Amount/g

In compliance with the MMFLA regulation, the action limits for foreign matter are as follows; no more that 2% organic matter, 5% stem material, and no presence of inorganic matter. Percent foreign contamination is based off of total surface area.

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
MEH QM Iron laboratories MEH QM

Iron Laboratories, LLC is an ISO/IEC 17025:2005 Testing Laboratory laboratory, accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 4 of 4