ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Marijuana Potency Analysis by
High Performance Liquid Chromatography
Testing Accreditation #: 4092-004 Test Certificate #: 124014-001
Client Name, Sample Details

45th Parallel Farms LLC
Dallas, OR 97338
Sample: Northern Wreck Littles
License: 010-100164183CE
Type: Adult Use Flower
Method: FE04U HPLC-UV
Metrc Test Pkg#: 1A4010300000DAD000003438
Metrc Source Pkg#: 1A4010300000DAD000003431
***Water Activity: 0.4875
***Moisture: 10.9356%
Test Conditions

Prepsheet ID#: ORP200511B
Scale: XS205-OR1
Temp: 22.3 °C
Baro Pressure: 1009 hPa
Analyst: HRM
Technician: TMR
Sample ID#: 124014

Lot #: Northern wreck 10/22/19
Batch #: 124014
Batch Weight (g): 6810
Harvest/Process Date: 10/22/2019
Date Received: 05/09/2020
Test Date: 05/11/2020
Sample #124014
Sample #124014 Sample #124014
Test
Compounds		 THC THCA CBD CBDA CBN CBG CBC THCV* CBDV Total
Cannabinoids*		 Total THC Total CBD Calc Max Total
Cannabinoids*
Amount (%) 3.35 22.22 N/D 0.98 0.09 0.21 0.10 N/D N/D 26.94 22.84 0.86 24.09
Amount (mg/g) 33.54 222.16 N/D 9.75 0.89 2.11 0.99 N/D N/D 269.44 228.37 8.55 240.91
Amount per Serving (mg) N\D N\D N\D N\D N\D N\D N\D N\D N\D 0.00 Serving Size~ (g): 0.00
LOQ (mg/g) 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5 0.5   %Decarb. THC CBD
±%RPD 11.36 13.50 +/-5% 11.58 2.02 9.58 6.62 +/-5% +/-5% 13 0

LOQ = Limit of Quantitation; %RPD = Relative Percent Deviation; %RSD = Relative Standard Deviation; N/D = Not Detected

*Designates values that are not currently included in the accredited scope of Iron Laboratories.

*** Designates tests that use the method FE-45. FE-45 is performed using AOAC 966.02 and 32.004-32.009. FE-45 has relative expanded (k=2) uncertainties of 1.098% for moisture, 1.754% for water activity for unprocessed plant materials, and 13.102% for water activity for infused products. Vitamin E acetate analysis has a relative expanded (k=2) uncertainty of 18.614%.

Total THC and CBD is the calculated sum of THC or CBD and the amount of THC or CBD derived from THCA or CBDA, respectively. These values are calculated by applying a molar correction factor of 0.877 to the THCA or the CBDA value. Calc Max Total Cannabinoids is the sum of Total THC, Total CBD, CBN, CBG, CBC, THCV, and CBDV.

%Decarb. THC and CBD refer to the percentage of THC or CBD relative to THCA or CBDA, respectively.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 1 of 4

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant QC Report
Testing Accreditation #: 4092-004 Test Certificate #: 124014-001
Client Name, Sample Details

45th Parallel Farms LLC
Dallas, OR 97338
Sample: Northern Wreck Littles
License: 010-100164183CE
Type: Adult Use Flower
Method: FE04U HPLC-UV
Metrc Test Pkg#: 1A4010300000DAD000003438
Metrc Source Pkg#: 1A4010300000DAD000003431
***Water Activity: 0.4875
***Moisture: 10.9356%
Test Conditions

Prepsheet ID#: ORP200511B
Scale: XS205-OR1
Temp: 22.3 °C
Baro Pressure: 1009 hPa
Analyst: HRM
Technician: TMR
Sample ID#: 124014

Lot #: Northern wreck 10/22/19
Batch #: 124014
Batch Weight (g): 6810
Harvest/Process Date: 10/22/2019
Date Received: 05/09/2020
Test Date: 05/11/2020
Sample #124014
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Cannabidivarin (CBDV) N.D. 1 0 0.00 0 0.00 0
Cannabidiolic Acid (CBDA) N.D. 10.87 11.51 105.89 10.25 94.30 11.58
Cannabigerol (CBG) N.D. 1.68 1.86 110.71 1.69 100.60 9.58
Cannabidiol (CBD) N.D. 1 0 0.00 0 0.00 0
Δ9-Tetrahydrocannabivarin (THCV) N.D. 1 0 0.00 0 0.00 0
Cannabinol (CBN) N.D. 0.51 0.49 96.08 0.5 98.04 2.02
Δ9-Tetrahydrocannabinol (THC) N.D. 29.86 33.76 113.06 30.13 100.90 11.36
Cannabichromene (CBC) N.D. 0.75 0.78 104.00 0.73 97.33 6.62
Tetrahydrocannabinolic acid (THCA) N.D. 143.03 158.81 111.03 138.73 96.99 13.50

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 2 of 4

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Pesticide Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-004 Test Certificate #: 124014-001
Client Name, Sample Details

45th Parallel Farms LLC
Dallas, OR 97338
Sample: Northern Wreck Littles
License: 010-100164183CE
Type: Adult Use Flower
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A4010300000DAD000003438
Metrc Source Pkg#: 1A4010300000DAD000003431
Test Conditions

Prepsheet ID#: ORPS200512a
Scale: 1129293203
Temp: 21.3 °C
Baro PE: 994.5 hPa
Analyst: JER
Technician: JER
Sample ID#: 124014

Lot #: Northern wreck 10/22/19
Batch #: 124014
Batch Weight (g): 6810
Harvest/Process Date: 10/22/2019
Date Received: 05/09/2020
Test Date: 05/13/2020
Sample #124014
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
Aldicarb 0.400 0.122 Pass/<LOD Abamectin**** 0.500 0.122 Pass/<LOD
Acephate 0.400 0.122 Pass/<LOD Acequinocyl 2.000 0.245 Pass/<LOD
Acetamiprid 0.200 0.122 Pass/<LOD Azoxystrobin 0.200 0.122 Pass/<LOD
Bifenazate 0.200 0.122 Pass/<LOD Bifenthrin 0.200 0.122 Pass/<LOD
Boscalid 0.400 0.122 Pass/<LOD Carbaryl 0.200 0.122 Pass/<LOD
Carbofuran 0.200 0.122 Pass/<LOD Chlorantraniliprole 0.200 0.122 Pass/<LOD
Chlorfenapyr 1.000 0.490 Pass/<LOD Chlorpyrifos 0.200 0.122 Pass/<LOD
Clofentezine 0.200 0.122 Pass/<LOD Cyfluthrin** 1.000 0.490 Pass/<LOD
Cypermethrin*** 1.000 0.490 Pass/<LOD Daminozide 1.000 0.122 Pass/<LOD
DDVP (Dichlorvos) 1.000 0.245 Pass/<LOD Diazinon 0.200 0.122 Pass/<LOD
Dimethoate 0.200 0.122 Pass/<LOD Ethoprophos 0.200 0.122 Pass/<LOD
Etofenprox 0.400 0.122 Pass/<LOD Etoxazole 0.200 0.122 Pass/<LOD
Fenoxycarb 0.200 0.122 Pass/<LOD Fenpyroximate 0.400 0.122 Pass/<LOD
Fipronil 0.400 0.122 Pass/<LOD Flonicamid 1.000 0.122 Pass/<LOD
Fludioxonil 0.400 0.122 Pass/<LOD Hexythiazox 1.000 0.122 Pass/<LOD
Imazalil 0.200 0.122 Pass/<LOD Imidacloprid 0.400 0.122 Pass/<LOD
Kresoxim Methyl 0.400 0.122 Pass/<LOD Malathion 0.200 0.122 Pass/<LOD
Metalaxyl 0.200 0.122 Pass/<LOD Methiocarb 0.200 0.122 Pass/<LOD
Methomyl 0.400 0.122 Pass/<LOD Methyl Parathion 0.200 0.122 Pass/<LOD
MGK-264‡ 0.200 0.122 Pass/<LOD Myclobutanil 0.000 0.122 Pass/<LOD
Naled 0.500 0.122 Pass/<LOD Oxamyl 1.000 0.122 Pass/<LOD
Paclobutrazol 0.400 0.122 Pass/<LOD Permethrins† 0.200 0.122 Pass/<LOD
Phosmet 0.200 0.122 Pass/<LOD Piperonyl Butoxide 2.000 0.122 Pass/<LOD
Prallethrin 0.200 0.122 Pass/<LOD Propiconazole 0.400 0.122 Pass/<LOD
Propoxur 0.200 0.122 Pass/<LOD Pyrethrins* 1.000 0.122 Pass/<LOD
Pyridaben 0.200 0.122 Pass/<LOD Spinosad***** 0.200 0.122 Pass/<LOD
Spiromesifen 0.200 0.122 Pass/<LOD Spirotetramat 0.200 0.122 Pass/<LOD
Spiroxamine‡ 0.400 0.122 Pass/<LOD Tebuconazole 0.400 0.122 Pass/<LOD
Thiacloprid 0.200 0.122 Pass/<LOD Thiamethoxam 0.200 0.122 Pass/<LOD
Trifloxystrobin 0.200 0.122 Pass/<LOD

* Pyrethrins are reported as the sum of Jasmolin I, Cinerin I, and Pyrethrin I
** Cyfluthrins are reported as the sum of isomers Cyfluthrin I, II, III, and IV
*** Cypermethrins are reported as the sum of isomers Cypermethrin I, II, III, and IV
**** Abamectin is reported as the sum of Avermectin B1a and Avermectin B1b
***** Spinosad is reported as the sum of Spinosyn A and Spinosyn D
† Permethrin and Prallethrin are reported as the sum of cis and trans isomers
‡ MGK-264 and Spiroximine are reported as the sum of isomers I and II
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 2 of 4

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Pesticide QC Report
Testing Accreditation #: 4092-004 Test Certificate #: 124014-001
Client Name, Sample Details

45th Parallel Farms LLC
Dallas, OR 97338
Sample: Northern Wreck Littles
License: 010-100164183CE
Type: Adult Use Flower
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A4010300000DAD000003438
Metrc Source Pkg#: 1A4010300000DAD000003431
Test Conditions

Prepsheet ID#: ORPS200512a
Scale: 1129293203
Temp: 21.3 °C
Baro PE: 994.5 hPa
Analyst: JER
Technician: JER
Sample ID#: 124014

Lot #: Northern wreck 10/22/19
Batch #: 124014
Batch Weight (g): 6810
Harvest/Process Date: 10/22/2019
Date Received: 05/09/2020
Test Date: 05/13/2020
Sample #124014
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS recovery% MSD recovery% Relative Percent Difference (%) QC Flag
Acephate N.D. 1 1.18 1.09 118.00 109.00 7.93
Acequinocyl N.D. 1 1.2 0.829 120.00 82.90 36.57 Q
Acetamiprid N.D. 1 1 0.896 100.00 89.60 10.97
Aldicarb N.D. 1 1 0.902 100.00 90.20 10.30
Avermectin B1a N.D. 0.97 1.04 0.915 107.22 94.33 12.79
Azoxystrobin N.D. 1 0.967 0.919 96.70 91.90 5.09
Bifenazate N.D. 1 0.627 0.563 62.70 56.30 10.76 LR
Bifenthrin N.D. 1 1.02 0.95 102.00 95.00 7.11
Boscalid N.D. 1 1.1 0.992 110.00 99.20 10.33
Carbaryl N.D. 1 1.03 1.04 103.00 104.00 0.97
Carbofuran N.D. 1 1.04 1.03 104.00 103.00 0.97
Chlorantraniliprole N.D. 1 1.04 0.898 104.00 89.80 14.65
Chlorfenapyr N.D. 1 0.872 0.975 87.20 97.50 11.15
Chlorpyriphos N.D. 1 1 0.9 100.00 90.00 10.53
Clofentezine N.D. 1 0.975 0.85 97.50 85.00 13.70
Cyfluthrin N.D. 1 1.16 0.974 116.00 97.40 17.43
Cypermethrin N.D. 1 1.22 1.01 122.00 101.00 18.83
Daminoside N.D. 1 0.719 0.618 71.90 61.80 15.11 LR
Diazanon N.D. 1 1.17 1.09 117.00 109.00 7.08
Dichlorvos N.D. 1 0.965 0.967 96.50 96.70 0.21
Dimethoate N.D. 1 1.1 0.974 110.00 97.40 12.15
Ethoprophos N.D. 1 1.01 0.889 101.00 88.90 12.74
Etofenprox N.D. 1 1.04 0.943 104.00 94.30 9.78
Etoxazole N.D. 1 1.17 1.04 117.00 104.00 11.76
Fenoxycarb N.D. 1 1.06 0.919 106.00 91.90 14.25
Fenpyroximate N.D. 1 1.2 0.988 120.00 98.80 19.38
Fipronil N.D. 1 0.976 0.975 97.60 97.50 0.10
Flonicamid N.D. 1 1.11 1.06 111.00 106.00 4.61
Fludioxonil N.D. 1 0.996 1.03 99.60 103.00 3.36
Hexythiazox N.D. 1 1.01 0.867 101.00 86.70 15.24
Imazalil N.D. 1 1.06 0.98 106.00 98.00 7.84
Imidacloprid 0.129 1 0.989 0.979 98.90 97.90 1.02 I
Kresoxim-methyl N.D. 1 1 0.973 100.00 97.30 2.74
Malathion N.D. 1 1.18 0.971 118.00 97.10 19.43
Metalaxyl N.D. 1 1.08 0.912 108.00 91.20 16.87
Methiocarb N.D. 1 1.05 0.878 105.00 87.80 17.84
Methomyl N.D. 1 1.07 0.932 107.00 93.20 13.79
MGK-264 N.D. 1 1.03 0.886 103.00 88.60 15.03
Myclobutanil N.D. 1 1.1 0.937 110.00 93.70 16.00
Naled (dibrom) N.D. 1 0.609 0.584 60.90 58.40 4.19 LR
Oxamyl N.D. 1 1.06 0.991 106.00 99.10 6.73
Paclobutrazol N.D. 1 0.957 0.901 95.70 90.10 6.03
Parathion-methyl N.D. 1 1.08 1.03 108.00 103.00 4.74
Permethrins N.D. 1 1.027 0.87 102.70 87.00 16.55 Q
Phosmet N.D. 1 1.06 0.95 106.00 95.00 10.95
Piperonyl butoxide N.D. 1 1.14 1.09 114.00 109.00 4.48
Prallethrin N.D. 1 1.08 0.943 108.00 94.30 13.54
Propiconazole N.D. 1 1.11 0.994 111.00 99.40 11.03
Propoxur N.D. 1 0.917 0.943 91.70 94.30 2.80
Pyrethrin N.D. 0.65 0.712 0.677 109.54 104.15 5.04
Pyridaben N.D. 1 1.04 0.877 104.00 87.70 17.01
SpinosynA N.D. 0.84 0.691 0.683 82.26 81.31 1.16
SpinosynD N.D. 0.16 0.15 0.146 93.75 91.25 2.70
Spiromesifen N.D. 1 0.499 0.407 49.90 40.70 20.31 LRQ
Spirotetramat N.D. 1 0.924 0.84 92.40 84.00 9.52
Spiroxamine N.D. 1 1.14 1.05 114.00 105.00 8.22
Tebuconazole N.D. 1 1.19 1.01 119.00 101.00 16.36
Thiacloprid N.D. 1 1.12 0.937 112.00 93.70 17.79
Thiamethoxam N.D. 1 1.05 0.921 105.00 92.10 13.09
Trifloxystrobin N.D. 1 1.01 0.91 101.00 91.00 10.42

N.D. = Not Detected

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 30%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (60-120%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 3 of 4
IRON Laboratories

Terpene Report by
Mass Spectrometer
Test Certificate #: 124014-001
Client Name, Sample Details

45th Parallel Farms LLC
Dallas, OR 97338
Sample: Northern Wreck Littles
License: 010-100164183CE
Type: Adult Use Flower
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A4010300000DAD000003438
Metrc Source Pkg#: 1A4010300000DAD000003431

Test Conditions

Scale: XS205-OR1
Temp: 22.1 °C
Baro Pressure: 1012 hPa
Analyst: HRM
Technician: HRM

Sample ID#: 124014

Lot #: Northern wreck 10/22/19
Batch #: 124014
Batch Weight (g): 6810
Harvest/Process Date: 10/22/2019
Date Received: 05/09/2020

Sample #124014
Sample #124014
  • α-Pinene (0.00%)
  • β-Ocimene (0.03%)
  • Camphene (0.00%)
  • Eucalyptol (1,8-Cineol) (0.02%)
  • Sabinene (0.00%)
  • γ-Terpinene (0.00%)
  • Myrcene (0.15%)
  • α-Terpinolene (0.00%)
  • β-Pinene (0.00%)
  • Linalool (0.10%)
  • ∆3-Carene (0.00%)
  • Fenchone (0.00%)
  • α-Terpinene (0.00%)
  • endo-Fenchol (0.02%)
  • α-Ocimene (0.00%)
  • Isopulegol (0.00%)
  • Limonene (0.04%)
  • Geraniol (0.00%)
  • p-Cymene (0.00%)
  • β-Caryophyllene (0.41%)
  • α-Humulene (0.30%)
  • Nerolidol 1 (cis) (0.00%)
  • Nerolidol 2 (trans) (0.05%)
  • Guaiol (0.18%)
  • Caryophyllene Oxide (0.14%)
  • α-Bisabolol (0.17%)
  • α-Phellandrene (0.00%)
  • α-Terpineol (0.03%)
  • Valenence (0.00%)

Total: 1.640%

Predominant Terpenes

0.41%   β-Caryophyllene Sweet, woody, spicy, clove 0.30%   α-Humulene Woody, oceanic-watery, spicy clove
0.18%   Guaiol Mild, guaiacwood, tea, rose 0.17%   α-Bisabolol Fruity, nutty, coconut
0.15%   Myrcene Peppery, spicy balsam 0.14%   Caryophyllene Oxide Sweet, fresh, woody, spicy

Value in parenthesis indicates percentage of terpene present in the total sample (weight percentage, wt/wt%).
Value in doughnut slice indicates individual terpene abundance with respect to the total terpenes detected.

This sample has not been tested according to OAR 333-007. These results should therefore be used for research and development or quality control purposes only.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 4 of 4