ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Marijuana Potency Analysis by
High Performance Liquid Chromatography
Testing Accreditation #: 4092-004 Test Certificate #: 123841-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Holy water
License: 030-1009646F7F8
Type: AU Tincture
Method: FE04U HPLC-UV
Metrc Test Pkg#: 1A401030002C949000000035
Metrc Source Pkg#: 1A401030002C949000000010
Test Conditions

Prepsheet ID#: ORP200501C
Scale: XS205-OR1
Temp: 22.7 °C
Baro Pressure: 1007 hPa
Analyst: HRM
Technician: TMR
Sample ID#: 123841

Lot #: Holy water 3/24/20 #1
Batch #: 123841
Batch Weight (g): 337.6
Harvest/Process Date: 03/24/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 04/30/2020
Test Date: 05/01/2020
Sample #123841
Sample #123841 Sample #123841
Test
Compounds		 THC THCA CBD CBDA CBN CBG CBC THCV* CBDV Total
Cannabinoids*		 Total THC Total CBD Calc Max Total
Cannabinoids*
Amount (%) 6.38 69.46 N/D 1.73 0.20 0.36 0.22 N/D N/D 78.35 67.29 1.52 69.59
Amount (mg/g) 63.77 694.61 N/D 17.32 2.03 3.58 2.17 N/D N/D 783.48 672.94 15.19 695.91
Amount per Serving (mg) 3.19 34.73 N\D 0.87 0.10 0.18 0.11 N\D N\D 39.17 Serving Size~ (g): 0.05
LOQ (mg/g) 2 2 2 2 2 2 2 2 2   %Decarb. THC CBD
±%RPD 2.59 7.50 2.68 2.41 1.81 2.20 2.77 2.46 2.95 8 0

LOQ = Limit of Quantitation; %RPD = Relative Percent Deviation; %RSD = Relative Standard Deviation; N/D = Not Detected

*Designates values that are not currently included in the accredited scope of Iron Laboratories.

*** Designates tests that use the method FE-45. FE-45 is performed using AOAC 966.02 and 32.004-32.009. FE-45 has relative expanded (k=2) uncertainties of 1.098% for moisture, 1.754% for water activity for unprocessed plant materials, and 13.102% for water activity for infused products. Vitamin E acetate analysis has a relative expanded (k=2) uncertainty of 18.614%.

Total THC and CBD is the calculated sum of THC or CBD and the amount of THC or CBD derived from THCA or CBDA, respectively. These values are calculated by applying a molar correction factor of 0.877 to the THCA or the CBDA value. Calc Max Total Cannabinoids is the sum of Total THC, Total CBD, CBN, CBG, CBC, THCV, and CBDV.

%Decarb. THC and CBD refer to the percentage of THC or CBD relative to THCA or CBDA, respectively.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 1 of 11

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant QC Report
Testing Accreditation #: 4092-004 Test Certificate #: 123841-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Holy water
License: 030-1009646F7F8
Type: AU Tincture
Method: FE04U HPLC-UV
Metrc Test Pkg#: 1A401030002C949000000035
Metrc Source Pkg#: 1A401030002C949000000010
Test Conditions

Prepsheet ID#: ORP200501C
Scale: XS205-OR1
Temp: 22.7 °C
Baro Pressure: 1007 hPa
Analyst: HRM
Technician: TMR
Sample ID#: 123841

Lot #: Holy water 3/24/20 #1
Batch #: 123841
Batch Weight (g): 337.6
Harvest/Process Date: 03/24/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 04/30/2020
Test Date: 05/01/2020
Sample #123841
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Cannabidivarin (CBDV) N.D. 5.59 6.01 107.51 6.19 110.73 2.95
Cannabidiolic Acid (CBDA) N.D. 5.61 6.14 109.45 6.29 112.12 2.41
Cannabigerol (CBG) N.D. 5.77 6.29 109.01 6.43 111.44 2.20
Cannabidiol (CBD) N.D. 6.07 6.63 109.23 6.81 112.19 2.68
Δ9-Tetrahydrocannabivarin (THCV) N.D. 5.64 6.03 106.91 6.18 109.57 2.46
Cannabinol (CBN) N.D. 5.59 6.01 107.51 6.12 109.48 1.81
Δ9-Tetrahydrocannabinol (THC) N.D. 6.18 6.49 105.02 6.66 107.77 2.59
Cannabichromene (CBC) N.D. 6.31 7.68 121.71 7.47 118.38 2.77
Tetrahydrocannabinolic acid (THCA) N.D. 5.39 6.36 118.00 5.9 109.46 7.50

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 2 of 11

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Pesticide Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-004 Test Certificate #: 123841-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Holy water
License: 030-1009646F7F8
Type: AU Tincture
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A401030002C949000000035
Metrc Source Pkg#: 1A401030002C949000000010
Test Conditions

Prepsheet ID#: ORPS200504a
Scale: 1129293203
Temp: 21.2 °C
Baro PE: 1005 hPa
Analyst: JER
Technician: JER
Sample ID#: 123841

Lot #: Holy water 3/24/20 #1
Batch #: 123841
Batch Weight (g): 337.6
Harvest/Process Date: 03/24/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 04/30/2020
Test Date: 05/05/2020
Sample #123841
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
Aldicarb 0.400 0.129 Pass/<LOD Abamectin**** 0.500 0.129 Pass/<LOD
Acephate 0.400 0.129 Pass/<LOD Acequinocyl 2.000 0.257 Pass/<LOD
Acetamiprid 0.200 0.129 Pass/<LOD Azoxystrobin 0.200 0.129 Pass/<LOD
Bifenazate 0.200 0.129 Pass/<LOD Bifenthrin 0.200 0.129 Pass/<LOD
Boscalid 0.400 0.129 Pass/<LOD Carbaryl 0.200 0.129 Pass/<LOD
Carbofuran 0.200 0.129 Pass/<LOD Chlorantraniliprole 0.200 0.129 Pass/<LOD
Chlorfenapyr 1.000 0.515 Pass/<LOD Chlorpyrifos 0.200 0.129 Pass/<LOD
Clofentezine 0.200 0.129 Pass/<LOD Cyfluthrin** 1.000 0.515 Pass/<LOD
Cypermethrin*** 1.000 0.515 Pass/<LOD Daminozide 1.000 0.129 Pass/<LOD
DDVP (Dichlorvos) 1.000 0.257 Pass/<LOD Diazinon 0.200 0.129 Pass/<LOD
Dimethoate 0.200 0.129 Pass/<LOD Ethoprophos 0.200 0.129 Pass/<LOD
Etofenprox 0.400 0.129 Pass/<LOD Etoxazole 0.200 0.129 Pass/<LOD
Fenoxycarb 0.200 0.129 Pass/<LOD Fenpyroximate 0.400 0.129 Pass/<LOD
Fipronil 0.400 0.129 Pass/<LOD Flonicamid 1.000 0.129 Pass/<LOD
Fludioxonil 0.400 0.129 Pass/<LOD Hexythiazox 1.000 0.129 Pass/<LOD
Imazalil 0.200 0.129 Pass/<LOD Imidacloprid 0.400 0.129 Pass/<LOD
Kresoxim Methyl 0.400 0.129 Pass/<LOD Malathion 0.200 0.129 Pass/<LOD
Metalaxyl 0.200 0.129 Pass/<LOD Methiocarb 0.200 0.129 Pass/<LOD
Methomyl 0.400 0.129 Pass/<LOD Methyl Parathion 0.200 0.129 Pass/<LOD
MGK-264‡ 0.200 0.129 Pass/<LOD Myclobutanil 0.000 0.129 Pass/<LOD
Naled 0.500 0.129 Pass/<LOD Oxamyl 1.000 0.129 Pass/<LOD
Paclobutrazol 0.400 0.129 Pass/<LOD Permethrins† 0.200 0.129 Pass/<LOD
Phosmet 0.200 0.129 Pass/<LOD Piperonyl Butoxide 2.000 0.129 Pass/<LOD
Prallethrin 0.200 0.129 Pass/<LOD Propiconazole 0.400 0.129 Pass/<LOD
Propoxur 0.200 0.129 Pass/<LOD Pyrethrins* 1.000 0.129 Pass/<LOD
Pyridaben 0.200 0.129 Pass/<LOD Spinosad***** 0.200 0.129 Pass/<LOD
Spiromesifen 0.200 0.129 Pass/<LOD Spirotetramat 0.200 0.129 Pass/<LOD
Spiroxamine‡ 0.400 0.129 Pass/<LOD Tebuconazole 0.400 0.129 Pass/<LOD
Thiacloprid 0.200 0.129 Pass/<LOD Thiamethoxam 0.200 0.129 Pass/<LOD
Trifloxystrobin 0.200 0.129 Pass/<LOD

* Pyrethrins are reported as the sum of Jasmolin I, Cinerin I, and Pyrethrin I
** Cyfluthrins are reported as the sum of isomers Cyfluthrin I, II, III, and IV
*** Cypermethrins are reported as the sum of isomers Cypermethrin I, II, III, and IV
**** Abamectin is reported as the sum of Avermectin B1a and Avermectin B1b
***** Spinosad is reported as the sum of Spinosyn A and Spinosyn D
† Permethrin and Prallethrin are reported as the sum of cis and trans isomers
‡ MGK-264 and Spiroximine are reported as the sum of isomers I and II
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 2 of 11

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Pesticide QC Report
Testing Accreditation #: 4092-004 Test Certificate #: 123841-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Holy water
License: 030-1009646F7F8
Type: AU Tincture
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A401030002C949000000035
Metrc Source Pkg#: 1A401030002C949000000010
Test Conditions

Prepsheet ID#: ORPS200504a
Scale: 1129293203
Temp: 21.2 °C
Baro PE: 1005 hPa
Analyst: JER
Technician: JER
Sample ID#: 123841

Lot #: Holy water 3/24/20 #1
Batch #: 123841
Batch Weight (g): 337.6
Harvest/Process Date: 03/24/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 04/30/2020
Test Date: 05/05/2020
Sample #123841
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS recovery% MSD recovery% Relative Percent Difference (%) QC Flag
Acephate N.D. 1 0.978 0.927 97.80 92.70 5.35
Acequinocyl N.D. 1 0.329 0.382 32.90 38.20 14.91 LR
Acetamiprid N.D. 1 1.07 0.991 107.00 99.10 7.67
Aldicarb N.D. 1 0.929 0.923 92.90 92.30 0.65
Avermectin B1a N.D. 0.97 1.45 1.16 149.48 119.59 22.22 HRQ
Azoxystrobin N.D. 1 1.06 0.941 106.00 94.10 11.89
Bifenazate N.D. 1 1.18 1.2 118.00 120.00 1.68
Bifenthrin N.D. 1 0.821 0.836 82.10 83.60 1.81
Boscalid N.D. 1 0.992 1.11 99.20 111.00 11.23
Carbaryl N.D. 1 1.09 0.977 109.00 97.70 10.93
Carbofuran N.D. 1 0.952 0.973 95.20 97.30 2.18
Chlorantraniliprole N.D. 1 1.34 1.44 134.00 144.00 7.19 HR
Chlorfenapyr N.D. 1 0.841 0.775 84.10 77.50 8.17
Chlorpyriphos N.D. 1 0.837 0.897 83.70 89.70 6.92
Clofentezine N.D. 1 0.916 0.954 91.60 95.40 4.06
Cyfluthrin N.D. 1 1.01 1.06 101.00 106.00 4.83
Cypermethrin N.D. 1 0.902 1.05 90.20 105.00 15.16
Daminoside N.D. 1 1.35 1.3 135.00 130.00 3.77 HR
Diazanon N.D. 1 1.21 1.12 121.00 112.00 7.73
Dichlorvos N.D. 1 0.935 0.811 93.50 81.10 14.20
Dimethoate N.D. 1 0.969 0.913 96.90 91.30 5.95
Ethoprophos N.D. 1 0.94 0.965 94.00 96.50 2.62
Etofenprox N.D. 1 0.646 0.709 64.60 70.90 9.30 LR
Etoxazole N.D. 1 1.03 1.02 103.00 102.00 0.98
Fenoxycarb N.D. 1 1.2 1.23 120.00 123.00 2.47
Fenpyroximate N.D. 1 0.981 0.99 98.10 99.00 0.91
Fipronil N.D. 1 1.01 1.04 101.00 104.00 2.93
Flonicamid N.D. 1 1 1.07 100.00 107.00 6.76
Fludioxonil N.D. 1 1 1.07 100.00 107.00 6.76
Hexythiazox N.D. 1 0.65 0.68 65.00 68.00 4.51 LR
Imazalil N.D. 1 1.39 1.31 139.00 131.00 5.93 HR
Imidacloprid N.D. 1 1.16 1.1 116.00 110.00 5.31
Kresoxim-methyl N.D. 1 1.42 1.37 142.00 137.00 3.58 HR
Malathion N.D. 1 0.998 1.15 99.80 115.00 14.15
Metalaxyl N.D. 1 1.21 1.35 121.00 135.00 10.94 HR
Methiocarb N.D. 1 0.984 0.971 98.40 97.10 1.33
Methomyl N.D. 1 1.11 1.15 111.00 115.00 3.54
MGK-264 N.D. 1 0.897 1 89.70 100.00 10.86
Myclobutanil N.D. 1 1.21 1.3 121.00 130.00 7.17
Naled (dibrom) N.D. 1 0.566 0.552 56.60 55.20 2.50 LR
Oxamyl N.D. 1 1.04 0.966 104.00 96.60 7.38
Paclobutrazol N.D. 1 1.62 1.54 162.00 154.00 5.06 HR
Parathion-methyl N.D. 1 0.885 1.02 88.50 102.00 14.17
Permethrins N.D. 1 0.71 0.772 71.00 77.20 8.37 LR
Phosmet N.D. 1 1.16 1.14 116.00 114.00 1.74
Piperonyl butoxide N.D. 1 1.13 0.91 113.00 91.00 21.57 Q
Prallethrin N.D. 1 1.17 1.14 117.00 114.00 2.60
Propiconazole N.D. 1 1.12 1.06 112.00 106.00 5.50
Propoxur N.D. 1 1.17 0.891 117.00 89.10 27.07 Q
Pyrethrin N.D. 0.65 0.711 0.691 109.38 106.31 2.85
Pyridaben N.D. 1 0.85 0.785 85.00 78.50 7.95
SpinosynA N.D. 0.84 1.15 0.97 136.90 115.48 16.98 HR
SpinosynD N.D. 0.16 0.207 0.202 129.38 126.25 2.44
Spiromesifen N.D. 1 0.412 0.473 41.20 47.30 13.79 LR
Spirotetramat N.D. 1 1.3 1.23 130.00 123.00 5.53
Spiroxamine N.D. 1 1.34 1.26 134.00 126.00 6.15 HR
Tebuconazole N.D. 1 1.37 1.4 137.00 140.00 2.17 HR
Thiacloprid N.D. 1 1.16 1.1 116.00 110.00 5.31
Thiamethoxam N.D. 1 1.38 1.34 138.00 134.00 2.94 HR
Trifloxystrobin N.D. 1 1.09 0.981 109.00 98.10 10.53

N.D. = Not Detected

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 30%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (60-120%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 3 of 11

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Pesticide Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-004 Test Certificate #: 123841-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Holy water
License: 030-1009646F7F8
Type: AU Tincture
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A401030002C949000000035
Metrc Source Pkg#: 1A401030002C949000000010
Test Conditions

Prepsheet ID#: ORPS200504a
Scale: 1129293203
Temp: 21.2 °C
Baro PE: 1005 hPa
Analyst: JER
Technician: JER
Sample ID#: 123841

Lot #: Holy water 3/24/20 #1
Batch #: 123841
Batch Weight (g): 337.6
Harvest/Process Date: 03/24/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 04/30/2020
Test Date: 05/05/2020
Sample #123841
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
Aldicarb 0.400 0.125 Pass/<LOD Abamectin**** 0.500 0.125 Pass/<LOD
Acephate 0.400 0.125 Pass/<LOD Acequinocyl 2.000 0.250 Pass/<LOD
Acetamiprid 0.200 0.125 Pass/<LOD Azoxystrobin 0.200 0.125 Pass/<LOD
Bifenazate 0.200 0.125 Pass/<LOD Bifenthrin 0.200 0.125 Pass/<LOD
Boscalid 0.400 0.125 Pass/<LOD Carbaryl 0.200 0.125 Pass/<LOD
Carbofuran 0.200 0.125 Pass/<LOD Chlorantraniliprole 0.200 0.125 Pass/<LOD
Chlorfenapyr 1.000 0.501 Pass/<LOD Chlorpyrifos 0.200 0.125 Pass/<LOD
Clofentezine 0.200 0.125 Pass/<LOD Cyfluthrin** 1.000 0.501 Pass/<LOD
Cypermethrin*** 1.000 0.501 Pass/<LOD Daminozide 1.000 0.125 Pass/<LOD
DDVP (Dichlorvos) 1.000 0.250 Pass/<LOD Diazinon 0.200 0.125 Pass/<LOD
Dimethoate 0.200 0.125 Pass/<LOD Ethoprophos 0.200 0.125 Pass/<LOD
Etofenprox 0.400 0.125 Pass/<LOD Etoxazole 0.200 0.125 Pass/<LOD
Fenoxycarb 0.200 0.125 Pass/<LOD Fenpyroximate 0.400 0.125 Pass/<LOD
Fipronil 0.400 0.125 Pass/<LOD Flonicamid 1.000 0.125 Pass/<LOD
Fludioxonil 0.400 0.125 Pass/<LOD Hexythiazox 1.000 0.125 Pass/<LOD
Imazalil 0.200 0.125 Pass/<LOD Imidacloprid 0.400 0.125 Pass/<LOD
Kresoxim Methyl 0.400 0.125 Pass/<LOD Malathion 0.200 0.125 Pass/<LOD
Metalaxyl 0.200 0.125 Pass/<LOD Methiocarb 0.200 0.125 Pass/<LOD
Methomyl 0.400 0.125 Pass/<LOD Methyl Parathion 0.200 0.125 Pass/<LOD
MGK-264‡ 0.200 0.125 Pass/<LOD Myclobutanil 0.000 0.125 Pass/<LOD
Naled 0.500 0.125 Pass/<LOD Oxamyl 1.000 0.125 Pass/<LOD
Paclobutrazol 0.400 0.125 Pass/<LOD Permethrins† 0.200 0.125 Pass/<LOD
Phosmet 0.200 0.125 Pass/<LOD Piperonyl Butoxide 2.000 0.125 Pass/<LOD
Prallethrin 0.200 0.125 Pass/<LOD Propiconazole 0.400 0.125 Pass/<LOD
Propoxur 0.200 0.125 Pass/<LOD Pyrethrins* 1.000 0.125 Pass/<LOD
Pyridaben 0.200 0.125 Pass/<LOD Spinosad***** 0.200 0.125 Pass/<LOD
Spiromesifen 0.200 0.125 Pass/<LOD Spirotetramat 0.200 0.125 Pass/<LOD
Spiroxamine‡ 0.400 0.125 Pass/<LOD Tebuconazole 0.400 0.125 Pass/<LOD
Thiacloprid 0.200 0.125 Pass/<LOD Thiamethoxam 0.200 0.125 Pass/<LOD
Trifloxystrobin 0.200 0.125 Pass/<LOD

* Pyrethrins are reported as the sum of Jasmolin I, Cinerin I, and Pyrethrin I
** Cyfluthrins are reported as the sum of isomers Cyfluthrin I, II, III, and IV
*** Cypermethrins are reported as the sum of isomers Cypermethrin I, II, III, and IV
**** Abamectin is reported as the sum of Avermectin B1a and Avermectin B1b
***** Spinosad is reported as the sum of Spinosyn A and Spinosyn D
† Permethrin and Prallethrin are reported as the sum of cis and trans isomers
‡ MGK-264 and Spiroximine are reported as the sum of isomers I and II
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 4 of 11

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Pesticide QC Report
Testing Accreditation #: 4092-004 Test Certificate #: 123841-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Holy water
License: 030-1009646F7F8
Type: AU Tincture
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A401030002C949000000035
Metrc Source Pkg#: 1A401030002C949000000010
Test Conditions

Prepsheet ID#: ORPS200504a
Scale: 1129293203
Temp: 21.2 °C
Baro PE: 1005 hPa
Analyst: JER
Technician: JER
Sample ID#: 123841

Lot #: Holy water 3/24/20 #1
Batch #: 123841
Batch Weight (g): 337.6
Harvest/Process Date: 03/24/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 04/30/2020
Test Date: 05/05/2020
Sample #123841
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS recovery% MSD recovery% Relative Percent Difference (%) QC Flag
Acephate N.D. 1 0.978 0.927 97.80 92.70 5.35
Acequinocyl N.D. 1 0.329 0.382 32.90 38.20 14.91 LR
Acetamiprid N.D. 1 1.07 0.991 107.00 99.10 7.67
Aldicarb N.D. 1 0.929 0.923 92.90 92.30 0.65
Avermectin B1a N.D. 0.97 1.45 1.16 149.48 119.59 22.22 HRQ
Azoxystrobin N.D. 1 1.06 0.941 106.00 94.10 11.89
Bifenazate N.D. 1 1.18 1.2 118.00 120.00 1.68
Bifenthrin N.D. 1 0.821 0.836 82.10 83.60 1.81
Boscalid N.D. 1 0.992 1.11 99.20 111.00 11.23
Carbaryl N.D. 1 1.09 0.977 109.00 97.70 10.93
Carbofuran N.D. 1 0.952 0.973 95.20 97.30 2.18
Chlorantraniliprole N.D. 1 1.34 1.44 134.00 144.00 7.19 HR
Chlorfenapyr N.D. 1 0.841 0.775 84.10 77.50 8.17
Chlorpyriphos N.D. 1 0.837 0.897 83.70 89.70 6.92
Clofentezine N.D. 1 0.916 0.954 91.60 95.40 4.06
Cyfluthrin N.D. 1 1.01 1.06 101.00 106.00 4.83
Cypermethrin N.D. 1 0.902 1.05 90.20 105.00 15.16
Daminoside N.D. 1 1.35 1.3 135.00 130.00 3.77 HR
Diazanon N.D. 1 1.21 1.12 121.00 112.00 7.73
Dichlorvos N.D. 1 0.935 0.811 93.50 81.10 14.20
Dimethoate N.D. 1 0.969 0.913 96.90 91.30 5.95
Ethoprophos N.D. 1 0.94 0.965 94.00 96.50 2.62
Etofenprox N.D. 1 0.646 0.709 64.60 70.90 9.30 LR
Etoxazole N.D. 1 1.03 1.02 103.00 102.00 0.98
Fenoxycarb N.D. 1 1.2 1.23 120.00 123.00 2.47
Fenpyroximate N.D. 1 0.981 0.99 98.10 99.00 0.91
Fipronil N.D. 1 1.01 1.04 101.00 104.00 2.93
Flonicamid N.D. 1 1 1.07 100.00 107.00 6.76
Fludioxonil N.D. 1 1 1.07 100.00 107.00 6.76
Hexythiazox N.D. 1 0.65 0.68 65.00 68.00 4.51 LR
Imazalil N.D. 1 1.39 1.31 139.00 131.00 5.93 HR
Imidacloprid N.D. 1 1.16 1.1 116.00 110.00 5.31
Kresoxim-methyl N.D. 1 1.42 1.37 142.00 137.00 3.58 HR
Malathion N.D. 1 0.998 1.15 99.80 115.00 14.15
Metalaxyl N.D. 1 1.21 1.35 121.00 135.00 10.94 HR
Methiocarb N.D. 1 0.984 0.971 98.40 97.10 1.33
Methomyl N.D. 1 1.11 1.15 111.00 115.00 3.54
MGK-264 N.D. 1 0.897 1 89.70 100.00 10.86
Myclobutanil N.D. 1 1.21 1.3 121.00 130.00 7.17
Naled (dibrom) N.D. 1 0.566 0.552 56.60 55.20 2.50 LR
Oxamyl N.D. 1 1.04 0.966 104.00 96.60 7.38
Paclobutrazol N.D. 1 1.62 1.54 162.00 154.00 5.06 HR
Parathion-methyl N.D. 1 0.885 1.02 88.50 102.00 14.17
Permethrins N.D. 1 0.71 0.772 71.00 77.20 8.37 LR
Phosmet N.D. 1 1.16 1.14 116.00 114.00 1.74
Piperonyl butoxide N.D. 1 1.13 0.91 113.00 91.00 21.57 Q
Prallethrin N.D. 1 1.17 1.14 117.00 114.00 2.60
Propiconazole N.D. 1 1.12 1.06 112.00 106.00 5.50
Propoxur N.D. 1 1.17 0.891 117.00 89.10 27.07 Q
Pyrethrin N.D. 0.65 0.711 0.691 109.38 106.31 2.85
Pyridaben N.D. 1 0.85 0.785 85.00 78.50 7.95
SpinosynA N.D. 0.84 1.15 0.97 136.90 115.48 16.98 HR
SpinosynD N.D. 0.16 0.207 0.202 129.38 126.25 2.44
Spiromesifen N.D. 1 0.412 0.473 41.20 47.30 13.79 LR
Spirotetramat N.D. 1 1.3 1.23 130.00 123.00 5.53
Spiroxamine N.D. 1 1.34 1.26 134.00 126.00 6.15 HR
Tebuconazole N.D. 1 1.37 1.4 137.00 140.00 2.17 HR
Thiacloprid N.D. 1 1.16 1.1 116.00 110.00 5.31
Thiamethoxam N.D. 1 1.38 1.34 138.00 134.00 2.94 HR
Trifloxystrobin N.D. 1 1.09 0.981 109.00 98.10 10.53

N.D. = Not Detected

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 30%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (60-120%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 5 of 11

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-004 Test Certificate #: 123841-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Holy water
License: 030-1009646F7F8
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A401030002C949000000035
Metrc Source Pkg#: 1A401030002C949000000010
Test Conditions

Prepsheet ID#: ORHS200501a
Scale: XS205-OR1
Temp: 22.1 °C
Baro PE: 1012 hPa
Analyst: HRM
Technician: HRM
Sample ID#: 123841

Lot #: Holy water 3/24/20 #1
Batch #: 123841
Batch Weight (g): 337.6
Harvest/Process Date: 03/24/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 04/30/2020
Test Date: 05/01/2020
Sample #123841
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
1,2-Dichloroethane 2 1 Pass/<LOD 1,2-Dimethoxyethane 100 5 Pass/<LOD
1,4-dioxane 380 200 Pass/<LOD 1-Butanol 5,000 100 Pass/<LOD
1-Pentanol 5,000 100 Pass/<LOD 1-Propanol 5,000 100 Pass/<LOD
2,2-Dimethylpropane (Neopentane) 5,000 100 Pass/<LOD 2,2-Dimethylbutane (Hexanes) 290 100 Pass/<LOD
2,3-Dimethylbutane (Hexanes) 290 100 Pass/<LOD 2-Butanol 5,000 100 Pass/<LOD
2-Butanone (MEK) 5,000 50 Pass/<LOD 2-Ethoxyethanol 160 40 Pass/<LOD
2-Methylbutane (Isopentane) 5,000 50 Pass/<LOD 2-Methylpentane (Hexanes) 290 50 Pass/<LOD
2-Methylpropane (Isobutane) 5,000 100 Pass/<LOD 2-propanol (Isopropyl Alcohol) 5,000 50 Pass/122
2-Propanone (Acetone) 5,000 50 Pass/<LOD 3-Methylpentane (Hexanes) 290 50 Pass/<LOD
Acetonitrile 410 100 Pass/<LOD Benzene 2 1 Pass/<LOD
Butane 5,000 100 Pass/1,135 Chloroform 2 1 Pass/<LOD
Cumene 70 50 Pass/<LOD Cyclohexane 3,880 1,000 Pass/<LOD
Dichloromethane 600 50 Pass/<LOD Dimethylsulfoxide (DMSO) 5,000 500 Pass/<LOD
Ethanol 5,000 500 Pass/<LOD Ethyl acetate 5,000 50 Pass/<LOD
Ethyl ether 5,000 500 Pass/<LOD Ethylene glycol 620 310 Pass/<LOD
Ethylene oxide 50 50 Pass/<LOD Heptane 5,000 50 Pass/<LOD
Hexane 290 290 Pass/<LOD Isopropyl acetate 5,000 50 Pass/<LOD
Methanol 3,000 500 Pass/<LOD Naptha 400 100 Pass/<LOD
N,N-Dimethylacetamide 1,090 100 Pass/<LOD N,N-Dimethylformamide (DMF) 880 500 Pass/<LOD
Pentane 5,000 50 Pass/<LOD Petroleum Ether 400 100 Pass/<LOD
Propane 5,000 100 Pass/<LOD Pyridine 200 10 Pass/<LOD
Sulfolane 160 200 Pass/<LOD Tetrahydrofuran (THF) 720 200 Pass/<LOD
Toluene 890 50 Pass/<LOD Trichloroethylene 25 5 Pass/<LOD
Xylenes* 2,170 50 Pass/<LOD

Total Butanes = 1135 ug/g (PASS); Total Pentanes = 0 ug/g (PASS); Total Hexanes = 0 ug/g (PASS)

* Xylenes are reported as the sum of o-xylene, m-xylene, p-xylene, and ethylbenzene
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 6 of 11

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents QC Report
Testing Accreditation #: 4092-004 Test Certificate #: 123841-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Holy water
License: 030-1009646F7F8
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A401030002C949000000035
Metrc Source Pkg#: 1A401030002C949000000010
Test Conditions

Prepsheet ID#: ORHS200501a
Scale: XS205-OR1
Temp: 22.1 °C
Baro PE: 1012 hPa
Analyst: HRM
Technician: HRM
Sample ID#: 123841

Lot #: Holy water 3/24/20 #1
Batch #: 123841
Batch Weight (g): 337.6
Harvest/Process Date: 03/24/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 04/30/2020
Test Date: 05/01/2020
Sample #123841
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS Recovery (%) MSD Recovery (%) Relative Percent Difference (%) QC Flag
1,2-Dichloroethane N.D. 0 0 0 nan nan
n-Propane N.D. 250 80 76 32.00 30.40 5.13 LR
Isobutane N.D. 250 126 132 50.40 52.80 4.65 LR
Methanol N.D. 250 239 229 95.60 91.60 4.27
n-Butane N.D. 250 144 146 57.60 58.40 1.38 LR
2,2-Dimethylpropane N.D. 250 152 157 60.80 62.80 3.24 LR
Ethanol N.D. 250 226 224 90.40 89.60 0.89
Isopentane N.D. 250 166 173 66.40 69.20 4.13 LR
Acetonitrile N.D. 250 207 209 82.80 83.60 0.96
Diethyl ether N.D. 250 218 235 87.20 94.00 7.51
2-propanone N.D. 250 258 263 103.20 105.20 1.92
2-propanol N.D. 250 218 269 87.20 107.60 20.94 Q
n-Pentane N.D. 250 116 123 46.40 49.20 5.86 LR
2,2-Dimethylbutane N.D. 250 194 196 77.60 78.40 1.03
2,3-Dimethylbutane N.D. 250 205 183 82.00 73.20 11.34
Methylene chloride N.D. 250 234 247 93.60 98.80 5.41
2-Methylpentane N.D. 250 198 204 79.20 81.60 2.99
3-Methylpentane N.D. 250 202 208 80.80 83.20 2.93
2-Butanol N.D. 250 247 264 98.80 105.60 6.65
n-Hexane N.D. 250 208 218 83.20 87.20 4.69
Ethyl acetate N.D. 250 240 250 96.00 100.00 4.08
Tetrahydrofuran N.D. 250 234 249 0.00 0.00 0.00
Trichloroethylene N.D. 0 0 0 nan nan
Isopropyl acetate N.D. 250 251 239 0.00 0.00 0.00
Benzene N.D. 250 239 243 95.60 97.20 1.66
Chloroform N.D. 0 0 0 nan nan
Cyclohexane N.D. 250 228 227 91.20 90.80 0.44
Ethylene glycol N.D. 250 173 200 69.20 80.00 14.48 LR
Heptane N.D. 250 203 218 81.20 87.20 7.13
2-Ethoxyethanol N.D. 250 193 198 77.20 79.20 2.56
1,4-Dioxane N.D. 250 243 239 97.20 95.60 1.66
Pyridine N.D. 0 0 0 0.00 0.00 0.00
Toluene N.D. 250 234 251 93.60 100.40 7.01
Chlorobenzene N.D. 0 0 0 0.00 0.00 0.00
Ethylbenzene N.D. 250 240 246 96.00 98.40 2.47
m-Xylene/p-Xylene N.D. 500 481 483 96.20 96.60 0.41
o-Xylene N.D. 250 236 242 94.40 96.80 2.51
Cumene N.D. 250 243 247 97.20 98.80 1.63
Ethylene oxide N.D. 250 224 233 89.60 93.20 3.94

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

N.D. = Not Detected

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 7 of 11

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-004 Test Certificate #: 123841-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Holy water
License: 030-1009646F7F8
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A401030002C949000000035
Metrc Source Pkg#: 1A401030002C949000000010
Test Conditions

Prepsheet ID#: ORHS200501a
Scale: XS205-OR1
Temp: 22.1 °C
Baro PE: 1012 hPa
Analyst: HRM
Technician: HRM
Sample ID#: 123841

Lot #: Holy water 3/24/20 #1
Batch #: 123841
Batch Weight (g): 337.6
Harvest/Process Date: 03/24/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 04/30/2020
Test Date: 05/01/2020
Sample #123841
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
1,2-Dichloroethane 2 1 Pass/<LOD 1,2-Dimethoxyethane 100 5 Pass/<LOD
1,4-dioxane 380 200 Pass/<LOD 1-Butanol 5,000 100 Pass/<LOD
1-Pentanol 5,000 100 Pass/<LOD 1-Propanol 5,000 100 Pass/<LOD
2,2-Dimethylpropane (Neopentane) 5,000 100 Pass/<LOD 2,2-Dimethylbutane (Hexanes) 290 100 Pass/<LOD
2,3-Dimethylbutane (Hexanes) 290 100 Pass/<LOD 2-Butanol 5,000 100 Pass/<LOD
2-Butanone (MEK) 5,000 50 Pass/<LOD 2-Ethoxyethanol 160 40 Pass/<LOD
2-Methylbutane (Isopentane) 5,000 50 Pass/<LOD 2-Methylpentane (Hexanes) 290 50 Pass/<LOD
2-Methylpropane (Isobutane) 5,000 100 Pass/<LOD 2-propanol (Isopropyl Alcohol) 5,000 50 Pass/119
2-Propanone (Acetone) 5,000 50 Pass/<LOD 3-Methylpentane (Hexanes) 290 50 Pass/<LOD
Acetonitrile 410 100 Pass/<LOD Benzene 2 1 Pass/<LOD
Butane 5,000 100 Pass/947 Chloroform 2 1 Pass/<LOD
Cumene 70 50 Pass/<LOD Cyclohexane 3,880 1,000 Pass/<LOD
Dichloromethane 600 50 Pass/<LOD Dimethylsulfoxide (DMSO) 5,000 500 Pass/<LOD
Ethanol 5,000 500 Pass/<LOD Ethyl acetate 5,000 50 Pass/<LOD
Ethyl ether 5,000 500 Pass/<LOD Ethylene glycol 620 310 Pass/<LOD
Ethylene oxide 50 50 Pass/<LOD Heptane 5,000 50 Pass/<LOD
Hexane 290 290 Pass/<LOD Isopropyl acetate 5,000 50 Pass/<LOD
Methanol 3,000 500 Pass/<LOD Naptha 400 100 Pass/<LOD
N,N-Dimethylacetamide 1,090 100 Pass/<LOD N,N-Dimethylformamide (DMF) 880 500 Pass/<LOD
Pentane 5,000 50 Pass/<LOD Petroleum Ether 400 100 Pass/<LOD
Propane 5,000 100 Pass/<LOD Pyridine 200 10 Pass/<LOD
Sulfolane 160 200 Pass/<LOD Tetrahydrofuran (THF) 720 200 Pass/<LOD
Toluene 890 50 Pass/<LOD Trichloroethylene 25 5 Pass/<LOD
Xylenes* 2,170 50 Pass/<LOD

Total Butanes = 948 ug/g (PASS); Total Pentanes = 0 ug/g (PASS); Total Hexanes = 0 ug/g (PASS)

* Xylenes are reported as the sum of o-xylene, m-xylene, p-xylene, and ethylbenzene
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 8 of 11

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents QC Report
Testing Accreditation #: 4092-004 Test Certificate #: 123841-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Holy water
License: 030-1009646F7F8
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A401030002C949000000035
Metrc Source Pkg#: 1A401030002C949000000010
Test Conditions

Prepsheet ID#: ORHS200501a
Scale: XS205-OR1
Temp: 22.1 °C
Baro PE: 1012 hPa
Analyst: HRM
Technician: HRM
Sample ID#: 123841

Lot #: Holy water 3/24/20 #1
Batch #: 123841
Batch Weight (g): 337.6
Harvest/Process Date: 03/24/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 04/30/2020
Test Date: 05/01/2020
Sample #123841
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS Recovery (%) MSD Recovery (%) Relative Percent Difference (%) QC Flag
1,2-Dichloroethane N.D. 0 0 0 nan nan
n-Propane N.D. 250 80 76 32.00 30.40 5.13 LR
Isobutane N.D. 250 126 132 50.40 52.80 4.65 LR
Methanol N.D. 250 239 229 95.60 91.60 4.27
n-Butane N.D. 250 144 146 57.60 58.40 1.38 LR
2,2-Dimethylpropane N.D. 250 152 157 60.80 62.80 3.24 LR
Ethanol N.D. 250 226 224 90.40 89.60 0.89
Isopentane N.D. 250 166 173 66.40 69.20 4.13 LR
Acetonitrile N.D. 250 207 209 82.80 83.60 0.96
Diethyl ether N.D. 250 218 235 87.20 94.00 7.51
2-propanone N.D. 250 258 263 103.20 105.20 1.92
2-propanol N.D. 250 218 269 87.20 107.60 20.94 Q
n-Pentane N.D. 250 116 123 46.40 49.20 5.86 LR
2,2-Dimethylbutane N.D. 250 194 196 77.60 78.40 1.03
2,3-Dimethylbutane N.D. 250 205 183 82.00 73.20 11.34
Methylene chloride N.D. 250 234 247 93.60 98.80 5.41
2-Methylpentane N.D. 250 198 204 79.20 81.60 2.99
3-Methylpentane N.D. 250 202 208 80.80 83.20 2.93
2-Butanol N.D. 250 247 264 98.80 105.60 6.65
n-Hexane N.D. 250 208 218 83.20 87.20 4.69
Ethyl acetate N.D. 250 240 250 96.00 100.00 4.08
Tetrahydrofuran N.D. 250 234 249 0.00 0.00 0.00
Trichloroethylene N.D. 0 0 0 nan nan
Isopropyl acetate N.D. 250 251 239 0.00 0.00 0.00
Benzene N.D. 250 239 243 95.60 97.20 1.66
Chloroform N.D. 0 0 0 nan nan
Cyclohexane N.D. 250 228 227 91.20 90.80 0.44
Ethylene glycol N.D. 250 173 200 69.20 80.00 14.48 LR
Heptane N.D. 250 203 218 81.20 87.20 7.13
2-Ethoxyethanol N.D. 250 193 198 77.20 79.20 2.56
1,4-Dioxane N.D. 250 243 239 97.20 95.60 1.66
Pyridine N.D. 0 0 0 0.00 0.00 0.00
Toluene N.D. 250 234 251 93.60 100.40 7.01
Chlorobenzene N.D. 0 0 0 0.00 0.00 0.00
Ethylbenzene N.D. 250 240 246 96.00 98.40 2.47
m-Xylene/p-Xylene N.D. 500 481 483 96.20 96.60 0.41
o-Xylene N.D. 250 236 242 94.40 96.80 2.51
Cumene N.D. 250 243 247 97.20 98.80 1.63
Ethylene oxide N.D. 250 224 233 89.60 93.20 3.94

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

N.D. = Not Detected

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 9 of 11

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Homogeneity Report by
High Performance Liquid Chromatography
Testing Accreditation #: 4092-004 Test Certificate #: 123841-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Holy water
License: 030-1009646F7F8
Type: AU Tincture
Metrc Test Pkg#: 1A401030002C949000000035
Metrc Source Pkg#: 1A401030002C949000000010
Sample ID#: 123841

Lot #: Holy water 3/24/20 #1
Batch #: 123841
Batch Weight (g): 337.6
Harvest/Process Date: 03/24/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 04/30/2020
Sample #123841
Increments Tested (mg/g) TOTAL THC TOTAL CBD THC THCA THCV CBD CBC CBDA CBDV CBG CBN
Increment 1 677.26 16.36 68.59 694.04 N.D. N.D. 2.31 18.66 N.D. 3.80 2.04
Increment 2 668.60 14.01 58.94 695.17 N.D. N.D. 2.02 15.97 N.D. 3.35 2.01
Average Value 672.93 15.19 63.77 694.61 N.D. N.D. 2.17 17.32 N.D. 3.58 2.03
Max Value 677.26 16.36 68.59 695.17 N.D. N.D. 2.31 18.66 N.D. 3.80 2.04
Min Value 668.60 14.01 58.94 694.04 N.D. N.D. 2.02 15.97 N.D. 3.35 2.01
Relative Percent Difference (RPD) ±1.29 ±15.54 ±15.13 ±0.16 N.D. N.D. ±13.39 ±15.54 N.D. ±12.59 ±1.48
Average Cannabinoids Per Package 672.93 15.19 63.77 694.61 N.D. N.D. 2.17 17.32 N.D. 3.58 2.03
Average Cannabinoids Per Serving 33.65 0.76 3.19 34.73 N.D. N.D. 0.11 0.87 N.D. 0.18 0.10
Max Concentration Per Serving (THC)   Pass
Max Concentration Per Package (THC)   Pass
Relative Percent Difference (RPD)   Pass
Control Study   Yes, MJ1957
Field Duplicate   Pass

N.D. = Not Detected, Min = Minimum, Max = Maximum

RPD is the relative percent difference between increment 1 and increment 2.

RSD is the relative standard deviation between all increments tested.

Total THC and CBD is the calculated sum of CBD or THC and the amount of CBD or THC derived from CBDA or THCA, respectively. These values are calculated by adding a molar correction factor of 0.877 to the CBDA or THCA value.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

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IRON Laboratories

Terpene Report by
Mass Spectrometer
Test Certificate #: 123841-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Holy water
License: 030-1009646F7F8
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A401030002C949000000035
Metrc Source Pkg#: 1A401030002C949000000010

Test Conditions

Scale: XS205-OR1
Temp: 22.1 °C
Baro Pressure: 1012 hPa
Analyst: HRM
Technician: HRM

Sample ID#: 123841

Lot #: Holy water 3/24/20 #1
Batch #: 123841
Batch Weight (g): 337.6
Harvest/Process Date: 03/24/2020
Serving Size (g): 0.05
Date Received: 04/30/2020

Sample #123841
Sample #123841
  • α-Pinene (0.24%)
  • β-Ocimene (0.19%)
  • Camphene (0.07%)
  • Eucalyptol (1,8-Cineol) (0.04%)
  • Sabinene (0.00%)
  • γ-Terpinene (0.03%)
  • Myrcene (0.56%)
  • α-Terpinolene (0.09%)
  • β-Pinene (0.65%)
  • Linalool (0.62%)
  • ∆3-Carene (0.00%)
  • Fenchone (0.00%)
  • α-Terpinene (0.03%)
  • endo-Fenchol (0.33%)
  • α-Ocimene (0.00%)
  • Isopulegol (0.00%)
  • Limonene (0.86%)
  • Geraniol (0.00%)
  • p-Cymene (0.00%)
  • β-Caryophyllene (3.05%)
  • α-Humulene (0.81%)
  • Nerolidol 1 (cis) (0.00%)
  • Nerolidol 2 (trans) (0.06%)
  • Guaiol (0.23%)
  • Caryophyllene Oxide (0.06%)
  • α-Bisabolol (0.19%)
  • α-Phellandrene (0.04%)
  • α-Terpineol (0.23%)
  • Valenence (0.00%)

Total: 8.380%

Predominant Terpenes

3.05%   β-Caryophyllene Sweet, woody, spicy, clove 0.86%   Limonene Citrus, orange, sweet
0.81%   α-Humulene Woody, oceanic-watery, spicy clove 0.65%   β-Pinene Woody, fresh pine, hay
0.62%   Linalool Citrus, floral, sweet, bois de rose, woody, green, blueberry 0.56%   Myrcene Peppery, spicy balsam

Value in parenthesis indicates percentage of terpene present in the total sample (weight percentage, wt/wt%).
Value in doughnut slice indicates individual terpene abundance with respect to the total terpenes detected.

This sample has not been tested according to OAR 333-007. These results should therefore be used for research and development or quality control purposes only.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 11 of 11