IRON LaboratoriesPJLA

ISO/IEC 17025:2005 Accredited

Marihuana Potency Analysis by
High Performance Liquid Chromatography
Testing Accreditation #: 77802 *Test Certificate #: 123691-002
Client Name, Sample Details

Holistic Healing Tim/RoseAnn
Troy, MI 48083
Sample: 7500 FSMCT
Type: Tincture
Method: FE04U HPLC-UV
Test Conditions

Prepsheet ID#: MIP200423
Scale: XS205-MI2
Temp: 21.9 °C
Baro Pressure: 973.8 hPa
Analyst: KEB
Technician: ANJ
Sample ID#: 123691

Harvest/Process Date: 04/22/2020
Serving Size (g): 0.92
Date Received: 04/22/2020
Test Date: 04/23/2020
Valid Through: 04/24/2021
Report Issued: 04/24/2020
Sample #123691
Sample #123691 Sample #123691
Test
Compounds		 THC THCA CBD CBDA CBN CBG* CBC* THCV* CBDV* Total
Cannabinoids*		 Total THC Total CBD Calc Max Total
Cannabinoids*
Amount (%) 0.3 N/D 29.9 0.2 0.2 0.8 0.5 N/D 0.2 32.1 0.3 30.0 32.1
Amount (mg/g) 2.9 N/D 298.7 1.6 1.8 8.3 5.3 N/D 2.1 320.7 2.9 300.1 320.6
Amount per Serving (mg) 2.7 N\D 274.8 1.5 1.7 7.6 4.9 N\D 1.9 295.0 Serving Size~ (g): 0.9
LOQ (mg/g) 0.08 0.08 0.08 0.08 0.08 0.08 0.08 0.08 0.08   %Decarb. THC CBD
±%RPD 0.18 4.12 2.03 1.05 0.61 0.09 1.10 1.04 0.17 100% 99

Serving size = 1 mL

LOQ = Limit of Quantitation; %RPD = Relative Percent Deviation; %RSD = Relative Standard Deviation; N/D = Not Detected

*Designates values that are not currently included in the accredited scope of Iron Laboratories.

*** Designates tests that use the method FE-45. FE-45 is performed using AOAC 966.02 and 32.004-32.009. FE-45 has relative expanded (k=2) uncertainties of 1.098% for moisture, 1.754% for water activity for unprocessed plant materials, and 13.102% for water activity for infused products. Vitamin E acetate analysis has a relative expanded (k=2) uncertainty of 18.614%.

Total THC and CBD is the calculated sum of THC or CBD and the amount of THC or CBD derived from THCA or CBDA, respectively. These values are calculated by applying a molar correction factor of 0.877 to the THCA or the CBDA value. Calc Max Total Cannabinoids is the sum of Total THC, Total CBD, CBN, CBG, CBC, THCV, and CBDV.

%Decarb. THC and CBD refer to the percentage of THC or CBD relative to THCA or CBDA, respectively.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Test Certificate No. 123691-002 supersedes Test Certificate No. 123691-001
JRT LM Iron laboratories JRT LM

Iron Laboratories, LLC is an ISO/IEC 17025:2005 Testing Laboratory laboratory, accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

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IRON LaboratoriesPJLA

ISO/IEC 17025:2005 Accredited

QC Report
Testing Accreditation #: 77802 *Test Certificate #: 123691-002
Client Name, Sample Details

Holistic Healing Tim/RoseAnn
Troy, MI 48083
Sample: 7500 FSMCT
Type: Tincture
Method: FE04U HPLC-UV
Test Conditions

Prepsheet ID#: MIP200423
Scale: XS205-MI2
Temp: 21.9 °C
Baro Pressure: 973.8 hPa
Analyst: KEB
Technician: ANJ
Sample ID#: 123691

Harvest/Process Date: 04/22/2020
Serving Size (g): 0.92
Date Received: 04/22/2020
Test Date: 04/23/2020
Valid Through: 04/24/2021
Report Issued: 04/24/2020
Sample #123691
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Cannabidivarin (CBDV) 0 5.87794 5.96862 101.54 5.95866 101.37 0.17
Cannabidiolic Acid (CBDA) 0 4.7973 5.01483 104.53 4.96269 103.45 1.05
Cannabigerol (CBG) 0 5.3562 5.58972 104.36 5.59454 104.45 0.09
Cannabidiol (CBD) 0 5.59185 5.94221 106.27 5.82286 104.13 2.03
Δ9-Tetrahydrocannabivarin (THCV) 0 6.00145 6.06311 101.03 6.00029 99.98 1.04
Cannabinol (CBN) 0 5.98521 6.11815 102.22 6.08076 101.60 0.61
Δ9-Tetrahydrocannabinol (THC) 0 6.11121 5.92489 96.95 5.91417 96.78 0.18
Cannabichromene (CBC) 0 3.90064 4.14747 106.33 4.19343 107.51 1.10
Tetrahydrocannabinolic acid (THCA) 0 4.36834 4.62503 105.88 4.43853 101.61 4.12

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Test Certificate No. 123691-002 supersedes Test Certificate No. 123691-001
JRT LM Iron laboratories JRT LM

Iron Laboratories, LLC is an ISO/IEC 17025:2005 Testing Laboratory laboratory, accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

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