IRON LaboratoriesPJLA

ISO/IEC 17025:2005 Accredited

Marihuana Potency Analysis by
High Performance Liquid Chromatography

Testing Accreditation #: 77802 Test Certificate #: 123470-001
Client Name, Sample Details

Dan Mcglinchey
Dearborn Heights, MI 48427
Sample: 3 W Cure
License: 238805-265124
Type: Flower
Method: FE04U HPLC-UV

Test Conditions

Prepsheet ID#: MIP200406
Scale: XS205-MI2
Temp: 21.6 °C
Baro Pressure: 984.1 hPa
Analyst: KEB
Technician: KEB/ANJ

Sample ID#: 123470

Harvest/Process Date: 04/06/2020
Serving Size (g): 1
Date Received: 04/06/2020
Test Date: 04/06/2020
Valid Through: 04/07/2021
Report Issued: 04/07/2020

Sample #123470
Sample #123470 Sample #123470
Test
Compounds
THC THCA CBD CBDA CBN CBG* CBC* THCV* CBDV* Total
Cannabinoids*
Total THC Total CBD Calc Max Total
Cannabinoids*
Amount (%) 2.4 23.8 N/D 0.3 N/D 0.1 N/D N/D N/D 26.6 23.3 0.3 23.6
Amount (mg/g) 23.6 238.2 N/D 3.4 N/D 1.0 N/D N/D N/D 266.2 232.5 3.0 236.5
Amount per Serving (mg) 23.6 238.2 N\D 3.4 N\D 1.0 N\D N\D N\D 266.2 Serving Size~ (g): 1.0
LOQ (mg/g) 0.99 0.99 0.99 0.99 0.99 0.99 0.99 0.99 0.99   %Decarb. THC CBD
±%RPD 2.53 5.19 0.46 1.42 0.49 0.80 1.05 0.81 0.03 9 0%

LOQ = Limit of Quantitation; %RPD = Relative Percent Deviation; %RSD = Relative Standard Deviation; N/D = Not Detected

*Designates values that are not currently included in the accredited scope of Iron Laboratories.

*** Designates tests that use the method FE-45. FE-45 is performed using AOAC 966.02 and 32.004-32.009. FE-45 has relative expanded (k=2) uncertainties of 1.098% for moisture, 1.754% for water activity for unprocessed plant materials, and 13.102% for water activity for infused products. Vitamin E acetate analysis has a relative expanded (k=2) uncertainty of 18.614%.

Total THC and CBD is the calculated sum of THC or CBD and the amount of THC or CBD derived from THCA or CBDA, respectively. These values are calculated by applying a molar correction factor of 0.877 to the THCA or the CBDA value. Calc Max Total Cannabinoids is the sum of Total THC, Total CBD, CBN, CBG, CBC, THCV, and CBDV.

%Decarb. THC and CBD refer to the percentage of THC or CBD relative to THCA or CBDA, respectively.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

JRT LM Iron laboratories JRT LM

Iron Laboratories, LLC is an ISO/IEC 17025:2005 Testing Laboratory laboratory, accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

Page 1 of 2

IRON LaboratoriesPJLA

ISO/IEC 17025:2005 Accredited

QC Report

Testing Accreditation #: 77802 Test Certificate #: 123470-001
Client Name, Sample Details

Dan Mcglinchey
Dearborn Heights, MI 48427
Sample: 3 W Cure
License: 238805-265124
Type: Flower
Method: FE04U HPLC-UV

Test Conditions

Prepsheet ID#: MIP200406
Scale: XS205-MI2
Temp: 21.6 °C
Baro Pressure: 984.1 hPa
Analyst: KEB
Technician: KEB/ANJ

Sample ID#: 123470

Harvest/Process Date: 04/06/2020
Serving Size (g): 1
Date Received: 04/06/2020
Test Date: 04/06/2020
Valid Through: 04/07/2021
Report Issued: 04/07/2020

Sample #123470
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Cannabidivarin (CBDV) 0 5.86712 6.08227 103.67 6.08073 103.64 0.03
Cannabidiolic Acid (CBDA) 0 4.77868 4.93837 103.34 5.00901 104.82 1.42
Cannabigerol (CBG) 0 5.32431 5.48235 102.97 5.52642 103.80 0.80
Cannabidiol (CBD) 0 5.62258 5.85506 104.13 5.88179 104.61 0.46
Δ9-Tetrahydrocannabivarin (THCV) 0 5.82952 6.00084 102.94 6.04993 103.78 0.81
Cannabinol (CBN) 0 5.99484 6.17707 103.04 6.20758 103.55 0.49
Δ9-Tetrahydrocannabinol (THC) 0 6.20014 6.34789 102.38 6.51086 105.01 2.53
Cannabichromene (CBC) 0 4.56636 4.52417 99.08 4.572 100.12 1.05
Tetrahydrocannabinolic acid (THCA) 0 4.28591 4.38408 102.29 4.61752 107.74 5.19

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

JRT LM Iron laboratories JRT LM

Iron Laboratories, LLC is an ISO/IEC 17025:2005 Testing Laboratory laboratory, accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

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IRON LaboratoriesPJLA

ISO/IEC 17025:2005 Accredited

Bio Analysis by
Microscopic Visual Inspection

Testing Accreditation #: 77802 Test Certificate #: 123470-001
Client Name, Sample Details

Dan Mcglinchey
Dearborn Heights, MI 48427
Sample: 3 W Cure
License: 238805-265124
Type: Flower
Method: FE02 Microscope Dissection

Test Conditions

Analyst: ACR
Technician: ACR

Sample ID#: 123470

Harvest/Process Date: 04/06/2020
Serving Size (g): 1
Date Received: 04/06/2020
Test Date: 04/23/2020
Valid Through: 04/23/2021
Report Issued: 04/23/2020

Sample #123470
Sample #123470 Sample #123470
Severity Rating
Mold and Mildew 0 Pass
Mites (not Russet) 0 Pass
Russet Mites 0 Pass
Thrips 0 Pass
Aphids 0 Pass
Other Pests 0 Pass
Other Organic Matter 0 Pass
Inorganic Matter 0 Pass
Total Organic Foreign Matter <2% Pass
Inorganic Foreign Matter 0% Pass
Stem Material <5% Pass
Severity Rating Key
Correlating %FM ≤2% FM >2% FM
Severity Rating 0 None 1 Mild 2 Moderate 3 Severe Units
Mold and Mildew <2 2 3 4+ Locations/g
Mites (not russet) <1 1-5 6-10 11+ Amount/g
Russet Mites <1 1-10 11-50 51+ Amount/g
Thrips <1 1-3 4-5 6+ Amount/g
Aphids <1 1 2-4 5+ Amount/g
Other Pests <1 1-5 6-10 11+ Amount/g
Other Organic Matter <1 1-5 6-10 11+ Amount/g
Inorganic Matter 0 >0 Amount/g

In compliance with the MMFLA regulation, the action limits for foreign matter are as follows; no more that 2% organic matter, 5% stem material, and no presence of inorganic matter. Percent foreign contamination is based off of total surface area.

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

MEH QM Iron laboratories MEH QM

Iron Laboratories, LLC is an ISO/IEC 17025:2005 Testing Laboratory laboratory, accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

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