ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Marijuana Potency Analysis by
High Performance Liquid Chromatography
Testing Accreditation #: 4092-004 Test Certificate #: 123371-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Northern Wreck Badder
License: 030-1009646F7F8
Type: AU Tincture
Method: FE04U HPLC-UV
Metrc Test Pkg#: 1A401030002C949000000017
Metrc Source Pkg#: 1A401030002C949000000016
Test Conditions

Prepsheet ID#: ORP200402b
Scale: XS205-OR1
Temp: 22.4 °C
Baro Pressure: 1007 hPa
Analyst: HRM
Technician: TMR
Sample ID#: 123371

Lot #: Northern wreck badder 3/30/20 #1
Batch #: 123371
Batch Weight (g): 1640.4
Harvest/Process Date: 03/31/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 03/31/2020
Test Date: 04/02/2020
Sample #123371
Sample #123371 Sample #123371
Test
Compounds		 THC THCA CBD CBDA CBN CBG CBC THCV* CBDV Total
Cannabinoids*		 Total THC Total CBD Calc Max Total
Cannabinoids*
Amount (%) 2.99 70.61 N/D 1.62 0.21 0.45 N/D N/D N/D 75.88 64.91 1.42 66.99
Amount (mg/g) 29.91 706.07 N/D 16.23 2.05 4.52 N/D N/D N/D 758.78 649.13 14.23 669.93
Amount per Serving (mg) 1.50 35.30 N\D 0.81 0.10 0.23 N\D N\D N\D 37.94 Serving Size~ (g): 0.05
LOQ (mg/g) 1.9 1.9 1.9 1.9 1.9 1.9 1.9 1.9 1.9   %Decarb. THC CBD
±%RPD 8.08 6.78 10.32 10.42 8.05 9.79 20.87 8.87 9.33 4 0

LOQ = Limit of Quantitation; %RPD = Relative Percent Deviation; %RSD = Relative Standard Deviation; N/D = Not Detected

*Designates values that are not currently included in the accredited scope of Iron Laboratories.

*** Designates tests that use the method FE-45. FE-45 is performed using AOAC 966.02 and 32.004-32.009. FE-45 has relative expanded (k=2) uncertainties of 1.098% for moisture, 1.754% for water activity for unprocessed plant materials, and 13.102% for water activity for infused products. Vitamin E acetate analysis has a relative expanded (k=2) uncertainty of 18.614%.

Total THC and CBD is the calculated sum of THC or CBD and the amount of THC or CBD derived from THCA or CBDA, respectively. These values are calculated by applying a molar correction factor of 0.877 to the THCA or the CBDA value. Calc Max Total Cannabinoids is the sum of Total THC, Total CBD, CBN, CBG, CBC, THCV, and CBDV.

%Decarb. THC and CBD refer to the percentage of THC or CBD relative to THCA or CBDA, respectively.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 1 of 67

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant QC Report
Testing Accreditation #: 4092-004 Test Certificate #: 123371-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Northern Wreck Badder
License: 030-1009646F7F8
Type: AU Tincture
Method: FE04U HPLC-UV
Metrc Test Pkg#: 1A401030002C949000000017
Metrc Source Pkg#: 1A401030002C949000000016
Test Conditions

Prepsheet ID#: ORP200402b
Scale: XS205-OR1
Temp: 22.4 °C
Baro Pressure: 1007 hPa
Analyst: HRM
Technician: TMR
Sample ID#: 123371

Lot #: Northern wreck badder 3/30/20 #1
Batch #: 123371
Batch Weight (g): 1640.4
Harvest/Process Date: 03/31/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 03/31/2020
Test Date: 04/02/2020
Sample #123371
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Cannabidivarin (CBDV) N.D. 5.5 5.62 102.18 6.17 112.18 9.33
Cannabidiolic Acid (CBDA) N.D. 5.27 5.55 105.31 6.16 116.89 10.42
Cannabigerol (CBG) N.D. 5.47 5.54 101.28 6.11 111.70 9.79
Cannabidiol (CBD) N.D. 5.66 5.88 103.89 6.52 115.19 10.32
Δ9-Tetrahydrocannabivarin (THCV) N.D. 5.24 5.28 100.76 5.77 110.11 8.87
Cannabinol (CBN) N.D. 5.52 5.6 101.45 6.07 109.96 8.05
Δ9-Tetrahydrocannabinol (THC) N.D. 5.48 5.58 101.82 6.05 110.40 8.08
Cannabichromene (CBC) N.D. 7.33 6.18 84.31 7.62 103.96 20.87
Tetrahydrocannabinolic acid (THCA) N.D. 5.13 5.27 102.73 5.64 109.94 6.78

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Himashi Mead Iron laboratories Himashi Mead

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 2 of 67

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Pesticide Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-004 Test Certificate #: 123371-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Northern Wreck Badder
License: 030-1009646F7F8
Type: AU Tincture
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A401030002C949000000017
Metrc Source Pkg#: 1A401030002C949000000016
Test Conditions

Prepsheet ID#: ORPS200403B
Scale: XS205-OR1
Temp: 21.7 °C
Baro PE: 1005 hPa
Analyst: JER
Technician: JER
Sample ID#: 123371

Lot #: Northern wreck badder 3/30/20 #1
Batch #: 123371
Batch Weight (g): 1640.4
Harvest/Process Date: 03/31/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 03/31/2020
Test Date: 04/06/2020
Sample #123371
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
Aldicarb 0.400 0.132 Pass/<LOD Abamectin**** 0.500 0.132 Pass/<LOD
Acephate 0.400 0.132 Pass/<LOD Acequinocyl 2.000 0.265 Pass/<LOD
Acetamiprid 0.200 0.132 Pass/<LOD Azoxystrobin 0.200 0.132 Pass/<LOD
Bifenazate 0.200 0.132 Pass/<LOD Bifenthrin 0.200 0.132 Pass/<LOD
Boscalid 0.400 0.132 Pass/<LOD Carbaryl 0.200 0.132 Pass/<LOD
Carbofuran 0.200 0.132 Pass/<LOD Chlorantraniliprole 0.200 0.132 Pass/<LOD
Chlorfenapyr 1.000 0.530 Pass/<LOD Chlorpyrifos 0.200 0.132 Pass/<LOD
Clofentezine 0.200 0.132 Pass/<LOD Cyfluthrin** 1.000 0.530 Pass/<LOD
Cypermethrin*** 1.000 0.530 Pass/<LOD Daminozide 1.000 0.132 Pass/<LOD
DDVP (Dichlorvos) 1.000 0.265 Pass/<LOD Diazinon 0.200 0.132 Pass/<LOD
Dimethoate 0.200 0.132 Pass/<LOD Ethoprophos 0.200 0.132 Pass/<LOD
Etofenprox 0.400 0.132 Pass/<LOD Etoxazole 0.200 0.132 Pass/<LOD
Fenoxycarb 0.200 0.132 Pass/<LOD Fenpyroximate 0.400 0.132 Pass/<LOD
Fipronil 0.400 0.132 Pass/<LOD Flonicamid 1.000 0.132 Pass/<LOD
Fludioxonil 0.400 0.132 Pass/<LOD Hexythiazox 1.000 0.132 Pass/<LOD
Imazalil 0.200 0.132 Pass/<LOD Imidacloprid 0.400 0.132 Pass/<LOD
Kresoxim Methyl 0.400 0.132 Pass/<LOD Malathion 0.200 0.132 Pass/<LOD
Metalaxyl 0.200 0.132 Pass/<LOD Methiocarb 0.200 0.132 Pass/<LOD
Methomyl 0.400 0.132 Pass/<LOD Methyl Parathion 0.200 0.132 Pass/<LOD
MGK-264‡ 0.200 0.132 Pass/<LOD Myclobutanil 0.000 0.132 Pass/<LOD
Naled 0.500 0.132 Pass/<LOD Oxamyl 1.000 0.132 Pass/<LOD
Paclobutrazol 0.400 0.132 Pass/<LOD Permethrins† 0.200 0.132 Pass/<LOD
Phosmet 0.200 0.132 Pass/<LOD Piperonyl Butoxide 2.000 0.132 Pass/<LOD
Prallethrin 0.200 0.132 Pass/<LOD Propiconazole 0.400 0.132 Pass/<LOD
Propoxur 0.200 0.132 Pass/<LOD Pyrethrins* 1.000 0.132 Pass/<LOD
Pyridaben 0.200 0.132 Pass/<LOD Spinosad***** 0.200 0.132 Pass/<LOD
Spiromesifen 0.200 0.132 Pass/<LOD Spirotetramat 0.200 0.132 Pass/<LOD
Spiroxamine‡ 0.400 0.132 Pass/<LOD Tebuconazole 0.400 0.132 Pass/<LOD
Thiacloprid 0.200 0.132 Pass/<LOD Thiamethoxam 0.200 0.132 Pass/<LOD
Trifloxystrobin 0.200 0.132 Pass/<LOD

* Pyrethrins are reported as the sum of Jasmolin I, Cinerin I, and Pyrethrin I
** Cyfluthrins are reported as the sum of isomers Cyfluthrin I, II, III, and IV
*** Cypermethrins are reported as the sum of isomers Cypermethrin I, II, III, and IV
**** Abamectin is reported as the sum of Avermectin B1a and Avermectin B1b
***** Spinosad is reported as the sum of Spinosyn A and Spinosyn D
† Permethrin and Prallethrin are reported as the sum of cis and trans isomers
‡ MGK-264 and Spiroximine are reported as the sum of isomers I and II
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 2 of 67

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Pesticide QC Report
Testing Accreditation #: 4092-004 Test Certificate #: 123371-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Northern Wreck Badder
License: 030-1009646F7F8
Type: AU Tincture
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A401030002C949000000017
Metrc Source Pkg#: 1A401030002C949000000016
Test Conditions

Prepsheet ID#: ORPS200403B
Scale: XS205-OR1
Temp: 21.7 °C
Baro PE: 1005 hPa
Analyst: JER
Technician: JER
Sample ID#: 123371

Lot #: Northern wreck badder 3/30/20 #1
Batch #: 123371
Batch Weight (g): 1640.4
Harvest/Process Date: 03/31/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 03/31/2020
Test Date: 04/06/2020
Sample #123371
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS recovery% MSD recovery% Relative Percent Difference (%) QC Flag
Acephate N.D. 1 1.04 0.908 104.00 90.80 13.55
Acequinocyl N.D. 1 0.518 0.531 51.80 53.10 2.48 LR
Acetamiprid N.D. 1 1.17 1.06 117.00 106.00 9.87
Aldicarb N.D. 1 0.871 0.817 87.10 81.70 6.40
Avermectin B1a N.D. 0.97 2.24 1.62 230.93 167.01 32.12 HRQ
Azoxystrobin N.D. 1 1.11 1.01 111.00 101.00 9.43
Bifenazate N.D. 1 1.08 0.909 108.00 90.90 17.19
Bifenthrin N.D. 1 0.805 0.829 80.50 82.90 2.94
Boscalid N.D. 1 0.87 0.998 87.00 99.80 13.70
Carbaryl N.D. 1 0.938 0.875 93.80 87.50 6.95
Carbofuran N.D. 1 1.09 1.01 109.00 101.00 7.62
Chlorantraniliprole N.D. 1 1.35 1.21 135.00 121.00 10.94 HR
Chlorfenapyr N.D. 1 0.82 0.878 82.00 87.80 6.83
Chlorpyriphos N.D. 1 0.91 0.886 91.00 88.60 2.67
Clofentezine N.D. 1 1.03 0.982 103.00 98.20 4.77
Cyfluthrin N.D. 1 1.1 1 110.00 100.00 9.52
Cypermethrin N.D. 1 1.16 1.06 116.00 106.00 9.01
Daminoside N.D. 1 1.16 1.12 116.00 112.00 3.51
Diazanon N.D. 1 1.12 1.06 112.00 106.00 5.50
Dichlorvos N.D. 1 0.806 0.644 80.60 64.40 22.34 LRQ
Dimethoate N.D. 1 1.06 0.908 106.00 90.80 15.45
Ethoprophos N.D. 1 0.879 0.8 87.90 80.00 9.41
Etofenprox N.D. 1 0.914 0.87 91.40 87.00 4.93
Etoxazole N.D. 1 1.09 0.966 109.00 96.60 12.06
Fenoxycarb N.D. 1 1.31 1.15 131.00 115.00 13.01 HR
Fenpyroximate N.D. 1 1.01 0.99 101.00 99.00 2.00
Fipronil N.D. 1 1.06 1.01 106.00 101.00 4.83
Flonicamid N.D. 1 1.05 0.955 105.00 95.50 9.48
Fludioxonil N.D. 1 1.01 0.989 101.00 98.90 2.10
Hexythiazox N.D. 1 0.763 0.737 76.30 73.70 3.47
Imazalil N.D. 1 1.55 1.23 155.00 123.00 23.02 HRQ
Imidacloprid N.D. 1 1.13 1 113.00 100.00 12.21
Kresoxim-methyl N.D. 1 1.56 1.33 156.00 133.00 15.92 HR
Malathion N.D. 1 1.17 1.19 117.00 119.00 1.69
Metalaxyl N.D. 1 1.29 1.23 129.00 123.00 4.76
Methiocarb N.D. 1 1.09 0.925 109.00 92.50 16.38
Methomyl N.D. 1 1.25 1.14 125.00 114.00 9.21
MGK-264 N.D. 1 0.905 0.759 90.50 75.90 17.55
Myclobutanil N.D. 1 1.32 1.29 132.00 129.00 2.30 HR
Naled (dibrom) N.D. 1 0.671 0.567 67.10 56.70 16.80 LR
Oxamyl N.D. 1 1.06 0.902 106.00 90.20 16.11
Paclobutrazol N.D. 1 1.69 1.48 169.00 148.00 13.25 HR
Parathion-methyl N.D. 1 1.11 0.896 111.00 89.60 21.34 Q
Permethrins N.D. 1 0.886 0.821 88.60 82.10 7.62
Phosmet N.D. 1 1.37 1.23 137.00 123.00 10.77 HR
Piperonyl butoxide N.D. 1 1.1 1.03 110.00 103.00 6.57
Prallethrin N.D. 1 1.43 1.43 143.00 143.00 0.00 HR
Propiconazole N.D. 1 1.12 1.07 112.00 107.00 4.57
Propoxur N.D. 1 1.07 0.945 107.00 94.50 12.41
Pyrethrin N.D. 0.65 0.788 0.735 121.23 113.08 6.96
Pyridaben N.D. 1 0.879 0.787 87.90 78.70 11.04
SpinosynA N.D. 0.84 1.23 1.08 146.43 128.57 12.99 HR
SpinosynD N.D. 0.16 0.232 0.227 145.00 141.88 2.18 HR
Spiromesifen N.D. 1 0.817 0.807 81.70 80.70 1.23
Spirotetramat N.D. 1 1.86 1.42 186.00 142.00 26.83 HRQ
Spiroxamine N.D. 1 1.42 1.26 142.00 126.00 11.94 HR
Tebuconazole N.D. 1 1.38 1.27 138.00 127.00 8.30 HR
Thiacloprid N.D. 1 1.16 1.02 116.00 102.00 12.84
Thiamethoxam N.D. 1 1.57 1.42 157.00 142.00 10.03 HR
Trifloxystrobin N.D. 1 1.12 0.996 112.00 99.60 11.72

N.D. = Not Detected

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 30%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (60-120%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 3 of 67

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Pesticide Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-004 Test Certificate #: 123371-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Northern Wreck Badder
License: 030-1009646F7F8
Type: AU Tincture
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A401030002C949000000017
Metrc Source Pkg#: 1A401030002C949000000016
Test Conditions

Prepsheet ID#: ORPS200403B
Scale: XS205-OR1
Temp: 21.7 °C
Baro PE: 1005 hPa
Analyst: JER
Technician: JER
Sample ID#: 123371

Lot #: Northern wreck badder 3/30/20 #1
Batch #: 123371
Batch Weight (g): 1640.4
Harvest/Process Date: 03/31/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 03/31/2020
Test Date: 04/06/2020
Sample #123371
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
Aldicarb 0.400 0.127 Pass/<LOD Abamectin**** 0.500 0.127 Pass/<LOD
Acephate 0.400 0.127 Pass/<LOD Acequinocyl 2.000 0.255 Pass/<LOD
Acetamiprid 0.200 0.127 Pass/<LOD Azoxystrobin 0.200 0.127 Pass/<LOD
Bifenazate 0.200 0.127 Pass/<LOD Bifenthrin 0.200 0.127 Pass/<LOD
Boscalid 0.400 0.127 Pass/<LOD Carbaryl 0.200 0.127 Pass/<LOD
Carbofuran 0.200 0.127 Pass/<LOD Chlorantraniliprole 0.200 0.127 Pass/<LOD
Chlorfenapyr 1.000 0.509 Pass/<LOD Chlorpyrifos 0.200 0.127 Pass/<LOD
Clofentezine 0.200 0.127 Pass/<LOD Cyfluthrin** 1.000 0.509 Pass/<LOD
Cypermethrin*** 1.000 0.509 Pass/<LOD Daminozide 1.000 0.127 Pass/<LOD
DDVP (Dichlorvos) 1.000 0.255 Pass/<LOD Diazinon 0.200 0.127 Pass/<LOD
Dimethoate 0.200 0.127 Pass/<LOD Ethoprophos 0.200 0.127 Pass/<LOD
Etofenprox 0.400 0.127 Pass/<LOD Etoxazole 0.200 0.127 Pass/<LOD
Fenoxycarb 0.200 0.127 Pass/<LOD Fenpyroximate 0.400 0.127 Pass/<LOD
Fipronil 0.400 0.127 Pass/<LOD Flonicamid 1.000 0.127 Pass/<LOD
Fludioxonil 0.400 0.127 Pass/<LOD Hexythiazox 1.000 0.127 Pass/<LOD
Imazalil 0.200 0.127 Pass/<LOD Imidacloprid 0.400 0.127 Pass/<LOD
Kresoxim Methyl 0.400 0.127 Pass/<LOD Malathion 0.200 0.127 Pass/<LOD
Metalaxyl 0.200 0.127 Pass/<LOD Methiocarb 0.200 0.127 Pass/<LOD
Methomyl 0.400 0.127 Pass/<LOD Methyl Parathion 0.200 0.127 Pass/<LOD
MGK-264‡ 0.200 0.127 Pass/<LOD Myclobutanil 0.000 0.127 Pass/<LOD
Naled 0.500 0.127 Pass/<LOD Oxamyl 1.000 0.127 Pass/<LOD
Paclobutrazol 0.400 0.127 Pass/<LOD Permethrins† 0.200 0.127 Pass/<LOD
Phosmet 0.200 0.127 Pass/<LOD Piperonyl Butoxide 2.000 0.127 Pass/<LOD
Prallethrin 0.200 0.127 Pass/<LOD Propiconazole 0.400 0.127 Pass/<LOD
Propoxur 0.200 0.127 Pass/<LOD Pyrethrins* 1.000 0.127 Pass/<LOD
Pyridaben 0.200 0.127 Pass/<LOD Spinosad***** 0.200 0.127 Pass/<LOD
Spiromesifen 0.200 0.127 Pass/<LOD Spirotetramat 0.200 0.127 Pass/<LOD
Spiroxamine‡ 0.400 0.127 Pass/<LOD Tebuconazole 0.400 0.127 Pass/<LOD
Thiacloprid 0.200 0.127 Pass/<LOD Thiamethoxam 0.200 0.127 Pass/<LOD
Trifloxystrobin 0.200 0.127 Pass/<LOD

* Pyrethrins are reported as the sum of Jasmolin I, Cinerin I, and Pyrethrin I
** Cyfluthrins are reported as the sum of isomers Cyfluthrin I, II, III, and IV
*** Cypermethrins are reported as the sum of isomers Cypermethrin I, II, III, and IV
**** Abamectin is reported as the sum of Avermectin B1a and Avermectin B1b
***** Spinosad is reported as the sum of Spinosyn A and Spinosyn D
† Permethrin and Prallethrin are reported as the sum of cis and trans isomers
‡ MGK-264 and Spiroximine are reported as the sum of isomers I and II
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 4 of 67

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Pesticide QC Report
Testing Accreditation #: 4092-004 Test Certificate #: 123371-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Northern Wreck Badder
License: 030-1009646F7F8
Type: AU Tincture
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A401030002C949000000017
Metrc Source Pkg#: 1A401030002C949000000016
Test Conditions

Prepsheet ID#: ORPS200403B
Scale: XS205-OR1
Temp: 21.7 °C
Baro PE: 1005 hPa
Analyst: JER
Technician: JER
Sample ID#: 123371

Lot #: Northern wreck badder 3/30/20 #1
Batch #: 123371
Batch Weight (g): 1640.4
Harvest/Process Date: 03/31/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 03/31/2020
Test Date: 04/06/2020
Sample #123371
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS recovery% MSD recovery% Relative Percent Difference (%) QC Flag
Acephate N.D. 1 1.04 0.908 104.00 90.80 13.55
Acequinocyl N.D. 1 0.518 0.531 51.80 53.10 2.48 LR
Acetamiprid N.D. 1 1.17 1.06 117.00 106.00 9.87
Aldicarb N.D. 1 0.871 0.817 87.10 81.70 6.40
Avermectin B1a N.D. 0.97 2.24 1.62 230.93 167.01 32.12 HRQ
Azoxystrobin N.D. 1 1.11 1.01 111.00 101.00 9.43
Bifenazate N.D. 1 1.08 0.909 108.00 90.90 17.19
Bifenthrin N.D. 1 0.805 0.829 80.50 82.90 2.94
Boscalid N.D. 1 0.87 0.998 87.00 99.80 13.70
Carbaryl N.D. 1 0.938 0.875 93.80 87.50 6.95
Carbofuran N.D. 1 1.09 1.01 109.00 101.00 7.62
Chlorantraniliprole N.D. 1 1.35 1.21 135.00 121.00 10.94 HR
Chlorfenapyr N.D. 1 0.82 0.878 82.00 87.80 6.83
Chlorpyriphos N.D. 1 0.91 0.886 91.00 88.60 2.67
Clofentezine N.D. 1 1.03 0.982 103.00 98.20 4.77
Cyfluthrin N.D. 1 1.1 1 110.00 100.00 9.52
Cypermethrin N.D. 1 1.16 1.06 116.00 106.00 9.01
Daminoside N.D. 1 1.16 1.12 116.00 112.00 3.51
Diazanon N.D. 1 1.12 1.06 112.00 106.00 5.50
Dichlorvos N.D. 1 0.806 0.644 80.60 64.40 22.34 LRQ
Dimethoate N.D. 1 1.06 0.908 106.00 90.80 15.45
Ethoprophos N.D. 1 0.879 0.8 87.90 80.00 9.41
Etofenprox N.D. 1 0.914 0.87 91.40 87.00 4.93
Etoxazole N.D. 1 1.09 0.966 109.00 96.60 12.06
Fenoxycarb N.D. 1 1.31 1.15 131.00 115.00 13.01 HR
Fenpyroximate N.D. 1 1.01 0.99 101.00 99.00 2.00
Fipronil N.D. 1 1.06 1.01 106.00 101.00 4.83
Flonicamid N.D. 1 1.05 0.955 105.00 95.50 9.48
Fludioxonil N.D. 1 1.01 0.989 101.00 98.90 2.10
Hexythiazox N.D. 1 0.763 0.737 76.30 73.70 3.47
Imazalil N.D. 1 1.55 1.23 155.00 123.00 23.02 HRQ
Imidacloprid N.D. 1 1.13 1 113.00 100.00 12.21
Kresoxim-methyl N.D. 1 1.56 1.33 156.00 133.00 15.92 HR
Malathion N.D. 1 1.17 1.19 117.00 119.00 1.69
Metalaxyl N.D. 1 1.29 1.23 129.00 123.00 4.76
Methiocarb N.D. 1 1.09 0.925 109.00 92.50 16.38
Methomyl N.D. 1 1.25 1.14 125.00 114.00 9.21
MGK-264 N.D. 1 0.905 0.759 90.50 75.90 17.55
Myclobutanil N.D. 1 1.32 1.29 132.00 129.00 2.30 HR
Naled (dibrom) N.D. 1 0.671 0.567 67.10 56.70 16.80 LR
Oxamyl N.D. 1 1.06 0.902 106.00 90.20 16.11
Paclobutrazol N.D. 1 1.69 1.48 169.00 148.00 13.25 HR
Parathion-methyl N.D. 1 1.11 0.896 111.00 89.60 21.34 Q
Permethrins N.D. 1 0.886 0.821 88.60 82.10 7.62
Phosmet N.D. 1 1.37 1.23 137.00 123.00 10.77 HR
Piperonyl butoxide N.D. 1 1.1 1.03 110.00 103.00 6.57
Prallethrin N.D. 1 1.43 1.43 143.00 143.00 0.00 HR
Propiconazole N.D. 1 1.12 1.07 112.00 107.00 4.57
Propoxur N.D. 1 1.07 0.945 107.00 94.50 12.41
Pyrethrin N.D. 0.65 0.788 0.735 121.23 113.08 6.96
Pyridaben N.D. 1 0.879 0.787 87.90 78.70 11.04
SpinosynA N.D. 0.84 1.23 1.08 146.43 128.57 12.99 HR
SpinosynD N.D. 0.16 0.232 0.227 145.00 141.88 2.18 HR
Spiromesifen N.D. 1 0.817 0.807 81.70 80.70 1.23
Spirotetramat N.D. 1 1.86 1.42 186.00 142.00 26.83 HRQ
Spiroxamine N.D. 1 1.42 1.26 142.00 126.00 11.94 HR
Tebuconazole N.D. 1 1.38 1.27 138.00 127.00 8.30 HR
Thiacloprid N.D. 1 1.16 1.02 116.00 102.00 12.84
Thiamethoxam N.D. 1 1.57 1.42 157.00 142.00 10.03 HR
Trifloxystrobin N.D. 1 1.12 0.996 112.00 99.60 11.72

N.D. = Not Detected

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 30%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (60-120%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 5 of 67

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Pesticide Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-004 Test Certificate #: 123371-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Northern Wreck Badder
License: 030-1009646F7F8
Type: AU Tincture
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A401030002C949000000017
Metrc Source Pkg#: 1A401030002C949000000016
Test Conditions

Prepsheet ID#: ORPS200403B
Scale: XS205-OR1
Temp: 21.7 °C
Baro PE: 1005 hPa
Analyst: JER
Technician: JER
Sample ID#: 123371

Lot #: Northern wreck badder 3/30/20 #1
Batch #: 123371
Batch Weight (g): 1640.4
Harvest/Process Date: 03/31/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 03/31/2020
Test Date: 04/06/2020
Sample #123371
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
Aldicarb 0.400 0.134 Pass/<LOD Abamectin**** 0.500 0.134 Pass/<LOD
Acephate 0.400 0.134 Pass/<LOD Acequinocyl 2.000 0.269 Pass/<LOD
Acetamiprid 0.200 0.134 Pass/<LOD Azoxystrobin 0.200 0.134 Pass/<LOD
Bifenazate 0.200 0.134 Pass/<LOD Bifenthrin 0.200 0.134 Pass/<LOD
Boscalid 0.400 0.134 Pass/<LOD Carbaryl 0.200 0.134 Pass/<LOD
Carbofuran 0.200 0.134 Pass/<LOD Chlorantraniliprole 0.200 0.134 Pass/<LOD
Chlorfenapyr 1.000 0.538 Pass/<LOD Chlorpyrifos 0.200 0.134 Pass/<LOD
Clofentezine 0.200 0.134 Pass/<LOD Cyfluthrin** 1.000 0.538 Pass/<LOD
Cypermethrin*** 1.000 0.538 Pass/<LOD Daminozide 1.000 0.134 Pass/<LOD
DDVP (Dichlorvos) 1.000 0.269 Pass/<LOD Diazinon 0.200 0.134 Pass/<LOD
Dimethoate 0.200 0.134 Pass/<LOD Ethoprophos 0.200 0.134 Pass/<LOD
Etofenprox 0.400 0.134 Pass/<LOD Etoxazole 0.200 0.134 Pass/<LOD
Fenoxycarb 0.200 0.134 Pass/<LOD Fenpyroximate 0.400 0.134 Pass/<LOD
Fipronil 0.400 0.134 Pass/<LOD Flonicamid 1.000 0.134 Pass/<LOD
Fludioxonil 0.400 0.134 Pass/<LOD Hexythiazox 1.000 0.134 Pass/<LOD
Imazalil 0.200 0.134 Pass/<LOD Imidacloprid 0.400 0.134 Pass/<LOD
Kresoxim Methyl 0.400 0.134 Pass/<LOD Malathion 0.200 0.134 Pass/<LOD
Metalaxyl 0.200 0.134 Pass/<LOD Methiocarb 0.200 0.134 Pass/<LOD
Methomyl 0.400 0.134 Pass/<LOD Methyl Parathion 0.200 0.134 Pass/<LOD
MGK-264‡ 0.200 0.134 Pass/<LOD Myclobutanil 0.000 0.134 Pass/<LOD
Naled 0.500 0.134 Pass/<LOD Oxamyl 1.000 0.134 Pass/<LOD
Paclobutrazol 0.400 0.134 Pass/<LOD Permethrins† 0.200 0.134 Pass/<LOD
Phosmet 0.200 0.134 Pass/<LOD Piperonyl Butoxide 2.000 0.134 Pass/<LOD
Prallethrin 0.200 0.134 Pass/<LOD Propiconazole 0.400 0.134 Pass/<LOD
Propoxur 0.200 0.134 Pass/<LOD Pyrethrins* 1.000 0.134 Pass/<LOD
Pyridaben 0.200 0.134 Pass/<LOD Spinosad***** 0.200 0.134 Pass/<LOD
Spiromesifen 0.200 0.134 Pass/<LOD Spirotetramat 0.200 0.134 Pass/<LOD
Spiroxamine‡ 0.400 0.134 Pass/<LOD Tebuconazole 0.400 0.134 Pass/<LOD
Thiacloprid 0.200 0.134 Pass/<LOD Thiamethoxam 0.200 0.134 Pass/<LOD
Trifloxystrobin 0.200 0.134 Pass/<LOD

* Pyrethrins are reported as the sum of Jasmolin I, Cinerin I, and Pyrethrin I
** Cyfluthrins are reported as the sum of isomers Cyfluthrin I, II, III, and IV
*** Cypermethrins are reported as the sum of isomers Cypermethrin I, II, III, and IV
**** Abamectin is reported as the sum of Avermectin B1a and Avermectin B1b
***** Spinosad is reported as the sum of Spinosyn A and Spinosyn D
† Permethrin and Prallethrin are reported as the sum of cis and trans isomers
‡ MGK-264 and Spiroximine are reported as the sum of isomers I and II
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 6 of 67

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Pesticide QC Report
Testing Accreditation #: 4092-004 Test Certificate #: 123371-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Northern Wreck Badder
License: 030-1009646F7F8
Type: AU Tincture
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A401030002C949000000017
Metrc Source Pkg#: 1A401030002C949000000016
Test Conditions

Prepsheet ID#: ORPS200403B
Scale: XS205-OR1
Temp: 21.7 °C
Baro PE: 1005 hPa
Analyst: JER
Technician: JER
Sample ID#: 123371

Lot #: Northern wreck badder 3/30/20 #1
Batch #: 123371
Batch Weight (g): 1640.4
Harvest/Process Date: 03/31/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 03/31/2020
Test Date: 04/06/2020
Sample #123371
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS recovery% MSD recovery% Relative Percent Difference (%) QC Flag
Acephate N.D. 1 1.04 0.908 104.00 90.80 13.55
Acequinocyl N.D. 1 0.518 0.531 51.80 53.10 2.48 LR
Acetamiprid N.D. 1 1.17 1.06 117.00 106.00 9.87
Aldicarb N.D. 1 0.871 0.817 87.10 81.70 6.40
Avermectin B1a N.D. 0.97 2.24 1.62 230.93 167.01 32.12 HRQ
Azoxystrobin N.D. 1 1.11 1.01 111.00 101.00 9.43
Bifenazate N.D. 1 1.08 0.909 108.00 90.90 17.19
Bifenthrin N.D. 1 0.805 0.829 80.50 82.90 2.94
Boscalid N.D. 1 0.87 0.998 87.00 99.80 13.70
Carbaryl N.D. 1 0.938 0.875 93.80 87.50 6.95
Carbofuran N.D. 1 1.09 1.01 109.00 101.00 7.62
Chlorantraniliprole N.D. 1 1.35 1.21 135.00 121.00 10.94 HR
Chlorfenapyr N.D. 1 0.82 0.878 82.00 87.80 6.83
Chlorpyriphos N.D. 1 0.91 0.886 91.00 88.60 2.67
Clofentezine N.D. 1 1.03 0.982 103.00 98.20 4.77
Cyfluthrin N.D. 1 1.1 1 110.00 100.00 9.52
Cypermethrin N.D. 1 1.16 1.06 116.00 106.00 9.01
Daminoside N.D. 1 1.16 1.12 116.00 112.00 3.51
Diazanon N.D. 1 1.12 1.06 112.00 106.00 5.50
Dichlorvos N.D. 1 0.806 0.644 80.60 64.40 22.34 LRQ
Dimethoate N.D. 1 1.06 0.908 106.00 90.80 15.45
Ethoprophos N.D. 1 0.879 0.8 87.90 80.00 9.41
Etofenprox N.D. 1 0.914 0.87 91.40 87.00 4.93
Etoxazole N.D. 1 1.09 0.966 109.00 96.60 12.06
Fenoxycarb N.D. 1 1.31 1.15 131.00 115.00 13.01 HR
Fenpyroximate N.D. 1 1.01 0.99 101.00 99.00 2.00
Fipronil N.D. 1 1.06 1.01 106.00 101.00 4.83
Flonicamid N.D. 1 1.05 0.955 105.00 95.50 9.48
Fludioxonil N.D. 1 1.01 0.989 101.00 98.90 2.10
Hexythiazox N.D. 1 0.763 0.737 76.30 73.70 3.47
Imazalil N.D. 1 1.55 1.23 155.00 123.00 23.02 HRQ
Imidacloprid N.D. 1 1.13 1 113.00 100.00 12.21
Kresoxim-methyl N.D. 1 1.56 1.33 156.00 133.00 15.92 HR
Malathion N.D. 1 1.17 1.19 117.00 119.00 1.69
Metalaxyl N.D. 1 1.29 1.23 129.00 123.00 4.76
Methiocarb N.D. 1 1.09 0.925 109.00 92.50 16.38
Methomyl N.D. 1 1.25 1.14 125.00 114.00 9.21
MGK-264 N.D. 1 0.905 0.759 90.50 75.90 17.55
Myclobutanil N.D. 1 1.32 1.29 132.00 129.00 2.30 HR
Naled (dibrom) N.D. 1 0.671 0.567 67.10 56.70 16.80 LR
Oxamyl N.D. 1 1.06 0.902 106.00 90.20 16.11
Paclobutrazol N.D. 1 1.69 1.48 169.00 148.00 13.25 HR
Parathion-methyl N.D. 1 1.11 0.896 111.00 89.60 21.34 Q
Permethrins N.D. 1 0.886 0.821 88.60 82.10 7.62
Phosmet N.D. 1 1.37 1.23 137.00 123.00 10.77 HR
Piperonyl butoxide N.D. 1 1.1 1.03 110.00 103.00 6.57
Prallethrin N.D. 1 1.43 1.43 143.00 143.00 0.00 HR
Propiconazole N.D. 1 1.12 1.07 112.00 107.00 4.57
Propoxur N.D. 1 1.07 0.945 107.00 94.50 12.41
Pyrethrin N.D. 0.65 0.788 0.735 121.23 113.08 6.96
Pyridaben N.D. 1 0.879 0.787 87.90 78.70 11.04
SpinosynA N.D. 0.84 1.23 1.08 146.43 128.57 12.99 HR
SpinosynD N.D. 0.16 0.232 0.227 145.00 141.88 2.18 HR
Spiromesifen N.D. 1 0.817 0.807 81.70 80.70 1.23
Spirotetramat N.D. 1 1.86 1.42 186.00 142.00 26.83 HRQ
Spiroxamine N.D. 1 1.42 1.26 142.00 126.00 11.94 HR
Tebuconazole N.D. 1 1.38 1.27 138.00 127.00 8.30 HR
Thiacloprid N.D. 1 1.16 1.02 116.00 102.00 12.84
Thiamethoxam N.D. 1 1.57 1.42 157.00 142.00 10.03 HR
Trifloxystrobin N.D. 1 1.12 0.996 112.00 99.60 11.72

N.D. = Not Detected

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 30%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (60-120%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 7 of 67

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Pesticide Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-004 Test Certificate #: 123371-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Northern Wreck Badder
License: 030-1009646F7F8
Type: AU Tincture
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A401030002C949000000017
Metrc Source Pkg#: 1A401030002C949000000016
Test Conditions

Prepsheet ID#: ORPS200403B
Scale: XS205-OR1
Temp: 21.7 °C
Baro PE: 1005 hPa
Analyst: JER
Technician: JER
Sample ID#: 123371

Lot #: Northern wreck badder 3/30/20 #1
Batch #: 123371
Batch Weight (g): 1640.4
Harvest/Process Date: 03/31/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 03/31/2020
Test Date: 04/06/2020
Sample #123371
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
Aldicarb 0.400 0.128 Pass/<LOD Abamectin**** 0.500 0.128 Pass/<LOD
Acephate 0.400 0.128 Pass/<LOD Acequinocyl 2.000 0.256 Pass/<LOD
Acetamiprid 0.200 0.128 Pass/<LOD Azoxystrobin 0.200 0.128 Pass/<LOD
Bifenazate 0.200 0.128 Pass/<LOD Bifenthrin 0.200 0.128 Pass/<LOD
Boscalid 0.400 0.128 Pass/<LOD Carbaryl 0.200 0.128 Pass/<LOD
Carbofuran 0.200 0.128 Pass/<LOD Chlorantraniliprole 0.200 0.128 Pass/<LOD
Chlorfenapyr 1.000 0.512 Pass/<LOD Chlorpyrifos 0.200 0.128 Pass/<LOD
Clofentezine 0.200 0.128 Pass/<LOD Cyfluthrin** 1.000 0.512 Pass/<LOD
Cypermethrin*** 1.000 0.512 Pass/<LOD Daminozide 1.000 0.128 Pass/<LOD
DDVP (Dichlorvos) 1.000 0.256 Pass/<LOD Diazinon 0.200 0.128 Pass/<LOD
Dimethoate 0.200 0.128 Pass/<LOD Ethoprophos 0.200 0.128 Pass/<LOD
Etofenprox 0.400 0.128 Pass/<LOD Etoxazole 0.200 0.128 Pass/<LOD
Fenoxycarb 0.200 0.128 Pass/<LOD Fenpyroximate 0.400 0.128 Pass/<LOD
Fipronil 0.400 0.128 Pass/<LOD Flonicamid 1.000 0.128 Pass/<LOD
Fludioxonil 0.400 0.128 Pass/<LOD Hexythiazox 1.000 0.128 Pass/<LOD
Imazalil 0.200 0.128 Pass/<LOD Imidacloprid 0.400 0.128 Pass/<LOD
Kresoxim Methyl 0.400 0.128 Pass/<LOD Malathion 0.200 0.128 Pass/<LOD
Metalaxyl 0.200 0.128 Pass/<LOD Methiocarb 0.200 0.128 Pass/<LOD
Methomyl 0.400 0.128 Pass/<LOD Methyl Parathion 0.200 0.128 Pass/<LOD
MGK-264‡ 0.200 0.128 Pass/<LOD Myclobutanil 0.000 0.128 Pass/<LOD
Naled 0.500 0.128 Pass/<LOD Oxamyl 1.000 0.128 Pass/<LOD
Paclobutrazol 0.400 0.128 Pass/<LOD Permethrins† 0.200 0.128 Pass/<LOD
Phosmet 0.200 0.128 Pass/<LOD Piperonyl Butoxide 2.000 0.128 Pass/<LOD
Prallethrin 0.200 0.128 Pass/<LOD Propiconazole 0.400 0.128 Pass/<LOD
Propoxur 0.200 0.128 Pass/<LOD Pyrethrins* 1.000 0.128 Pass/<LOD
Pyridaben 0.200 0.128 Pass/<LOD Spinosad***** 0.200 0.128 Pass/<LOD
Spiromesifen 0.200 0.128 Pass/<LOD Spirotetramat 0.200 0.128 Pass/<LOD
Spiroxamine‡ 0.400 0.128 Pass/<LOD Tebuconazole 0.400 0.128 Pass/<LOD
Thiacloprid 0.200 0.128 Pass/<LOD Thiamethoxam 0.200 0.128 Pass/<LOD
Trifloxystrobin 0.200 0.128 Pass/<LOD

* Pyrethrins are reported as the sum of Jasmolin I, Cinerin I, and Pyrethrin I
** Cyfluthrins are reported as the sum of isomers Cyfluthrin I, II, III, and IV
*** Cypermethrins are reported as the sum of isomers Cypermethrin I, II, III, and IV
**** Abamectin is reported as the sum of Avermectin B1a and Avermectin B1b
***** Spinosad is reported as the sum of Spinosyn A and Spinosyn D
† Permethrin and Prallethrin are reported as the sum of cis and trans isomers
‡ MGK-264 and Spiroximine are reported as the sum of isomers I and II
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 8 of 67

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Pesticide QC Report
Testing Accreditation #: 4092-004 Test Certificate #: 123371-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Northern Wreck Badder
License: 030-1009646F7F8
Type: AU Tincture
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A401030002C949000000017
Metrc Source Pkg#: 1A401030002C949000000016
Test Conditions

Prepsheet ID#: ORPS200403B
Scale: XS205-OR1
Temp: 21.7 °C
Baro PE: 1005 hPa
Analyst: JER
Technician: JER
Sample ID#: 123371

Lot #: Northern wreck badder 3/30/20 #1
Batch #: 123371
Batch Weight (g): 1640.4
Harvest/Process Date: 03/31/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 03/31/2020
Test Date: 04/06/2020
Sample #123371
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS recovery% MSD recovery% Relative Percent Difference (%) QC Flag
Acephate N.D. 1 1.04 0.908 104.00 90.80 13.55
Acequinocyl N.D. 1 0.518 0.531 51.80 53.10 2.48 LR
Acetamiprid N.D. 1 1.17 1.06 117.00 106.00 9.87
Aldicarb N.D. 1 0.871 0.817 87.10 81.70 6.40
Avermectin B1a N.D. 0.97 2.24 1.62 230.93 167.01 32.12 HRQ
Azoxystrobin N.D. 1 1.11 1.01 111.00 101.00 9.43
Bifenazate N.D. 1 1.08 0.909 108.00 90.90 17.19
Bifenthrin N.D. 1 0.805 0.829 80.50 82.90 2.94
Boscalid N.D. 1 0.87 0.998 87.00 99.80 13.70
Carbaryl N.D. 1 0.938 0.875 93.80 87.50 6.95
Carbofuran N.D. 1 1.09 1.01 109.00 101.00 7.62
Chlorantraniliprole N.D. 1 1.35 1.21 135.00 121.00 10.94 HR
Chlorfenapyr N.D. 1 0.82 0.878 82.00 87.80 6.83
Chlorpyriphos N.D. 1 0.91 0.886 91.00 88.60 2.67
Clofentezine N.D. 1 1.03 0.982 103.00 98.20 4.77
Cyfluthrin N.D. 1 1.1 1 110.00 100.00 9.52
Cypermethrin N.D. 1 1.16 1.06 116.00 106.00 9.01
Daminoside N.D. 1 1.16 1.12 116.00 112.00 3.51
Diazanon N.D. 1 1.12 1.06 112.00 106.00 5.50
Dichlorvos N.D. 1 0.806 0.644 80.60 64.40 22.34 LRQ
Dimethoate N.D. 1 1.06 0.908 106.00 90.80 15.45
Ethoprophos N.D. 1 0.879 0.8 87.90 80.00 9.41
Etofenprox N.D. 1 0.914 0.87 91.40 87.00 4.93
Etoxazole N.D. 1 1.09 0.966 109.00 96.60 12.06
Fenoxycarb N.D. 1 1.31 1.15 131.00 115.00 13.01 HR
Fenpyroximate N.D. 1 1.01 0.99 101.00 99.00 2.00
Fipronil N.D. 1 1.06 1.01 106.00 101.00 4.83
Flonicamid N.D. 1 1.05 0.955 105.00 95.50 9.48
Fludioxonil N.D. 1 1.01 0.989 101.00 98.90 2.10
Hexythiazox N.D. 1 0.763 0.737 76.30 73.70 3.47
Imazalil N.D. 1 1.55 1.23 155.00 123.00 23.02 HRQ
Imidacloprid N.D. 1 1.13 1 113.00 100.00 12.21
Kresoxim-methyl N.D. 1 1.56 1.33 156.00 133.00 15.92 HR
Malathion N.D. 1 1.17 1.19 117.00 119.00 1.69
Metalaxyl N.D. 1 1.29 1.23 129.00 123.00 4.76
Methiocarb N.D. 1 1.09 0.925 109.00 92.50 16.38
Methomyl N.D. 1 1.25 1.14 125.00 114.00 9.21
MGK-264 N.D. 1 0.905 0.759 90.50 75.90 17.55
Myclobutanil N.D. 1 1.32 1.29 132.00 129.00 2.30 HR
Naled (dibrom) N.D. 1 0.671 0.567 67.10 56.70 16.80 LR
Oxamyl N.D. 1 1.06 0.902 106.00 90.20 16.11
Paclobutrazol N.D. 1 1.69 1.48 169.00 148.00 13.25 HR
Parathion-methyl N.D. 1 1.11 0.896 111.00 89.60 21.34 Q
Permethrins N.D. 1 0.886 0.821 88.60 82.10 7.62
Phosmet N.D. 1 1.37 1.23 137.00 123.00 10.77 HR
Piperonyl butoxide N.D. 1 1.1 1.03 110.00 103.00 6.57
Prallethrin N.D. 1 1.43 1.43 143.00 143.00 0.00 HR
Propiconazole N.D. 1 1.12 1.07 112.00 107.00 4.57
Propoxur N.D. 1 1.07 0.945 107.00 94.50 12.41
Pyrethrin N.D. 0.65 0.788 0.735 121.23 113.08 6.96
Pyridaben N.D. 1 0.879 0.787 87.90 78.70 11.04
SpinosynA N.D. 0.84 1.23 1.08 146.43 128.57 12.99 HR
SpinosynD N.D. 0.16 0.232 0.227 145.00 141.88 2.18 HR
Spiromesifen N.D. 1 0.817 0.807 81.70 80.70 1.23
Spirotetramat N.D. 1 1.86 1.42 186.00 142.00 26.83 HRQ
Spiroxamine N.D. 1 1.42 1.26 142.00 126.00 11.94 HR
Tebuconazole N.D. 1 1.38 1.27 138.00 127.00 8.30 HR
Thiacloprid N.D. 1 1.16 1.02 116.00 102.00 12.84
Thiamethoxam N.D. 1 1.57 1.42 157.00 142.00 10.03 HR
Trifloxystrobin N.D. 1 1.12 0.996 112.00 99.60 11.72

N.D. = Not Detected

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 30%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (60-120%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 9 of 67

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Pesticide Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-004 Test Certificate #: 123371-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Northern Wreck Badder
License: 030-1009646F7F8
Type: AU Tincture
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A401030002C949000000017
Metrc Source Pkg#: 1A401030002C949000000016
Test Conditions

Prepsheet ID#: ORPS200403B
Scale: XS205-OR1
Temp: 21.7 °C
Baro PE: 1005 hPa
Analyst: JER
Technician: JER
Sample ID#: 123371

Lot #: Northern wreck badder 3/30/20 #1
Batch #: 123371
Batch Weight (g): 1640.4
Harvest/Process Date: 03/31/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 03/31/2020
Test Date: 04/06/2020
Sample #123371
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
Aldicarb 0.400 0.131 Pass/<LOD Abamectin**** 0.500 0.131 Pass/<LOD
Acephate 0.400 0.131 Pass/<LOD Acequinocyl 2.000 0.261 Pass/<LOD
Acetamiprid 0.200 0.131 Pass/<LOD Azoxystrobin 0.200 0.131 Pass/<LOD
Bifenazate 0.200 0.131 Pass/<LOD Bifenthrin 0.200 0.131 Pass/<LOD
Boscalid 0.400 0.131 Pass/<LOD Carbaryl 0.200 0.131 Pass/<LOD
Carbofuran 0.200 0.131 Pass/<LOD Chlorantraniliprole 0.200 0.131 Pass/<LOD
Chlorfenapyr 1.000 0.523 Pass/<LOD Chlorpyrifos 0.200 0.131 Pass/<LOD
Clofentezine 0.200 0.131 Pass/<LOD Cyfluthrin** 1.000 0.523 Pass/<LOD
Cypermethrin*** 1.000 0.523 Pass/<LOD Daminozide 1.000 0.131 Pass/<LOD
DDVP (Dichlorvos) 1.000 0.261 Pass/<LOD Diazinon 0.200 0.131 Pass/<LOD
Dimethoate 0.200 0.131 Pass/<LOD Ethoprophos 0.200 0.131 Pass/<LOD
Etofenprox 0.400 0.131 Pass/<LOD Etoxazole 0.200 0.131 Pass/<LOD
Fenoxycarb 0.200 0.131 Pass/<LOD Fenpyroximate 0.400 0.131 Pass/<LOD
Fipronil 0.400 0.131 Pass/<LOD Flonicamid 1.000 0.131 Pass/<LOD
Fludioxonil 0.400 0.131 Pass/<LOD Hexythiazox 1.000 0.131 Pass/<LOD
Imazalil 0.200 0.131 Pass/<LOD Imidacloprid 0.400 0.131 Pass/<LOD
Kresoxim Methyl 0.400 0.131 Pass/<LOD Malathion 0.200 0.131 Pass/<LOD
Metalaxyl 0.200 0.131 Pass/<LOD Methiocarb 0.200 0.131 Pass/<LOD
Methomyl 0.400 0.131 Pass/<LOD Methyl Parathion 0.200 0.131 Pass/<LOD
MGK-264‡ 0.200 0.131 Pass/<LOD Myclobutanil 0.000 0.131 Pass/<LOD
Naled 0.500 0.131 Pass/<LOD Oxamyl 1.000 0.131 Pass/<LOD
Paclobutrazol 0.400 0.131 Pass/<LOD Permethrins† 0.200 0.131 Pass/<LOD
Phosmet 0.200 0.131 Pass/<LOD Piperonyl Butoxide 2.000 0.131 Pass/<LOD
Prallethrin 0.200 0.131 Pass/<LOD Propiconazole 0.400 0.131 Pass/<LOD
Propoxur 0.200 0.131 Pass/<LOD Pyrethrins* 1.000 0.131 Pass/<LOD
Pyridaben 0.200 0.131 Pass/<LOD Spinosad***** 0.200 0.131 Pass/<LOD
Spiromesifen 0.200 0.131 Pass/<LOD Spirotetramat 0.200 0.131 Pass/<LOD
Spiroxamine‡ 0.400 0.131 Pass/<LOD Tebuconazole 0.400 0.131 Pass/<LOD
Thiacloprid 0.200 0.131 Pass/<LOD Thiamethoxam 0.200 0.131 Pass/<LOD
Trifloxystrobin 0.200 0.131 Pass/<LOD

* Pyrethrins are reported as the sum of Jasmolin I, Cinerin I, and Pyrethrin I
** Cyfluthrins are reported as the sum of isomers Cyfluthrin I, II, III, and IV
*** Cypermethrins are reported as the sum of isomers Cypermethrin I, II, III, and IV
**** Abamectin is reported as the sum of Avermectin B1a and Avermectin B1b
***** Spinosad is reported as the sum of Spinosyn A and Spinosyn D
† Permethrin and Prallethrin are reported as the sum of cis and trans isomers
‡ MGK-264 and Spiroximine are reported as the sum of isomers I and II
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 10 of 67

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Pesticide QC Report
Testing Accreditation #: 4092-004 Test Certificate #: 123371-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Northern Wreck Badder
License: 030-1009646F7F8
Type: AU Tincture
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A401030002C949000000017
Metrc Source Pkg#: 1A401030002C949000000016
Test Conditions

Prepsheet ID#: ORPS200403B
Scale: XS205-OR1
Temp: 21.7 °C
Baro PE: 1005 hPa
Analyst: JER
Technician: JER
Sample ID#: 123371

Lot #: Northern wreck badder 3/30/20 #1
Batch #: 123371
Batch Weight (g): 1640.4
Harvest/Process Date: 03/31/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 03/31/2020
Test Date: 04/06/2020
Sample #123371
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS recovery% MSD recovery% Relative Percent Difference (%) QC Flag
Acephate N.D. 1 1.04 0.908 104.00 90.80 13.55
Acequinocyl N.D. 1 0.518 0.531 51.80 53.10 2.48 LR
Acetamiprid N.D. 1 1.17 1.06 117.00 106.00 9.87
Aldicarb N.D. 1 0.871 0.817 87.10 81.70 6.40
Avermectin B1a N.D. 0.97 2.24 1.62 230.93 167.01 32.12 HRQ
Azoxystrobin N.D. 1 1.11 1.01 111.00 101.00 9.43
Bifenazate N.D. 1 1.08 0.909 108.00 90.90 17.19
Bifenthrin N.D. 1 0.805 0.829 80.50 82.90 2.94
Boscalid N.D. 1 0.87 0.998 87.00 99.80 13.70
Carbaryl N.D. 1 0.938 0.875 93.80 87.50 6.95
Carbofuran N.D. 1 1.09 1.01 109.00 101.00 7.62
Chlorantraniliprole N.D. 1 1.35 1.21 135.00 121.00 10.94 HR
Chlorfenapyr N.D. 1 0.82 0.878 82.00 87.80 6.83
Chlorpyriphos N.D. 1 0.91 0.886 91.00 88.60 2.67
Clofentezine N.D. 1 1.03 0.982 103.00 98.20 4.77
Cyfluthrin N.D. 1 1.1 1 110.00 100.00 9.52
Cypermethrin N.D. 1 1.16 1.06 116.00 106.00 9.01
Daminoside N.D. 1 1.16 1.12 116.00 112.00 3.51
Diazanon N.D. 1 1.12 1.06 112.00 106.00 5.50
Dichlorvos N.D. 1 0.806 0.644 80.60 64.40 22.34 LRQ
Dimethoate N.D. 1 1.06 0.908 106.00 90.80 15.45
Ethoprophos N.D. 1 0.879 0.8 87.90 80.00 9.41
Etofenprox N.D. 1 0.914 0.87 91.40 87.00 4.93
Etoxazole N.D. 1 1.09 0.966 109.00 96.60 12.06
Fenoxycarb N.D. 1 1.31 1.15 131.00 115.00 13.01 HR
Fenpyroximate N.D. 1 1.01 0.99 101.00 99.00 2.00
Fipronil N.D. 1 1.06 1.01 106.00 101.00 4.83
Flonicamid N.D. 1 1.05 0.955 105.00 95.50 9.48
Fludioxonil N.D. 1 1.01 0.989 101.00 98.90 2.10
Hexythiazox N.D. 1 0.763 0.737 76.30 73.70 3.47
Imazalil N.D. 1 1.55 1.23 155.00 123.00 23.02 HRQ
Imidacloprid N.D. 1 1.13 1 113.00 100.00 12.21
Kresoxim-methyl N.D. 1 1.56 1.33 156.00 133.00 15.92 HR
Malathion N.D. 1 1.17 1.19 117.00 119.00 1.69
Metalaxyl N.D. 1 1.29 1.23 129.00 123.00 4.76
Methiocarb N.D. 1 1.09 0.925 109.00 92.50 16.38
Methomyl N.D. 1 1.25 1.14 125.00 114.00 9.21
MGK-264 N.D. 1 0.905 0.759 90.50 75.90 17.55
Myclobutanil N.D. 1 1.32 1.29 132.00 129.00 2.30 HR
Naled (dibrom) N.D. 1 0.671 0.567 67.10 56.70 16.80 LR
Oxamyl N.D. 1 1.06 0.902 106.00 90.20 16.11
Paclobutrazol N.D. 1 1.69 1.48 169.00 148.00 13.25 HR
Parathion-methyl N.D. 1 1.11 0.896 111.00 89.60 21.34 Q
Permethrins N.D. 1 0.886 0.821 88.60 82.10 7.62
Phosmet N.D. 1 1.37 1.23 137.00 123.00 10.77 HR
Piperonyl butoxide N.D. 1 1.1 1.03 110.00 103.00 6.57
Prallethrin N.D. 1 1.43 1.43 143.00 143.00 0.00 HR
Propiconazole N.D. 1 1.12 1.07 112.00 107.00 4.57
Propoxur N.D. 1 1.07 0.945 107.00 94.50 12.41
Pyrethrin N.D. 0.65 0.788 0.735 121.23 113.08 6.96
Pyridaben N.D. 1 0.879 0.787 87.90 78.70 11.04
SpinosynA N.D. 0.84 1.23 1.08 146.43 128.57 12.99 HR
SpinosynD N.D. 0.16 0.232 0.227 145.00 141.88 2.18 HR
Spiromesifen N.D. 1 0.817 0.807 81.70 80.70 1.23
Spirotetramat N.D. 1 1.86 1.42 186.00 142.00 26.83 HRQ
Spiroxamine N.D. 1 1.42 1.26 142.00 126.00 11.94 HR
Tebuconazole N.D. 1 1.38 1.27 138.00 127.00 8.30 HR
Thiacloprid N.D. 1 1.16 1.02 116.00 102.00 12.84
Thiamethoxam N.D. 1 1.57 1.42 157.00 142.00 10.03 HR
Trifloxystrobin N.D. 1 1.12 0.996 112.00 99.60 11.72

N.D. = Not Detected

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 30%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (60-120%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 11 of 67

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Pesticide Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-004 Test Certificate #: 123371-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Northern Wreck Badder
License: 030-1009646F7F8
Type: AU Tincture
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A401030002C949000000017
Metrc Source Pkg#: 1A401030002C949000000016
Test Conditions

Prepsheet ID#: ORPS200403B
Scale: XS205-OR1
Temp: 21.7 °C
Baro PE: 1005 hPa
Analyst: JER
Technician: JER
Sample ID#: 123371

Lot #: Northern wreck badder 3/30/20 #1
Batch #: 123371
Batch Weight (g): 1640.4
Harvest/Process Date: 03/31/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 03/31/2020
Test Date: 04/06/2020
Sample #123371
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
Aldicarb 0.400 0.130 Pass/<LOD Abamectin**** 0.500 0.130 Pass/<LOD
Acephate 0.400 0.130 Pass/<LOD Acequinocyl 2.000 0.260 Pass/<LOD
Acetamiprid 0.200 0.130 Pass/<LOD Azoxystrobin 0.200 0.130 Pass/<LOD
Bifenazate 0.200 0.130 Pass/<LOD Bifenthrin 0.200 0.130 Pass/<LOD
Boscalid 0.400 0.130 Pass/<LOD Carbaryl 0.200 0.130 Pass/<LOD
Carbofuran 0.200 0.130 Pass/<LOD Chlorantraniliprole 0.200 0.130 Pass/<LOD
Chlorfenapyr 1.000 0.520 Pass/<LOD Chlorpyrifos 0.200 0.130 Pass/<LOD
Clofentezine 0.200 0.130 Pass/<LOD Cyfluthrin** 1.000 0.520 Pass/<LOD
Cypermethrin*** 1.000 0.520 Pass/<LOD Daminozide 1.000 0.130 Pass/<LOD
DDVP (Dichlorvos) 1.000 0.260 Pass/<LOD Diazinon 0.200 0.130 Pass/<LOD
Dimethoate 0.200 0.130 Pass/<LOD Ethoprophos 0.200 0.130 Pass/<LOD
Etofenprox 0.400 0.130 Pass/<LOD Etoxazole 0.200 0.130 Pass/<LOD
Fenoxycarb 0.200 0.130 Pass/<LOD Fenpyroximate 0.400 0.130 Pass/<LOD
Fipronil 0.400 0.130 Pass/<LOD Flonicamid 1.000 0.130 Pass/<LOD
Fludioxonil 0.400 0.130 Pass/<LOD Hexythiazox 1.000 0.130 Pass/<LOD
Imazalil 0.200 0.130 Pass/<LOD Imidacloprid 0.400 0.130 Pass/<LOD
Kresoxim Methyl 0.400 0.130 Pass/<LOD Malathion 0.200 0.130 Pass/<LOD
Metalaxyl 0.200 0.130 Pass/<LOD Methiocarb 0.200 0.130 Pass/<LOD
Methomyl 0.400 0.130 Pass/<LOD Methyl Parathion 0.200 0.130 Pass/<LOD
MGK-264‡ 0.200 0.130 Pass/<LOD Myclobutanil 0.000 0.130 Pass/<LOD
Naled 0.500 0.130 Pass/<LOD Oxamyl 1.000 0.130 Pass/<LOD
Paclobutrazol 0.400 0.130 Pass/<LOD Permethrins† 0.200 0.130 Pass/<LOD
Phosmet 0.200 0.130 Pass/<LOD Piperonyl Butoxide 2.000 0.130 Pass/<LOD
Prallethrin 0.200 0.130 Pass/<LOD Propiconazole 0.400 0.130 Pass/<LOD
Propoxur 0.200 0.130 Pass/<LOD Pyrethrins* 1.000 0.130 Pass/<LOD
Pyridaben 0.200 0.130 Pass/<LOD Spinosad***** 0.200 0.130 Pass/<LOD
Spiromesifen 0.200 0.130 Pass/<LOD Spirotetramat 0.200 0.130 Pass/<LOD
Spiroxamine‡ 0.400 0.130 Pass/<LOD Tebuconazole 0.400 0.130 Pass/<LOD
Thiacloprid 0.200 0.130 Pass/<LOD Thiamethoxam 0.200 0.130 Pass/<LOD
Trifloxystrobin 0.200 0.130 Pass/<LOD

* Pyrethrins are reported as the sum of Jasmolin I, Cinerin I, and Pyrethrin I
** Cyfluthrins are reported as the sum of isomers Cyfluthrin I, II, III, and IV
*** Cypermethrins are reported as the sum of isomers Cypermethrin I, II, III, and IV
**** Abamectin is reported as the sum of Avermectin B1a and Avermectin B1b
***** Spinosad is reported as the sum of Spinosyn A and Spinosyn D
† Permethrin and Prallethrin are reported as the sum of cis and trans isomers
‡ MGK-264 and Spiroximine are reported as the sum of isomers I and II
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 12 of 67

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Pesticide QC Report
Testing Accreditation #: 4092-004 Test Certificate #: 123371-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Northern Wreck Badder
License: 030-1009646F7F8
Type: AU Tincture
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A401030002C949000000017
Metrc Source Pkg#: 1A401030002C949000000016
Test Conditions

Prepsheet ID#: ORPS200403B
Scale: XS205-OR1
Temp: 21.7 °C
Baro PE: 1005 hPa
Analyst: JER
Technician: JER
Sample ID#: 123371

Lot #: Northern wreck badder 3/30/20 #1
Batch #: 123371
Batch Weight (g): 1640.4
Harvest/Process Date: 03/31/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 03/31/2020
Test Date: 04/06/2020
Sample #123371
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS recovery% MSD recovery% Relative Percent Difference (%) QC Flag
Acephate N.D. 1 1.04 0.908 104.00 90.80 13.55
Acequinocyl N.D. 1 0.518 0.531 51.80 53.10 2.48 LR
Acetamiprid N.D. 1 1.17 1.06 117.00 106.00 9.87
Aldicarb N.D. 1 0.871 0.817 87.10 81.70 6.40
Avermectin B1a N.D. 0.97 2.24 1.62 230.93 167.01 32.12 HRQ
Azoxystrobin N.D. 1 1.11 1.01 111.00 101.00 9.43
Bifenazate N.D. 1 1.08 0.909 108.00 90.90 17.19
Bifenthrin N.D. 1 0.805 0.829 80.50 82.90 2.94
Boscalid N.D. 1 0.87 0.998 87.00 99.80 13.70
Carbaryl N.D. 1 0.938 0.875 93.80 87.50 6.95
Carbofuran N.D. 1 1.09 1.01 109.00 101.00 7.62
Chlorantraniliprole N.D. 1 1.35 1.21 135.00 121.00 10.94 HR
Chlorfenapyr N.D. 1 0.82 0.878 82.00 87.80 6.83
Chlorpyriphos N.D. 1 0.91 0.886 91.00 88.60 2.67
Clofentezine N.D. 1 1.03 0.982 103.00 98.20 4.77
Cyfluthrin N.D. 1 1.1 1 110.00 100.00 9.52
Cypermethrin N.D. 1 1.16 1.06 116.00 106.00 9.01
Daminoside N.D. 1 1.16 1.12 116.00 112.00 3.51
Diazanon N.D. 1 1.12 1.06 112.00 106.00 5.50
Dichlorvos N.D. 1 0.806 0.644 80.60 64.40 22.34 LRQ
Dimethoate N.D. 1 1.06 0.908 106.00 90.80 15.45
Ethoprophos N.D. 1 0.879 0.8 87.90 80.00 9.41
Etofenprox N.D. 1 0.914 0.87 91.40 87.00 4.93
Etoxazole N.D. 1 1.09 0.966 109.00 96.60 12.06
Fenoxycarb N.D. 1 1.31 1.15 131.00 115.00 13.01 HR
Fenpyroximate N.D. 1 1.01 0.99 101.00 99.00 2.00
Fipronil N.D. 1 1.06 1.01 106.00 101.00 4.83
Flonicamid N.D. 1 1.05 0.955 105.00 95.50 9.48
Fludioxonil N.D. 1 1.01 0.989 101.00 98.90 2.10
Hexythiazox N.D. 1 0.763 0.737 76.30 73.70 3.47
Imazalil N.D. 1 1.55 1.23 155.00 123.00 23.02 HRQ
Imidacloprid N.D. 1 1.13 1 113.00 100.00 12.21
Kresoxim-methyl N.D. 1 1.56 1.33 156.00 133.00 15.92 HR
Malathion N.D. 1 1.17 1.19 117.00 119.00 1.69
Metalaxyl N.D. 1 1.29 1.23 129.00 123.00 4.76
Methiocarb N.D. 1 1.09 0.925 109.00 92.50 16.38
Methomyl N.D. 1 1.25 1.14 125.00 114.00 9.21
MGK-264 N.D. 1 0.905 0.759 90.50 75.90 17.55
Myclobutanil N.D. 1 1.32 1.29 132.00 129.00 2.30 HR
Naled (dibrom) N.D. 1 0.671 0.567 67.10 56.70 16.80 LR
Oxamyl N.D. 1 1.06 0.902 106.00 90.20 16.11
Paclobutrazol N.D. 1 1.69 1.48 169.00 148.00 13.25 HR
Parathion-methyl N.D. 1 1.11 0.896 111.00 89.60 21.34 Q
Permethrins N.D. 1 0.886 0.821 88.60 82.10 7.62
Phosmet N.D. 1 1.37 1.23 137.00 123.00 10.77 HR
Piperonyl butoxide N.D. 1 1.1 1.03 110.00 103.00 6.57
Prallethrin N.D. 1 1.43 1.43 143.00 143.00 0.00 HR
Propiconazole N.D. 1 1.12 1.07 112.00 107.00 4.57
Propoxur N.D. 1 1.07 0.945 107.00 94.50 12.41
Pyrethrin N.D. 0.65 0.788 0.735 121.23 113.08 6.96
Pyridaben N.D. 1 0.879 0.787 87.90 78.70 11.04
SpinosynA N.D. 0.84 1.23 1.08 146.43 128.57 12.99 HR
SpinosynD N.D. 0.16 0.232 0.227 145.00 141.88 2.18 HR
Spiromesifen N.D. 1 0.817 0.807 81.70 80.70 1.23
Spirotetramat N.D. 1 1.86 1.42 186.00 142.00 26.83 HRQ
Spiroxamine N.D. 1 1.42 1.26 142.00 126.00 11.94 HR
Tebuconazole N.D. 1 1.38 1.27 138.00 127.00 8.30 HR
Thiacloprid N.D. 1 1.16 1.02 116.00 102.00 12.84
Thiamethoxam N.D. 1 1.57 1.42 157.00 142.00 10.03 HR
Trifloxystrobin N.D. 1 1.12 0.996 112.00 99.60 11.72

N.D. = Not Detected

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 30%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (60-120%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 13 of 67

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Pesticide Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-004 Test Certificate #: 123371-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Northern Wreck Badder
License: 030-1009646F7F8
Type: AU Tincture
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A401030002C949000000017
Metrc Source Pkg#: 1A401030002C949000000016
Test Conditions

Prepsheet ID#: ORPS200403B
Scale: XS205-OR1
Temp: 21.7 °C
Baro PE: 1005 hPa
Analyst: JER
Technician: JER
Sample ID#: 123371

Lot #: Northern wreck badder 3/30/20 #1
Batch #: 123371
Batch Weight (g): 1640.4
Harvest/Process Date: 03/31/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 03/31/2020
Test Date: 04/06/2020
Sample #123371
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
Aldicarb 0.400 0.133 Pass/<LOD Abamectin**** 0.500 0.133 Pass/<LOD
Acephate 0.400 0.133 Pass/<LOD Acequinocyl 2.000 0.266 Pass/<LOD
Acetamiprid 0.200 0.133 Pass/<LOD Azoxystrobin 0.200 0.133 Pass/<LOD
Bifenazate 0.200 0.133 Pass/<LOD Bifenthrin 0.200 0.133 Pass/<LOD
Boscalid 0.400 0.133 Pass/<LOD Carbaryl 0.200 0.133 Pass/<LOD
Carbofuran 0.200 0.133 Pass/<LOD Chlorantraniliprole 0.200 0.133 Pass/<LOD
Chlorfenapyr 1.000 0.532 Pass/<LOD Chlorpyrifos 0.200 0.133 Pass/<LOD
Clofentezine 0.200 0.133 Pass/<LOD Cyfluthrin** 1.000 0.532 Pass/<LOD
Cypermethrin*** 1.000 0.532 Pass/<LOD Daminozide 1.000 0.133 Pass/<LOD
DDVP (Dichlorvos) 1.000 0.266 Pass/<LOD Diazinon 0.200 0.133 Pass/<LOD
Dimethoate 0.200 0.133 Pass/<LOD Ethoprophos 0.200 0.133 Pass/<LOD
Etofenprox 0.400 0.133 Pass/<LOD Etoxazole 0.200 0.133 Pass/<LOD
Fenoxycarb 0.200 0.133 Pass/<LOD Fenpyroximate 0.400 0.133 Pass/<LOD
Fipronil 0.400 0.133 Pass/<LOD Flonicamid 1.000 0.133 Pass/<LOD
Fludioxonil 0.400 0.133 Pass/<LOD Hexythiazox 1.000 0.133 Pass/<LOD
Imazalil 0.200 0.133 Pass/<LOD Imidacloprid 0.400 0.133 Pass/<LOD
Kresoxim Methyl 0.400 0.133 Pass/<LOD Malathion 0.200 0.133 Pass/<LOD
Metalaxyl 0.200 0.133 Pass/<LOD Methiocarb 0.200 0.133 Pass/<LOD
Methomyl 0.400 0.133 Pass/<LOD Methyl Parathion 0.200 0.133 Pass/<LOD
MGK-264‡ 0.200 0.133 Pass/<LOD Myclobutanil 0.000 0.133 Pass/<LOD
Naled 0.500 0.133 Pass/<LOD Oxamyl 1.000 0.133 Pass/<LOD
Paclobutrazol 0.400 0.133 Pass/<LOD Permethrins† 0.200 0.133 Pass/<LOD
Phosmet 0.200 0.133 Pass/<LOD Piperonyl Butoxide 2.000 0.133 Pass/<LOD
Prallethrin 0.200 0.133 Pass/<LOD Propiconazole 0.400 0.133 Pass/<LOD
Propoxur 0.200 0.133 Pass/<LOD Pyrethrins* 1.000 0.133 Pass/<LOD
Pyridaben 0.200 0.133 Pass/<LOD Spinosad***** 0.200 0.133 Pass/<LOD
Spiromesifen 0.200 0.133 Pass/<LOD Spirotetramat 0.200 0.133 Pass/<LOD
Spiroxamine‡ 0.400 0.133 Pass/<LOD Tebuconazole 0.400 0.133 Pass/<LOD
Thiacloprid 0.200 0.133 Pass/<LOD Thiamethoxam 0.200 0.133 Pass/<LOD
Trifloxystrobin 0.200 0.133 Pass/<LOD

* Pyrethrins are reported as the sum of Jasmolin I, Cinerin I, and Pyrethrin I
** Cyfluthrins are reported as the sum of isomers Cyfluthrin I, II, III, and IV
*** Cypermethrins are reported as the sum of isomers Cypermethrin I, II, III, and IV
**** Abamectin is reported as the sum of Avermectin B1a and Avermectin B1b
***** Spinosad is reported as the sum of Spinosyn A and Spinosyn D
† Permethrin and Prallethrin are reported as the sum of cis and trans isomers
‡ MGK-264 and Spiroximine are reported as the sum of isomers I and II
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 14 of 67

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Pesticide QC Report
Testing Accreditation #: 4092-004 Test Certificate #: 123371-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Northern Wreck Badder
License: 030-1009646F7F8
Type: AU Tincture
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A401030002C949000000017
Metrc Source Pkg#: 1A401030002C949000000016
Test Conditions

Prepsheet ID#: ORPS200403B
Scale: XS205-OR1
Temp: 21.7 °C
Baro PE: 1005 hPa
Analyst: JER
Technician: JER
Sample ID#: 123371

Lot #: Northern wreck badder 3/30/20 #1
Batch #: 123371
Batch Weight (g): 1640.4
Harvest/Process Date: 03/31/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 03/31/2020
Test Date: 04/06/2020
Sample #123371
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS recovery% MSD recovery% Relative Percent Difference (%) QC Flag
Acephate N.D. 1 1.04 0.908 104.00 90.80 13.55
Acequinocyl N.D. 1 0.518 0.531 51.80 53.10 2.48 LR
Acetamiprid N.D. 1 1.17 1.06 117.00 106.00 9.87
Aldicarb N.D. 1 0.871 0.817 87.10 81.70 6.40
Avermectin B1a N.D. 0.97 2.24 1.62 230.93 167.01 32.12 HRQ
Azoxystrobin N.D. 1 1.11 1.01 111.00 101.00 9.43
Bifenazate N.D. 1 1.08 0.909 108.00 90.90 17.19
Bifenthrin N.D. 1 0.805 0.829 80.50 82.90 2.94
Boscalid N.D. 1 0.87 0.998 87.00 99.80 13.70
Carbaryl N.D. 1 0.938 0.875 93.80 87.50 6.95
Carbofuran N.D. 1 1.09 1.01 109.00 101.00 7.62
Chlorantraniliprole N.D. 1 1.35 1.21 135.00 121.00 10.94 HR
Chlorfenapyr N.D. 1 0.82 0.878 82.00 87.80 6.83
Chlorpyriphos N.D. 1 0.91 0.886 91.00 88.60 2.67
Clofentezine N.D. 1 1.03 0.982 103.00 98.20 4.77
Cyfluthrin N.D. 1 1.1 1 110.00 100.00 9.52
Cypermethrin N.D. 1 1.16 1.06 116.00 106.00 9.01
Daminoside N.D. 1 1.16 1.12 116.00 112.00 3.51
Diazanon N.D. 1 1.12 1.06 112.00 106.00 5.50
Dichlorvos N.D. 1 0.806 0.644 80.60 64.40 22.34 LRQ
Dimethoate N.D. 1 1.06 0.908 106.00 90.80 15.45
Ethoprophos N.D. 1 0.879 0.8 87.90 80.00 9.41
Etofenprox N.D. 1 0.914 0.87 91.40 87.00 4.93
Etoxazole N.D. 1 1.09 0.966 109.00 96.60 12.06
Fenoxycarb N.D. 1 1.31 1.15 131.00 115.00 13.01 HR
Fenpyroximate N.D. 1 1.01 0.99 101.00 99.00 2.00
Fipronil N.D. 1 1.06 1.01 106.00 101.00 4.83
Flonicamid N.D. 1 1.05 0.955 105.00 95.50 9.48
Fludioxonil N.D. 1 1.01 0.989 101.00 98.90 2.10
Hexythiazox N.D. 1 0.763 0.737 76.30 73.70 3.47
Imazalil N.D. 1 1.55 1.23 155.00 123.00 23.02 HRQ
Imidacloprid N.D. 1 1.13 1 113.00 100.00 12.21
Kresoxim-methyl N.D. 1 1.56 1.33 156.00 133.00 15.92 HR
Malathion N.D. 1 1.17 1.19 117.00 119.00 1.69
Metalaxyl N.D. 1 1.29 1.23 129.00 123.00 4.76
Methiocarb N.D. 1 1.09 0.925 109.00 92.50 16.38
Methomyl N.D. 1 1.25 1.14 125.00 114.00 9.21
MGK-264 N.D. 1 0.905 0.759 90.50 75.90 17.55
Myclobutanil N.D. 1 1.32 1.29 132.00 129.00 2.30 HR
Naled (dibrom) N.D. 1 0.671 0.567 67.10 56.70 16.80 LR
Oxamyl N.D. 1 1.06 0.902 106.00 90.20 16.11
Paclobutrazol N.D. 1 1.69 1.48 169.00 148.00 13.25 HR
Parathion-methyl N.D. 1 1.11 0.896 111.00 89.60 21.34 Q
Permethrins N.D. 1 0.886 0.821 88.60 82.10 7.62
Phosmet N.D. 1 1.37 1.23 137.00 123.00 10.77 HR
Piperonyl butoxide N.D. 1 1.1 1.03 110.00 103.00 6.57
Prallethrin N.D. 1 1.43 1.43 143.00 143.00 0.00 HR
Propiconazole N.D. 1 1.12 1.07 112.00 107.00 4.57
Propoxur N.D. 1 1.07 0.945 107.00 94.50 12.41
Pyrethrin N.D. 0.65 0.788 0.735 121.23 113.08 6.96
Pyridaben N.D. 1 0.879 0.787 87.90 78.70 11.04
SpinosynA N.D. 0.84 1.23 1.08 146.43 128.57 12.99 HR
SpinosynD N.D. 0.16 0.232 0.227 145.00 141.88 2.18 HR
Spiromesifen N.D. 1 0.817 0.807 81.70 80.70 1.23
Spirotetramat N.D. 1 1.86 1.42 186.00 142.00 26.83 HRQ
Spiroxamine N.D. 1 1.42 1.26 142.00 126.00 11.94 HR
Tebuconazole N.D. 1 1.38 1.27 138.00 127.00 8.30 HR
Thiacloprid N.D. 1 1.16 1.02 116.00 102.00 12.84
Thiamethoxam N.D. 1 1.57 1.42 157.00 142.00 10.03 HR
Trifloxystrobin N.D. 1 1.12 0.996 112.00 99.60 11.72

N.D. = Not Detected

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 30%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (60-120%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 15 of 67

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Pesticide Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-004 Test Certificate #: 123371-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Northern Wreck Badder
License: 030-1009646F7F8
Type: AU Tincture
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A401030002C949000000017
Metrc Source Pkg#: 1A401030002C949000000016
Test Conditions

Prepsheet ID#: ORPS200403B
Scale: XS205-OR1
Temp: 21.7 °C
Baro PE: 1005 hPa
Analyst: JER
Technician: JER
Sample ID#: 123371

Lot #: Northern wreck badder 3/30/20 #1
Batch #: 123371
Batch Weight (g): 1640.4
Harvest/Process Date: 03/31/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 03/31/2020
Test Date: 04/06/2020
Sample #123371
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
Aldicarb 0.400 0.133 Pass/<LOD Abamectin**** 0.500 0.133 Pass/<LOD
Acephate 0.400 0.133 Pass/<LOD Acequinocyl 2.000 0.265 Pass/<LOD
Acetamiprid 0.200 0.133 Pass/<LOD Azoxystrobin 0.200 0.133 Pass/<LOD
Bifenazate 0.200 0.133 Pass/<LOD Bifenthrin 0.200 0.133 Pass/<LOD
Boscalid 0.400 0.133 Pass/<LOD Carbaryl 0.200 0.133 Pass/<LOD
Carbofuran 0.200 0.133 Pass/<LOD Chlorantraniliprole 0.200 0.133 Pass/<LOD
Chlorfenapyr 1.000 0.531 Pass/<LOD Chlorpyrifos 0.200 0.133 Pass/<LOD
Clofentezine 0.200 0.133 Pass/<LOD Cyfluthrin** 1.000 0.531 Pass/<LOD
Cypermethrin*** 1.000 0.531 Pass/<LOD Daminozide 1.000 0.133 Pass/<LOD
DDVP (Dichlorvos) 1.000 0.265 Pass/<LOD Diazinon 0.200 0.133 Pass/<LOD
Dimethoate 0.200 0.133 Pass/<LOD Ethoprophos 0.200 0.133 Pass/<LOD
Etofenprox 0.400 0.133 Pass/<LOD Etoxazole 0.200 0.133 Pass/<LOD
Fenoxycarb 0.200 0.133 Pass/<LOD Fenpyroximate 0.400 0.133 Pass/<LOD
Fipronil 0.400 0.133 Pass/<LOD Flonicamid 1.000 0.133 Pass/<LOD
Fludioxonil 0.400 0.133 Pass/<LOD Hexythiazox 1.000 0.133 Pass/<LOD
Imazalil 0.200 0.133 Pass/<LOD Imidacloprid 0.400 0.133 Pass/<LOD
Kresoxim Methyl 0.400 0.133 Pass/<LOD Malathion 0.200 0.133 Pass/<LOD
Metalaxyl 0.200 0.133 Pass/<LOD Methiocarb 0.200 0.133 Pass/<LOD
Methomyl 0.400 0.133 Pass/<LOD Methyl Parathion 0.200 0.133 Pass/<LOD
MGK-264‡ 0.200 0.133 Pass/<LOD Myclobutanil 0.000 0.133 Pass/<LOD
Naled 0.500 0.133 Pass/<LOD Oxamyl 1.000 0.133 Pass/<LOD
Paclobutrazol 0.400 0.133 Pass/<LOD Permethrins† 0.200 0.133 Pass/<LOD
Phosmet 0.200 0.133 Pass/<LOD Piperonyl Butoxide 2.000 0.133 Pass/<LOD
Prallethrin 0.200 0.133 Pass/<LOD Propiconazole 0.400 0.133 Pass/<LOD
Propoxur 0.200 0.133 Pass/<LOD Pyrethrins* 1.000 0.133 Pass/<LOD
Pyridaben 0.200 0.133 Pass/<LOD Spinosad***** 0.200 0.133 Pass/<LOD
Spiromesifen 0.200 0.133 Pass/<LOD Spirotetramat 0.200 0.133 Pass/<LOD
Spiroxamine‡ 0.400 0.133 Pass/<LOD Tebuconazole 0.400 0.133 Pass/<LOD
Thiacloprid 0.200 0.133 Pass/<LOD Thiamethoxam 0.200 0.133 Pass/<LOD
Trifloxystrobin 0.200 0.133 Pass/<LOD

* Pyrethrins are reported as the sum of Jasmolin I, Cinerin I, and Pyrethrin I
** Cyfluthrins are reported as the sum of isomers Cyfluthrin I, II, III, and IV
*** Cypermethrins are reported as the sum of isomers Cypermethrin I, II, III, and IV
**** Abamectin is reported as the sum of Avermectin B1a and Avermectin B1b
***** Spinosad is reported as the sum of Spinosyn A and Spinosyn D
† Permethrin and Prallethrin are reported as the sum of cis and trans isomers
‡ MGK-264 and Spiroximine are reported as the sum of isomers I and II
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 16 of 67

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Pesticide QC Report
Testing Accreditation #: 4092-004 Test Certificate #: 123371-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Northern Wreck Badder
License: 030-1009646F7F8
Type: AU Tincture
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A401030002C949000000017
Metrc Source Pkg#: 1A401030002C949000000016
Test Conditions

Prepsheet ID#: ORPS200403B
Scale: XS205-OR1
Temp: 21.7 °C
Baro PE: 1005 hPa
Analyst: JER
Technician: JER
Sample ID#: 123371

Lot #: Northern wreck badder 3/30/20 #1
Batch #: 123371
Batch Weight (g): 1640.4
Harvest/Process Date: 03/31/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 03/31/2020
Test Date: 04/06/2020
Sample #123371
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS recovery% MSD recovery% Relative Percent Difference (%) QC Flag
Acephate N.D. 1 1.04 0.908 104.00 90.80 13.55
Acequinocyl N.D. 1 0.518 0.531 51.80 53.10 2.48 LR
Acetamiprid N.D. 1 1.17 1.06 117.00 106.00 9.87
Aldicarb N.D. 1 0.871 0.817 87.10 81.70 6.40
Avermectin B1a N.D. 0.97 2.24 1.62 230.93 167.01 32.12 HRQ
Azoxystrobin N.D. 1 1.11 1.01 111.00 101.00 9.43
Bifenazate N.D. 1 1.08 0.909 108.00 90.90 17.19
Bifenthrin N.D. 1 0.805 0.829 80.50 82.90 2.94
Boscalid N.D. 1 0.87 0.998 87.00 99.80 13.70
Carbaryl N.D. 1 0.938 0.875 93.80 87.50 6.95
Carbofuran N.D. 1 1.09 1.01 109.00 101.00 7.62
Chlorantraniliprole N.D. 1 1.35 1.21 135.00 121.00 10.94 HR
Chlorfenapyr N.D. 1 0.82 0.878 82.00 87.80 6.83
Chlorpyriphos N.D. 1 0.91 0.886 91.00 88.60 2.67
Clofentezine N.D. 1 1.03 0.982 103.00 98.20 4.77
Cyfluthrin N.D. 1 1.1 1 110.00 100.00 9.52
Cypermethrin N.D. 1 1.16 1.06 116.00 106.00 9.01
Daminoside N.D. 1 1.16 1.12 116.00 112.00 3.51
Diazanon N.D. 1 1.12 1.06 112.00 106.00 5.50
Dichlorvos N.D. 1 0.806 0.644 80.60 64.40 22.34 LRQ
Dimethoate N.D. 1 1.06 0.908 106.00 90.80 15.45
Ethoprophos N.D. 1 0.879 0.8 87.90 80.00 9.41
Etofenprox N.D. 1 0.914 0.87 91.40 87.00 4.93
Etoxazole N.D. 1 1.09 0.966 109.00 96.60 12.06
Fenoxycarb N.D. 1 1.31 1.15 131.00 115.00 13.01 HR
Fenpyroximate N.D. 1 1.01 0.99 101.00 99.00 2.00
Fipronil N.D. 1 1.06 1.01 106.00 101.00 4.83
Flonicamid N.D. 1 1.05 0.955 105.00 95.50 9.48
Fludioxonil N.D. 1 1.01 0.989 101.00 98.90 2.10
Hexythiazox N.D. 1 0.763 0.737 76.30 73.70 3.47
Imazalil N.D. 1 1.55 1.23 155.00 123.00 23.02 HRQ
Imidacloprid N.D. 1 1.13 1 113.00 100.00 12.21
Kresoxim-methyl N.D. 1 1.56 1.33 156.00 133.00 15.92 HR
Malathion N.D. 1 1.17 1.19 117.00 119.00 1.69
Metalaxyl N.D. 1 1.29 1.23 129.00 123.00 4.76
Methiocarb N.D. 1 1.09 0.925 109.00 92.50 16.38
Methomyl N.D. 1 1.25 1.14 125.00 114.00 9.21
MGK-264 N.D. 1 0.905 0.759 90.50 75.90 17.55
Myclobutanil N.D. 1 1.32 1.29 132.00 129.00 2.30 HR
Naled (dibrom) N.D. 1 0.671 0.567 67.10 56.70 16.80 LR
Oxamyl N.D. 1 1.06 0.902 106.00 90.20 16.11
Paclobutrazol N.D. 1 1.69 1.48 169.00 148.00 13.25 HR
Parathion-methyl N.D. 1 1.11 0.896 111.00 89.60 21.34 Q
Permethrins N.D. 1 0.886 0.821 88.60 82.10 7.62
Phosmet N.D. 1 1.37 1.23 137.00 123.00 10.77 HR
Piperonyl butoxide N.D. 1 1.1 1.03 110.00 103.00 6.57
Prallethrin N.D. 1 1.43 1.43 143.00 143.00 0.00 HR
Propiconazole N.D. 1 1.12 1.07 112.00 107.00 4.57
Propoxur N.D. 1 1.07 0.945 107.00 94.50 12.41
Pyrethrin N.D. 0.65 0.788 0.735 121.23 113.08 6.96
Pyridaben N.D. 1 0.879 0.787 87.90 78.70 11.04
SpinosynA N.D. 0.84 1.23 1.08 146.43 128.57 12.99 HR
SpinosynD N.D. 0.16 0.232 0.227 145.00 141.88 2.18 HR
Spiromesifen N.D. 1 0.817 0.807 81.70 80.70 1.23
Spirotetramat N.D. 1 1.86 1.42 186.00 142.00 26.83 HRQ
Spiroxamine N.D. 1 1.42 1.26 142.00 126.00 11.94 HR
Tebuconazole N.D. 1 1.38 1.27 138.00 127.00 8.30 HR
Thiacloprid N.D. 1 1.16 1.02 116.00 102.00 12.84
Thiamethoxam N.D. 1 1.57 1.42 157.00 142.00 10.03 HR
Trifloxystrobin N.D. 1 1.12 0.996 112.00 99.60 11.72

N.D. = Not Detected

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 30%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (60-120%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 17 of 67

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Pesticide Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-004 Test Certificate #: 123371-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Northern Wreck Badder
License: 030-1009646F7F8
Type: AU Tincture
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A401030002C949000000017
Metrc Source Pkg#: 1A401030002C949000000016
Test Conditions

Prepsheet ID#: ORPS200403B
Scale: XS205-OR1
Temp: 21.7 °C
Baro PE: 1005 hPa
Analyst: JER
Technician: JER
Sample ID#: 123371

Lot #: Northern wreck badder 3/30/20 #1
Batch #: 123371
Batch Weight (g): 1640.4
Harvest/Process Date: 03/31/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 03/31/2020
Test Date: 04/06/2020
Sample #123371
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
Aldicarb 0.400 0.130 Pass/<LOD Abamectin**** 0.500 0.130 Pass/<LOD
Acephate 0.400 0.130 Pass/<LOD Acequinocyl 2.000 0.261 Pass/<LOD
Acetamiprid 0.200 0.130 Pass/<LOD Azoxystrobin 0.200 0.130 Pass/<LOD
Bifenazate 0.200 0.130 Pass/<LOD Bifenthrin 0.200 0.130 Pass/<LOD
Boscalid 0.400 0.130 Pass/<LOD Carbaryl 0.200 0.130 Pass/<LOD
Carbofuran 0.200 0.130 Pass/<LOD Chlorantraniliprole 0.200 0.130 Pass/<LOD
Chlorfenapyr 1.000 0.522 Pass/<LOD Chlorpyrifos 0.200 0.130 Pass/<LOD
Clofentezine 0.200 0.130 Pass/<LOD Cyfluthrin** 1.000 0.522 Pass/<LOD
Cypermethrin*** 1.000 0.522 Pass/<LOD Daminozide 1.000 0.130 Pass/<LOD
DDVP (Dichlorvos) 1.000 0.261 Pass/<LOD Diazinon 0.200 0.130 Pass/<LOD
Dimethoate 0.200 0.130 Pass/<LOD Ethoprophos 0.200 0.130 Pass/<LOD
Etofenprox 0.400 0.130 Pass/<LOD Etoxazole 0.200 0.130 Pass/<LOD
Fenoxycarb 0.200 0.130 Pass/<LOD Fenpyroximate 0.400 0.130 Pass/<LOD
Fipronil 0.400 0.130 Pass/<LOD Flonicamid 1.000 0.130 Pass/<LOD
Fludioxonil 0.400 0.130 Pass/<LOD Hexythiazox 1.000 0.130 Pass/<LOD
Imazalil 0.200 0.130 Pass/<LOD Imidacloprid 0.400 0.130 Pass/<LOD
Kresoxim Methyl 0.400 0.130 Pass/<LOD Malathion 0.200 0.130 Pass/<LOD
Metalaxyl 0.200 0.130 Pass/<LOD Methiocarb 0.200 0.130 Pass/<LOD
Methomyl 0.400 0.130 Pass/<LOD Methyl Parathion 0.200 0.130 Pass/<LOD
MGK-264‡ 0.200 0.130 Pass/<LOD Myclobutanil 0.000 0.130 Pass/<LOD
Naled 0.500 0.130 Pass/<LOD Oxamyl 1.000 0.130 Pass/<LOD
Paclobutrazol 0.400 0.130 Pass/<LOD Permethrins† 0.200 0.130 Pass/<LOD
Phosmet 0.200 0.130 Pass/<LOD Piperonyl Butoxide 2.000 0.130 Pass/<LOD
Prallethrin 0.200 0.130 Pass/<LOD Propiconazole 0.400 0.130 Pass/<LOD
Propoxur 0.200 0.130 Pass/<LOD Pyrethrins* 1.000 0.130 Pass/<LOD
Pyridaben 0.200 0.130 Pass/<LOD Spinosad***** 0.200 0.130 Pass/<LOD
Spiromesifen 0.200 0.130 Pass/<LOD Spirotetramat 0.200 0.130 Pass/<LOD
Spiroxamine‡ 0.400 0.130 Pass/<LOD Tebuconazole 0.400 0.130 Pass/<LOD
Thiacloprid 0.200 0.130 Pass/<LOD Thiamethoxam 0.200 0.130 Pass/<LOD
Trifloxystrobin 0.200 0.130 Pass/<LOD

* Pyrethrins are reported as the sum of Jasmolin I, Cinerin I, and Pyrethrin I
** Cyfluthrins are reported as the sum of isomers Cyfluthrin I, II, III, and IV
*** Cypermethrins are reported as the sum of isomers Cypermethrin I, II, III, and IV
**** Abamectin is reported as the sum of Avermectin B1a and Avermectin B1b
***** Spinosad is reported as the sum of Spinosyn A and Spinosyn D
† Permethrin and Prallethrin are reported as the sum of cis and trans isomers
‡ MGK-264 and Spiroximine are reported as the sum of isomers I and II
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 18 of 67

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Pesticide QC Report
Testing Accreditation #: 4092-004 Test Certificate #: 123371-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Northern Wreck Badder
License: 030-1009646F7F8
Type: AU Tincture
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A401030002C949000000017
Metrc Source Pkg#: 1A401030002C949000000016
Test Conditions

Prepsheet ID#: ORPS200403B
Scale: XS205-OR1
Temp: 21.7 °C
Baro PE: 1005 hPa
Analyst: JER
Technician: JER
Sample ID#: 123371

Lot #: Northern wreck badder 3/30/20 #1
Batch #: 123371
Batch Weight (g): 1640.4
Harvest/Process Date: 03/31/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 03/31/2020
Test Date: 04/06/2020
Sample #123371
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS recovery% MSD recovery% Relative Percent Difference (%) QC Flag
Acephate N.D. 1 1.04 0.908 104.00 90.80 13.55
Acequinocyl N.D. 1 0.518 0.531 51.80 53.10 2.48 LR
Acetamiprid N.D. 1 1.17 1.06 117.00 106.00 9.87
Aldicarb N.D. 1 0.871 0.817 87.10 81.70 6.40
Avermectin B1a N.D. 0.97 2.24 1.62 230.93 167.01 32.12 HRQ
Azoxystrobin N.D. 1 1.11 1.01 111.00 101.00 9.43
Bifenazate N.D. 1 1.08 0.909 108.00 90.90 17.19
Bifenthrin N.D. 1 0.805 0.829 80.50 82.90 2.94
Boscalid N.D. 1 0.87 0.998 87.00 99.80 13.70
Carbaryl N.D. 1 0.938 0.875 93.80 87.50 6.95
Carbofuran N.D. 1 1.09 1.01 109.00 101.00 7.62
Chlorantraniliprole N.D. 1 1.35 1.21 135.00 121.00 10.94 HR
Chlorfenapyr N.D. 1 0.82 0.878 82.00 87.80 6.83
Chlorpyriphos N.D. 1 0.91 0.886 91.00 88.60 2.67
Clofentezine N.D. 1 1.03 0.982 103.00 98.20 4.77
Cyfluthrin N.D. 1 1.1 1 110.00 100.00 9.52
Cypermethrin N.D. 1 1.16 1.06 116.00 106.00 9.01
Daminoside N.D. 1 1.16 1.12 116.00 112.00 3.51
Diazanon N.D. 1 1.12 1.06 112.00 106.00 5.50
Dichlorvos N.D. 1 0.806 0.644 80.60 64.40 22.34 LRQ
Dimethoate N.D. 1 1.06 0.908 106.00 90.80 15.45
Ethoprophos N.D. 1 0.879 0.8 87.90 80.00 9.41
Etofenprox N.D. 1 0.914 0.87 91.40 87.00 4.93
Etoxazole N.D. 1 1.09 0.966 109.00 96.60 12.06
Fenoxycarb N.D. 1 1.31 1.15 131.00 115.00 13.01 HR
Fenpyroximate N.D. 1 1.01 0.99 101.00 99.00 2.00
Fipronil N.D. 1 1.06 1.01 106.00 101.00 4.83
Flonicamid N.D. 1 1.05 0.955 105.00 95.50 9.48
Fludioxonil N.D. 1 1.01 0.989 101.00 98.90 2.10
Hexythiazox N.D. 1 0.763 0.737 76.30 73.70 3.47
Imazalil N.D. 1 1.55 1.23 155.00 123.00 23.02 HRQ
Imidacloprid N.D. 1 1.13 1 113.00 100.00 12.21
Kresoxim-methyl N.D. 1 1.56 1.33 156.00 133.00 15.92 HR
Malathion N.D. 1 1.17 1.19 117.00 119.00 1.69
Metalaxyl N.D. 1 1.29 1.23 129.00 123.00 4.76
Methiocarb N.D. 1 1.09 0.925 109.00 92.50 16.38
Methomyl N.D. 1 1.25 1.14 125.00 114.00 9.21
MGK-264 N.D. 1 0.905 0.759 90.50 75.90 17.55
Myclobutanil N.D. 1 1.32 1.29 132.00 129.00 2.30 HR
Naled (dibrom) N.D. 1 0.671 0.567 67.10 56.70 16.80 LR
Oxamyl N.D. 1 1.06 0.902 106.00 90.20 16.11
Paclobutrazol N.D. 1 1.69 1.48 169.00 148.00 13.25 HR
Parathion-methyl N.D. 1 1.11 0.896 111.00 89.60 21.34 Q
Permethrins N.D. 1 0.886 0.821 88.60 82.10 7.62
Phosmet N.D. 1 1.37 1.23 137.00 123.00 10.77 HR
Piperonyl butoxide N.D. 1 1.1 1.03 110.00 103.00 6.57
Prallethrin N.D. 1 1.43 1.43 143.00 143.00 0.00 HR
Propiconazole N.D. 1 1.12 1.07 112.00 107.00 4.57
Propoxur N.D. 1 1.07 0.945 107.00 94.50 12.41
Pyrethrin N.D. 0.65 0.788 0.735 121.23 113.08 6.96
Pyridaben N.D. 1 0.879 0.787 87.90 78.70 11.04
SpinosynA N.D. 0.84 1.23 1.08 146.43 128.57 12.99 HR
SpinosynD N.D. 0.16 0.232 0.227 145.00 141.88 2.18 HR
Spiromesifen N.D. 1 0.817 0.807 81.70 80.70 1.23
Spirotetramat N.D. 1 1.86 1.42 186.00 142.00 26.83 HRQ
Spiroxamine N.D. 1 1.42 1.26 142.00 126.00 11.94 HR
Tebuconazole N.D. 1 1.38 1.27 138.00 127.00 8.30 HR
Thiacloprid N.D. 1 1.16 1.02 116.00 102.00 12.84
Thiamethoxam N.D. 1 1.57 1.42 157.00 142.00 10.03 HR
Trifloxystrobin N.D. 1 1.12 0.996 112.00 99.60 11.72

N.D. = Not Detected

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 30%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (60-120%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 19 of 67

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Pesticide Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-004 Test Certificate #: 123371-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Northern Wreck Badder
License: 030-1009646F7F8
Type: AU Tincture
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A401030002C949000000017
Metrc Source Pkg#: 1A401030002C949000000016
Test Conditions

Prepsheet ID#: ORPS200403B
Scale: XS205-OR1
Temp: 21.7 °C
Baro PE: 1005 hPa
Analyst: JER
Technician: JER
Sample ID#: 123371

Lot #: Northern wreck badder 3/30/20 #1
Batch #: 123371
Batch Weight (g): 1640.4
Harvest/Process Date: 03/31/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 03/31/2020
Test Date: 04/06/2020
Sample #123371
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
Aldicarb 0.400 0.130 Pass/<LOD Abamectin**** 0.500 0.130 Pass/<LOD
Acephate 0.400 0.130 Pass/<LOD Acequinocyl 2.000 0.260 Pass/<LOD
Acetamiprid 0.200 0.130 Pass/<LOD Azoxystrobin 0.200 0.130 Pass/<LOD
Bifenazate 0.200 0.130 Pass/<LOD Bifenthrin 0.200 0.130 Pass/<LOD
Boscalid 0.400 0.130 Pass/<LOD Carbaryl 0.200 0.130 Pass/<LOD
Carbofuran 0.200 0.130 Pass/<LOD Chlorantraniliprole 0.200 0.130 Pass/<LOD
Chlorfenapyr 1.000 0.519 Pass/<LOD Chlorpyrifos 0.200 0.130 Pass/<LOD
Clofentezine 0.200 0.130 Pass/<LOD Cyfluthrin** 1.000 0.519 Pass/<LOD
Cypermethrin*** 1.000 0.519 Pass/<LOD Daminozide 1.000 0.130 Pass/<LOD
DDVP (Dichlorvos) 1.000 0.260 Pass/<LOD Diazinon 0.200 0.130 Pass/<LOD
Dimethoate 0.200 0.130 Pass/<LOD Ethoprophos 0.200 0.130 Pass/<LOD
Etofenprox 0.400 0.130 Pass/<LOD Etoxazole 0.200 0.130 Pass/<LOD
Fenoxycarb 0.200 0.130 Pass/<LOD Fenpyroximate 0.400 0.130 Pass/<LOD
Fipronil 0.400 0.130 Pass/<LOD Flonicamid 1.000 0.130 Pass/<LOD
Fludioxonil 0.400 0.130 Pass/<LOD Hexythiazox 1.000 0.130 Pass/<LOD
Imazalil 0.200 0.130 Pass/<LOD Imidacloprid 0.400 0.130 Pass/<LOD
Kresoxim Methyl 0.400 0.130 Pass/<LOD Malathion 0.200 0.130 Pass/<LOD
Metalaxyl 0.200 0.130 Pass/<LOD Methiocarb 0.200 0.130 Pass/<LOD
Methomyl 0.400 0.130 Pass/<LOD Methyl Parathion 0.200 0.130 Pass/<LOD
MGK-264‡ 0.200 0.130 Pass/<LOD Myclobutanil 0.000 0.130 Pass/<LOD
Naled 0.500 0.130 Pass/<LOD Oxamyl 1.000 0.130 Pass/<LOD
Paclobutrazol 0.400 0.130 Pass/<LOD Permethrins† 0.200 0.130 Pass/<LOD
Phosmet 0.200 0.130 Pass/<LOD Piperonyl Butoxide 2.000 0.130 Pass/<LOD
Prallethrin 0.200 0.130 Pass/<LOD Propiconazole 0.400 0.130 Pass/<LOD
Propoxur 0.200 0.130 Pass/<LOD Pyrethrins* 1.000 0.130 Pass/<LOD
Pyridaben 0.200 0.130 Pass/<LOD Spinosad***** 0.200 0.130 Pass/<LOD
Spiromesifen 0.200 0.130 Pass/<LOD Spirotetramat 0.200 0.130 Pass/<LOD
Spiroxamine‡ 0.400 0.130 Pass/<LOD Tebuconazole 0.400 0.130 Pass/<LOD
Thiacloprid 0.200 0.130 Pass/<LOD Thiamethoxam 0.200 0.130 Pass/<LOD
Trifloxystrobin 0.200 0.130 Pass/<LOD

* Pyrethrins are reported as the sum of Jasmolin I, Cinerin I, and Pyrethrin I
** Cyfluthrins are reported as the sum of isomers Cyfluthrin I, II, III, and IV
*** Cypermethrins are reported as the sum of isomers Cypermethrin I, II, III, and IV
**** Abamectin is reported as the sum of Avermectin B1a and Avermectin B1b
***** Spinosad is reported as the sum of Spinosyn A and Spinosyn D
† Permethrin and Prallethrin are reported as the sum of cis and trans isomers
‡ MGK-264 and Spiroximine are reported as the sum of isomers I and II
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 20 of 67

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Pesticide QC Report
Testing Accreditation #: 4092-004 Test Certificate #: 123371-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Northern Wreck Badder
License: 030-1009646F7F8
Type: AU Tincture
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A401030002C949000000017
Metrc Source Pkg#: 1A401030002C949000000016
Test Conditions

Prepsheet ID#: ORPS200403B
Scale: XS205-OR1
Temp: 21.7 °C
Baro PE: 1005 hPa
Analyst: JER
Technician: JER
Sample ID#: 123371

Lot #: Northern wreck badder 3/30/20 #1
Batch #: 123371
Batch Weight (g): 1640.4
Harvest/Process Date: 03/31/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 03/31/2020
Test Date: 04/06/2020
Sample #123371
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS recovery% MSD recovery% Relative Percent Difference (%) QC Flag
Acephate N.D. 1 1.04 0.908 104.00 90.80 13.55
Acequinocyl N.D. 1 0.518 0.531 51.80 53.10 2.48 LR
Acetamiprid N.D. 1 1.17 1.06 117.00 106.00 9.87
Aldicarb N.D. 1 0.871 0.817 87.10 81.70 6.40
Avermectin B1a N.D. 0.97 2.24 1.62 230.93 167.01 32.12 HRQ
Azoxystrobin N.D. 1 1.11 1.01 111.00 101.00 9.43
Bifenazate N.D. 1 1.08 0.909 108.00 90.90 17.19
Bifenthrin N.D. 1 0.805 0.829 80.50 82.90 2.94
Boscalid N.D. 1 0.87 0.998 87.00 99.80 13.70
Carbaryl N.D. 1 0.938 0.875 93.80 87.50 6.95
Carbofuran N.D. 1 1.09 1.01 109.00 101.00 7.62
Chlorantraniliprole N.D. 1 1.35 1.21 135.00 121.00 10.94 HR
Chlorfenapyr N.D. 1 0.82 0.878 82.00 87.80 6.83
Chlorpyriphos N.D. 1 0.91 0.886 91.00 88.60 2.67
Clofentezine N.D. 1 1.03 0.982 103.00 98.20 4.77
Cyfluthrin N.D. 1 1.1 1 110.00 100.00 9.52
Cypermethrin N.D. 1 1.16 1.06 116.00 106.00 9.01
Daminoside N.D. 1 1.16 1.12 116.00 112.00 3.51
Diazanon N.D. 1 1.12 1.06 112.00 106.00 5.50
Dichlorvos N.D. 1 0.806 0.644 80.60 64.40 22.34 LRQ
Dimethoate N.D. 1 1.06 0.908 106.00 90.80 15.45
Ethoprophos N.D. 1 0.879 0.8 87.90 80.00 9.41
Etofenprox N.D. 1 0.914 0.87 91.40 87.00 4.93
Etoxazole N.D. 1 1.09 0.966 109.00 96.60 12.06
Fenoxycarb N.D. 1 1.31 1.15 131.00 115.00 13.01 HR
Fenpyroximate N.D. 1 1.01 0.99 101.00 99.00 2.00
Fipronil N.D. 1 1.06 1.01 106.00 101.00 4.83
Flonicamid N.D. 1 1.05 0.955 105.00 95.50 9.48
Fludioxonil N.D. 1 1.01 0.989 101.00 98.90 2.10
Hexythiazox N.D. 1 0.763 0.737 76.30 73.70 3.47
Imazalil N.D. 1 1.55 1.23 155.00 123.00 23.02 HRQ
Imidacloprid N.D. 1 1.13 1 113.00 100.00 12.21
Kresoxim-methyl N.D. 1 1.56 1.33 156.00 133.00 15.92 HR
Malathion N.D. 1 1.17 1.19 117.00 119.00 1.69
Metalaxyl N.D. 1 1.29 1.23 129.00 123.00 4.76
Methiocarb N.D. 1 1.09 0.925 109.00 92.50 16.38
Methomyl N.D. 1 1.25 1.14 125.00 114.00 9.21
MGK-264 N.D. 1 0.905 0.759 90.50 75.90 17.55
Myclobutanil N.D. 1 1.32 1.29 132.00 129.00 2.30 HR
Naled (dibrom) N.D. 1 0.671 0.567 67.10 56.70 16.80 LR
Oxamyl N.D. 1 1.06 0.902 106.00 90.20 16.11
Paclobutrazol N.D. 1 1.69 1.48 169.00 148.00 13.25 HR
Parathion-methyl N.D. 1 1.11 0.896 111.00 89.60 21.34 Q
Permethrins N.D. 1 0.886 0.821 88.60 82.10 7.62
Phosmet N.D. 1 1.37 1.23 137.00 123.00 10.77 HR
Piperonyl butoxide N.D. 1 1.1 1.03 110.00 103.00 6.57
Prallethrin N.D. 1 1.43 1.43 143.00 143.00 0.00 HR
Propiconazole N.D. 1 1.12 1.07 112.00 107.00 4.57
Propoxur N.D. 1 1.07 0.945 107.00 94.50 12.41
Pyrethrin N.D. 0.65 0.788 0.735 121.23 113.08 6.96
Pyridaben N.D. 1 0.879 0.787 87.90 78.70 11.04
SpinosynA N.D. 0.84 1.23 1.08 146.43 128.57 12.99 HR
SpinosynD N.D. 0.16 0.232 0.227 145.00 141.88 2.18 HR
Spiromesifen N.D. 1 0.817 0.807 81.70 80.70 1.23
Spirotetramat N.D. 1 1.86 1.42 186.00 142.00 26.83 HRQ
Spiroxamine N.D. 1 1.42 1.26 142.00 126.00 11.94 HR
Tebuconazole N.D. 1 1.38 1.27 138.00 127.00 8.30 HR
Thiacloprid N.D. 1 1.16 1.02 116.00 102.00 12.84
Thiamethoxam N.D. 1 1.57 1.42 157.00 142.00 10.03 HR
Trifloxystrobin N.D. 1 1.12 0.996 112.00 99.60 11.72

N.D. = Not Detected

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 30%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (60-120%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 21 of 67

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Pesticide Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-004 Test Certificate #: 123371-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Northern Wreck Badder
License: 030-1009646F7F8
Type: AU Tincture
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A401030002C949000000017
Metrc Source Pkg#: 1A401030002C949000000016
Test Conditions

Prepsheet ID#: ORPS200403B
Scale: XS205-OR1
Temp: 21.7 °C
Baro PE: 1005 hPa
Analyst: JER
Technician: JER
Sample ID#: 123371

Lot #: Northern wreck badder 3/30/20 #1
Batch #: 123371
Batch Weight (g): 1640.4
Harvest/Process Date: 03/31/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 03/31/2020
Test Date: 04/06/2020
Sample #123371
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
Aldicarb 0.400 0.129 Pass/<LOD Abamectin**** 0.500 0.129 Pass/<LOD
Acephate 0.400 0.129 Pass/<LOD Acequinocyl 2.000 0.258 Pass/<LOD
Acetamiprid 0.200 0.129 Pass/<LOD Azoxystrobin 0.200 0.129 Pass/<LOD
Bifenazate 0.200 0.129 Pass/<LOD Bifenthrin 0.200 0.129 Pass/<LOD
Boscalid 0.400 0.129 Pass/<LOD Carbaryl 0.200 0.129 Pass/<LOD
Carbofuran 0.200 0.129 Pass/<LOD Chlorantraniliprole 0.200 0.129 Pass/<LOD
Chlorfenapyr 1.000 0.517 Pass/<LOD Chlorpyrifos 0.200 0.129 Pass/<LOD
Clofentezine 0.200 0.129 Pass/<LOD Cyfluthrin** 1.000 0.517 Pass/<LOD
Cypermethrin*** 1.000 0.517 Pass/<LOD Daminozide 1.000 0.129 Pass/<LOD
DDVP (Dichlorvos) 1.000 0.258 Pass/<LOD Diazinon 0.200 0.129 Pass/<LOD
Dimethoate 0.200 0.129 Pass/<LOD Ethoprophos 0.200 0.129 Pass/<LOD
Etofenprox 0.400 0.129 Pass/<LOD Etoxazole 0.200 0.129 Pass/<LOD
Fenoxycarb 0.200 0.129 Pass/<LOD Fenpyroximate 0.400 0.129 Pass/<LOD
Fipronil 0.400 0.129 Pass/<LOD Flonicamid 1.000 0.129 Pass/<LOD
Fludioxonil 0.400 0.129 Pass/<LOD Hexythiazox 1.000 0.129 Pass/<LOD
Imazalil 0.200 0.129 Pass/<LOD Imidacloprid 0.400 0.129 Pass/<LOD
Kresoxim Methyl 0.400 0.129 Pass/<LOD Malathion 0.200 0.129 Pass/<LOD
Metalaxyl 0.200 0.129 Pass/<LOD Methiocarb 0.200 0.129 Pass/<LOD
Methomyl 0.400 0.129 Pass/<LOD Methyl Parathion 0.200 0.129 Pass/<LOD
MGK-264‡ 0.200 0.129 Pass/<LOD Myclobutanil 0.000 0.129 Pass/<LOD
Naled 0.500 0.129 Pass/<LOD Oxamyl 1.000 0.129 Pass/<LOD
Paclobutrazol 0.400 0.129 Pass/<LOD Permethrins† 0.200 0.129 Pass/<LOD
Phosmet 0.200 0.129 Pass/<LOD Piperonyl Butoxide 2.000 0.129 Pass/<LOD
Prallethrin 0.200 0.129 Pass/<LOD Propiconazole 0.400 0.129 Pass/<LOD
Propoxur 0.200 0.129 Pass/<LOD Pyrethrins* 1.000 0.129 Pass/<LOD
Pyridaben 0.200 0.129 Pass/<LOD Spinosad***** 0.200 0.129 Pass/<LOD
Spiromesifen 0.200 0.129 Pass/<LOD Spirotetramat 0.200 0.129 Pass/<LOD
Spiroxamine‡ 0.400 0.129 Pass/<LOD Tebuconazole 0.400 0.129 Pass/<LOD
Thiacloprid 0.200 0.129 Pass/<LOD Thiamethoxam 0.200 0.129 Pass/<LOD
Trifloxystrobin 0.200 0.129 Pass/<LOD

* Pyrethrins are reported as the sum of Jasmolin I, Cinerin I, and Pyrethrin I
** Cyfluthrins are reported as the sum of isomers Cyfluthrin I, II, III, and IV
*** Cypermethrins are reported as the sum of isomers Cypermethrin I, II, III, and IV
**** Abamectin is reported as the sum of Avermectin B1a and Avermectin B1b
***** Spinosad is reported as the sum of Spinosyn A and Spinosyn D
† Permethrin and Prallethrin are reported as the sum of cis and trans isomers
‡ MGK-264 and Spiroximine are reported as the sum of isomers I and II
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 22 of 67

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Pesticide QC Report
Testing Accreditation #: 4092-004 Test Certificate #: 123371-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Northern Wreck Badder
License: 030-1009646F7F8
Type: AU Tincture
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A401030002C949000000017
Metrc Source Pkg#: 1A401030002C949000000016
Test Conditions

Prepsheet ID#: ORPS200403B
Scale: XS205-OR1
Temp: 21.7 °C
Baro PE: 1005 hPa
Analyst: JER
Technician: JER
Sample ID#: 123371

Lot #: Northern wreck badder 3/30/20 #1
Batch #: 123371
Batch Weight (g): 1640.4
Harvest/Process Date: 03/31/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 03/31/2020
Test Date: 04/06/2020
Sample #123371
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS recovery% MSD recovery% Relative Percent Difference (%) QC Flag
Acephate N.D. 1 1.04 0.908 104.00 90.80 13.55
Acequinocyl N.D. 1 0.518 0.531 51.80 53.10 2.48 LR
Acetamiprid N.D. 1 1.17 1.06 117.00 106.00 9.87
Aldicarb N.D. 1 0.871 0.817 87.10 81.70 6.40
Avermectin B1a N.D. 0.97 2.24 1.62 230.93 167.01 32.12 HRQ
Azoxystrobin N.D. 1 1.11 1.01 111.00 101.00 9.43
Bifenazate N.D. 1 1.08 0.909 108.00 90.90 17.19
Bifenthrin N.D. 1 0.805 0.829 80.50 82.90 2.94
Boscalid N.D. 1 0.87 0.998 87.00 99.80 13.70
Carbaryl N.D. 1 0.938 0.875 93.80 87.50 6.95
Carbofuran N.D. 1 1.09 1.01 109.00 101.00 7.62
Chlorantraniliprole N.D. 1 1.35 1.21 135.00 121.00 10.94 HR
Chlorfenapyr N.D. 1 0.82 0.878 82.00 87.80 6.83
Chlorpyriphos N.D. 1 0.91 0.886 91.00 88.60 2.67
Clofentezine N.D. 1 1.03 0.982 103.00 98.20 4.77
Cyfluthrin N.D. 1 1.1 1 110.00 100.00 9.52
Cypermethrin N.D. 1 1.16 1.06 116.00 106.00 9.01
Daminoside N.D. 1 1.16 1.12 116.00 112.00 3.51
Diazanon N.D. 1 1.12 1.06 112.00 106.00 5.50
Dichlorvos N.D. 1 0.806 0.644 80.60 64.40 22.34 LRQ
Dimethoate N.D. 1 1.06 0.908 106.00 90.80 15.45
Ethoprophos N.D. 1 0.879 0.8 87.90 80.00 9.41
Etofenprox N.D. 1 0.914 0.87 91.40 87.00 4.93
Etoxazole N.D. 1 1.09 0.966 109.00 96.60 12.06
Fenoxycarb N.D. 1 1.31 1.15 131.00 115.00 13.01 HR
Fenpyroximate N.D. 1 1.01 0.99 101.00 99.00 2.00
Fipronil N.D. 1 1.06 1.01 106.00 101.00 4.83
Flonicamid N.D. 1 1.05 0.955 105.00 95.50 9.48
Fludioxonil N.D. 1 1.01 0.989 101.00 98.90 2.10
Hexythiazox N.D. 1 0.763 0.737 76.30 73.70 3.47
Imazalil N.D. 1 1.55 1.23 155.00 123.00 23.02 HRQ
Imidacloprid N.D. 1 1.13 1 113.00 100.00 12.21
Kresoxim-methyl N.D. 1 1.56 1.33 156.00 133.00 15.92 HR
Malathion N.D. 1 1.17 1.19 117.00 119.00 1.69
Metalaxyl N.D. 1 1.29 1.23 129.00 123.00 4.76
Methiocarb N.D. 1 1.09 0.925 109.00 92.50 16.38
Methomyl N.D. 1 1.25 1.14 125.00 114.00 9.21
MGK-264 N.D. 1 0.905 0.759 90.50 75.90 17.55
Myclobutanil N.D. 1 1.32 1.29 132.00 129.00 2.30 HR
Naled (dibrom) N.D. 1 0.671 0.567 67.10 56.70 16.80 LR
Oxamyl N.D. 1 1.06 0.902 106.00 90.20 16.11
Paclobutrazol N.D. 1 1.69 1.48 169.00 148.00 13.25 HR
Parathion-methyl N.D. 1 1.11 0.896 111.00 89.60 21.34 Q
Permethrins N.D. 1 0.886 0.821 88.60 82.10 7.62
Phosmet N.D. 1 1.37 1.23 137.00 123.00 10.77 HR
Piperonyl butoxide N.D. 1 1.1 1.03 110.00 103.00 6.57
Prallethrin N.D. 1 1.43 1.43 143.00 143.00 0.00 HR
Propiconazole N.D. 1 1.12 1.07 112.00 107.00 4.57
Propoxur N.D. 1 1.07 0.945 107.00 94.50 12.41
Pyrethrin N.D. 0.65 0.788 0.735 121.23 113.08 6.96
Pyridaben N.D. 1 0.879 0.787 87.90 78.70 11.04
SpinosynA N.D. 0.84 1.23 1.08 146.43 128.57 12.99 HR
SpinosynD N.D. 0.16 0.232 0.227 145.00 141.88 2.18 HR
Spiromesifen N.D. 1 0.817 0.807 81.70 80.70 1.23
Spirotetramat N.D. 1 1.86 1.42 186.00 142.00 26.83 HRQ
Spiroxamine N.D. 1 1.42 1.26 142.00 126.00 11.94 HR
Tebuconazole N.D. 1 1.38 1.27 138.00 127.00 8.30 HR
Thiacloprid N.D. 1 1.16 1.02 116.00 102.00 12.84
Thiamethoxam N.D. 1 1.57 1.42 157.00 142.00 10.03 HR
Trifloxystrobin N.D. 1 1.12 0.996 112.00 99.60 11.72

N.D. = Not Detected

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 30%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (60-120%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 23 of 67

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Pesticide Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-004 Test Certificate #: 123371-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Northern Wreck Badder
License: 030-1009646F7F8
Type: AU Tincture
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A401030002C949000000017
Metrc Source Pkg#: 1A401030002C949000000016
Test Conditions

Prepsheet ID#: ORPS200403B
Scale: XS205-OR1
Temp: 21.7 °C
Baro PE: 1005 hPa
Analyst: JER
Technician: JER
Sample ID#: 123371

Lot #: Northern wreck badder 3/30/20 #1
Batch #: 123371
Batch Weight (g): 1640.4
Harvest/Process Date: 03/31/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 03/31/2020
Test Date: 04/06/2020
Sample #123371
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
Aldicarb 0.400 0.132 Pass/<LOD Abamectin**** 0.500 0.132 Pass/<LOD
Acephate 0.400 0.132 Pass/<LOD Acequinocyl 2.000 0.264 Pass/<LOD
Acetamiprid 0.200 0.132 Pass/<LOD Azoxystrobin 0.200 0.132 Pass/<LOD
Bifenazate 0.200 0.132 Pass/<LOD Bifenthrin 0.200 0.132 Pass/<LOD
Boscalid 0.400 0.132 Pass/<LOD Carbaryl 0.200 0.132 Pass/<LOD
Carbofuran 0.200 0.132 Pass/<LOD Chlorantraniliprole 0.200 0.132 Pass/<LOD
Chlorfenapyr 1.000 0.527 Pass/<LOD Chlorpyrifos 0.200 0.132 Pass/<LOD
Clofentezine 0.200 0.132 Pass/<LOD Cyfluthrin** 1.000 0.527 Pass/<LOD
Cypermethrin*** 1.000 0.527 Pass/<LOD Daminozide 1.000 0.132 Pass/<LOD
DDVP (Dichlorvos) 1.000 0.264 Pass/<LOD Diazinon 0.200 0.132 Pass/<LOD
Dimethoate 0.200 0.132 Pass/<LOD Ethoprophos 0.200 0.132 Pass/<LOD
Etofenprox 0.400 0.132 Pass/<LOD Etoxazole 0.200 0.132 Pass/<LOD
Fenoxycarb 0.200 0.132 Pass/<LOD Fenpyroximate 0.400 0.132 Pass/<LOD
Fipronil 0.400 0.132 Pass/<LOD Flonicamid 1.000 0.132 Pass/<LOD
Fludioxonil 0.400 0.132 Pass/<LOD Hexythiazox 1.000 0.132 Pass/<LOD
Imazalil 0.200 0.132 Pass/<LOD Imidacloprid 0.400 0.132 Pass/<LOD
Kresoxim Methyl 0.400 0.132 Pass/<LOD Malathion 0.200 0.132 Pass/<LOD
Metalaxyl 0.200 0.132 Pass/<LOD Methiocarb 0.200 0.132 Pass/<LOD
Methomyl 0.400 0.132 Pass/<LOD Methyl Parathion 0.200 0.132 Pass/<LOD
MGK-264‡ 0.200 0.132 Pass/<LOD Myclobutanil 0.000 0.132 Pass/<LOD
Naled 0.500 0.132 Pass/<LOD Oxamyl 1.000 0.132 Pass/<LOD
Paclobutrazol 0.400 0.132 Pass/<LOD Permethrins† 0.200 0.132 Pass/<LOD
Phosmet 0.200 0.132 Pass/<LOD Piperonyl Butoxide 2.000 0.132 Pass/<LOD
Prallethrin 0.200 0.132 Pass/<LOD Propiconazole 0.400 0.132 Pass/<LOD
Propoxur 0.200 0.132 Pass/<LOD Pyrethrins* 1.000 0.132 Pass/<LOD
Pyridaben 0.200 0.132 Pass/<LOD Spinosad***** 0.200 0.132 Pass/<LOD
Spiromesifen 0.200 0.132 Pass/<LOD Spirotetramat 0.200 0.132 Pass/<LOD
Spiroxamine‡ 0.400 0.132 Pass/<LOD Tebuconazole 0.400 0.132 Pass/<LOD
Thiacloprid 0.200 0.132 Pass/<LOD Thiamethoxam 0.200 0.132 Pass/<LOD
Trifloxystrobin 0.200 0.132 Pass/<LOD

* Pyrethrins are reported as the sum of Jasmolin I, Cinerin I, and Pyrethrin I
** Cyfluthrins are reported as the sum of isomers Cyfluthrin I, II, III, and IV
*** Cypermethrins are reported as the sum of isomers Cypermethrin I, II, III, and IV
**** Abamectin is reported as the sum of Avermectin B1a and Avermectin B1b
***** Spinosad is reported as the sum of Spinosyn A and Spinosyn D
† Permethrin and Prallethrin are reported as the sum of cis and trans isomers
‡ MGK-264 and Spiroximine are reported as the sum of isomers I and II
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 24 of 67

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Pesticide QC Report
Testing Accreditation #: 4092-004 Test Certificate #: 123371-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Northern Wreck Badder
License: 030-1009646F7F8
Type: AU Tincture
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A401030002C949000000017
Metrc Source Pkg#: 1A401030002C949000000016
Test Conditions

Prepsheet ID#: ORPS200403B
Scale: XS205-OR1
Temp: 21.7 °C
Baro PE: 1005 hPa
Analyst: JER
Technician: JER
Sample ID#: 123371

Lot #: Northern wreck badder 3/30/20 #1
Batch #: 123371
Batch Weight (g): 1640.4
Harvest/Process Date: 03/31/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 03/31/2020
Test Date: 04/06/2020
Sample #123371
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS recovery% MSD recovery% Relative Percent Difference (%) QC Flag
Acephate N.D. 1 1.04 0.908 104.00 90.80 13.55
Acequinocyl N.D. 1 0.518 0.531 51.80 53.10 2.48 LR
Acetamiprid N.D. 1 1.17 1.06 117.00 106.00 9.87
Aldicarb N.D. 1 0.871 0.817 87.10 81.70 6.40
Avermectin B1a N.D. 0.97 2.24 1.62 230.93 167.01 32.12 HRQ
Azoxystrobin N.D. 1 1.11 1.01 111.00 101.00 9.43
Bifenazate N.D. 1 1.08 0.909 108.00 90.90 17.19
Bifenthrin N.D. 1 0.805 0.829 80.50 82.90 2.94
Boscalid N.D. 1 0.87 0.998 87.00 99.80 13.70
Carbaryl N.D. 1 0.938 0.875 93.80 87.50 6.95
Carbofuran N.D. 1 1.09 1.01 109.00 101.00 7.62
Chlorantraniliprole N.D. 1 1.35 1.21 135.00 121.00 10.94 HR
Chlorfenapyr N.D. 1 0.82 0.878 82.00 87.80 6.83
Chlorpyriphos N.D. 1 0.91 0.886 91.00 88.60 2.67
Clofentezine N.D. 1 1.03 0.982 103.00 98.20 4.77
Cyfluthrin N.D. 1 1.1 1 110.00 100.00 9.52
Cypermethrin N.D. 1 1.16 1.06 116.00 106.00 9.01
Daminoside N.D. 1 1.16 1.12 116.00 112.00 3.51
Diazanon N.D. 1 1.12 1.06 112.00 106.00 5.50
Dichlorvos N.D. 1 0.806 0.644 80.60 64.40 22.34 LRQ
Dimethoate N.D. 1 1.06 0.908 106.00 90.80 15.45
Ethoprophos N.D. 1 0.879 0.8 87.90 80.00 9.41
Etofenprox N.D. 1 0.914 0.87 91.40 87.00 4.93
Etoxazole N.D. 1 1.09 0.966 109.00 96.60 12.06
Fenoxycarb N.D. 1 1.31 1.15 131.00 115.00 13.01 HR
Fenpyroximate N.D. 1 1.01 0.99 101.00 99.00 2.00
Fipronil N.D. 1 1.06 1.01 106.00 101.00 4.83
Flonicamid N.D. 1 1.05 0.955 105.00 95.50 9.48
Fludioxonil N.D. 1 1.01 0.989 101.00 98.90 2.10
Hexythiazox N.D. 1 0.763 0.737 76.30 73.70 3.47
Imazalil N.D. 1 1.55 1.23 155.00 123.00 23.02 HRQ
Imidacloprid N.D. 1 1.13 1 113.00 100.00 12.21
Kresoxim-methyl N.D. 1 1.56 1.33 156.00 133.00 15.92 HR
Malathion N.D. 1 1.17 1.19 117.00 119.00 1.69
Metalaxyl N.D. 1 1.29 1.23 129.00 123.00 4.76
Methiocarb N.D. 1 1.09 0.925 109.00 92.50 16.38
Methomyl N.D. 1 1.25 1.14 125.00 114.00 9.21
MGK-264 N.D. 1 0.905 0.759 90.50 75.90 17.55
Myclobutanil N.D. 1 1.32 1.29 132.00 129.00 2.30 HR
Naled (dibrom) N.D. 1 0.671 0.567 67.10 56.70 16.80 LR
Oxamyl N.D. 1 1.06 0.902 106.00 90.20 16.11
Paclobutrazol N.D. 1 1.69 1.48 169.00 148.00 13.25 HR
Parathion-methyl N.D. 1 1.11 0.896 111.00 89.60 21.34 Q
Permethrins N.D. 1 0.886 0.821 88.60 82.10 7.62
Phosmet N.D. 1 1.37 1.23 137.00 123.00 10.77 HR
Piperonyl butoxide N.D. 1 1.1 1.03 110.00 103.00 6.57
Prallethrin N.D. 1 1.43 1.43 143.00 143.00 0.00 HR
Propiconazole N.D. 1 1.12 1.07 112.00 107.00 4.57
Propoxur N.D. 1 1.07 0.945 107.00 94.50 12.41
Pyrethrin N.D. 0.65 0.788 0.735 121.23 113.08 6.96
Pyridaben N.D. 1 0.879 0.787 87.90 78.70 11.04
SpinosynA N.D. 0.84 1.23 1.08 146.43 128.57 12.99 HR
SpinosynD N.D. 0.16 0.232 0.227 145.00 141.88 2.18 HR
Spiromesifen N.D. 1 0.817 0.807 81.70 80.70 1.23
Spirotetramat N.D. 1 1.86 1.42 186.00 142.00 26.83 HRQ
Spiroxamine N.D. 1 1.42 1.26 142.00 126.00 11.94 HR
Tebuconazole N.D. 1 1.38 1.27 138.00 127.00 8.30 HR
Thiacloprid N.D. 1 1.16 1.02 116.00 102.00 12.84
Thiamethoxam N.D. 1 1.57 1.42 157.00 142.00 10.03 HR
Trifloxystrobin N.D. 1 1.12 0.996 112.00 99.60 11.72

N.D. = Not Detected

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 30%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (60-120%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 25 of 67

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Pesticide Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-004 Test Certificate #: 123371-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Northern Wreck Badder
License: 030-1009646F7F8
Type: AU Tincture
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A401030002C949000000017
Metrc Source Pkg#: 1A401030002C949000000016
Test Conditions

Prepsheet ID#: ORPS200403B
Scale: XS205-OR1
Temp: 21.7 °C
Baro PE: 1005 hPa
Analyst: JER
Technician: JER
Sample ID#: 123371

Lot #: Northern wreck badder 3/30/20 #1
Batch #: 123371
Batch Weight (g): 1640.4
Harvest/Process Date: 03/31/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 03/31/2020
Test Date: 04/06/2020
Sample #123371
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
Aldicarb 0.400 0.133 Pass/<LOD Abamectin**** 0.500 0.133 Pass/<LOD
Acephate 0.400 0.133 Pass/<LOD Acequinocyl 2.000 0.265 Pass/<LOD
Acetamiprid 0.200 0.133 Pass/<LOD Azoxystrobin 0.200 0.133 Pass/<LOD
Bifenazate 0.200 0.133 Pass/<LOD Bifenthrin 0.200 0.133 Pass/<LOD
Boscalid 0.400 0.133 Pass/<LOD Carbaryl 0.200 0.133 Pass/<LOD
Carbofuran 0.200 0.133 Pass/<LOD Chlorantraniliprole 0.200 0.133 Pass/<LOD
Chlorfenapyr 1.000 0.531 Pass/<LOD Chlorpyrifos 0.200 0.133 Pass/<LOD
Clofentezine 0.200 0.133 Pass/<LOD Cyfluthrin** 1.000 0.531 Pass/<LOD
Cypermethrin*** 1.000 0.531 Pass/<LOD Daminozide 1.000 0.133 Pass/<LOD
DDVP (Dichlorvos) 1.000 0.265 Pass/<LOD Diazinon 0.200 0.133 Pass/<LOD
Dimethoate 0.200 0.133 Pass/<LOD Ethoprophos 0.200 0.133 Pass/<LOD
Etofenprox 0.400 0.133 Pass/<LOD Etoxazole 0.200 0.133 Pass/<LOD
Fenoxycarb 0.200 0.133 Pass/<LOD Fenpyroximate 0.400 0.133 Pass/<LOD
Fipronil 0.400 0.133 Pass/<LOD Flonicamid 1.000 0.133 Pass/<LOD
Fludioxonil 0.400 0.133 Pass/<LOD Hexythiazox 1.000 0.133 Pass/<LOD
Imazalil 0.200 0.133 Pass/<LOD Imidacloprid 0.400 0.133 Pass/<LOD
Kresoxim Methyl 0.400 0.133 Pass/<LOD Malathion 0.200 0.133 Pass/<LOD
Metalaxyl 0.200 0.133 Pass/<LOD Methiocarb 0.200 0.133 Pass/<LOD
Methomyl 0.400 0.133 Pass/<LOD Methyl Parathion 0.200 0.133 Pass/<LOD
MGK-264‡ 0.200 0.133 Pass/<LOD Myclobutanil 0.000 0.133 Pass/<LOD
Naled 0.500 0.133 Pass/<LOD Oxamyl 1.000 0.133 Pass/<LOD
Paclobutrazol 0.400 0.133 Pass/<LOD Permethrins† 0.200 0.133 Pass/<LOD
Phosmet 0.200 0.133 Pass/<LOD Piperonyl Butoxide 2.000 0.133 Pass/<LOD
Prallethrin 0.200 0.133 Pass/<LOD Propiconazole 0.400 0.133 Pass/<LOD
Propoxur 0.200 0.133 Pass/<LOD Pyrethrins* 1.000 0.133 Pass/<LOD
Pyridaben 0.200 0.133 Pass/<LOD Spinosad***** 0.200 0.133 Pass/<LOD
Spiromesifen 0.200 0.133 Pass/<LOD Spirotetramat 0.200 0.133 Pass/<LOD
Spiroxamine‡ 0.400 0.133 Pass/<LOD Tebuconazole 0.400 0.133 Pass/<LOD
Thiacloprid 0.200 0.133 Pass/<LOD Thiamethoxam 0.200 0.133 Pass/<LOD
Trifloxystrobin 0.200 0.133 Pass/<LOD

* Pyrethrins are reported as the sum of Jasmolin I, Cinerin I, and Pyrethrin I
** Cyfluthrins are reported as the sum of isomers Cyfluthrin I, II, III, and IV
*** Cypermethrins are reported as the sum of isomers Cypermethrin I, II, III, and IV
**** Abamectin is reported as the sum of Avermectin B1a and Avermectin B1b
***** Spinosad is reported as the sum of Spinosyn A and Spinosyn D
† Permethrin and Prallethrin are reported as the sum of cis and trans isomers
‡ MGK-264 and Spiroximine are reported as the sum of isomers I and II
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 26 of 67

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Pesticide QC Report
Testing Accreditation #: 4092-004 Test Certificate #: 123371-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Northern Wreck Badder
License: 030-1009646F7F8
Type: AU Tincture
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A401030002C949000000017
Metrc Source Pkg#: 1A401030002C949000000016
Test Conditions

Prepsheet ID#: ORPS200403B
Scale: XS205-OR1
Temp: 21.7 °C
Baro PE: 1005 hPa
Analyst: JER
Technician: JER
Sample ID#: 123371

Lot #: Northern wreck badder 3/30/20 #1
Batch #: 123371
Batch Weight (g): 1640.4
Harvest/Process Date: 03/31/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 03/31/2020
Test Date: 04/06/2020
Sample #123371
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS recovery% MSD recovery% Relative Percent Difference (%) QC Flag
Acephate N.D. 1 1.04 0.908 104.00 90.80 13.55
Acequinocyl N.D. 1 0.518 0.531 51.80 53.10 2.48 LR
Acetamiprid N.D. 1 1.17 1.06 117.00 106.00 9.87
Aldicarb N.D. 1 0.871 0.817 87.10 81.70 6.40
Avermectin B1a N.D. 0.97 2.24 1.62 230.93 167.01 32.12 HRQ
Azoxystrobin N.D. 1 1.11 1.01 111.00 101.00 9.43
Bifenazate N.D. 1 1.08 0.909 108.00 90.90 17.19
Bifenthrin N.D. 1 0.805 0.829 80.50 82.90 2.94
Boscalid N.D. 1 0.87 0.998 87.00 99.80 13.70
Carbaryl N.D. 1 0.938 0.875 93.80 87.50 6.95
Carbofuran N.D. 1 1.09 1.01 109.00 101.00 7.62
Chlorantraniliprole N.D. 1 1.35 1.21 135.00 121.00 10.94 HR
Chlorfenapyr N.D. 1 0.82 0.878 82.00 87.80 6.83
Chlorpyriphos N.D. 1 0.91 0.886 91.00 88.60 2.67
Clofentezine N.D. 1 1.03 0.982 103.00 98.20 4.77
Cyfluthrin N.D. 1 1.1 1 110.00 100.00 9.52
Cypermethrin N.D. 1 1.16 1.06 116.00 106.00 9.01
Daminoside N.D. 1 1.16 1.12 116.00 112.00 3.51
Diazanon N.D. 1 1.12 1.06 112.00 106.00 5.50
Dichlorvos N.D. 1 0.806 0.644 80.60 64.40 22.34 LRQ
Dimethoate N.D. 1 1.06 0.908 106.00 90.80 15.45
Ethoprophos N.D. 1 0.879 0.8 87.90 80.00 9.41
Etofenprox N.D. 1 0.914 0.87 91.40 87.00 4.93
Etoxazole N.D. 1 1.09 0.966 109.00 96.60 12.06
Fenoxycarb N.D. 1 1.31 1.15 131.00 115.00 13.01 HR
Fenpyroximate N.D. 1 1.01 0.99 101.00 99.00 2.00
Fipronil N.D. 1 1.06 1.01 106.00 101.00 4.83
Flonicamid N.D. 1 1.05 0.955 105.00 95.50 9.48
Fludioxonil N.D. 1 1.01 0.989 101.00 98.90 2.10
Hexythiazox N.D. 1 0.763 0.737 76.30 73.70 3.47
Imazalil N.D. 1 1.55 1.23 155.00 123.00 23.02 HRQ
Imidacloprid N.D. 1 1.13 1 113.00 100.00 12.21
Kresoxim-methyl N.D. 1 1.56 1.33 156.00 133.00 15.92 HR
Malathion N.D. 1 1.17 1.19 117.00 119.00 1.69
Metalaxyl N.D. 1 1.29 1.23 129.00 123.00 4.76
Methiocarb N.D. 1 1.09 0.925 109.00 92.50 16.38
Methomyl N.D. 1 1.25 1.14 125.00 114.00 9.21
MGK-264 N.D. 1 0.905 0.759 90.50 75.90 17.55
Myclobutanil N.D. 1 1.32 1.29 132.00 129.00 2.30 HR
Naled (dibrom) N.D. 1 0.671 0.567 67.10 56.70 16.80 LR
Oxamyl N.D. 1 1.06 0.902 106.00 90.20 16.11
Paclobutrazol N.D. 1 1.69 1.48 169.00 148.00 13.25 HR
Parathion-methyl N.D. 1 1.11 0.896 111.00 89.60 21.34 Q
Permethrins N.D. 1 0.886 0.821 88.60 82.10 7.62
Phosmet N.D. 1 1.37 1.23 137.00 123.00 10.77 HR
Piperonyl butoxide N.D. 1 1.1 1.03 110.00 103.00 6.57
Prallethrin N.D. 1 1.43 1.43 143.00 143.00 0.00 HR
Propiconazole N.D. 1 1.12 1.07 112.00 107.00 4.57
Propoxur N.D. 1 1.07 0.945 107.00 94.50 12.41
Pyrethrin N.D. 0.65 0.788 0.735 121.23 113.08 6.96
Pyridaben N.D. 1 0.879 0.787 87.90 78.70 11.04
SpinosynA N.D. 0.84 1.23 1.08 146.43 128.57 12.99 HR
SpinosynD N.D. 0.16 0.232 0.227 145.00 141.88 2.18 HR
Spiromesifen N.D. 1 0.817 0.807 81.70 80.70 1.23
Spirotetramat N.D. 1 1.86 1.42 186.00 142.00 26.83 HRQ
Spiroxamine N.D. 1 1.42 1.26 142.00 126.00 11.94 HR
Tebuconazole N.D. 1 1.38 1.27 138.00 127.00 8.30 HR
Thiacloprid N.D. 1 1.16 1.02 116.00 102.00 12.84
Thiamethoxam N.D. 1 1.57 1.42 157.00 142.00 10.03 HR
Trifloxystrobin N.D. 1 1.12 0.996 112.00 99.60 11.72

N.D. = Not Detected

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 30%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (60-120%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 27 of 67

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Pesticide Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-004 Test Certificate #: 123371-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Northern Wreck Badder
License: 030-1009646F7F8
Type: AU Tincture
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A401030002C949000000017
Metrc Source Pkg#: 1A401030002C949000000016
Test Conditions

Prepsheet ID#: ORPS200403B
Scale: XS205-OR1
Temp: 21.7 °C
Baro PE: 1005 hPa
Analyst: JER
Technician: JER
Sample ID#: 123371

Lot #: Northern wreck badder 3/30/20 #1
Batch #: 123371
Batch Weight (g): 1640.4
Harvest/Process Date: 03/31/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 03/31/2020
Test Date: 04/06/2020
Sample #123371
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
Aldicarb 0.400 0.130 Pass/<LOD Abamectin**** 0.500 0.130 Pass/<LOD
Acephate 0.400 0.130 Pass/<LOD Acequinocyl 2.000 0.259 Pass/<LOD
Acetamiprid 0.200 0.130 Pass/<LOD Azoxystrobin 0.200 0.130 Pass/<LOD
Bifenazate 0.200 0.130 Pass/<LOD Bifenthrin 0.200 0.130 Pass/<LOD
Boscalid 0.400 0.130 Pass/<LOD Carbaryl 0.200 0.130 Pass/<LOD
Carbofuran 0.200 0.130 Pass/<LOD Chlorantraniliprole 0.200 0.130 Pass/<LOD
Chlorfenapyr 1.000 0.519 Pass/<LOD Chlorpyrifos 0.200 0.130 Pass/<LOD
Clofentezine 0.200 0.130 Pass/<LOD Cyfluthrin** 1.000 0.519 Pass/<LOD
Cypermethrin*** 1.000 0.519 Pass/<LOD Daminozide 1.000 0.130 Pass/<LOD
DDVP (Dichlorvos) 1.000 0.259 Pass/<LOD Diazinon 0.200 0.130 Pass/<LOD
Dimethoate 0.200 0.130 Pass/<LOD Ethoprophos 0.200 0.130 Pass/<LOD
Etofenprox 0.400 0.130 Pass/<LOD Etoxazole 0.200 0.130 Pass/<LOD
Fenoxycarb 0.200 0.130 Pass/<LOD Fenpyroximate 0.400 0.130 Pass/<LOD
Fipronil 0.400 0.130 Pass/<LOD Flonicamid 1.000 0.130 Pass/<LOD
Fludioxonil 0.400 0.130 Pass/<LOD Hexythiazox 1.000 0.130 Pass/<LOD
Imazalil 0.200 0.130 Pass/<LOD Imidacloprid 0.400 0.130 Pass/<LOD
Kresoxim Methyl 0.400 0.130 Pass/<LOD Malathion 0.200 0.130 Pass/<LOD
Metalaxyl 0.200 0.130 Pass/<LOD Methiocarb 0.200 0.130 Pass/<LOD
Methomyl 0.400 0.130 Pass/<LOD Methyl Parathion 0.200 0.130 Pass/<LOD
MGK-264‡ 0.200 0.130 Pass/<LOD Myclobutanil 0.000 0.130 Pass/<LOD
Naled 0.500 0.130 Pass/<LOD Oxamyl 1.000 0.130 Pass/<LOD
Paclobutrazol 0.400 0.130 Pass/<LOD Permethrins† 0.200 0.130 Pass/<LOD
Phosmet 0.200 0.130 Pass/<LOD Piperonyl Butoxide 2.000 0.130 Pass/<LOD
Prallethrin 0.200 0.130 Pass/<LOD Propiconazole 0.400 0.130 Pass/<LOD
Propoxur 0.200 0.130 Pass/<LOD Pyrethrins* 1.000 0.130 Pass/<LOD
Pyridaben 0.200 0.130 Pass/<LOD Spinosad***** 0.200 0.130 Pass/<LOD
Spiromesifen 0.200 0.130 Pass/<LOD Spirotetramat 0.200 0.130 Pass/<LOD
Spiroxamine‡ 0.400 0.130 Pass/<LOD Tebuconazole 0.400 0.130 Pass/<LOD
Thiacloprid 0.200 0.130 Pass/<LOD Thiamethoxam 0.200 0.130 Pass/<LOD
Trifloxystrobin 0.200 0.130 Pass/<LOD

* Pyrethrins are reported as the sum of Jasmolin I, Cinerin I, and Pyrethrin I
** Cyfluthrins are reported as the sum of isomers Cyfluthrin I, II, III, and IV
*** Cypermethrins are reported as the sum of isomers Cypermethrin I, II, III, and IV
**** Abamectin is reported as the sum of Avermectin B1a and Avermectin B1b
***** Spinosad is reported as the sum of Spinosyn A and Spinosyn D
† Permethrin and Prallethrin are reported as the sum of cis and trans isomers
‡ MGK-264 and Spiroximine are reported as the sum of isomers I and II
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 28 of 67

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Pesticide QC Report
Testing Accreditation #: 4092-004 Test Certificate #: 123371-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Northern Wreck Badder
License: 030-1009646F7F8
Type: AU Tincture
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A401030002C949000000017
Metrc Source Pkg#: 1A401030002C949000000016
Test Conditions

Prepsheet ID#: ORPS200403B
Scale: XS205-OR1
Temp: 21.7 °C
Baro PE: 1005 hPa
Analyst: JER
Technician: JER
Sample ID#: 123371

Lot #: Northern wreck badder 3/30/20 #1
Batch #: 123371
Batch Weight (g): 1640.4
Harvest/Process Date: 03/31/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 03/31/2020
Test Date: 04/06/2020
Sample #123371
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS recovery% MSD recovery% Relative Percent Difference (%) QC Flag
Acephate N.D. 1 1.04 0.908 104.00 90.80 13.55
Acequinocyl N.D. 1 0.518 0.531 51.80 53.10 2.48 LR
Acetamiprid N.D. 1 1.17 1.06 117.00 106.00 9.87
Aldicarb N.D. 1 0.871 0.817 87.10 81.70 6.40
Avermectin B1a N.D. 0.97 2.24 1.62 230.93 167.01 32.12 HRQ
Azoxystrobin N.D. 1 1.11 1.01 111.00 101.00 9.43
Bifenazate N.D. 1 1.08 0.909 108.00 90.90 17.19
Bifenthrin N.D. 1 0.805 0.829 80.50 82.90 2.94
Boscalid N.D. 1 0.87 0.998 87.00 99.80 13.70
Carbaryl N.D. 1 0.938 0.875 93.80 87.50 6.95
Carbofuran N.D. 1 1.09 1.01 109.00 101.00 7.62
Chlorantraniliprole N.D. 1 1.35 1.21 135.00 121.00 10.94 HR
Chlorfenapyr N.D. 1 0.82 0.878 82.00 87.80 6.83
Chlorpyriphos N.D. 1 0.91 0.886 91.00 88.60 2.67
Clofentezine N.D. 1 1.03 0.982 103.00 98.20 4.77
Cyfluthrin N.D. 1 1.1 1 110.00 100.00 9.52
Cypermethrin N.D. 1 1.16 1.06 116.00 106.00 9.01
Daminoside N.D. 1 1.16 1.12 116.00 112.00 3.51
Diazanon N.D. 1 1.12 1.06 112.00 106.00 5.50
Dichlorvos N.D. 1 0.806 0.644 80.60 64.40 22.34 LRQ
Dimethoate N.D. 1 1.06 0.908 106.00 90.80 15.45
Ethoprophos N.D. 1 0.879 0.8 87.90 80.00 9.41
Etofenprox N.D. 1 0.914 0.87 91.40 87.00 4.93
Etoxazole N.D. 1 1.09 0.966 109.00 96.60 12.06
Fenoxycarb N.D. 1 1.31 1.15 131.00 115.00 13.01 HR
Fenpyroximate N.D. 1 1.01 0.99 101.00 99.00 2.00
Fipronil N.D. 1 1.06 1.01 106.00 101.00 4.83
Flonicamid N.D. 1 1.05 0.955 105.00 95.50 9.48
Fludioxonil N.D. 1 1.01 0.989 101.00 98.90 2.10
Hexythiazox N.D. 1 0.763 0.737 76.30 73.70 3.47
Imazalil N.D. 1 1.55 1.23 155.00 123.00 23.02 HRQ
Imidacloprid N.D. 1 1.13 1 113.00 100.00 12.21
Kresoxim-methyl N.D. 1 1.56 1.33 156.00 133.00 15.92 HR
Malathion N.D. 1 1.17 1.19 117.00 119.00 1.69
Metalaxyl N.D. 1 1.29 1.23 129.00 123.00 4.76
Methiocarb N.D. 1 1.09 0.925 109.00 92.50 16.38
Methomyl N.D. 1 1.25 1.14 125.00 114.00 9.21
MGK-264 N.D. 1 0.905 0.759 90.50 75.90 17.55
Myclobutanil N.D. 1 1.32 1.29 132.00 129.00 2.30 HR
Naled (dibrom) N.D. 1 0.671 0.567 67.10 56.70 16.80 LR
Oxamyl N.D. 1 1.06 0.902 106.00 90.20 16.11
Paclobutrazol N.D. 1 1.69 1.48 169.00 148.00 13.25 HR
Parathion-methyl N.D. 1 1.11 0.896 111.00 89.60 21.34 Q
Permethrins N.D. 1 0.886 0.821 88.60 82.10 7.62
Phosmet N.D. 1 1.37 1.23 137.00 123.00 10.77 HR
Piperonyl butoxide N.D. 1 1.1 1.03 110.00 103.00 6.57
Prallethrin N.D. 1 1.43 1.43 143.00 143.00 0.00 HR
Propiconazole N.D. 1 1.12 1.07 112.00 107.00 4.57
Propoxur N.D. 1 1.07 0.945 107.00 94.50 12.41
Pyrethrin N.D. 0.65 0.788 0.735 121.23 113.08 6.96
Pyridaben N.D. 1 0.879 0.787 87.90 78.70 11.04
SpinosynA N.D. 0.84 1.23 1.08 146.43 128.57 12.99 HR
SpinosynD N.D. 0.16 0.232 0.227 145.00 141.88 2.18 HR
Spiromesifen N.D. 1 0.817 0.807 81.70 80.70 1.23
Spirotetramat N.D. 1 1.86 1.42 186.00 142.00 26.83 HRQ
Spiroxamine N.D. 1 1.42 1.26 142.00 126.00 11.94 HR
Tebuconazole N.D. 1 1.38 1.27 138.00 127.00 8.30 HR
Thiacloprid N.D. 1 1.16 1.02 116.00 102.00 12.84
Thiamethoxam N.D. 1 1.57 1.42 157.00 142.00 10.03 HR
Trifloxystrobin N.D. 1 1.12 0.996 112.00 99.60 11.72

N.D. = Not Detected

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 30%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (60-120%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 29 of 67

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Pesticide Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-004 Test Certificate #: 123371-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Northern Wreck Badder
License: 030-1009646F7F8
Type: AU Tincture
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A401030002C949000000017
Metrc Source Pkg#: 1A401030002C949000000016
Test Conditions

Prepsheet ID#: ORPS200403B
Scale: XS205-OR1
Temp: 21.7 °C
Baro PE: 1005 hPa
Analyst: JER
Technician: JER
Sample ID#: 123371

Lot #: Northern wreck badder 3/30/20 #1
Batch #: 123371
Batch Weight (g): 1640.4
Harvest/Process Date: 03/31/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 03/31/2020
Test Date: 04/06/2020
Sample #123371
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
Aldicarb 0.400 0.128 Pass/<LOD Abamectin**** 0.500 0.128 Pass/<LOD
Acephate 0.400 0.128 Pass/<LOD Acequinocyl 2.000 0.256 Pass/<LOD
Acetamiprid 0.200 0.128 Pass/<LOD Azoxystrobin 0.200 0.128 Pass/<LOD
Bifenazate 0.200 0.128 Pass/<LOD Bifenthrin 0.200 0.128 Pass/<LOD
Boscalid 0.400 0.128 Pass/<LOD Carbaryl 0.200 0.128 Pass/<LOD
Carbofuran 0.200 0.128 Pass/<LOD Chlorantraniliprole 0.200 0.128 Pass/<LOD
Chlorfenapyr 1.000 0.512 Pass/<LOD Chlorpyrifos 0.200 0.128 Pass/<LOD
Clofentezine 0.200 0.128 Pass/<LOD Cyfluthrin** 1.000 0.512 Pass/<LOD
Cypermethrin*** 1.000 0.512 Pass/<LOD Daminozide 1.000 0.128 Pass/<LOD
DDVP (Dichlorvos) 1.000 0.256 Pass/<LOD Diazinon 0.200 0.128 Pass/<LOD
Dimethoate 0.200 0.128 Pass/<LOD Ethoprophos 0.200 0.128 Pass/<LOD
Etofenprox 0.400 0.128 Pass/<LOD Etoxazole 0.200 0.128 Pass/<LOD
Fenoxycarb 0.200 0.128 Pass/<LOD Fenpyroximate 0.400 0.128 Pass/<LOD
Fipronil 0.400 0.128 Pass/<LOD Flonicamid 1.000 0.128 Pass/<LOD
Fludioxonil 0.400 0.128 Pass/<LOD Hexythiazox 1.000 0.128 Pass/<LOD
Imazalil 0.200 0.128 Pass/<LOD Imidacloprid 0.400 0.128 Pass/<LOD
Kresoxim Methyl 0.400 0.128 Pass/<LOD Malathion 0.200 0.128 Pass/<LOD
Metalaxyl 0.200 0.128 Pass/<LOD Methiocarb 0.200 0.128 Pass/<LOD
Methomyl 0.400 0.128 Pass/<LOD Methyl Parathion 0.200 0.128 Pass/<LOD
MGK-264‡ 0.200 0.128 Pass/<LOD Myclobutanil 0.000 0.128 Pass/<LOD
Naled 0.500 0.128 Pass/<LOD Oxamyl 1.000 0.128 Pass/<LOD
Paclobutrazol 0.400 0.128 Pass/<LOD Permethrins† 0.200 0.128 Pass/<LOD
Phosmet 0.200 0.128 Pass/<LOD Piperonyl Butoxide 2.000 0.128 Pass/<LOD
Prallethrin 0.200 0.128 Pass/<LOD Propiconazole 0.400 0.128 Pass/<LOD
Propoxur 0.200 0.128 Pass/<LOD Pyrethrins* 1.000 0.128 Pass/<LOD
Pyridaben 0.200 0.128 Pass/<LOD Spinosad***** 0.200 0.128 Pass/<LOD
Spiromesifen 0.200 0.128 Pass/<LOD Spirotetramat 0.200 0.128 Pass/<LOD
Spiroxamine‡ 0.400 0.128 Pass/<LOD Tebuconazole 0.400 0.128 Pass/<LOD
Thiacloprid 0.200 0.128 Pass/<LOD Thiamethoxam 0.200 0.128 Pass/<LOD
Trifloxystrobin 0.200 0.128 Pass/<LOD

* Pyrethrins are reported as the sum of Jasmolin I, Cinerin I, and Pyrethrin I
** Cyfluthrins are reported as the sum of isomers Cyfluthrin I, II, III, and IV
*** Cypermethrins are reported as the sum of isomers Cypermethrin I, II, III, and IV
**** Abamectin is reported as the sum of Avermectin B1a and Avermectin B1b
***** Spinosad is reported as the sum of Spinosyn A and Spinosyn D
† Permethrin and Prallethrin are reported as the sum of cis and trans isomers
‡ MGK-264 and Spiroximine are reported as the sum of isomers I and II
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 30 of 67

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Pesticide QC Report
Testing Accreditation #: 4092-004 Test Certificate #: 123371-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Northern Wreck Badder
License: 030-1009646F7F8
Type: AU Tincture
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A401030002C949000000017
Metrc Source Pkg#: 1A401030002C949000000016
Test Conditions

Prepsheet ID#: ORPS200403B
Scale: XS205-OR1
Temp: 21.7 °C
Baro PE: 1005 hPa
Analyst: JER
Technician: JER
Sample ID#: 123371

Lot #: Northern wreck badder 3/30/20 #1
Batch #: 123371
Batch Weight (g): 1640.4
Harvest/Process Date: 03/31/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 03/31/2020
Test Date: 04/06/2020
Sample #123371
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS recovery% MSD recovery% Relative Percent Difference (%) QC Flag
Acephate N.D. 1 1.04 0.908 104.00 90.80 13.55
Acequinocyl N.D. 1 0.518 0.531 51.80 53.10 2.48 LR
Acetamiprid N.D. 1 1.17 1.06 117.00 106.00 9.87
Aldicarb N.D. 1 0.871 0.817 87.10 81.70 6.40
Avermectin B1a N.D. 0.97 2.24 1.62 230.93 167.01 32.12 HRQ
Azoxystrobin N.D. 1 1.11 1.01 111.00 101.00 9.43
Bifenazate N.D. 1 1.08 0.909 108.00 90.90 17.19
Bifenthrin N.D. 1 0.805 0.829 80.50 82.90 2.94
Boscalid N.D. 1 0.87 0.998 87.00 99.80 13.70
Carbaryl N.D. 1 0.938 0.875 93.80 87.50 6.95
Carbofuran N.D. 1 1.09 1.01 109.00 101.00 7.62
Chlorantraniliprole N.D. 1 1.35 1.21 135.00 121.00 10.94 HR
Chlorfenapyr N.D. 1 0.82 0.878 82.00 87.80 6.83
Chlorpyriphos N.D. 1 0.91 0.886 91.00 88.60 2.67
Clofentezine N.D. 1 1.03 0.982 103.00 98.20 4.77
Cyfluthrin N.D. 1 1.1 1 110.00 100.00 9.52
Cypermethrin N.D. 1 1.16 1.06 116.00 106.00 9.01
Daminoside N.D. 1 1.16 1.12 116.00 112.00 3.51
Diazanon N.D. 1 1.12 1.06 112.00 106.00 5.50
Dichlorvos N.D. 1 0.806 0.644 80.60 64.40 22.34 LRQ
Dimethoate N.D. 1 1.06 0.908 106.00 90.80 15.45
Ethoprophos N.D. 1 0.879 0.8 87.90 80.00 9.41
Etofenprox N.D. 1 0.914 0.87 91.40 87.00 4.93
Etoxazole N.D. 1 1.09 0.966 109.00 96.60 12.06
Fenoxycarb N.D. 1 1.31 1.15 131.00 115.00 13.01 HR
Fenpyroximate N.D. 1 1.01 0.99 101.00 99.00 2.00
Fipronil N.D. 1 1.06 1.01 106.00 101.00 4.83
Flonicamid N.D. 1 1.05 0.955 105.00 95.50 9.48
Fludioxonil N.D. 1 1.01 0.989 101.00 98.90 2.10
Hexythiazox N.D. 1 0.763 0.737 76.30 73.70 3.47
Imazalil N.D. 1 1.55 1.23 155.00 123.00 23.02 HRQ
Imidacloprid N.D. 1 1.13 1 113.00 100.00 12.21
Kresoxim-methyl N.D. 1 1.56 1.33 156.00 133.00 15.92 HR
Malathion N.D. 1 1.17 1.19 117.00 119.00 1.69
Metalaxyl N.D. 1 1.29 1.23 129.00 123.00 4.76
Methiocarb N.D. 1 1.09 0.925 109.00 92.50 16.38
Methomyl N.D. 1 1.25 1.14 125.00 114.00 9.21
MGK-264 N.D. 1 0.905 0.759 90.50 75.90 17.55
Myclobutanil N.D. 1 1.32 1.29 132.00 129.00 2.30 HR
Naled (dibrom) N.D. 1 0.671 0.567 67.10 56.70 16.80 LR
Oxamyl N.D. 1 1.06 0.902 106.00 90.20 16.11
Paclobutrazol N.D. 1 1.69 1.48 169.00 148.00 13.25 HR
Parathion-methyl N.D. 1 1.11 0.896 111.00 89.60 21.34 Q
Permethrins N.D. 1 0.886 0.821 88.60 82.10 7.62
Phosmet N.D. 1 1.37 1.23 137.00 123.00 10.77 HR
Piperonyl butoxide N.D. 1 1.1 1.03 110.00 103.00 6.57
Prallethrin N.D. 1 1.43 1.43 143.00 143.00 0.00 HR
Propiconazole N.D. 1 1.12 1.07 112.00 107.00 4.57
Propoxur N.D. 1 1.07 0.945 107.00 94.50 12.41
Pyrethrin N.D. 0.65 0.788 0.735 121.23 113.08 6.96
Pyridaben N.D. 1 0.879 0.787 87.90 78.70 11.04
SpinosynA N.D. 0.84 1.23 1.08 146.43 128.57 12.99 HR
SpinosynD N.D. 0.16 0.232 0.227 145.00 141.88 2.18 HR
Spiromesifen N.D. 1 0.817 0.807 81.70 80.70 1.23
Spirotetramat N.D. 1 1.86 1.42 186.00 142.00 26.83 HRQ
Spiroxamine N.D. 1 1.42 1.26 142.00 126.00 11.94 HR
Tebuconazole N.D. 1 1.38 1.27 138.00 127.00 8.30 HR
Thiacloprid N.D. 1 1.16 1.02 116.00 102.00 12.84
Thiamethoxam N.D. 1 1.57 1.42 157.00 142.00 10.03 HR
Trifloxystrobin N.D. 1 1.12 0.996 112.00 99.60 11.72

N.D. = Not Detected

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 30%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (60-120%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 31 of 67

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Pesticide Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-004 Test Certificate #: 123371-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Northern Wreck Badder
License: 030-1009646F7F8
Type: AU Tincture
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A401030002C949000000017
Metrc Source Pkg#: 1A401030002C949000000016
Test Conditions

Prepsheet ID#: ORPS200403B
Scale: XS205-OR1
Temp: 21.7 °C
Baro PE: 1005 hPa
Analyst: JER
Technician: JER
Sample ID#: 123371

Lot #: Northern wreck badder 3/30/20 #1
Batch #: 123371
Batch Weight (g): 1640.4
Harvest/Process Date: 03/31/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 03/31/2020
Test Date: 04/06/2020
Sample #123371
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
Aldicarb 0.400 0.133 Pass/<LOD Abamectin**** 0.500 0.133 Pass/<LOD
Acephate 0.400 0.133 Pass/<LOD Acequinocyl 2.000 0.267 Pass/<LOD
Acetamiprid 0.200 0.133 Pass/<LOD Azoxystrobin 0.200 0.133 Pass/<LOD
Bifenazate 0.200 0.133 Pass/<LOD Bifenthrin 0.200 0.133 Pass/<LOD
Boscalid 0.400 0.133 Pass/<LOD Carbaryl 0.200 0.133 Pass/<LOD
Carbofuran 0.200 0.133 Pass/<LOD Chlorantraniliprole 0.200 0.133 Pass/<LOD
Chlorfenapyr 1.000 0.533 Pass/<LOD Chlorpyrifos 0.200 0.133 Pass/<LOD
Clofentezine 0.200 0.133 Pass/<LOD Cyfluthrin** 1.000 0.533 Pass/<LOD
Cypermethrin*** 1.000 0.533 Pass/<LOD Daminozide 1.000 0.133 Pass/<LOD
DDVP (Dichlorvos) 1.000 0.267 Pass/<LOD Diazinon 0.200 0.133 Pass/<LOD
Dimethoate 0.200 0.133 Pass/<LOD Ethoprophos 0.200 0.133 Pass/<LOD
Etofenprox 0.400 0.133 Pass/<LOD Etoxazole 0.200 0.133 Pass/<LOD
Fenoxycarb 0.200 0.133 Pass/<LOD Fenpyroximate 0.400 0.133 Pass/<LOD
Fipronil 0.400 0.133 Pass/<LOD Flonicamid 1.000 0.133 Pass/<LOD
Fludioxonil 0.400 0.133 Pass/<LOD Hexythiazox 1.000 0.133 Pass/<LOD
Imazalil 0.200 0.133 Pass/<LOD Imidacloprid 0.400 0.133 Pass/<LOD
Kresoxim Methyl 0.400 0.133 Pass/<LOD Malathion 0.200 0.133 Pass/<LOD
Metalaxyl 0.200 0.133 Pass/<LOD Methiocarb 0.200 0.133 Pass/<LOD
Methomyl 0.400 0.133 Pass/<LOD Methyl Parathion 0.200 0.133 Pass/<LOD
MGK-264‡ 0.200 0.133 Pass/<LOD Myclobutanil 0.000 0.133 Pass/<LOD
Naled 0.500 0.133 Pass/<LOD Oxamyl 1.000 0.133 Pass/<LOD
Paclobutrazol 0.400 0.133 Pass/<LOD Permethrins† 0.200 0.133 Pass/<LOD
Phosmet 0.200 0.133 Pass/<LOD Piperonyl Butoxide 2.000 0.133 Pass/<LOD
Prallethrin 0.200 0.133 Pass/<LOD Propiconazole 0.400 0.133 Pass/<LOD
Propoxur 0.200 0.133 Pass/<LOD Pyrethrins* 1.000 0.133 Pass/<LOD
Pyridaben 0.200 0.133 Pass/<LOD Spinosad***** 0.200 0.133 Pass/<LOD
Spiromesifen 0.200 0.133 Pass/<LOD Spirotetramat 0.200 0.133 Pass/<LOD
Spiroxamine‡ 0.400 0.133 Pass/<LOD Tebuconazole 0.400 0.133 Pass/<LOD
Thiacloprid 0.200 0.133 Pass/<LOD Thiamethoxam 0.200 0.133 Pass/<LOD
Trifloxystrobin 0.200 0.133 Pass/<LOD

* Pyrethrins are reported as the sum of Jasmolin I, Cinerin I, and Pyrethrin I
** Cyfluthrins are reported as the sum of isomers Cyfluthrin I, II, III, and IV
*** Cypermethrins are reported as the sum of isomers Cypermethrin I, II, III, and IV
**** Abamectin is reported as the sum of Avermectin B1a and Avermectin B1b
***** Spinosad is reported as the sum of Spinosyn A and Spinosyn D
† Permethrin and Prallethrin are reported as the sum of cis and trans isomers
‡ MGK-264 and Spiroximine are reported as the sum of isomers I and II
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 32 of 67

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Pesticide QC Report
Testing Accreditation #: 4092-004 Test Certificate #: 123371-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Northern Wreck Badder
License: 030-1009646F7F8
Type: AU Tincture
Method: FE-52 (EN 15662 & AOAC 2007.01)
Metrc Test Pkg#: 1A401030002C949000000017
Metrc Source Pkg#: 1A401030002C949000000016
Test Conditions

Prepsheet ID#: ORPS200403B
Scale: XS205-OR1
Temp: 21.7 °C
Baro PE: 1005 hPa
Analyst: JER
Technician: JER
Sample ID#: 123371

Lot #: Northern wreck badder 3/30/20 #1
Batch #: 123371
Batch Weight (g): 1640.4
Harvest/Process Date: 03/31/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 03/31/2020
Test Date: 04/06/2020
Sample #123371
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS recovery% MSD recovery% Relative Percent Difference (%) QC Flag
Acephate N.D. 1 1.04 0.908 104.00 90.80 13.55
Acequinocyl N.D. 1 0.518 0.531 51.80 53.10 2.48 LR
Acetamiprid N.D. 1 1.17 1.06 117.00 106.00 9.87
Aldicarb N.D. 1 0.871 0.817 87.10 81.70 6.40
Avermectin B1a N.D. 0.97 2.24 1.62 230.93 167.01 32.12 HRQ
Azoxystrobin N.D. 1 1.11 1.01 111.00 101.00 9.43
Bifenazate N.D. 1 1.08 0.909 108.00 90.90 17.19
Bifenthrin N.D. 1 0.805 0.829 80.50 82.90 2.94
Boscalid N.D. 1 0.87 0.998 87.00 99.80 13.70
Carbaryl N.D. 1 0.938 0.875 93.80 87.50 6.95
Carbofuran N.D. 1 1.09 1.01 109.00 101.00 7.62
Chlorantraniliprole N.D. 1 1.35 1.21 135.00 121.00 10.94 HR
Chlorfenapyr N.D. 1 0.82 0.878 82.00 87.80 6.83
Chlorpyriphos N.D. 1 0.91 0.886 91.00 88.60 2.67
Clofentezine N.D. 1 1.03 0.982 103.00 98.20 4.77
Cyfluthrin N.D. 1 1.1 1 110.00 100.00 9.52
Cypermethrin N.D. 1 1.16 1.06 116.00 106.00 9.01
Daminoside N.D. 1 1.16 1.12 116.00 112.00 3.51
Diazanon N.D. 1 1.12 1.06 112.00 106.00 5.50
Dichlorvos N.D. 1 0.806 0.644 80.60 64.40 22.34 LRQ
Dimethoate N.D. 1 1.06 0.908 106.00 90.80 15.45
Ethoprophos N.D. 1 0.879 0.8 87.90 80.00 9.41
Etofenprox N.D. 1 0.914 0.87 91.40 87.00 4.93
Etoxazole N.D. 1 1.09 0.966 109.00 96.60 12.06
Fenoxycarb N.D. 1 1.31 1.15 131.00 115.00 13.01 HR
Fenpyroximate N.D. 1 1.01 0.99 101.00 99.00 2.00
Fipronil N.D. 1 1.06 1.01 106.00 101.00 4.83
Flonicamid N.D. 1 1.05 0.955 105.00 95.50 9.48
Fludioxonil N.D. 1 1.01 0.989 101.00 98.90 2.10
Hexythiazox N.D. 1 0.763 0.737 76.30 73.70 3.47
Imazalil N.D. 1 1.55 1.23 155.00 123.00 23.02 HRQ
Imidacloprid N.D. 1 1.13 1 113.00 100.00 12.21
Kresoxim-methyl N.D. 1 1.56 1.33 156.00 133.00 15.92 HR
Malathion N.D. 1 1.17 1.19 117.00 119.00 1.69
Metalaxyl N.D. 1 1.29 1.23 129.00 123.00 4.76
Methiocarb N.D. 1 1.09 0.925 109.00 92.50 16.38
Methomyl N.D. 1 1.25 1.14 125.00 114.00 9.21
MGK-264 N.D. 1 0.905 0.759 90.50 75.90 17.55
Myclobutanil N.D. 1 1.32 1.29 132.00 129.00 2.30 HR
Naled (dibrom) N.D. 1 0.671 0.567 67.10 56.70 16.80 LR
Oxamyl N.D. 1 1.06 0.902 106.00 90.20 16.11
Paclobutrazol N.D. 1 1.69 1.48 169.00 148.00 13.25 HR
Parathion-methyl N.D. 1 1.11 0.896 111.00 89.60 21.34 Q
Permethrins N.D. 1 0.886 0.821 88.60 82.10 7.62
Phosmet N.D. 1 1.37 1.23 137.00 123.00 10.77 HR
Piperonyl butoxide N.D. 1 1.1 1.03 110.00 103.00 6.57
Prallethrin N.D. 1 1.43 1.43 143.00 143.00 0.00 HR
Propiconazole N.D. 1 1.12 1.07 112.00 107.00 4.57
Propoxur N.D. 1 1.07 0.945 107.00 94.50 12.41
Pyrethrin N.D. 0.65 0.788 0.735 121.23 113.08 6.96
Pyridaben N.D. 1 0.879 0.787 87.90 78.70 11.04
SpinosynA N.D. 0.84 1.23 1.08 146.43 128.57 12.99 HR
SpinosynD N.D. 0.16 0.232 0.227 145.00 141.88 2.18 HR
Spiromesifen N.D. 1 0.817 0.807 81.70 80.70 1.23
Spirotetramat N.D. 1 1.86 1.42 186.00 142.00 26.83 HRQ
Spiroxamine N.D. 1 1.42 1.26 142.00 126.00 11.94 HR
Tebuconazole N.D. 1 1.38 1.27 138.00 127.00 8.30 HR
Thiacloprid N.D. 1 1.16 1.02 116.00 102.00 12.84
Thiamethoxam N.D. 1 1.57 1.42 157.00 142.00 10.03 HR
Trifloxystrobin N.D. 1 1.12 0.996 112.00 99.60 11.72

N.D. = Not Detected

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 30%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (60-120%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 33 of 67

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-004 Test Certificate #: 123371-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Northern Wreck Badder
License: 030-1009646F7F8
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A401030002C949000000017
Metrc Source Pkg#: 1A401030002C949000000016
Test Conditions

Prepsheet ID#: ORHS200402b
Scale: XS205-OR1
Temp: 22.1 °C
Baro PE: 1012 hPa
Analyst: HRM
Technician: HRM
Sample ID#: 123371

Lot #: Northern wreck badder 3/30/20 #1
Batch #: 123371
Batch Weight (g): 1640.4
Harvest/Process Date: 03/31/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 03/31/2020
Test Date: 04/02/2020
Sample #123371
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
1,2-Dichloroethane 2 1 Not Tested 1,2-Dimethoxyethane 100 5 Pass/<LOD
1,4-dioxane 380 200 Pass/<LOD 1-Butanol 5,000 100 Pass/<LOD
1-Pentanol 5,000 100 Pass/<LOD 1-Propanol 5,000 100 Pass/<LOD
2,2-Dimethylpropane (Neopentane) 5,000 100 Pass/<LOD 2,2-Dimethylbutane (Hexanes) 290 100 Pass/<LOD
2,3-Dimethylbutane (Hexanes) 290 100 Pass/<LOD 2-Butanol 5,000 100 Pass/<LOD
2-Butanone (MEK) 5,000 50 Pass/<LOD 2-Ethoxyethanol 160 40 Pass/<LOD
2-Methylbutane (Isopentane) 5,000 50 Pass/<LOD 2-Methylpentane (Hexanes) 290 50 Pass/<LOD
2-Methylpropane (Isobutane) 5,000 100 Pass/<LOD 2-propanol (Isopropyl Alcohol) 5,000 50 Pass/66
2-Propanone (Acetone) 5,000 50 Pass/51 3-Methylpentane (Hexanes) 290 50 Pass/<LOD
Acetonitrile 410 100 Pass/<LOD Benzene 2 1 Pass/<LOD
Butane 5,000 100 Pass/171 Chloroform 2 1 Pass/<LOD
Cumene 70 50 Pass/<LOD Cyclohexane 3,880 1,000 Pass/<LOD
Dichloromethane 600 50 Pass/<LOD Dimethylsulfoxide (DMSO) 5,000 500 Pass/<LOD
Ethanol 5,000 500 Pass/<LOD Ethyl acetate 5,000 50 Pass/<LOD
Ethyl ether 5,000 500 Pass/<LOD Ethylene glycol 620 310 Pass/<LOD
Ethylene oxide 50 50 Pass/<LOD Heptane 5,000 50 Pass/<LOD
Hexane 290 290 Pass/<LOD Isopropyl acetate 5,000 50 Pass/<LOD
Methanol 3,000 500 Pass/<LOD Naptha 400 100 Not Tested
N,N-Dimethylacetamide 1,090 100 Pass/<LOD N,N-Dimethylformamide (DMF) 880 500 Pass/<LOD
Pentane 5,000 50 Pass/<LOD Petroleum Ether 400 100 Not Tested
Propane 5,000 100 Pass/<LOD Pyridine 200 10 Pass/<LOD
Sulfolane 160 200 Pass/<LOD Tetrahydrofuran (THF) 720 200 Pass/<LOD
Toluene 890 50 Pass/<LOD Trichloroethylene 25 5 Not Tested
Xylenes* 2,170 50 Pass/<LOD

Total Butanes = 171 ug/g (PASS); Total Pentanes = 0 ug/g (PASS); Total Hexanes = 0 ug/g (PASS)

* Xylenes are reported as the sum of o-xylene, m-xylene, p-xylene, and ethylbenzene
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 34 of 67

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents QC Report
Testing Accreditation #: 4092-004 Test Certificate #: 123371-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Northern Wreck Badder
License: 030-1009646F7F8
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A401030002C949000000017
Metrc Source Pkg#: 1A401030002C949000000016
Test Conditions

Prepsheet ID#: ORHS200402b
Scale: XS205-OR1
Temp: 22.1 °C
Baro PE: 1012 hPa
Analyst: HRM
Technician: HRM
Sample ID#: 123371

Lot #: Northern wreck badder 3/30/20 #1
Batch #: 123371
Batch Weight (g): 1640.4
Harvest/Process Date: 03/31/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 03/31/2020
Test Date: 04/02/2020
Sample #123371
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS Recovery (%) MSD Recovery (%) Relative Percent Difference (%) QC Flag
1,2-Dichloroethane N.D. 0 0 0 nan nan
n-Propane N.D. 250 64 64 25.60 25.60 0.00 LR
Isobutane N.D. 250 101 97 40.40 38.80 4.04 LR
Methanol N.D. 250 177 160 70.80 64.00 10.09 LR
n-Butane N.D. 250 117 119 46.80 47.60 1.69 LR
2,2-Dimethylpropane N.D. 250 126 127 50.40 50.80 0.79 LR
Ethanol N.D. 250 187 185 74.80 74.00 1.08
Isopentane N.D. 250 144 141 57.60 56.40 2.11 LR
Acetonitrile N.D. 250 169 154 67.60 61.60 9.29 LR
Diethyl ether N.D. 250 183 178 73.20 71.20 2.77
2-propanone N.D. 250 207 204 82.80 81.60 1.46
2-propanol N.D. 250 334 341 133.60 136.40 2.07 HR
n-Pentane N.D. 250 153 83 61.20 33.20 59.32 LRQ
2,2-Dimethylbutane N.D. 250 170 171 68.00 68.40 0.59 LR
2,3-Dimethylbutane N.D. 250 158 151 63.20 60.40 4.53 LR
Methylene chloride N.D. 250 190 194 76.00 77.60 2.08
2-Methylpentane N.D. 250 170 171 68.00 68.40 0.59 LR
3-Methylpentane N.D. 250 178 172 71.20 68.80 3.43 LR
2-Butanol N.D. 250 208 208 83.20 83.20 0.00
n-Hexane N.D. 250 180 177 72.00 70.80 1.68
Ethyl acetate N.D. 250 196 199 78.40 79.60 1.52
Tetrahydrofuran N.D. 250 188 183 0.00 0.00 0.00
Trichloroethylene N.D. 0 0 0 nan nan
Isopropyl acetate N.D. 250 196 199 0.00 0.00 0.00
Benzene N.D. 250 196 194 78.40 77.60 1.03
Chloroform N.D. 0 0 0 nan nan
Cyclohexane N.D. 250 186 185 74.40 74.00 0.54
Ethylene glycol N.D. 250 156 197 62.40 78.80 23.23 LRQ
Heptane N.D. 250 159 160 63.60 64.00 0.63 LR
2-Ethoxyethanol N.D. 250 167 190 66.80 76.00 12.89 LR
1,4-Dioxane N.D. 250 199 200 79.60 80.00 0.50
Pyridine N.D. 0 0 0 0.00 0.00 0.00
Toluene N.D. 250 204 198 81.60 79.20 2.99
Chlorobenzene N.D. 0 0 0 0.00 0.00 0.00
Ethylbenzene N.D. 250 207 202 82.80 80.80 2.44
m-Xylene/p-Xylene N.D. 500 412 408 82.40 81.60 0.98
o-Xylene N.D. 250 208 207 83.20 82.80 0.48
Cumene N.D. 250 198 200 79.20 80.00 1.01
Ethylene oxide N.D. 250 184 184 73.60 73.60 0.00

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

N.D. = Not Detected

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 35 of 67

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-004 Test Certificate #: 123371-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Northern Wreck Badder
License: 030-1009646F7F8
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A401030002C949000000017
Metrc Source Pkg#: 1A401030002C949000000016
Test Conditions

Prepsheet ID#: ORHS200402b
Scale: XS205-OR1
Temp: 22.1 °C
Baro PE: 1012 hPa
Analyst: HRM
Technician: HRM
Sample ID#: 123371

Lot #: Northern wreck badder 3/30/20 #1
Batch #: 123371
Batch Weight (g): 1640.4
Harvest/Process Date: 03/31/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 03/31/2020
Test Date: 04/02/2020
Sample #123371
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
1,2-Dichloroethane 2 1 Not Tested 1,2-Dimethoxyethane 100 5 Pass/<LOD
1,4-dioxane 380 200 Pass/<LOD 1-Butanol 5,000 100 Pass/<LOD
1-Pentanol 5,000 100 Pass/<LOD 1-Propanol 5,000 100 Pass/<LOD
2,2-Dimethylpropane (Neopentane) 5,000 100 Pass/<LOD 2,2-Dimethylbutane (Hexanes) 290 100 Pass/<LOD
2,3-Dimethylbutane (Hexanes) 290 100 Pass/<LOD 2-Butanol 5,000 100 Pass/<LOD
2-Butanone (MEK) 5,000 50 Pass/<LOD 2-Ethoxyethanol 160 40 Pass/<LOD
2-Methylbutane (Isopentane) 5,000 50 Pass/<LOD 2-Methylpentane (Hexanes) 290 50 Pass/<LOD
2-Methylpropane (Isobutane) 5,000 100 Pass/<LOD 2-propanol (Isopropyl Alcohol) 5,000 50 Pass/97
2-Propanone (Acetone) 5,000 50 Pass/<LOD 3-Methylpentane (Hexanes) 290 50 Pass/<LOD
Acetonitrile 410 100 Pass/<LOD Benzene 2 1 Pass/<LOD
Butane 5,000 100 Pass/141 Chloroform 2 1 Pass/<LOD
Cumene 70 50 Pass/<LOD Cyclohexane 3,880 1,000 Pass/<LOD
Dichloromethane 600 50 Pass/<LOD Dimethylsulfoxide (DMSO) 5,000 500 Pass/<LOD
Ethanol 5,000 500 Pass/<LOD Ethyl acetate 5,000 50 Pass/<LOD
Ethyl ether 5,000 500 Pass/<LOD Ethylene glycol 620 310 Pass/<LOD
Ethylene oxide 50 50 Pass/<LOD Heptane 5,000 50 Pass/<LOD
Hexane 290 290 Pass/<LOD Isopropyl acetate 5,000 50 Pass/<LOD
Methanol 3,000 500 Pass/<LOD Naptha 400 100 Not Tested
N,N-Dimethylacetamide 1,090 100 Pass/<LOD N,N-Dimethylformamide (DMF) 880 500 Pass/<LOD
Pentane 5,000 50 Pass/<LOD Petroleum Ether 400 100 Not Tested
Propane 5,000 100 Pass/<LOD Pyridine 200 10 Pass/<LOD
Sulfolane 160 200 Pass/<LOD Tetrahydrofuran (THF) 720 200 Pass/<LOD
Toluene 890 50 Pass/<LOD Trichloroethylene 25 5 Not Tested
Xylenes* 2,170 50 Pass/<LOD

Total Butanes = 141 ug/g (PASS); Total Pentanes = 0 ug/g (PASS); Total Hexanes = 0 ug/g (PASS)

* Xylenes are reported as the sum of o-xylene, m-xylene, p-xylene, and ethylbenzene
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 36 of 67

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents QC Report
Testing Accreditation #: 4092-004 Test Certificate #: 123371-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Northern Wreck Badder
License: 030-1009646F7F8
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A401030002C949000000017
Metrc Source Pkg#: 1A401030002C949000000016
Test Conditions

Prepsheet ID#: ORHS200402b
Scale: XS205-OR1
Temp: 22.1 °C
Baro PE: 1012 hPa
Analyst: HRM
Technician: HRM
Sample ID#: 123371

Lot #: Northern wreck badder 3/30/20 #1
Batch #: 123371
Batch Weight (g): 1640.4
Harvest/Process Date: 03/31/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 03/31/2020
Test Date: 04/02/2020
Sample #123371
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS Recovery (%) MSD Recovery (%) Relative Percent Difference (%) QC Flag
1,2-Dichloroethane N.D. 0 0 0 nan nan
n-Propane N.D. 250 64 64 25.60 25.60 0.00 LR
Isobutane N.D. 250 101 97 40.40 38.80 4.04 LR
Methanol N.D. 250 177 160 70.80 64.00 10.09 LR
n-Butane N.D. 250 117 119 46.80 47.60 1.69 LR
2,2-Dimethylpropane N.D. 250 126 127 50.40 50.80 0.79 LR
Ethanol N.D. 250 187 185 74.80 74.00 1.08
Isopentane N.D. 250 144 141 57.60 56.40 2.11 LR
Acetonitrile N.D. 250 169 154 67.60 61.60 9.29 LR
Diethyl ether N.D. 250 183 178 73.20 71.20 2.77
2-propanone N.D. 250 207 204 82.80 81.60 1.46
2-propanol N.D. 250 334 341 133.60 136.40 2.07 HR
n-Pentane N.D. 250 153 83 61.20 33.20 59.32 LRQ
2,2-Dimethylbutane N.D. 250 170 171 68.00 68.40 0.59 LR
2,3-Dimethylbutane N.D. 250 158 151 63.20 60.40 4.53 LR
Methylene chloride N.D. 250 190 194 76.00 77.60 2.08
2-Methylpentane N.D. 250 170 171 68.00 68.40 0.59 LR
3-Methylpentane N.D. 250 178 172 71.20 68.80 3.43 LR
2-Butanol N.D. 250 208 208 83.20 83.20 0.00
n-Hexane N.D. 250 180 177 72.00 70.80 1.68
Ethyl acetate N.D. 250 196 199 78.40 79.60 1.52
Tetrahydrofuran N.D. 250 188 183 0.00 0.00 0.00
Trichloroethylene N.D. 0 0 0 nan nan
Isopropyl acetate N.D. 250 196 199 0.00 0.00 0.00
Benzene N.D. 250 196 194 78.40 77.60 1.03
Chloroform N.D. 0 0 0 nan nan
Cyclohexane N.D. 250 186 185 74.40 74.00 0.54
Ethylene glycol N.D. 250 156 197 62.40 78.80 23.23 LRQ
Heptane N.D. 250 159 160 63.60 64.00 0.63 LR
2-Ethoxyethanol N.D. 250 167 190 66.80 76.00 12.89 LR
1,4-Dioxane N.D. 250 199 200 79.60 80.00 0.50
Pyridine N.D. 0 0 0 0.00 0.00 0.00
Toluene N.D. 250 204 198 81.60 79.20 2.99
Chlorobenzene N.D. 0 0 0 0.00 0.00 0.00
Ethylbenzene N.D. 250 207 202 82.80 80.80 2.44
m-Xylene/p-Xylene N.D. 500 412 408 82.40 81.60 0.98
o-Xylene N.D. 250 208 207 83.20 82.80 0.48
Cumene N.D. 250 198 200 79.20 80.00 1.01
Ethylene oxide N.D. 250 184 184 73.60 73.60 0.00

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

N.D. = Not Detected

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 37 of 67

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-004 Test Certificate #: 123371-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Northern Wreck Badder
License: 030-1009646F7F8
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A401030002C949000000017
Metrc Source Pkg#: 1A401030002C949000000016
Test Conditions

Prepsheet ID#: ORHS200402b
Scale: XS205-OR1
Temp: 22.1 °C
Baro PE: 1012 hPa
Analyst: HRM
Technician: HRM
Sample ID#: 123371

Lot #: Northern wreck badder 3/30/20 #1
Batch #: 123371
Batch Weight (g): 1640.4
Harvest/Process Date: 03/31/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 03/31/2020
Test Date: 04/02/2020
Sample #123371
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
1,2-Dichloroethane 2 1 Not Tested 1,2-Dimethoxyethane 100 5 Pass/<LOD
1,4-dioxane 380 200 Pass/<LOD 1-Butanol 5,000 100 Pass/<LOD
1-Pentanol 5,000 100 Pass/<LOD 1-Propanol 5,000 100 Pass/<LOD
2,2-Dimethylpropane (Neopentane) 5,000 100 Pass/<LOD 2,2-Dimethylbutane (Hexanes) 290 100 Pass/<LOD
2,3-Dimethylbutane (Hexanes) 290 100 Pass/<LOD 2-Butanol 5,000 100 Pass/<LOD
2-Butanone (MEK) 5,000 50 Pass/<LOD 2-Ethoxyethanol 160 40 Pass/<LOD
2-Methylbutane (Isopentane) 5,000 50 Pass/<LOD 2-Methylpentane (Hexanes) 290 50 Pass/<LOD
2-Methylpropane (Isobutane) 5,000 100 Pass/<LOD 2-propanol (Isopropyl Alcohol) 5,000 50 Pass/108
2-Propanone (Acetone) 5,000 50 Pass/<LOD 3-Methylpentane (Hexanes) 290 50 Pass/<LOD
Acetonitrile 410 100 Pass/<LOD Benzene 2 1 Pass/<LOD
Butane 5,000 100 Pass/<LOD Chloroform 2 1 Pass/<LOD
Cumene 70 50 Pass/<LOD Cyclohexane 3,880 1,000 Pass/<LOD
Dichloromethane 600 50 Pass/<LOD Dimethylsulfoxide (DMSO) 5,000 500 Pass/<LOD
Ethanol 5,000 500 Pass/<LOD Ethyl acetate 5,000 50 Pass/<LOD
Ethyl ether 5,000 500 Pass/<LOD Ethylene glycol 620 310 Pass/<LOD
Ethylene oxide 50 50 Pass/<LOD Heptane 5,000 50 Pass/<LOD
Hexane 290 290 Pass/<LOD Isopropyl acetate 5,000 50 Pass/<LOD
Methanol 3,000 500 Pass/<LOD Naptha 400 100 Not Tested
N,N-Dimethylacetamide 1,090 100 Pass/<LOD N,N-Dimethylformamide (DMF) 880 500 Pass/<LOD
Pentane 5,000 50 Pass/<LOD Petroleum Ether 400 100 Not Tested
Propane 5,000 100 Pass/<LOD Pyridine 200 10 Pass/<LOD
Sulfolane 160 200 Pass/<LOD Tetrahydrofuran (THF) 720 200 Pass/<LOD
Toluene 890 50 Pass/<LOD Trichloroethylene 25 5 Not Tested
Xylenes* 2,170 50 Pass/<LOD

Total Butanes = 95 ug/g (PASS); Total Pentanes = 0 ug/g (PASS); Total Hexanes = 0 ug/g (PASS)

* Xylenes are reported as the sum of o-xylene, m-xylene, p-xylene, and ethylbenzene
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 38 of 67

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents QC Report
Testing Accreditation #: 4092-004 Test Certificate #: 123371-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Northern Wreck Badder
License: 030-1009646F7F8
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A401030002C949000000017
Metrc Source Pkg#: 1A401030002C949000000016
Test Conditions

Prepsheet ID#: ORHS200402b
Scale: XS205-OR1
Temp: 22.1 °C
Baro PE: 1012 hPa
Analyst: HRM
Technician: HRM
Sample ID#: 123371

Lot #: Northern wreck badder 3/30/20 #1
Batch #: 123371
Batch Weight (g): 1640.4
Harvest/Process Date: 03/31/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 03/31/2020
Test Date: 04/02/2020
Sample #123371
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS Recovery (%) MSD Recovery (%) Relative Percent Difference (%) QC Flag
1,2-Dichloroethane N.D. 0 0 0 nan nan
n-Propane N.D. 250 64 64 25.60 25.60 0.00 LR
Isobutane N.D. 250 101 97 40.40 38.80 4.04 LR
Methanol N.D. 250 177 160 70.80 64.00 10.09 LR
n-Butane N.D. 250 117 119 46.80 47.60 1.69 LR
2,2-Dimethylpropane N.D. 250 126 127 50.40 50.80 0.79 LR
Ethanol N.D. 250 187 185 74.80 74.00 1.08
Isopentane N.D. 250 144 141 57.60 56.40 2.11 LR
Acetonitrile N.D. 250 169 154 67.60 61.60 9.29 LR
Diethyl ether N.D. 250 183 178 73.20 71.20 2.77
2-propanone N.D. 250 207 204 82.80 81.60 1.46
2-propanol N.D. 250 334 341 133.60 136.40 2.07 HR
n-Pentane N.D. 250 153 83 61.20 33.20 59.32 LRQ
2,2-Dimethylbutane N.D. 250 170 171 68.00 68.40 0.59 LR
2,3-Dimethylbutane N.D. 250 158 151 63.20 60.40 4.53 LR
Methylene chloride N.D. 250 190 194 76.00 77.60 2.08
2-Methylpentane N.D. 250 170 171 68.00 68.40 0.59 LR
3-Methylpentane N.D. 250 178 172 71.20 68.80 3.43 LR
2-Butanol N.D. 250 208 208 83.20 83.20 0.00
n-Hexane N.D. 250 180 177 72.00 70.80 1.68
Ethyl acetate N.D. 250 196 199 78.40 79.60 1.52
Tetrahydrofuran N.D. 250 188 183 0.00 0.00 0.00
Trichloroethylene N.D. 0 0 0 nan nan
Isopropyl acetate N.D. 250 196 199 0.00 0.00 0.00
Benzene N.D. 250 196 194 78.40 77.60 1.03
Chloroform N.D. 0 0 0 nan nan
Cyclohexane N.D. 250 186 185 74.40 74.00 0.54
Ethylene glycol N.D. 250 156 197 62.40 78.80 23.23 LRQ
Heptane N.D. 250 159 160 63.60 64.00 0.63 LR
2-Ethoxyethanol N.D. 250 167 190 66.80 76.00 12.89 LR
1,4-Dioxane N.D. 250 199 200 79.60 80.00 0.50
Pyridine N.D. 0 0 0 0.00 0.00 0.00
Toluene N.D. 250 204 198 81.60 79.20 2.99
Chlorobenzene N.D. 0 0 0 0.00 0.00 0.00
Ethylbenzene N.D. 250 207 202 82.80 80.80 2.44
m-Xylene/p-Xylene N.D. 500 412 408 82.40 81.60 0.98
o-Xylene N.D. 250 208 207 83.20 82.80 0.48
Cumene N.D. 250 198 200 79.20 80.00 1.01
Ethylene oxide N.D. 250 184 184 73.60 73.60 0.00

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

N.D. = Not Detected

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 39 of 67

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-004 Test Certificate #: 123371-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Northern Wreck Badder
License: 030-1009646F7F8
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A401030002C949000000017
Metrc Source Pkg#: 1A401030002C949000000016
Test Conditions

Prepsheet ID#: ORHS200402b
Scale: XS205-OR1
Temp: 22.1 °C
Baro PE: 1012 hPa
Analyst: HRM
Technician: HRM
Sample ID#: 123371

Lot #: Northern wreck badder 3/30/20 #1
Batch #: 123371
Batch Weight (g): 1640.4
Harvest/Process Date: 03/31/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 03/31/2020
Test Date: 04/02/2020
Sample #123371
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
1,2-Dichloroethane 2 1 Not Tested 1,2-Dimethoxyethane 100 5 Pass/<LOD
1,4-dioxane 380 200 Pass/<LOD 1-Butanol 5,000 100 Pass/<LOD
1-Pentanol 5,000 100 Pass/<LOD 1-Propanol 5,000 100 Pass/<LOD
2,2-Dimethylpropane (Neopentane) 5,000 100 Pass/<LOD 2,2-Dimethylbutane (Hexanes) 290 100 Pass/<LOD
2,3-Dimethylbutane (Hexanes) 290 100 Pass/<LOD 2-Butanol 5,000 100 Pass/<LOD
2-Butanone (MEK) 5,000 50 Pass/<LOD 2-Ethoxyethanol 160 40 Pass/<LOD
2-Methylbutane (Isopentane) 5,000 50 Pass/<LOD 2-Methylpentane (Hexanes) 290 50 Pass/<LOD
2-Methylpropane (Isobutane) 5,000 100 Pass/<LOD 2-propanol (Isopropyl Alcohol) 5,000 50 Pass/76
2-Propanone (Acetone) 5,000 50 Pass/<LOD 3-Methylpentane (Hexanes) 290 50 Pass/<LOD
Acetonitrile 410 100 Pass/<LOD Benzene 2 1 Pass/<LOD
Butane 5,000 100 Pass/127 Chloroform 2 1 Pass/<LOD
Cumene 70 50 Pass/<LOD Cyclohexane 3,880 1,000 Pass/<LOD
Dichloromethane 600 50 Pass/<LOD Dimethylsulfoxide (DMSO) 5,000 500 Pass/<LOD
Ethanol 5,000 500 Pass/<LOD Ethyl acetate 5,000 50 Pass/<LOD
Ethyl ether 5,000 500 Pass/<LOD Ethylene glycol 620 310 Pass/<LOD
Ethylene oxide 50 50 Pass/<LOD Heptane 5,000 50 Pass/<LOD
Hexane 290 290 Pass/<LOD Isopropyl acetate 5,000 50 Pass/<LOD
Methanol 3,000 500 Pass/<LOD Naptha 400 100 Not Tested
N,N-Dimethylacetamide 1,090 100 Pass/<LOD N,N-Dimethylformamide (DMF) 880 500 Pass/<LOD
Pentane 5,000 50 Pass/<LOD Petroleum Ether 400 100 Not Tested
Propane 5,000 100 Pass/<LOD Pyridine 200 10 Pass/<LOD
Sulfolane 160 200 Pass/<LOD Tetrahydrofuran (THF) 720 200 Pass/<LOD
Toluene 890 50 Pass/<LOD Trichloroethylene 25 5 Not Tested
Xylenes* 2,170 50 Pass/<LOD

Total Butanes = 127 ug/g (PASS); Total Pentanes = 0 ug/g (PASS); Total Hexanes = 0 ug/g (PASS)

* Xylenes are reported as the sum of o-xylene, m-xylene, p-xylene, and ethylbenzene
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 40 of 67

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents QC Report
Testing Accreditation #: 4092-004 Test Certificate #: 123371-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Northern Wreck Badder
License: 030-1009646F7F8
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A401030002C949000000017
Metrc Source Pkg#: 1A401030002C949000000016
Test Conditions

Prepsheet ID#: ORHS200402b
Scale: XS205-OR1
Temp: 22.1 °C
Baro PE: 1012 hPa
Analyst: HRM
Technician: HRM
Sample ID#: 123371

Lot #: Northern wreck badder 3/30/20 #1
Batch #: 123371
Batch Weight (g): 1640.4
Harvest/Process Date: 03/31/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 03/31/2020
Test Date: 04/02/2020
Sample #123371
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS Recovery (%) MSD Recovery (%) Relative Percent Difference (%) QC Flag
1,2-Dichloroethane N.D. 0 0 0 nan nan
n-Propane N.D. 250 64 64 25.60 25.60 0.00 LR
Isobutane N.D. 250 101 97 40.40 38.80 4.04 LR
Methanol N.D. 250 177 160 70.80 64.00 10.09 LR
n-Butane N.D. 250 117 119 46.80 47.60 1.69 LR
2,2-Dimethylpropane N.D. 250 126 127 50.40 50.80 0.79 LR
Ethanol N.D. 250 187 185 74.80 74.00 1.08
Isopentane N.D. 250 144 141 57.60 56.40 2.11 LR
Acetonitrile N.D. 250 169 154 67.60 61.60 9.29 LR
Diethyl ether N.D. 250 183 178 73.20 71.20 2.77
2-propanone N.D. 250 207 204 82.80 81.60 1.46
2-propanol N.D. 250 334 341 133.60 136.40 2.07 HR
n-Pentane N.D. 250 153 83 61.20 33.20 59.32 LRQ
2,2-Dimethylbutane N.D. 250 170 171 68.00 68.40 0.59 LR
2,3-Dimethylbutane N.D. 250 158 151 63.20 60.40 4.53 LR
Methylene chloride N.D. 250 190 194 76.00 77.60 2.08
2-Methylpentane N.D. 250 170 171 68.00 68.40 0.59 LR
3-Methylpentane N.D. 250 178 172 71.20 68.80 3.43 LR
2-Butanol N.D. 250 208 208 83.20 83.20 0.00
n-Hexane N.D. 250 180 177 72.00 70.80 1.68
Ethyl acetate N.D. 250 196 199 78.40 79.60 1.52
Tetrahydrofuran N.D. 250 188 183 0.00 0.00 0.00
Trichloroethylene N.D. 0 0 0 nan nan
Isopropyl acetate N.D. 250 196 199 0.00 0.00 0.00
Benzene N.D. 250 196 194 78.40 77.60 1.03
Chloroform N.D. 0 0 0 nan nan
Cyclohexane N.D. 250 186 185 74.40 74.00 0.54
Ethylene glycol N.D. 250 156 197 62.40 78.80 23.23 LRQ
Heptane N.D. 250 159 160 63.60 64.00 0.63 LR
2-Ethoxyethanol N.D. 250 167 190 66.80 76.00 12.89 LR
1,4-Dioxane N.D. 250 199 200 79.60 80.00 0.50
Pyridine N.D. 0 0 0 0.00 0.00 0.00
Toluene N.D. 250 204 198 81.60 79.20 2.99
Chlorobenzene N.D. 0 0 0 0.00 0.00 0.00
Ethylbenzene N.D. 250 207 202 82.80 80.80 2.44
m-Xylene/p-Xylene N.D. 500 412 408 82.40 81.60 0.98
o-Xylene N.D. 250 208 207 83.20 82.80 0.48
Cumene N.D. 250 198 200 79.20 80.00 1.01
Ethylene oxide N.D. 250 184 184 73.60 73.60 0.00

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

N.D. = Not Detected

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 41 of 67

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-004 Test Certificate #: 123371-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Northern Wreck Badder
License: 030-1009646F7F8
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A401030002C949000000017
Metrc Source Pkg#: 1A401030002C949000000016
Test Conditions

Prepsheet ID#: ORHS200402b
Scale: XS205-OR1
Temp: 22.1 °C
Baro PE: 1012 hPa
Analyst: HRM
Technician: HRM
Sample ID#: 123371

Lot #: Northern wreck badder 3/30/20 #1
Batch #: 123371
Batch Weight (g): 1640.4
Harvest/Process Date: 03/31/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 03/31/2020
Test Date: 04/02/2020
Sample #123371
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
1,2-Dichloroethane 2 1 Not Tested 1,2-Dimethoxyethane 100 5 Pass/<LOD
1,4-dioxane 380 200 Pass/<LOD 1-Butanol 5,000 100 Pass/<LOD
1-Pentanol 5,000 100 Pass/<LOD 1-Propanol 5,000 100 Pass/<LOD
2,2-Dimethylpropane (Neopentane) 5,000 100 Pass/<LOD 2,2-Dimethylbutane (Hexanes) 290 100 Pass/<LOD
2,3-Dimethylbutane (Hexanes) 290 100 Pass/<LOD 2-Butanol 5,000 100 Pass/<LOD
2-Butanone (MEK) 5,000 50 Pass/<LOD 2-Ethoxyethanol 160 40 Pass/<LOD
2-Methylbutane (Isopentane) 5,000 50 Pass/<LOD 2-Methylpentane (Hexanes) 290 50 Pass/<LOD
2-Methylpropane (Isobutane) 5,000 100 Pass/<LOD 2-propanol (Isopropyl Alcohol) 5,000 50 Pass/79
2-Propanone (Acetone) 5,000 50 Pass/61 3-Methylpentane (Hexanes) 290 50 Pass/<LOD
Acetonitrile 410 100 Pass/<LOD Benzene 2 1 Pass/<LOD
Butane 5,000 100 Pass/113 Chloroform 2 1 Pass/<LOD
Cumene 70 50 Pass/<LOD Cyclohexane 3,880 1,000 Pass/<LOD
Dichloromethane 600 50 Pass/<LOD Dimethylsulfoxide (DMSO) 5,000 500 Pass/<LOD
Ethanol 5,000 500 Pass/<LOD Ethyl acetate 5,000 50 Pass/<LOD
Ethyl ether 5,000 500 Pass/<LOD Ethylene glycol 620 310 Pass/<LOD
Ethylene oxide 50 50 Pass/<LOD Heptane 5,000 50 Pass/<LOD
Hexane 290 290 Pass/<LOD Isopropyl acetate 5,000 50 Pass/<LOD
Methanol 3,000 500 Pass/<LOD Naptha 400 100 Not Tested
N,N-Dimethylacetamide 1,090 100 Pass/<LOD N,N-Dimethylformamide (DMF) 880 500 Pass/<LOD
Pentane 5,000 50 Pass/<LOD Petroleum Ether 400 100 Not Tested
Propane 5,000 100 Pass/<LOD Pyridine 200 10 Pass/<LOD
Sulfolane 160 200 Pass/<LOD Tetrahydrofuran (THF) 720 200 Pass/<LOD
Toluene 890 50 Pass/<LOD Trichloroethylene 25 5 Not Tested
Xylenes* 2,170 50 Pass/<LOD

Total Butanes = 113 ug/g (PASS); Total Pentanes = 0 ug/g (PASS); Total Hexanes = 0 ug/g (PASS)

* Xylenes are reported as the sum of o-xylene, m-xylene, p-xylene, and ethylbenzene
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 42 of 67

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents QC Report
Testing Accreditation #: 4092-004 Test Certificate #: 123371-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Northern Wreck Badder
License: 030-1009646F7F8
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A401030002C949000000017
Metrc Source Pkg#: 1A401030002C949000000016
Test Conditions

Prepsheet ID#: ORHS200402b
Scale: XS205-OR1
Temp: 22.1 °C
Baro PE: 1012 hPa
Analyst: HRM
Technician: HRM
Sample ID#: 123371

Lot #: Northern wreck badder 3/30/20 #1
Batch #: 123371
Batch Weight (g): 1640.4
Harvest/Process Date: 03/31/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 03/31/2020
Test Date: 04/02/2020
Sample #123371
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS Recovery (%) MSD Recovery (%) Relative Percent Difference (%) QC Flag
1,2-Dichloroethane N.D. 0 0 0 nan nan
n-Propane N.D. 250 64 64 25.60 25.60 0.00 LR
Isobutane N.D. 250 101 97 40.40 38.80 4.04 LR
Methanol N.D. 250 177 160 70.80 64.00 10.09 LR
n-Butane N.D. 250 117 119 46.80 47.60 1.69 LR
2,2-Dimethylpropane N.D. 250 126 127 50.40 50.80 0.79 LR
Ethanol N.D. 250 187 185 74.80 74.00 1.08
Isopentane N.D. 250 144 141 57.60 56.40 2.11 LR
Acetonitrile N.D. 250 169 154 67.60 61.60 9.29 LR
Diethyl ether N.D. 250 183 178 73.20 71.20 2.77
2-propanone N.D. 250 207 204 82.80 81.60 1.46
2-propanol N.D. 250 334 341 133.60 136.40 2.07 HR
n-Pentane N.D. 250 153 83 61.20 33.20 59.32 LRQ
2,2-Dimethylbutane N.D. 250 170 171 68.00 68.40 0.59 LR
2,3-Dimethylbutane N.D. 250 158 151 63.20 60.40 4.53 LR
Methylene chloride N.D. 250 190 194 76.00 77.60 2.08
2-Methylpentane N.D. 250 170 171 68.00 68.40 0.59 LR
3-Methylpentane N.D. 250 178 172 71.20 68.80 3.43 LR
2-Butanol N.D. 250 208 208 83.20 83.20 0.00
n-Hexane N.D. 250 180 177 72.00 70.80 1.68
Ethyl acetate N.D. 250 196 199 78.40 79.60 1.52
Tetrahydrofuran N.D. 250 188 183 0.00 0.00 0.00
Trichloroethylene N.D. 0 0 0 nan nan
Isopropyl acetate N.D. 250 196 199 0.00 0.00 0.00
Benzene N.D. 250 196 194 78.40 77.60 1.03
Chloroform N.D. 0 0 0 nan nan
Cyclohexane N.D. 250 186 185 74.40 74.00 0.54
Ethylene glycol N.D. 250 156 197 62.40 78.80 23.23 LRQ
Heptane N.D. 250 159 160 63.60 64.00 0.63 LR
2-Ethoxyethanol N.D. 250 167 190 66.80 76.00 12.89 LR
1,4-Dioxane N.D. 250 199 200 79.60 80.00 0.50
Pyridine N.D. 0 0 0 0.00 0.00 0.00
Toluene N.D. 250 204 198 81.60 79.20 2.99
Chlorobenzene N.D. 0 0 0 0.00 0.00 0.00
Ethylbenzene N.D. 250 207 202 82.80 80.80 2.44
m-Xylene/p-Xylene N.D. 500 412 408 82.40 81.60 0.98
o-Xylene N.D. 250 208 207 83.20 82.80 0.48
Cumene N.D. 250 198 200 79.20 80.00 1.01
Ethylene oxide N.D. 250 184 184 73.60 73.60 0.00

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

N.D. = Not Detected

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 43 of 67

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-004 Test Certificate #: 123371-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Northern Wreck Badder
License: 030-1009646F7F8
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A401030002C949000000017
Metrc Source Pkg#: 1A401030002C949000000016
Test Conditions

Prepsheet ID#: ORHS200402b
Scale: XS205-OR1
Temp: 22.1 °C
Baro PE: 1012 hPa
Analyst: HRM
Technician: HRM
Sample ID#: 123371

Lot #: Northern wreck badder 3/30/20 #1
Batch #: 123371
Batch Weight (g): 1640.4
Harvest/Process Date: 03/31/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 03/31/2020
Test Date: 04/02/2020
Sample #123371
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
1,2-Dichloroethane 2 1 Not Tested 1,2-Dimethoxyethane 100 5 Pass/<LOD
1,4-dioxane 380 200 Pass/<LOD 1-Butanol 5,000 100 Pass/<LOD
1-Pentanol 5,000 100 Pass/<LOD 1-Propanol 5,000 100 Pass/<LOD
2,2-Dimethylpropane (Neopentane) 5,000 100 Pass/<LOD 2,2-Dimethylbutane (Hexanes) 290 100 Pass/<LOD
2,3-Dimethylbutane (Hexanes) 290 100 Pass/<LOD 2-Butanol 5,000 100 Pass/<LOD
2-Butanone (MEK) 5,000 50 Pass/<LOD 2-Ethoxyethanol 160 40 Pass/<LOD
2-Methylbutane (Isopentane) 5,000 50 Pass/<LOD 2-Methylpentane (Hexanes) 290 50 Pass/<LOD
2-Methylpropane (Isobutane) 5,000 100 Pass/<LOD 2-propanol (Isopropyl Alcohol) 5,000 50 Pass/60
2-Propanone (Acetone) 5,000 50 Pass/55 3-Methylpentane (Hexanes) 290 50 Pass/<LOD
Acetonitrile 410 100 Pass/<LOD Benzene 2 1 Pass/<LOD
Butane 5,000 100 Pass/118 Chloroform 2 1 Pass/<LOD
Cumene 70 50 Pass/<LOD Cyclohexane 3,880 1,000 Pass/<LOD
Dichloromethane 600 50 Pass/<LOD Dimethylsulfoxide (DMSO) 5,000 500 Pass/<LOD
Ethanol 5,000 500 Pass/<LOD Ethyl acetate 5,000 50 Pass/<LOD
Ethyl ether 5,000 500 Pass/<LOD Ethylene glycol 620 310 Pass/<LOD
Ethylene oxide 50 50 Pass/<LOD Heptane 5,000 50 Pass/<LOD
Hexane 290 290 Pass/<LOD Isopropyl acetate 5,000 50 Pass/<LOD
Methanol 3,000 500 Pass/<LOD Naptha 400 100 Not Tested
N,N-Dimethylacetamide 1,090 100 Pass/<LOD N,N-Dimethylformamide (DMF) 880 500 Pass/<LOD
Pentane 5,000 50 Pass/<LOD Petroleum Ether 400 100 Not Tested
Propane 5,000 100 Pass/<LOD Pyridine 200 10 Pass/<LOD
Sulfolane 160 200 Pass/<LOD Tetrahydrofuran (THF) 720 200 Pass/<LOD
Toluene 890 50 Pass/<LOD Trichloroethylene 25 5 Not Tested
Xylenes* 2,170 50 Pass/<LOD

Total Butanes = 118 ug/g (PASS); Total Pentanes = 0 ug/g (PASS); Total Hexanes = 0 ug/g (PASS)

* Xylenes are reported as the sum of o-xylene, m-xylene, p-xylene, and ethylbenzene
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 44 of 67

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents QC Report
Testing Accreditation #: 4092-004 Test Certificate #: 123371-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Northern Wreck Badder
License: 030-1009646F7F8
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A401030002C949000000017
Metrc Source Pkg#: 1A401030002C949000000016
Test Conditions

Prepsheet ID#: ORHS200402b
Scale: XS205-OR1
Temp: 22.1 °C
Baro PE: 1012 hPa
Analyst: HRM
Technician: HRM
Sample ID#: 123371

Lot #: Northern wreck badder 3/30/20 #1
Batch #: 123371
Batch Weight (g): 1640.4
Harvest/Process Date: 03/31/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 03/31/2020
Test Date: 04/02/2020
Sample #123371
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS Recovery (%) MSD Recovery (%) Relative Percent Difference (%) QC Flag
1,2-Dichloroethane N.D. 0 0 0 nan nan
n-Propane N.D. 250 64 64 25.60 25.60 0.00 LR
Isobutane N.D. 250 101 97 40.40 38.80 4.04 LR
Methanol N.D. 250 177 160 70.80 64.00 10.09 LR
n-Butane N.D. 250 117 119 46.80 47.60 1.69 LR
2,2-Dimethylpropane N.D. 250 126 127 50.40 50.80 0.79 LR
Ethanol N.D. 250 187 185 74.80 74.00 1.08
Isopentane N.D. 250 144 141 57.60 56.40 2.11 LR
Acetonitrile N.D. 250 169 154 67.60 61.60 9.29 LR
Diethyl ether N.D. 250 183 178 73.20 71.20 2.77
2-propanone N.D. 250 207 204 82.80 81.60 1.46
2-propanol N.D. 250 334 341 133.60 136.40 2.07 HR
n-Pentane N.D. 250 153 83 61.20 33.20 59.32 LRQ
2,2-Dimethylbutane N.D. 250 170 171 68.00 68.40 0.59 LR
2,3-Dimethylbutane N.D. 250 158 151 63.20 60.40 4.53 LR
Methylene chloride N.D. 250 190 194 76.00 77.60 2.08
2-Methylpentane N.D. 250 170 171 68.00 68.40 0.59 LR
3-Methylpentane N.D. 250 178 172 71.20 68.80 3.43 LR
2-Butanol N.D. 250 208 208 83.20 83.20 0.00
n-Hexane N.D. 250 180 177 72.00 70.80 1.68
Ethyl acetate N.D. 250 196 199 78.40 79.60 1.52
Tetrahydrofuran N.D. 250 188 183 0.00 0.00 0.00
Trichloroethylene N.D. 0 0 0 nan nan
Isopropyl acetate N.D. 250 196 199 0.00 0.00 0.00
Benzene N.D. 250 196 194 78.40 77.60 1.03
Chloroform N.D. 0 0 0 nan nan
Cyclohexane N.D. 250 186 185 74.40 74.00 0.54
Ethylene glycol N.D. 250 156 197 62.40 78.80 23.23 LRQ
Heptane N.D. 250 159 160 63.60 64.00 0.63 LR
2-Ethoxyethanol N.D. 250 167 190 66.80 76.00 12.89 LR
1,4-Dioxane N.D. 250 199 200 79.60 80.00 0.50
Pyridine N.D. 0 0 0 0.00 0.00 0.00
Toluene N.D. 250 204 198 81.60 79.20 2.99
Chlorobenzene N.D. 0 0 0 0.00 0.00 0.00
Ethylbenzene N.D. 250 207 202 82.80 80.80 2.44
m-Xylene/p-Xylene N.D. 500 412 408 82.40 81.60 0.98
o-Xylene N.D. 250 208 207 83.20 82.80 0.48
Cumene N.D. 250 198 200 79.20 80.00 1.01
Ethylene oxide N.D. 250 184 184 73.60 73.60 0.00

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

N.D. = Not Detected

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 45 of 67

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-004 Test Certificate #: 123371-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Northern Wreck Badder
License: 030-1009646F7F8
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A401030002C949000000017
Metrc Source Pkg#: 1A401030002C949000000016
Test Conditions

Prepsheet ID#: ORHS200402b
Scale: XS205-OR1
Temp: 22.1 °C
Baro PE: 1012 hPa
Analyst: HRM
Technician: HRM
Sample ID#: 123371

Lot #: Northern wreck badder 3/30/20 #1
Batch #: 123371
Batch Weight (g): 1640.4
Harvest/Process Date: 03/31/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 03/31/2020
Test Date: 04/02/2020
Sample #123371
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
1,2-Dichloroethane 2 1 Not Tested 1,2-Dimethoxyethane 100 5 Pass/<LOD
1,4-dioxane 380 200 Pass/<LOD 1-Butanol 5,000 100 Pass/<LOD
1-Pentanol 5,000 100 Pass/<LOD 1-Propanol 5,000 100 Pass/<LOD
2,2-Dimethylpropane (Neopentane) 5,000 100 Pass/<LOD 2,2-Dimethylbutane (Hexanes) 290 100 Pass/<LOD
2,3-Dimethylbutane (Hexanes) 290 100 Pass/<LOD 2-Butanol 5,000 100 Pass/<LOD
2-Butanone (MEK) 5,000 50 Pass/<LOD 2-Ethoxyethanol 160 40 Pass/<LOD
2-Methylbutane (Isopentane) 5,000 50 Pass/<LOD 2-Methylpentane (Hexanes) 290 50 Pass/<LOD
2-Methylpropane (Isobutane) 5,000 100 Pass/<LOD 2-propanol (Isopropyl Alcohol) 5,000 50 Pass/95
2-Propanone (Acetone) 5,000 50 Pass/55 3-Methylpentane (Hexanes) 290 50 Pass/<LOD
Acetonitrile 410 100 Pass/<LOD Benzene 2 1 Pass/<LOD
Butane 5,000 100 Pass/<LOD Chloroform 2 1 Pass/<LOD
Cumene 70 50 Pass/<LOD Cyclohexane 3,880 1,000 Pass/<LOD
Dichloromethane 600 50 Pass/<LOD Dimethylsulfoxide (DMSO) 5,000 500 Pass/<LOD
Ethanol 5,000 500 Pass/<LOD Ethyl acetate 5,000 50 Pass/<LOD
Ethyl ether 5,000 500 Pass/<LOD Ethylene glycol 620 310 Pass/<LOD
Ethylene oxide 50 50 Pass/<LOD Heptane 5,000 50 Pass/<LOD
Hexane 290 290 Pass/<LOD Isopropyl acetate 5,000 50 Pass/<LOD
Methanol 3,000 500 Pass/<LOD Naptha 400 100 Not Tested
N,N-Dimethylacetamide 1,090 100 Pass/<LOD N,N-Dimethylformamide (DMF) 880 500 Pass/<LOD
Pentane 5,000 50 Pass/<LOD Petroleum Ether 400 100 Not Tested
Propane 5,000 100 Pass/<LOD Pyridine 200 10 Pass/<LOD
Sulfolane 160 200 Pass/<LOD Tetrahydrofuran (THF) 720 200 Pass/<LOD
Toluene 890 50 Pass/<LOD Trichloroethylene 25 5 Not Tested
Xylenes* 2,170 50 Pass/<LOD

Total Butanes = 84 ug/g (PASS); Total Pentanes = 0 ug/g (PASS); Total Hexanes = 0 ug/g (PASS)

* Xylenes are reported as the sum of o-xylene, m-xylene, p-xylene, and ethylbenzene
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 46 of 67

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents QC Report
Testing Accreditation #: 4092-004 Test Certificate #: 123371-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Northern Wreck Badder
License: 030-1009646F7F8
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A401030002C949000000017
Metrc Source Pkg#: 1A401030002C949000000016
Test Conditions

Prepsheet ID#: ORHS200402b
Scale: XS205-OR1
Temp: 22.1 °C
Baro PE: 1012 hPa
Analyst: HRM
Technician: HRM
Sample ID#: 123371

Lot #: Northern wreck badder 3/30/20 #1
Batch #: 123371
Batch Weight (g): 1640.4
Harvest/Process Date: 03/31/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 03/31/2020
Test Date: 04/02/2020
Sample #123371
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS Recovery (%) MSD Recovery (%) Relative Percent Difference (%) QC Flag
1,2-Dichloroethane N.D. 0 0 0 nan nan
n-Propane N.D. 250 64 64 25.60 25.60 0.00 LR
Isobutane N.D. 250 101 97 40.40 38.80 4.04 LR
Methanol N.D. 250 177 160 70.80 64.00 10.09 LR
n-Butane N.D. 250 117 119 46.80 47.60 1.69 LR
2,2-Dimethylpropane N.D. 250 126 127 50.40 50.80 0.79 LR
Ethanol N.D. 250 187 185 74.80 74.00 1.08
Isopentane N.D. 250 144 141 57.60 56.40 2.11 LR
Acetonitrile N.D. 250 169 154 67.60 61.60 9.29 LR
Diethyl ether N.D. 250 183 178 73.20 71.20 2.77
2-propanone N.D. 250 207 204 82.80 81.60 1.46
2-propanol N.D. 250 334 341 133.60 136.40 2.07 HR
n-Pentane N.D. 250 153 83 61.20 33.20 59.32 LRQ
2,2-Dimethylbutane N.D. 250 170 171 68.00 68.40 0.59 LR
2,3-Dimethylbutane N.D. 250 158 151 63.20 60.40 4.53 LR
Methylene chloride N.D. 250 190 194 76.00 77.60 2.08
2-Methylpentane N.D. 250 170 171 68.00 68.40 0.59 LR
3-Methylpentane N.D. 250 178 172 71.20 68.80 3.43 LR
2-Butanol N.D. 250 208 208 83.20 83.20 0.00
n-Hexane N.D. 250 180 177 72.00 70.80 1.68
Ethyl acetate N.D. 250 196 199 78.40 79.60 1.52
Tetrahydrofuran N.D. 250 188 183 0.00 0.00 0.00
Trichloroethylene N.D. 0 0 0 nan nan
Isopropyl acetate N.D. 250 196 199 0.00 0.00 0.00
Benzene N.D. 250 196 194 78.40 77.60 1.03
Chloroform N.D. 0 0 0 nan nan
Cyclohexane N.D. 250 186 185 74.40 74.00 0.54
Ethylene glycol N.D. 250 156 197 62.40 78.80 23.23 LRQ
Heptane N.D. 250 159 160 63.60 64.00 0.63 LR
2-Ethoxyethanol N.D. 250 167 190 66.80 76.00 12.89 LR
1,4-Dioxane N.D. 250 199 200 79.60 80.00 0.50
Pyridine N.D. 0 0 0 0.00 0.00 0.00
Toluene N.D. 250 204 198 81.60 79.20 2.99
Chlorobenzene N.D. 0 0 0 0.00 0.00 0.00
Ethylbenzene N.D. 250 207 202 82.80 80.80 2.44
m-Xylene/p-Xylene N.D. 500 412 408 82.40 81.60 0.98
o-Xylene N.D. 250 208 207 83.20 82.80 0.48
Cumene N.D. 250 198 200 79.20 80.00 1.01
Ethylene oxide N.D. 250 184 184 73.60 73.60 0.00

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

N.D. = Not Detected

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 47 of 67

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-004 Test Certificate #: 123371-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Northern Wreck Badder
License: 030-1009646F7F8
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A401030002C949000000017
Metrc Source Pkg#: 1A401030002C949000000016
Test Conditions

Prepsheet ID#: ORHS200402b
Scale: XS205-OR1
Temp: 22.1 °C
Baro PE: 1012 hPa
Analyst: HRM
Technician: HRM
Sample ID#: 123371

Lot #: Northern wreck badder 3/30/20 #1
Batch #: 123371
Batch Weight (g): 1640.4
Harvest/Process Date: 03/31/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 03/31/2020
Test Date: 04/02/2020
Sample #123371
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
1,2-Dichloroethane 2 1 Not Tested 1,2-Dimethoxyethane 100 5 Pass/<LOD
1,4-dioxane 380 200 Pass/<LOD 1-Butanol 5,000 100 Pass/<LOD
1-Pentanol 5,000 100 Pass/<LOD 1-Propanol 5,000 100 Pass/<LOD
2,2-Dimethylpropane (Neopentane) 5,000 100 Pass/<LOD 2,2-Dimethylbutane (Hexanes) 290 100 Pass/<LOD
2,3-Dimethylbutane (Hexanes) 290 100 Pass/<LOD 2-Butanol 5,000 100 Pass/<LOD
2-Butanone (MEK) 5,000 50 Pass/<LOD 2-Ethoxyethanol 160 40 Pass/<LOD
2-Methylbutane (Isopentane) 5,000 50 Pass/<LOD 2-Methylpentane (Hexanes) 290 50 Pass/<LOD
2-Methylpropane (Isobutane) 5,000 100 Pass/<LOD 2-propanol (Isopropyl Alcohol) 5,000 50 Pass/<LOD
2-Propanone (Acetone) 5,000 50 Pass/<LOD 3-Methylpentane (Hexanes) 290 50 Pass/<LOD
Acetonitrile 410 100 Pass/<LOD Benzene 2 1 Pass/<LOD
Butane 5,000 100 Pass/<LOD Chloroform 2 1 Pass/<LOD
Cumene 70 50 Pass/<LOD Cyclohexane 3,880 1,000 Pass/<LOD
Dichloromethane 600 50 Pass/<LOD Dimethylsulfoxide (DMSO) 5,000 500 Pass/<LOD
Ethanol 5,000 500 Pass/<LOD Ethyl acetate 5,000 50 Pass/<LOD
Ethyl ether 5,000 500 Pass/<LOD Ethylene glycol 620 310 Pass/<LOD
Ethylene oxide 50 50 Pass/<LOD Heptane 5,000 50 Pass/<LOD
Hexane 290 290 Pass/<LOD Isopropyl acetate 5,000 50 Pass/<LOD
Methanol 3,000 500 Pass/<LOD Naptha 400 100 Not Tested
N,N-Dimethylacetamide 1,090 100 Pass/<LOD N,N-Dimethylformamide (DMF) 880 500 Pass/<LOD
Pentane 5,000 50 Pass/<LOD Petroleum Ether 400 100 Not Tested
Propane 5,000 100 Pass/<LOD Pyridine 200 10 Pass/<LOD
Sulfolane 160 200 Pass/<LOD Tetrahydrofuran (THF) 720 200 Pass/<LOD
Toluene 890 50 Pass/<LOD Trichloroethylene 25 5 Not Tested
Xylenes* 2,170 50 Pass/<LOD

Total Butanes = 0 ug/g (PASS); Total Pentanes = 0 ug/g (PASS); Total Hexanes = 0 ug/g (PASS)

* Xylenes are reported as the sum of o-xylene, m-xylene, p-xylene, and ethylbenzene
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 48 of 67

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents QC Report
Testing Accreditation #: 4092-004 Test Certificate #: 123371-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Northern Wreck Badder
License: 030-1009646F7F8
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A401030002C949000000017
Metrc Source Pkg#: 1A401030002C949000000016
Test Conditions

Prepsheet ID#: ORHS200402b
Scale: XS205-OR1
Temp: 22.1 °C
Baro PE: 1012 hPa
Analyst: HRM
Technician: HRM
Sample ID#: 123371

Lot #: Northern wreck badder 3/30/20 #1
Batch #: 123371
Batch Weight (g): 1640.4
Harvest/Process Date: 03/31/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 03/31/2020
Test Date: 04/02/2020
Sample #123371
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS Recovery (%) MSD Recovery (%) Relative Percent Difference (%) QC Flag
1,2-Dichloroethane N.D. 0 0 0 nan nan
n-Propane N.D. 250 64 64 25.60 25.60 0.00 LR
Isobutane N.D. 250 101 97 40.40 38.80 4.04 LR
Methanol N.D. 250 177 160 70.80 64.00 10.09 LR
n-Butane N.D. 250 117 119 46.80 47.60 1.69 LR
2,2-Dimethylpropane N.D. 250 126 127 50.40 50.80 0.79 LR
Ethanol N.D. 250 187 185 74.80 74.00 1.08
Isopentane N.D. 250 144 141 57.60 56.40 2.11 LR
Acetonitrile N.D. 250 169 154 67.60 61.60 9.29 LR
Diethyl ether N.D. 250 183 178 73.20 71.20 2.77
2-propanone N.D. 250 207 204 82.80 81.60 1.46
2-propanol N.D. 250 334 341 133.60 136.40 2.07 HR
n-Pentane N.D. 250 153 83 61.20 33.20 59.32 LRQ
2,2-Dimethylbutane N.D. 250 170 171 68.00 68.40 0.59 LR
2,3-Dimethylbutane N.D. 250 158 151 63.20 60.40 4.53 LR
Methylene chloride N.D. 250 190 194 76.00 77.60 2.08
2-Methylpentane N.D. 250 170 171 68.00 68.40 0.59 LR
3-Methylpentane N.D. 250 178 172 71.20 68.80 3.43 LR
2-Butanol N.D. 250 208 208 83.20 83.20 0.00
n-Hexane N.D. 250 180 177 72.00 70.80 1.68
Ethyl acetate N.D. 250 196 199 78.40 79.60 1.52
Tetrahydrofuran N.D. 250 188 183 0.00 0.00 0.00
Trichloroethylene N.D. 0 0 0 nan nan
Isopropyl acetate N.D. 250 196 199 0.00 0.00 0.00
Benzene N.D. 250 196 194 78.40 77.60 1.03
Chloroform N.D. 0 0 0 nan nan
Cyclohexane N.D. 250 186 185 74.40 74.00 0.54
Ethylene glycol N.D. 250 156 197 62.40 78.80 23.23 LRQ
Heptane N.D. 250 159 160 63.60 64.00 0.63 LR
2-Ethoxyethanol N.D. 250 167 190 66.80 76.00 12.89 LR
1,4-Dioxane N.D. 250 199 200 79.60 80.00 0.50
Pyridine N.D. 0 0 0 0.00 0.00 0.00
Toluene N.D. 250 204 198 81.60 79.20 2.99
Chlorobenzene N.D. 0 0 0 0.00 0.00 0.00
Ethylbenzene N.D. 250 207 202 82.80 80.80 2.44
m-Xylene/p-Xylene N.D. 500 412 408 82.40 81.60 0.98
o-Xylene N.D. 250 208 207 83.20 82.80 0.48
Cumene N.D. 250 198 200 79.20 80.00 1.01
Ethylene oxide N.D. 250 184 184 73.60 73.60 0.00

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

N.D. = Not Detected

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 49 of 67

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-004 Test Certificate #: 123371-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Northern Wreck Badder
License: 030-1009646F7F8
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A401030002C949000000017
Metrc Source Pkg#: 1A401030002C949000000016
Test Conditions

Prepsheet ID#: ORHS200402b
Scale: XS205-OR1
Temp: 22.1 °C
Baro PE: 1012 hPa
Analyst: HRM
Technician: HRM
Sample ID#: 123371

Lot #: Northern wreck badder 3/30/20 #1
Batch #: 123371
Batch Weight (g): 1640.4
Harvest/Process Date: 03/31/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 03/31/2020
Test Date: 04/02/2020
Sample #123371
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
1,2-Dichloroethane 2 1 Not Tested 1,2-Dimethoxyethane 100 5 Pass/<LOD
1,4-dioxane 380 200 Pass/<LOD 1-Butanol 5,000 100 Pass/<LOD
1-Pentanol 5,000 100 Pass/<LOD 1-Propanol 5,000 100 Pass/<LOD
2,2-Dimethylpropane (Neopentane) 5,000 100 Pass/<LOD 2,2-Dimethylbutane (Hexanes) 290 100 Pass/<LOD
2,3-Dimethylbutane (Hexanes) 290 100 Pass/<LOD 2-Butanol 5,000 100 Pass/<LOD
2-Butanone (MEK) 5,000 50 Pass/<LOD 2-Ethoxyethanol 160 40 Pass/<LOD
2-Methylbutane (Isopentane) 5,000 50 Pass/<LOD 2-Methylpentane (Hexanes) 290 50 Pass/<LOD
2-Methylpropane (Isobutane) 5,000 100 Pass/<LOD 2-propanol (Isopropyl Alcohol) 5,000 50 Pass/51
2-Propanone (Acetone) 5,000 50 Pass/57 3-Methylpentane (Hexanes) 290 50 Pass/<LOD
Acetonitrile 410 100 Pass/<LOD Benzene 2 1 Pass/<LOD
Butane 5,000 100 Pass/159 Chloroform 2 1 Pass/<LOD
Cumene 70 50 Pass/<LOD Cyclohexane 3,880 1,000 Pass/<LOD
Dichloromethane 600 50 Pass/<LOD Dimethylsulfoxide (DMSO) 5,000 500 Pass/<LOD
Ethanol 5,000 500 Pass/<LOD Ethyl acetate 5,000 50 Pass/<LOD
Ethyl ether 5,000 500 Pass/<LOD Ethylene glycol 620 310 Pass/<LOD
Ethylene oxide 50 50 Pass/<LOD Heptane 5,000 50 Pass/<LOD
Hexane 290 290 Pass/<LOD Isopropyl acetate 5,000 50 Pass/<LOD
Methanol 3,000 500 Pass/<LOD Naptha 400 100 Not Tested
N,N-Dimethylacetamide 1,090 100 Pass/<LOD N,N-Dimethylformamide (DMF) 880 500 Pass/<LOD
Pentane 5,000 50 Pass/<LOD Petroleum Ether 400 100 Not Tested
Propane 5,000 100 Pass/<LOD Pyridine 200 10 Pass/<LOD
Sulfolane 160 200 Pass/<LOD Tetrahydrofuran (THF) 720 200 Pass/<LOD
Toluene 890 50 Pass/<LOD Trichloroethylene 25 5 Not Tested
Xylenes* 2,170 50 Pass/<LOD

Total Butanes = 159 ug/g (PASS); Total Pentanes = 0 ug/g (PASS); Total Hexanes = 0 ug/g (PASS)

* Xylenes are reported as the sum of o-xylene, m-xylene, p-xylene, and ethylbenzene
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 50 of 67

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents QC Report
Testing Accreditation #: 4092-004 Test Certificate #: 123371-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Northern Wreck Badder
License: 030-1009646F7F8
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A401030002C949000000017
Metrc Source Pkg#: 1A401030002C949000000016
Test Conditions

Prepsheet ID#: ORHS200402b
Scale: XS205-OR1
Temp: 22.1 °C
Baro PE: 1012 hPa
Analyst: HRM
Technician: HRM
Sample ID#: 123371

Lot #: Northern wreck badder 3/30/20 #1
Batch #: 123371
Batch Weight (g): 1640.4
Harvest/Process Date: 03/31/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 03/31/2020
Test Date: 04/02/2020
Sample #123371
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS Recovery (%) MSD Recovery (%) Relative Percent Difference (%) QC Flag
1,2-Dichloroethane N.D. 0 0 0 nan nan
n-Propane N.D. 250 64 64 25.60 25.60 0.00 LR
Isobutane N.D. 250 101 97 40.40 38.80 4.04 LR
Methanol N.D. 250 177 160 70.80 64.00 10.09 LR
n-Butane N.D. 250 117 119 46.80 47.60 1.69 LR
2,2-Dimethylpropane N.D. 250 126 127 50.40 50.80 0.79 LR
Ethanol N.D. 250 187 185 74.80 74.00 1.08
Isopentane N.D. 250 144 141 57.60 56.40 2.11 LR
Acetonitrile N.D. 250 169 154 67.60 61.60 9.29 LR
Diethyl ether N.D. 250 183 178 73.20 71.20 2.77
2-propanone N.D. 250 207 204 82.80 81.60 1.46
2-propanol N.D. 250 334 341 133.60 136.40 2.07 HR
n-Pentane N.D. 250 153 83 61.20 33.20 59.32 LRQ
2,2-Dimethylbutane N.D. 250 170 171 68.00 68.40 0.59 LR
2,3-Dimethylbutane N.D. 250 158 151 63.20 60.40 4.53 LR
Methylene chloride N.D. 250 190 194 76.00 77.60 2.08
2-Methylpentane N.D. 250 170 171 68.00 68.40 0.59 LR
3-Methylpentane N.D. 250 178 172 71.20 68.80 3.43 LR
2-Butanol N.D. 250 208 208 83.20 83.20 0.00
n-Hexane N.D. 250 180 177 72.00 70.80 1.68
Ethyl acetate N.D. 250 196 199 78.40 79.60 1.52
Tetrahydrofuran N.D. 250 188 183 0.00 0.00 0.00
Trichloroethylene N.D. 0 0 0 nan nan
Isopropyl acetate N.D. 250 196 199 0.00 0.00 0.00
Benzene N.D. 250 196 194 78.40 77.60 1.03
Chloroform N.D. 0 0 0 nan nan
Cyclohexane N.D. 250 186 185 74.40 74.00 0.54
Ethylene glycol N.D. 250 156 197 62.40 78.80 23.23 LRQ
Heptane N.D. 250 159 160 63.60 64.00 0.63 LR
2-Ethoxyethanol N.D. 250 167 190 66.80 76.00 12.89 LR
1,4-Dioxane N.D. 250 199 200 79.60 80.00 0.50
Pyridine N.D. 0 0 0 0.00 0.00 0.00
Toluene N.D. 250 204 198 81.60 79.20 2.99
Chlorobenzene N.D. 0 0 0 0.00 0.00 0.00
Ethylbenzene N.D. 250 207 202 82.80 80.80 2.44
m-Xylene/p-Xylene N.D. 500 412 408 82.40 81.60 0.98
o-Xylene N.D. 250 208 207 83.20 82.80 0.48
Cumene N.D. 250 198 200 79.20 80.00 1.01
Ethylene oxide N.D. 250 184 184 73.60 73.60 0.00

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

N.D. = Not Detected

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 51 of 67

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-004 Test Certificate #: 123371-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Northern Wreck Badder
License: 030-1009646F7F8
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A401030002C949000000017
Metrc Source Pkg#: 1A401030002C949000000016
Test Conditions

Prepsheet ID#: ORHS200402b
Scale: XS205-OR1
Temp: 22.1 °C
Baro PE: 1012 hPa
Analyst: HRM
Technician: HRM
Sample ID#: 123371

Lot #: Northern wreck badder 3/30/20 #1
Batch #: 123371
Batch Weight (g): 1640.4
Harvest/Process Date: 03/31/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 03/31/2020
Test Date: 04/02/2020
Sample #123371
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
1,2-Dichloroethane 2 1 Not Tested 1,2-Dimethoxyethane 100 5 Pass/<LOD
1,4-dioxane 380 200 Pass/<LOD 1-Butanol 5,000 100 Pass/<LOD
1-Pentanol 5,000 100 Pass/<LOD 1-Propanol 5,000 100 Pass/<LOD
2,2-Dimethylpropane (Neopentane) 5,000 100 Pass/<LOD 2,2-Dimethylbutane (Hexanes) 290 100 Pass/<LOD
2,3-Dimethylbutane (Hexanes) 290 100 Pass/<LOD 2-Butanol 5,000 100 Pass/<LOD
2-Butanone (MEK) 5,000 50 Pass/<LOD 2-Ethoxyethanol 160 40 Pass/<LOD
2-Methylbutane (Isopentane) 5,000 50 Pass/<LOD 2-Methylpentane (Hexanes) 290 50 Pass/<LOD
2-Methylpropane (Isobutane) 5,000 100 Pass/<LOD 2-propanol (Isopropyl Alcohol) 5,000 50 Pass/99
2-Propanone (Acetone) 5,000 50 Pass/52 3-Methylpentane (Hexanes) 290 50 Pass/<LOD
Acetonitrile 410 100 Pass/<LOD Benzene 2 1 Pass/<LOD
Butane 5,000 100 Pass/109 Chloroform 2 1 Pass/<LOD
Cumene 70 50 Pass/<LOD Cyclohexane 3,880 1,000 Pass/<LOD
Dichloromethane 600 50 Pass/<LOD Dimethylsulfoxide (DMSO) 5,000 500 Pass/<LOD
Ethanol 5,000 500 Pass/<LOD Ethyl acetate 5,000 50 Pass/<LOD
Ethyl ether 5,000 500 Pass/<LOD Ethylene glycol 620 310 Pass/<LOD
Ethylene oxide 50 50 Pass/<LOD Heptane 5,000 50 Pass/<LOD
Hexane 290 290 Pass/<LOD Isopropyl acetate 5,000 50 Pass/<LOD
Methanol 3,000 500 Pass/<LOD Naptha 400 100 Not Tested
N,N-Dimethylacetamide 1,090 100 Pass/<LOD N,N-Dimethylformamide (DMF) 880 500 Pass/<LOD
Pentane 5,000 50 Pass/<LOD Petroleum Ether 400 100 Not Tested
Propane 5,000 100 Pass/<LOD Pyridine 200 10 Pass/<LOD
Sulfolane 160 200 Pass/<LOD Tetrahydrofuran (THF) 720 200 Pass/<LOD
Toluene 890 50 Pass/<LOD Trichloroethylene 25 5 Not Tested
Xylenes* 2,170 50 Pass/<LOD

Total Butanes = 109 ug/g (PASS); Total Pentanes = 0 ug/g (PASS); Total Hexanes = 0 ug/g (PASS)

* Xylenes are reported as the sum of o-xylene, m-xylene, p-xylene, and ethylbenzene
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 52 of 67

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents QC Report
Testing Accreditation #: 4092-004 Test Certificate #: 123371-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Northern Wreck Badder
License: 030-1009646F7F8
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A401030002C949000000017
Metrc Source Pkg#: 1A401030002C949000000016
Test Conditions

Prepsheet ID#: ORHS200402b
Scale: XS205-OR1
Temp: 22.1 °C
Baro PE: 1012 hPa
Analyst: HRM
Technician: HRM
Sample ID#: 123371

Lot #: Northern wreck badder 3/30/20 #1
Batch #: 123371
Batch Weight (g): 1640.4
Harvest/Process Date: 03/31/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 03/31/2020
Test Date: 04/02/2020
Sample #123371
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS Recovery (%) MSD Recovery (%) Relative Percent Difference (%) QC Flag
1,2-Dichloroethane N.D. 0 0 0 nan nan
n-Propane N.D. 250 64 64 25.60 25.60 0.00 LR
Isobutane N.D. 250 101 97 40.40 38.80 4.04 LR
Methanol N.D. 250 177 160 70.80 64.00 10.09 LR
n-Butane N.D. 250 117 119 46.80 47.60 1.69 LR
2,2-Dimethylpropane N.D. 250 126 127 50.40 50.80 0.79 LR
Ethanol N.D. 250 187 185 74.80 74.00 1.08
Isopentane N.D. 250 144 141 57.60 56.40 2.11 LR
Acetonitrile N.D. 250 169 154 67.60 61.60 9.29 LR
Diethyl ether N.D. 250 183 178 73.20 71.20 2.77
2-propanone N.D. 250 207 204 82.80 81.60 1.46
2-propanol N.D. 250 334 341 133.60 136.40 2.07 HR
n-Pentane N.D. 250 153 83 61.20 33.20 59.32 LRQ
2,2-Dimethylbutane N.D. 250 170 171 68.00 68.40 0.59 LR
2,3-Dimethylbutane N.D. 250 158 151 63.20 60.40 4.53 LR
Methylene chloride N.D. 250 190 194 76.00 77.60 2.08
2-Methylpentane N.D. 250 170 171 68.00 68.40 0.59 LR
3-Methylpentane N.D. 250 178 172 71.20 68.80 3.43 LR
2-Butanol N.D. 250 208 208 83.20 83.20 0.00
n-Hexane N.D. 250 180 177 72.00 70.80 1.68
Ethyl acetate N.D. 250 196 199 78.40 79.60 1.52
Tetrahydrofuran N.D. 250 188 183 0.00 0.00 0.00
Trichloroethylene N.D. 0 0 0 nan nan
Isopropyl acetate N.D. 250 196 199 0.00 0.00 0.00
Benzene N.D. 250 196 194 78.40 77.60 1.03
Chloroform N.D. 0 0 0 nan nan
Cyclohexane N.D. 250 186 185 74.40 74.00 0.54
Ethylene glycol N.D. 250 156 197 62.40 78.80 23.23 LRQ
Heptane N.D. 250 159 160 63.60 64.00 0.63 LR
2-Ethoxyethanol N.D. 250 167 190 66.80 76.00 12.89 LR
1,4-Dioxane N.D. 250 199 200 79.60 80.00 0.50
Pyridine N.D. 0 0 0 0.00 0.00 0.00
Toluene N.D. 250 204 198 81.60 79.20 2.99
Chlorobenzene N.D. 0 0 0 0.00 0.00 0.00
Ethylbenzene N.D. 250 207 202 82.80 80.80 2.44
m-Xylene/p-Xylene N.D. 500 412 408 82.40 81.60 0.98
o-Xylene N.D. 250 208 207 83.20 82.80 0.48
Cumene N.D. 250 198 200 79.20 80.00 1.01
Ethylene oxide N.D. 250 184 184 73.60 73.60 0.00

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

N.D. = Not Detected

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 53 of 67

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-004 Test Certificate #: 123371-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Northern Wreck Badder
License: 030-1009646F7F8
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A401030002C949000000017
Metrc Source Pkg#: 1A401030002C949000000016
Test Conditions

Prepsheet ID#: ORHS200402b
Scale: XS205-OR1
Temp: 22.1 °C
Baro PE: 1012 hPa
Analyst: HRM
Technician: HRM
Sample ID#: 123371

Lot #: Northern wreck badder 3/30/20 #1
Batch #: 123371
Batch Weight (g): 1640.4
Harvest/Process Date: 03/31/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 03/31/2020
Test Date: 04/02/2020
Sample #123371
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
1,2-Dichloroethane 2 1 Not Tested 1,2-Dimethoxyethane 100 5 Pass/<LOD
1,4-dioxane 380 200 Pass/<LOD 1-Butanol 5,000 100 Pass/<LOD
1-Pentanol 5,000 100 Pass/<LOD 1-Propanol 5,000 100 Pass/<LOD
2,2-Dimethylpropane (Neopentane) 5,000 100 Pass/<LOD 2,2-Dimethylbutane (Hexanes) 290 100 Pass/<LOD
2,3-Dimethylbutane (Hexanes) 290 100 Pass/<LOD 2-Butanol 5,000 100 Pass/<LOD
2-Butanone (MEK) 5,000 50 Pass/<LOD 2-Ethoxyethanol 160 40 Pass/<LOD
2-Methylbutane (Isopentane) 5,000 50 Pass/<LOD 2-Methylpentane (Hexanes) 290 50 Pass/<LOD
2-Methylpropane (Isobutane) 5,000 100 Pass/<LOD 2-propanol (Isopropyl Alcohol) 5,000 50 Pass/72
2-Propanone (Acetone) 5,000 50 Pass/50 3-Methylpentane (Hexanes) 290 50 Pass/<LOD
Acetonitrile 410 100 Pass/<LOD Benzene 2 1 Pass/<LOD
Butane 5,000 100 Pass/106 Chloroform 2 1 Pass/<LOD
Cumene 70 50 Pass/<LOD Cyclohexane 3,880 1,000 Pass/<LOD
Dichloromethane 600 50 Pass/<LOD Dimethylsulfoxide (DMSO) 5,000 500 Pass/<LOD
Ethanol 5,000 500 Pass/<LOD Ethyl acetate 5,000 50 Pass/<LOD
Ethyl ether 5,000 500 Pass/<LOD Ethylene glycol 620 310 Pass/<LOD
Ethylene oxide 50 50 Pass/<LOD Heptane 5,000 50 Pass/<LOD
Hexane 290 290 Pass/<LOD Isopropyl acetate 5,000 50 Pass/<LOD
Methanol 3,000 500 Pass/<LOD Naptha 400 100 Not Tested
N,N-Dimethylacetamide 1,090 100 Pass/<LOD N,N-Dimethylformamide (DMF) 880 500 Pass/<LOD
Pentane 5,000 50 Pass/<LOD Petroleum Ether 400 100 Not Tested
Propane 5,000 100 Pass/<LOD Pyridine 200 10 Pass/<LOD
Sulfolane 160 200 Pass/<LOD Tetrahydrofuran (THF) 720 200 Pass/<LOD
Toluene 890 50 Pass/<LOD Trichloroethylene 25 5 Not Tested
Xylenes* 2,170 50 Pass/<LOD

Total Butanes = 106 ug/g (PASS); Total Pentanes = 0 ug/g (PASS); Total Hexanes = 0 ug/g (PASS)

* Xylenes are reported as the sum of o-xylene, m-xylene, p-xylene, and ethylbenzene
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 54 of 67

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents QC Report
Testing Accreditation #: 4092-004 Test Certificate #: 123371-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Northern Wreck Badder
License: 030-1009646F7F8
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A401030002C949000000017
Metrc Source Pkg#: 1A401030002C949000000016
Test Conditions

Prepsheet ID#: ORHS200402b
Scale: XS205-OR1
Temp: 22.1 °C
Baro PE: 1012 hPa
Analyst: HRM
Technician: HRM
Sample ID#: 123371

Lot #: Northern wreck badder 3/30/20 #1
Batch #: 123371
Batch Weight (g): 1640.4
Harvest/Process Date: 03/31/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 03/31/2020
Test Date: 04/02/2020
Sample #123371
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS Recovery (%) MSD Recovery (%) Relative Percent Difference (%) QC Flag
1,2-Dichloroethane N.D. 0 0 0 nan nan
n-Propane N.D. 250 64 64 25.60 25.60 0.00 LR
Isobutane N.D. 250 101 97 40.40 38.80 4.04 LR
Methanol N.D. 250 177 160 70.80 64.00 10.09 LR
n-Butane N.D. 250 117 119 46.80 47.60 1.69 LR
2,2-Dimethylpropane N.D. 250 126 127 50.40 50.80 0.79 LR
Ethanol N.D. 250 187 185 74.80 74.00 1.08
Isopentane N.D. 250 144 141 57.60 56.40 2.11 LR
Acetonitrile N.D. 250 169 154 67.60 61.60 9.29 LR
Diethyl ether N.D. 250 183 178 73.20 71.20 2.77
2-propanone N.D. 250 207 204 82.80 81.60 1.46
2-propanol N.D. 250 334 341 133.60 136.40 2.07 HR
n-Pentane N.D. 250 153 83 61.20 33.20 59.32 LRQ
2,2-Dimethylbutane N.D. 250 170 171 68.00 68.40 0.59 LR
2,3-Dimethylbutane N.D. 250 158 151 63.20 60.40 4.53 LR
Methylene chloride N.D. 250 190 194 76.00 77.60 2.08
2-Methylpentane N.D. 250 170 171 68.00 68.40 0.59 LR
3-Methylpentane N.D. 250 178 172 71.20 68.80 3.43 LR
2-Butanol N.D. 250 208 208 83.20 83.20 0.00
n-Hexane N.D. 250 180 177 72.00 70.80 1.68
Ethyl acetate N.D. 250 196 199 78.40 79.60 1.52
Tetrahydrofuran N.D. 250 188 183 0.00 0.00 0.00
Trichloroethylene N.D. 0 0 0 nan nan
Isopropyl acetate N.D. 250 196 199 0.00 0.00 0.00
Benzene N.D. 250 196 194 78.40 77.60 1.03
Chloroform N.D. 0 0 0 nan nan
Cyclohexane N.D. 250 186 185 74.40 74.00 0.54
Ethylene glycol N.D. 250 156 197 62.40 78.80 23.23 LRQ
Heptane N.D. 250 159 160 63.60 64.00 0.63 LR
2-Ethoxyethanol N.D. 250 167 190 66.80 76.00 12.89 LR
1,4-Dioxane N.D. 250 199 200 79.60 80.00 0.50
Pyridine N.D. 0 0 0 0.00 0.00 0.00
Toluene N.D. 250 204 198 81.60 79.20 2.99
Chlorobenzene N.D. 0 0 0 0.00 0.00 0.00
Ethylbenzene N.D. 250 207 202 82.80 80.80 2.44
m-Xylene/p-Xylene N.D. 500 412 408 82.40 81.60 0.98
o-Xylene N.D. 250 208 207 83.20 82.80 0.48
Cumene N.D. 250 198 200 79.20 80.00 1.01
Ethylene oxide N.D. 250 184 184 73.60 73.60 0.00

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

N.D. = Not Detected

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 55 of 67

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-004 Test Certificate #: 123371-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Northern Wreck Badder
License: 030-1009646F7F8
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A401030002C949000000017
Metrc Source Pkg#: 1A401030002C949000000016
Test Conditions

Prepsheet ID#: ORHS200402b
Scale: XS205-OR1
Temp: 22.1 °C
Baro PE: 1012 hPa
Analyst: HRM
Technician: HRM
Sample ID#: 123371

Lot #: Northern wreck badder 3/30/20 #1
Batch #: 123371
Batch Weight (g): 1640.4
Harvest/Process Date: 03/31/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 03/31/2020
Test Date: 04/02/2020
Sample #123371
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
1,2-Dichloroethane 2 1 Not Tested 1,2-Dimethoxyethane 100 5 Pass/<LOD
1,4-dioxane 380 200 Pass/<LOD 1-Butanol 5,000 100 Pass/<LOD
1-Pentanol 5,000 100 Pass/<LOD 1-Propanol 5,000 100 Pass/<LOD
2,2-Dimethylpropane (Neopentane) 5,000 100 Pass/<LOD 2,2-Dimethylbutane (Hexanes) 290 100 Pass/<LOD
2,3-Dimethylbutane (Hexanes) 290 100 Pass/<LOD 2-Butanol 5,000 100 Pass/<LOD
2-Butanone (MEK) 5,000 50 Pass/<LOD 2-Ethoxyethanol 160 40 Pass/<LOD
2-Methylbutane (Isopentane) 5,000 50 Pass/<LOD 2-Methylpentane (Hexanes) 290 50 Pass/<LOD
2-Methylpropane (Isobutane) 5,000 100 Pass/<LOD 2-propanol (Isopropyl Alcohol) 5,000 50 Pass/52
2-Propanone (Acetone) 5,000 50 Pass/51 3-Methylpentane (Hexanes) 290 50 Pass/<LOD
Acetonitrile 410 100 Pass/<LOD Benzene 2 1 Pass/<LOD
Butane 5,000 100 Pass/<LOD Chloroform 2 1 Pass/<LOD
Cumene 70 50 Pass/<LOD Cyclohexane 3,880 1,000 Pass/<LOD
Dichloromethane 600 50 Pass/<LOD Dimethylsulfoxide (DMSO) 5,000 500 Pass/<LOD
Ethanol 5,000 500 Pass/<LOD Ethyl acetate 5,000 50 Pass/<LOD
Ethyl ether 5,000 500 Pass/<LOD Ethylene glycol 620 310 Pass/<LOD
Ethylene oxide 50 50 Pass/<LOD Heptane 5,000 50 Pass/<LOD
Hexane 290 290 Pass/<LOD Isopropyl acetate 5,000 50 Pass/<LOD
Methanol 3,000 500 Pass/<LOD Naptha 400 100 Not Tested
N,N-Dimethylacetamide 1,090 100 Pass/<LOD N,N-Dimethylformamide (DMF) 880 500 Pass/<LOD
Pentane 5,000 50 Pass/<LOD Petroleum Ether 400 100 Not Tested
Propane 5,000 100 Pass/<LOD Pyridine 200 10 Pass/<LOD
Sulfolane 160 200 Pass/<LOD Tetrahydrofuran (THF) 720 200 Pass/<LOD
Toluene 890 50 Pass/<LOD Trichloroethylene 25 5 Not Tested
Xylenes* 2,170 50 Pass/<LOD

Total Butanes = 73 ug/g (PASS); Total Pentanes = 0 ug/g (PASS); Total Hexanes = 0 ug/g (PASS)

* Xylenes are reported as the sum of o-xylene, m-xylene, p-xylene, and ethylbenzene
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 56 of 67

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents QC Report
Testing Accreditation #: 4092-004 Test Certificate #: 123371-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Northern Wreck Badder
License: 030-1009646F7F8
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A401030002C949000000017
Metrc Source Pkg#: 1A401030002C949000000016
Test Conditions

Prepsheet ID#: ORHS200402b
Scale: XS205-OR1
Temp: 22.1 °C
Baro PE: 1012 hPa
Analyst: HRM
Technician: HRM
Sample ID#: 123371

Lot #: Northern wreck badder 3/30/20 #1
Batch #: 123371
Batch Weight (g): 1640.4
Harvest/Process Date: 03/31/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 03/31/2020
Test Date: 04/02/2020
Sample #123371
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS Recovery (%) MSD Recovery (%) Relative Percent Difference (%) QC Flag
1,2-Dichloroethane N.D. 0 0 0 nan nan
n-Propane N.D. 250 64 64 25.60 25.60 0.00 LR
Isobutane N.D. 250 101 97 40.40 38.80 4.04 LR
Methanol N.D. 250 177 160 70.80 64.00 10.09 LR
n-Butane N.D. 250 117 119 46.80 47.60 1.69 LR
2,2-Dimethylpropane N.D. 250 126 127 50.40 50.80 0.79 LR
Ethanol N.D. 250 187 185 74.80 74.00 1.08
Isopentane N.D. 250 144 141 57.60 56.40 2.11 LR
Acetonitrile N.D. 250 169 154 67.60 61.60 9.29 LR
Diethyl ether N.D. 250 183 178 73.20 71.20 2.77
2-propanone N.D. 250 207 204 82.80 81.60 1.46
2-propanol N.D. 250 334 341 133.60 136.40 2.07 HR
n-Pentane N.D. 250 153 83 61.20 33.20 59.32 LRQ
2,2-Dimethylbutane N.D. 250 170 171 68.00 68.40 0.59 LR
2,3-Dimethylbutane N.D. 250 158 151 63.20 60.40 4.53 LR
Methylene chloride N.D. 250 190 194 76.00 77.60 2.08
2-Methylpentane N.D. 250 170 171 68.00 68.40 0.59 LR
3-Methylpentane N.D. 250 178 172 71.20 68.80 3.43 LR
2-Butanol N.D. 250 208 208 83.20 83.20 0.00
n-Hexane N.D. 250 180 177 72.00 70.80 1.68
Ethyl acetate N.D. 250 196 199 78.40 79.60 1.52
Tetrahydrofuran N.D. 250 188 183 0.00 0.00 0.00
Trichloroethylene N.D. 0 0 0 nan nan
Isopropyl acetate N.D. 250 196 199 0.00 0.00 0.00
Benzene N.D. 250 196 194 78.40 77.60 1.03
Chloroform N.D. 0 0 0 nan nan
Cyclohexane N.D. 250 186 185 74.40 74.00 0.54
Ethylene glycol N.D. 250 156 197 62.40 78.80 23.23 LRQ
Heptane N.D. 250 159 160 63.60 64.00 0.63 LR
2-Ethoxyethanol N.D. 250 167 190 66.80 76.00 12.89 LR
1,4-Dioxane N.D. 250 199 200 79.60 80.00 0.50
Pyridine N.D. 0 0 0 0.00 0.00 0.00
Toluene N.D. 250 204 198 81.60 79.20 2.99
Chlorobenzene N.D. 0 0 0 0.00 0.00 0.00
Ethylbenzene N.D. 250 207 202 82.80 80.80 2.44
m-Xylene/p-Xylene N.D. 500 412 408 82.40 81.60 0.98
o-Xylene N.D. 250 208 207 83.20 82.80 0.48
Cumene N.D. 250 198 200 79.20 80.00 1.01
Ethylene oxide N.D. 250 184 184 73.60 73.60 0.00

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

N.D. = Not Detected

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 57 of 67

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-004 Test Certificate #: 123371-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Northern Wreck Badder
License: 030-1009646F7F8
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A401030002C949000000017
Metrc Source Pkg#: 1A401030002C949000000016
Test Conditions

Prepsheet ID#: ORHS200402b
Scale: XS205-OR1
Temp: 22.1 °C
Baro PE: 1012 hPa
Analyst: HRM
Technician: HRM
Sample ID#: 123371

Lot #: Northern wreck badder 3/30/20 #1
Batch #: 123371
Batch Weight (g): 1640.4
Harvest/Process Date: 03/31/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 03/31/2020
Test Date: 04/02/2020
Sample #123371
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
1,2-Dichloroethane 2 1 Not Tested 1,2-Dimethoxyethane 100 5 Pass/<LOD
1,4-dioxane 380 200 Pass/<LOD 1-Butanol 5,000 100 Pass/<LOD
1-Pentanol 5,000 100 Pass/<LOD 1-Propanol 5,000 100 Pass/<LOD
2,2-Dimethylpropane (Neopentane) 5,000 100 Pass/<LOD 2,2-Dimethylbutane (Hexanes) 290 100 Pass/<LOD
2,3-Dimethylbutane (Hexanes) 290 100 Pass/<LOD 2-Butanol 5,000 100 Pass/<LOD
2-Butanone (MEK) 5,000 50 Pass/<LOD 2-Ethoxyethanol 160 40 Pass/<LOD
2-Methylbutane (Isopentane) 5,000 50 Pass/<LOD 2-Methylpentane (Hexanes) 290 50 Pass/<LOD
2-Methylpropane (Isobutane) 5,000 100 Pass/<LOD 2-propanol (Isopropyl Alcohol) 5,000 50 Pass/100
2-Propanone (Acetone) 5,000 50 Pass/52 3-Methylpentane (Hexanes) 290 50 Pass/<LOD
Acetonitrile 410 100 Pass/<LOD Benzene 2 1 Pass/<LOD
Butane 5,000 100 Pass/114 Chloroform 2 1 Pass/<LOD
Cumene 70 50 Pass/<LOD Cyclohexane 3,880 1,000 Pass/<LOD
Dichloromethane 600 50 Pass/<LOD Dimethylsulfoxide (DMSO) 5,000 500 Pass/<LOD
Ethanol 5,000 500 Pass/<LOD Ethyl acetate 5,000 50 Pass/<LOD
Ethyl ether 5,000 500 Pass/<LOD Ethylene glycol 620 310 Pass/<LOD
Ethylene oxide 50 50 Pass/<LOD Heptane 5,000 50 Pass/<LOD
Hexane 290 290 Pass/<LOD Isopropyl acetate 5,000 50 Pass/<LOD
Methanol 3,000 500 Pass/<LOD Naptha 400 100 Not Tested
N,N-Dimethylacetamide 1,090 100 Pass/<LOD N,N-Dimethylformamide (DMF) 880 500 Pass/<LOD
Pentane 5,000 50 Pass/<LOD Petroleum Ether 400 100 Not Tested
Propane 5,000 100 Pass/<LOD Pyridine 200 10 Pass/<LOD
Sulfolane 160 200 Pass/<LOD Tetrahydrofuran (THF) 720 200 Pass/<LOD
Toluene 890 50 Pass/<LOD Trichloroethylene 25 5 Not Tested
Xylenes* 2,170 50 Pass/<LOD

Total Butanes = 114 ug/g (PASS); Total Pentanes = 0 ug/g (PASS); Total Hexanes = 0 ug/g (PASS)

* Xylenes are reported as the sum of o-xylene, m-xylene, p-xylene, and ethylbenzene
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 58 of 67

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents QC Report
Testing Accreditation #: 4092-004 Test Certificate #: 123371-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Northern Wreck Badder
License: 030-1009646F7F8
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A401030002C949000000017
Metrc Source Pkg#: 1A401030002C949000000016
Test Conditions

Prepsheet ID#: ORHS200402b
Scale: XS205-OR1
Temp: 22.1 °C
Baro PE: 1012 hPa
Analyst: HRM
Technician: HRM
Sample ID#: 123371

Lot #: Northern wreck badder 3/30/20 #1
Batch #: 123371
Batch Weight (g): 1640.4
Harvest/Process Date: 03/31/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 03/31/2020
Test Date: 04/02/2020
Sample #123371
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS Recovery (%) MSD Recovery (%) Relative Percent Difference (%) QC Flag
1,2-Dichloroethane N.D. 0 0 0 nan nan
n-Propane N.D. 250 64 64 25.60 25.60 0.00 LR
Isobutane N.D. 250 101 97 40.40 38.80 4.04 LR
Methanol N.D. 250 177 160 70.80 64.00 10.09 LR
n-Butane N.D. 250 117 119 46.80 47.60 1.69 LR
2,2-Dimethylpropane N.D. 250 126 127 50.40 50.80 0.79 LR
Ethanol N.D. 250 187 185 74.80 74.00 1.08
Isopentane N.D. 250 144 141 57.60 56.40 2.11 LR
Acetonitrile N.D. 250 169 154 67.60 61.60 9.29 LR
Diethyl ether N.D. 250 183 178 73.20 71.20 2.77
2-propanone N.D. 250 207 204 82.80 81.60 1.46
2-propanol N.D. 250 334 341 133.60 136.40 2.07 HR
n-Pentane N.D. 250 153 83 61.20 33.20 59.32 LRQ
2,2-Dimethylbutane N.D. 250 170 171 68.00 68.40 0.59 LR
2,3-Dimethylbutane N.D. 250 158 151 63.20 60.40 4.53 LR
Methylene chloride N.D. 250 190 194 76.00 77.60 2.08
2-Methylpentane N.D. 250 170 171 68.00 68.40 0.59 LR
3-Methylpentane N.D. 250 178 172 71.20 68.80 3.43 LR
2-Butanol N.D. 250 208 208 83.20 83.20 0.00
n-Hexane N.D. 250 180 177 72.00 70.80 1.68
Ethyl acetate N.D. 250 196 199 78.40 79.60 1.52
Tetrahydrofuran N.D. 250 188 183 0.00 0.00 0.00
Trichloroethylene N.D. 0 0 0 nan nan
Isopropyl acetate N.D. 250 196 199 0.00 0.00 0.00
Benzene N.D. 250 196 194 78.40 77.60 1.03
Chloroform N.D. 0 0 0 nan nan
Cyclohexane N.D. 250 186 185 74.40 74.00 0.54
Ethylene glycol N.D. 250 156 197 62.40 78.80 23.23 LRQ
Heptane N.D. 250 159 160 63.60 64.00 0.63 LR
2-Ethoxyethanol N.D. 250 167 190 66.80 76.00 12.89 LR
1,4-Dioxane N.D. 250 199 200 79.60 80.00 0.50
Pyridine N.D. 0 0 0 0.00 0.00 0.00
Toluene N.D. 250 204 198 81.60 79.20 2.99
Chlorobenzene N.D. 0 0 0 0.00 0.00 0.00
Ethylbenzene N.D. 250 207 202 82.80 80.80 2.44
m-Xylene/p-Xylene N.D. 500 412 408 82.40 81.60 0.98
o-Xylene N.D. 250 208 207 83.20 82.80 0.48
Cumene N.D. 250 198 200 79.20 80.00 1.01
Ethylene oxide N.D. 250 184 184 73.60 73.60 0.00

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

N.D. = Not Detected

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 59 of 67

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-004 Test Certificate #: 123371-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Northern Wreck Badder
License: 030-1009646F7F8
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A401030002C949000000017
Metrc Source Pkg#: 1A401030002C949000000016
Test Conditions

Prepsheet ID#: ORHS200402b
Scale: XS205-OR1
Temp: 22.1 °C
Baro PE: 1012 hPa
Analyst: HRM
Technician: HRM
Sample ID#: 123371

Lot #: Northern wreck badder 3/30/20 #1
Batch #: 123371
Batch Weight (g): 1640.4
Harvest/Process Date: 03/31/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 03/31/2020
Test Date: 04/02/2020
Sample #123371
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
1,2-Dichloroethane 2 1 Not Tested 1,2-Dimethoxyethane 100 5 Pass/<LOD
1,4-dioxane 380 200 Pass/<LOD 1-Butanol 5,000 100 Pass/<LOD
1-Pentanol 5,000 100 Pass/<LOD 1-Propanol 5,000 100 Pass/<LOD
2,2-Dimethylpropane (Neopentane) 5,000 100 Pass/<LOD 2,2-Dimethylbutane (Hexanes) 290 100 Pass/<LOD
2,3-Dimethylbutane (Hexanes) 290 100 Pass/<LOD 2-Butanol 5,000 100 Pass/<LOD
2-Butanone (MEK) 5,000 50 Pass/<LOD 2-Ethoxyethanol 160 40 Pass/<LOD
2-Methylbutane (Isopentane) 5,000 50 Pass/<LOD 2-Methylpentane (Hexanes) 290 50 Pass/<LOD
2-Methylpropane (Isobutane) 5,000 100 Pass/<LOD 2-propanol (Isopropyl Alcohol) 5,000 50 Pass/101
2-Propanone (Acetone) 5,000 50 Pass/<LOD 3-Methylpentane (Hexanes) 290 50 Pass/<LOD
Acetonitrile 410 100 Pass/<LOD Benzene 2 1 Pass/<LOD
Butane 5,000 100 Pass/137 Chloroform 2 1 Pass/<LOD
Cumene 70 50 Pass/<LOD Cyclohexane 3,880 1,000 Pass/<LOD
Dichloromethane 600 50 Pass/<LOD Dimethylsulfoxide (DMSO) 5,000 500 Pass/<LOD
Ethanol 5,000 500 Pass/<LOD Ethyl acetate 5,000 50 Pass/<LOD
Ethyl ether 5,000 500 Pass/<LOD Ethylene glycol 620 310 Pass/<LOD
Ethylene oxide 50 50 Pass/<LOD Heptane 5,000 50 Pass/<LOD
Hexane 290 290 Pass/<LOD Isopropyl acetate 5,000 50 Pass/<LOD
Methanol 3,000 500 Pass/<LOD Naptha 400 100 Not Tested
N,N-Dimethylacetamide 1,090 100 Pass/<LOD N,N-Dimethylformamide (DMF) 880 500 Pass/<LOD
Pentane 5,000 50 Pass/<LOD Petroleum Ether 400 100 Not Tested
Propane 5,000 100 Pass/<LOD Pyridine 200 10 Pass/<LOD
Sulfolane 160 200 Pass/<LOD Tetrahydrofuran (THF) 720 200 Pass/<LOD
Toluene 890 50 Pass/<LOD Trichloroethylene 25 5 Not Tested
Xylenes* 2,170 50 Pass/<LOD

Total Butanes = 137 ug/g (PASS); Total Pentanes = 0 ug/g (PASS); Total Hexanes = 0 ug/g (PASS)

* Xylenes are reported as the sum of o-xylene, m-xylene, p-xylene, and ethylbenzene
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 60 of 67

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents QC Report
Testing Accreditation #: 4092-004 Test Certificate #: 123371-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Northern Wreck Badder
License: 030-1009646F7F8
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A401030002C949000000017
Metrc Source Pkg#: 1A401030002C949000000016
Test Conditions

Prepsheet ID#: ORHS200402b
Scale: XS205-OR1
Temp: 22.1 °C
Baro PE: 1012 hPa
Analyst: HRM
Technician: HRM
Sample ID#: 123371

Lot #: Northern wreck badder 3/30/20 #1
Batch #: 123371
Batch Weight (g): 1640.4
Harvest/Process Date: 03/31/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 03/31/2020
Test Date: 04/02/2020
Sample #123371
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS Recovery (%) MSD Recovery (%) Relative Percent Difference (%) QC Flag
1,2-Dichloroethane N.D. 0 0 0 nan nan
n-Propane N.D. 250 64 64 25.60 25.60 0.00 LR
Isobutane N.D. 250 101 97 40.40 38.80 4.04 LR
Methanol N.D. 250 177 160 70.80 64.00 10.09 LR
n-Butane N.D. 250 117 119 46.80 47.60 1.69 LR
2,2-Dimethylpropane N.D. 250 126 127 50.40 50.80 0.79 LR
Ethanol N.D. 250 187 185 74.80 74.00 1.08
Isopentane N.D. 250 144 141 57.60 56.40 2.11 LR
Acetonitrile N.D. 250 169 154 67.60 61.60 9.29 LR
Diethyl ether N.D. 250 183 178 73.20 71.20 2.77
2-propanone N.D. 250 207 204 82.80 81.60 1.46
2-propanol N.D. 250 334 341 133.60 136.40 2.07 HR
n-Pentane N.D. 250 153 83 61.20 33.20 59.32 LRQ
2,2-Dimethylbutane N.D. 250 170 171 68.00 68.40 0.59 LR
2,3-Dimethylbutane N.D. 250 158 151 63.20 60.40 4.53 LR
Methylene chloride N.D. 250 190 194 76.00 77.60 2.08
2-Methylpentane N.D. 250 170 171 68.00 68.40 0.59 LR
3-Methylpentane N.D. 250 178 172 71.20 68.80 3.43 LR
2-Butanol N.D. 250 208 208 83.20 83.20 0.00
n-Hexane N.D. 250 180 177 72.00 70.80 1.68
Ethyl acetate N.D. 250 196 199 78.40 79.60 1.52
Tetrahydrofuran N.D. 250 188 183 0.00 0.00 0.00
Trichloroethylene N.D. 0 0 0 nan nan
Isopropyl acetate N.D. 250 196 199 0.00 0.00 0.00
Benzene N.D. 250 196 194 78.40 77.60 1.03
Chloroform N.D. 0 0 0 nan nan
Cyclohexane N.D. 250 186 185 74.40 74.00 0.54
Ethylene glycol N.D. 250 156 197 62.40 78.80 23.23 LRQ
Heptane N.D. 250 159 160 63.60 64.00 0.63 LR
2-Ethoxyethanol N.D. 250 167 190 66.80 76.00 12.89 LR
1,4-Dioxane N.D. 250 199 200 79.60 80.00 0.50
Pyridine N.D. 0 0 0 0.00 0.00 0.00
Toluene N.D. 250 204 198 81.60 79.20 2.99
Chlorobenzene N.D. 0 0 0 0.00 0.00 0.00
Ethylbenzene N.D. 250 207 202 82.80 80.80 2.44
m-Xylene/p-Xylene N.D. 500 412 408 82.40 81.60 0.98
o-Xylene N.D. 250 208 207 83.20 82.80 0.48
Cumene N.D. 250 198 200 79.20 80.00 1.01
Ethylene oxide N.D. 250 184 184 73.60 73.60 0.00

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

N.D. = Not Detected

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 61 of 67

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-004 Test Certificate #: 123371-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Northern Wreck Badder
License: 030-1009646F7F8
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A401030002C949000000017
Metrc Source Pkg#: 1A401030002C949000000016
Test Conditions

Prepsheet ID#: ORHS200402b
Scale: XS205-OR1
Temp: 22.1 °C
Baro PE: 1012 hPa
Analyst: HRM
Technician: HRM
Sample ID#: 123371

Lot #: Northern wreck badder 3/30/20 #1
Batch #: 123371
Batch Weight (g): 1640.4
Harvest/Process Date: 03/31/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 03/31/2020
Test Date: 04/02/2020
Sample #123371
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
1,2-Dichloroethane 2 1 Not Tested 1,2-Dimethoxyethane 100 5 Pass/<LOD
1,4-dioxane 380 200 Pass/<LOD 1-Butanol 5,000 100 Pass/<LOD
1-Pentanol 5,000 100 Pass/<LOD 1-Propanol 5,000 100 Pass/<LOD
2,2-Dimethylpropane (Neopentane) 5,000 100 Pass/<LOD 2,2-Dimethylbutane (Hexanes) 290 100 Pass/<LOD
2,3-Dimethylbutane (Hexanes) 290 100 Pass/<LOD 2-Butanol 5,000 100 Pass/<LOD
2-Butanone (MEK) 5,000 50 Pass/<LOD 2-Ethoxyethanol 160 40 Pass/<LOD
2-Methylbutane (Isopentane) 5,000 50 Pass/<LOD 2-Methylpentane (Hexanes) 290 50 Pass/<LOD
2-Methylpropane (Isobutane) 5,000 100 Pass/<LOD 2-propanol (Isopropyl Alcohol) 5,000 50 Pass/108
2-Propanone (Acetone) 5,000 50 Pass/51 3-Methylpentane (Hexanes) 290 50 Pass/<LOD
Acetonitrile 410 100 Pass/<LOD Benzene 2 1 Pass/<LOD
Butane 5,000 100 Pass/113 Chloroform 2 1 Pass/<LOD
Cumene 70 50 Pass/<LOD Cyclohexane 3,880 1,000 Pass/<LOD
Dichloromethane 600 50 Pass/<LOD Dimethylsulfoxide (DMSO) 5,000 500 Pass/<LOD
Ethanol 5,000 500 Pass/<LOD Ethyl acetate 5,000 50 Pass/<LOD
Ethyl ether 5,000 500 Pass/<LOD Ethylene glycol 620 310 Pass/<LOD
Ethylene oxide 50 50 Pass/<LOD Heptane 5,000 50 Pass/<LOD
Hexane 290 290 Pass/<LOD Isopropyl acetate 5,000 50 Pass/<LOD
Methanol 3,000 500 Pass/<LOD Naptha 400 100 Not Tested
N,N-Dimethylacetamide 1,090 100 Pass/<LOD N,N-Dimethylformamide (DMF) 880 500 Pass/<LOD
Pentane 5,000 50 Pass/<LOD Petroleum Ether 400 100 Not Tested
Propane 5,000 100 Pass/<LOD Pyridine 200 10 Pass/<LOD
Sulfolane 160 200 Pass/<LOD Tetrahydrofuran (THF) 720 200 Pass/<LOD
Toluene 890 50 Pass/<LOD Trichloroethylene 25 5 Not Tested
Xylenes* 2,170 50 Pass/<LOD

Total Butanes = 113 ug/g (PASS); Total Pentanes = 0 ug/g (PASS); Total Hexanes = 0 ug/g (PASS)

* Xylenes are reported as the sum of o-xylene, m-xylene, p-xylene, and ethylbenzene
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 62 of 67

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents QC Report
Testing Accreditation #: 4092-004 Test Certificate #: 123371-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Northern Wreck Badder
License: 030-1009646F7F8
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A401030002C949000000017
Metrc Source Pkg#: 1A401030002C949000000016
Test Conditions

Prepsheet ID#: ORHS200402b
Scale: XS205-OR1
Temp: 22.1 °C
Baro PE: 1012 hPa
Analyst: HRM
Technician: HRM
Sample ID#: 123371

Lot #: Northern wreck badder 3/30/20 #1
Batch #: 123371
Batch Weight (g): 1640.4
Harvest/Process Date: 03/31/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 03/31/2020
Test Date: 04/02/2020
Sample #123371
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS Recovery (%) MSD Recovery (%) Relative Percent Difference (%) QC Flag
1,2-Dichloroethane N.D. 0 0 0 nan nan
n-Propane N.D. 250 64 64 25.60 25.60 0.00 LR
Isobutane N.D. 250 101 97 40.40 38.80 4.04 LR
Methanol N.D. 250 177 160 70.80 64.00 10.09 LR
n-Butane N.D. 250 117 119 46.80 47.60 1.69 LR
2,2-Dimethylpropane N.D. 250 126 127 50.40 50.80 0.79 LR
Ethanol N.D. 250 187 185 74.80 74.00 1.08
Isopentane N.D. 250 144 141 57.60 56.40 2.11 LR
Acetonitrile N.D. 250 169 154 67.60 61.60 9.29 LR
Diethyl ether N.D. 250 183 178 73.20 71.20 2.77
2-propanone N.D. 250 207 204 82.80 81.60 1.46
2-propanol N.D. 250 334 341 133.60 136.40 2.07 HR
n-Pentane N.D. 250 153 83 61.20 33.20 59.32 LRQ
2,2-Dimethylbutane N.D. 250 170 171 68.00 68.40 0.59 LR
2,3-Dimethylbutane N.D. 250 158 151 63.20 60.40 4.53 LR
Methylene chloride N.D. 250 190 194 76.00 77.60 2.08
2-Methylpentane N.D. 250 170 171 68.00 68.40 0.59 LR
3-Methylpentane N.D. 250 178 172 71.20 68.80 3.43 LR
2-Butanol N.D. 250 208 208 83.20 83.20 0.00
n-Hexane N.D. 250 180 177 72.00 70.80 1.68
Ethyl acetate N.D. 250 196 199 78.40 79.60 1.52
Tetrahydrofuran N.D. 250 188 183 0.00 0.00 0.00
Trichloroethylene N.D. 0 0 0 nan nan
Isopropyl acetate N.D. 250 196 199 0.00 0.00 0.00
Benzene N.D. 250 196 194 78.40 77.60 1.03
Chloroform N.D. 0 0 0 nan nan
Cyclohexane N.D. 250 186 185 74.40 74.00 0.54
Ethylene glycol N.D. 250 156 197 62.40 78.80 23.23 LRQ
Heptane N.D. 250 159 160 63.60 64.00 0.63 LR
2-Ethoxyethanol N.D. 250 167 190 66.80 76.00 12.89 LR
1,4-Dioxane N.D. 250 199 200 79.60 80.00 0.50
Pyridine N.D. 0 0 0 0.00 0.00 0.00
Toluene N.D. 250 204 198 81.60 79.20 2.99
Chlorobenzene N.D. 0 0 0 0.00 0.00 0.00
Ethylbenzene N.D. 250 207 202 82.80 80.80 2.44
m-Xylene/p-Xylene N.D. 500 412 408 82.40 81.60 0.98
o-Xylene N.D. 250 208 207 83.20 82.80 0.48
Cumene N.D. 250 198 200 79.20 80.00 1.01
Ethylene oxide N.D. 250 184 184 73.60 73.60 0.00

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

N.D. = Not Detected

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 63 of 67

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents Analysis by
Mass Spectrometer
Testing Accreditation #: 4092-004 Test Certificate #: 123371-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Northern Wreck Badder
License: 030-1009646F7F8
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A401030002C949000000017
Metrc Source Pkg#: 1A401030002C949000000016
Test Conditions

Prepsheet ID#: ORHS200402b
Scale: XS205-OR1
Temp: 22.1 °C
Baro PE: 1012 hPa
Analyst: HRM
Technician: HRM
Sample ID#: 123371

Lot #: Northern wreck badder 3/30/20 #1
Batch #: 123371
Batch Weight (g): 1640.4
Harvest/Process Date: 03/31/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 03/31/2020
Test Date: 04/02/2020
Sample #123371
Compound MRL (µg/g) LOD (µg/g) Status (µg/g)   Compound MRL (µg/g) LOD (µg/g) Status (µg/g)
1,2-Dichloroethane 2 1 Not Tested 1,2-Dimethoxyethane 100 5 Pass/<LOD
1,4-dioxane 380 200 Pass/<LOD 1-Butanol 5,000 100 Pass/<LOD
1-Pentanol 5,000 100 Pass/<LOD 1-Propanol 5,000 100 Pass/<LOD
2,2-Dimethylpropane (Neopentane) 5,000 100 Pass/<LOD 2,2-Dimethylbutane (Hexanes) 290 100 Pass/<LOD
2,3-Dimethylbutane (Hexanes) 290 100 Pass/<LOD 2-Butanol 5,000 100 Pass/<LOD
2-Butanone (MEK) 5,000 50 Pass/<LOD 2-Ethoxyethanol 160 40 Pass/<LOD
2-Methylbutane (Isopentane) 5,000 50 Pass/<LOD 2-Methylpentane (Hexanes) 290 50 Pass/<LOD
2-Methylpropane (Isobutane) 5,000 100 Pass/<LOD 2-propanol (Isopropyl Alcohol) 5,000 50 Pass/88
2-Propanone (Acetone) 5,000 50 Pass/50 3-Methylpentane (Hexanes) 290 50 Pass/<LOD
Acetonitrile 410 100 Pass/<LOD Benzene 2 1 Pass/<LOD
Butane 5,000 100 Pass/<LOD Chloroform 2 1 Pass/<LOD
Cumene 70 50 Pass/<LOD Cyclohexane 3,880 1,000 Pass/<LOD
Dichloromethane 600 50 Pass/<LOD Dimethylsulfoxide (DMSO) 5,000 500 Pass/<LOD
Ethanol 5,000 500 Pass/<LOD Ethyl acetate 5,000 50 Pass/<LOD
Ethyl ether 5,000 500 Pass/<LOD Ethylene glycol 620 310 Pass/<LOD
Ethylene oxide 50 50 Pass/<LOD Heptane 5,000 50 Pass/<LOD
Hexane 290 290 Pass/<LOD Isopropyl acetate 5,000 50 Pass/<LOD
Methanol 3,000 500 Pass/<LOD Naptha 400 100 Not Tested
N,N-Dimethylacetamide 1,090 100 Pass/<LOD N,N-Dimethylformamide (DMF) 880 500 Pass/<LOD
Pentane 5,000 50 Pass/<LOD Petroleum Ether 400 100 Not Tested
Propane 5,000 100 Pass/<LOD Pyridine 200 10 Pass/<LOD
Sulfolane 160 200 Pass/<LOD Tetrahydrofuran (THF) 720 200 Pass/<LOD
Toluene 890 50 Pass/<LOD Trichloroethylene 25 5 Not Tested
Xylenes* 2,170 50 Pass/<LOD

Total Butanes = 78 ug/g (PASS); Total Pentanes = 0 ug/g (PASS); Total Hexanes = 0 ug/g (PASS)

* Xylenes are reported as the sum of o-xylene, m-xylene, p-xylene, and ethylbenzene
MRL - Maximum Residue Limit; LOD - Limit of Detection

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 64 of 67

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Residual Solvents QC Report
Testing Accreditation #: 4092-004 Test Certificate #: 123371-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Northern Wreck Badder
License: 030-1009646F7F8
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A401030002C949000000017
Metrc Source Pkg#: 1A401030002C949000000016
Test Conditions

Prepsheet ID#: ORHS200402b
Scale: XS205-OR1
Temp: 22.1 °C
Baro PE: 1012 hPa
Analyst: HRM
Technician: HRM
Sample ID#: 123371

Lot #: Northern wreck badder 3/30/20 #1
Batch #: 123371
Batch Weight (g): 1640.4
Harvest/Process Date: 03/31/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 03/31/2020
Test Date: 04/02/2020
Sample #123371
Target Compound Name Method Blank (μg/g) QC Spike (μg/g) Matrix Spike (μg/g) Matrix Spike Duplicate (μg/g) MS Recovery (%) MSD Recovery (%) Relative Percent Difference (%) QC Flag
1,2-Dichloroethane N.D. 0 0 0 nan nan
n-Propane N.D. 250 64 64 25.60 25.60 0.00 LR
Isobutane N.D. 250 101 97 40.40 38.80 4.04 LR
Methanol N.D. 250 177 160 70.80 64.00 10.09 LR
n-Butane N.D. 250 117 119 46.80 47.60 1.69 LR
2,2-Dimethylpropane N.D. 250 126 127 50.40 50.80 0.79 LR
Ethanol N.D. 250 187 185 74.80 74.00 1.08
Isopentane N.D. 250 144 141 57.60 56.40 2.11 LR
Acetonitrile N.D. 250 169 154 67.60 61.60 9.29 LR
Diethyl ether N.D. 250 183 178 73.20 71.20 2.77
2-propanone N.D. 250 207 204 82.80 81.60 1.46
2-propanol N.D. 250 334 341 133.60 136.40 2.07 HR
n-Pentane N.D. 250 153 83 61.20 33.20 59.32 LRQ
2,2-Dimethylbutane N.D. 250 170 171 68.00 68.40 0.59 LR
2,3-Dimethylbutane N.D. 250 158 151 63.20 60.40 4.53 LR
Methylene chloride N.D. 250 190 194 76.00 77.60 2.08
2-Methylpentane N.D. 250 170 171 68.00 68.40 0.59 LR
3-Methylpentane N.D. 250 178 172 71.20 68.80 3.43 LR
2-Butanol N.D. 250 208 208 83.20 83.20 0.00
n-Hexane N.D. 250 180 177 72.00 70.80 1.68
Ethyl acetate N.D. 250 196 199 78.40 79.60 1.52
Tetrahydrofuran N.D. 250 188 183 0.00 0.00 0.00
Trichloroethylene N.D. 0 0 0 nan nan
Isopropyl acetate N.D. 250 196 199 0.00 0.00 0.00
Benzene N.D. 250 196 194 78.40 77.60 1.03
Chloroform N.D. 0 0 0 nan nan
Cyclohexane N.D. 250 186 185 74.40 74.00 0.54
Ethylene glycol N.D. 250 156 197 62.40 78.80 23.23 LRQ
Heptane N.D. 250 159 160 63.60 64.00 0.63 LR
2-Ethoxyethanol N.D. 250 167 190 66.80 76.00 12.89 LR
1,4-Dioxane N.D. 250 199 200 79.60 80.00 0.50
Pyridine N.D. 0 0 0 0.00 0.00 0.00
Toluene N.D. 250 204 198 81.60 79.20 2.99
Chlorobenzene N.D. 0 0 0 0.00 0.00 0.00
Ethylbenzene N.D. 250 207 202 82.80 80.80 2.44
m-Xylene/p-Xylene N.D. 500 412 408 82.40 81.60 0.98
o-Xylene N.D. 250 208 207 83.20 82.80 0.48
Cumene N.D. 250 198 200 79.20 80.00 1.01
Ethylene oxide N.D. 250 184 184 73.60 73.60 0.00

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

R = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery could indicate there is actually more compound present than detected; while high recoveries should be scrutinized for possible fails as more compound may be detected than is actually residual on the sample.

N.D. = Not Detected

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 65 of 67

ORELAP     IRON Laboratories     NELAP Accredited Laboratory

ORELAP Cert No. 4092-004
OLCC No. 1002158CD2E

Oregon Compliant Homogeneity Report by
High Performance Liquid Chromatography
Testing Accreditation #: 4092-004 Test Certificate #: 123371-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Northern Wreck Badder
License: 030-1009646F7F8
Type: AU Tincture
Metrc Test Pkg#: 1A401030002C949000000017
Metrc Source Pkg#: 1A401030002C949000000016
Sample ID#: 123371

Lot #: Northern wreck badder 3/30/20 #1
Batch #: 123371
Batch Weight (g): 1640.4
Harvest/Process Date: 03/31/2020
Serving Size (g): 0.05
Package Weight (g):1
Date Received: 03/31/2020
Sample #123371
Increments Tested (mg/g) TOTAL THC TOTAL CBD THC THCA THCV CBD CBC CBDA CBDV CBG CBN
Increment 1 675.53 12.28 27.57 738.84 N.D. N.D. N.D. 14.00 N.D. 4.13 2.02
Increment 2 694.57 15.26 28.88 759.05 N.D. N.D. N.D. 17.40 N.D. 4.79 2.26
Increment 3 625.45 14.45 27.12 682.25 N.D. N.D. N.D. 16.48 N.D. 4.56 1.98
Increment 4 661.02 13.85 29.73 719.83 N.D. N.D. N.D. 15.79 N.D. 4.50 2.12
Increment 5 650.98 13.40 28.02 710.33 N.D. N.D. N.D. 15.28 N.D. 4.36 2.00
Increment 6 661.44 13.34 30.29 719.67 N.D. N.D. N.D. 15.21 N.D. 4.35 2.04
Increment 7 628.00 13.94 25.53 686.97 N.D. N.D. N.D. 15.90 N.D. 4.36 2.03
Increment 8 653.71 15.61 31.71 709.24 N.D. N.D. N.D. 17.80 N.D. 4.93 2.12
Increment 9 612.39 15.40 30.94 663.00 N.D. N.D. N.D. 17.56 N.D. 4.78 1.95
Increment 10 644.04 15.91 29.17 701.11 N.D. N.D. N.D. 18.14 N.D. 4.82 2.12
Increment 11 669.71 13.79 30.26 729.13 N.D. N.D. N.D. 15.72 N.D. 4.49 2.06
Increment 12 639.04 13.64 31.39 692.87 N.D. N.D. N.D. 15.55 N.D. 4.41 2.03
Increment 13 652.87 14.44 30.47 709.69 N.D. N.D. N.D. 16.46 N.D. 4.52 2.07
Increment 14 612.83 13.43 27.32 667.63 N.D. N.D. N.D. 15.31 N.D. 4.26 1.87
Increment 15 665.60 14.98 30.17 724.55 N.D. N.D. N.D. 17.08 N.D. 4.64 2.12
Increment 16 627.76 13.98 28.85 682.91 N.D. N.D. N.D. 15.94 N.D. 4.45 1.99
Average Value 648.43 14.23 29.21 706.07 N.D. N.D. N.D. 16.23 N.D. 4.52 2.05
Max Value 694.57 15.91 31.71 759.05 N.D. N.D. N.D. 18.14 N.D. 4.93 2.26
Min Value 612.39 12.28 25.53 663.00 N.D. N.D. N.D. 14.00 N.D. 4.13 1.87
Relative Standard Deviation (RSD) ±3.46% ±6.71% ±5.73% ±3.57% N.D. N.D. N.D. ±6.71% N.D. ±4.73% ±4.22%
Average Cannabinoids Per Package 648.43 14.23 29.21 706.07 N.D. N.D. N.D. 16.23 N.D. 4.52 2.05
Average Cannabinoids Per Serving 32.42 0.71 1.46 35.30 N.D. N.D. N.D. 0.81 N.D. 0.23 0.10
Max Concentration Per Serving (THC)   Pass
Max Concentration Per Package (THC)   Pass
Relative Standard Deviation (RSD)   Pass
Control Study   Yes, In progress
Field Duplicate   N/A

N.D. = Not Detected, Min = Minimum, Max = Maximum

RPD is the relative percent difference between increment 1 and increment 2.

RSD is the relative standard deviation between all increments tested.

Total THC and CBD is the calculated sum of CBD or THC and the amount of CBD or THC derived from CBDA or THCA, respectively. These values are calculated by adding a molar correction factor of 0.877 to the CBDA or THCA value.

SOP FE-01-OR9 was used in accordance with OAR 333-007 for sampling. All marijuana items are sampled and tested in accordance with OAR 333-007-0300 to 333-007-490 and OAR 333-064-0100 to 333-064-0110.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Iron Labs Oregon complies with 2009 TNI Environmental Laboratory Standards.

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

Page 66 of 67
IRON Laboratories

Terpene Report by
Mass Spectrometer
Test Certificate #: 123371-001
Client Name, Sample Details

Hash Hamilton Extracts
Salem, OR 97301
Sample: Northern Wreck Badder
License: 030-1009646F7F8
Type: AU Tincture
Method: SOP FE-44-OR3
Metrc Test Pkg#: 1A401030002C949000000017
Metrc Source Pkg#: 1A401030002C949000000016

Test Conditions

Scale: XS205-OR1
Temp: 21.9 °C
Baro Pressure: 979.2 hPa
Analyst: HRM
Technician: HRM

Sample ID#: 123371

Lot #: Northern wreck badder 3/30/20 #1
Batch #: 123371
Batch Weight (g): 1640.4
Harvest/Process Date: 03/31/2020
Serving Size (g): 0.05
Date Received: 03/31/2020

Sample #123371
Sample #123371
  • α-Pinene (0.04%)
  • β-Ocimene (0.21%)
  • Camphene (0.00%)
  • Eucalyptol (1,8-Cineol) (0.00%)
  • Sabinene (0.00%)
  • γ-Terpinene (0.02%)
  • Myrcene (1.07%)
  • α-Terpinolene (0.06%)
  • β-Pinene (0.07%)
  • Linalool (0.20%)
  • ∆3-Carene (0.00%)
  • Fenchone (0.00%)
  • α-Terpinene (0.03%)
  • endo-Fenchol (0.04%)
  • α-Ocimene (0.02%)
  • Isopulegol (0.00%)
  • Limonene (0.31%)
  • Geraniol (0.00%)
  • p-Cymene (0.00%)
  • β-Caryophyllene (2.24%)
  • α-Humulene (0.81%)
  • Nerolidol 1 (cis) (0.00%)
  • Nerolidol 2 (trans) (0.06%)
  • Guaiol (0.29%)
  • Caryophyllene Oxide (0.00%)
  • α-Bisabolol (0.44%)
  • α-Phellandrene (0.06%)
  • α-Terpineol (0.02%)
  • Valenence (0.29%)

Total: 6.280%

Predominant Terpenes

2.24%   β-Caryophyllene Sweet, woody, spicy, clove 1.07%   Myrcene Peppery, spicy balsam
0.81%   α-Humulene Woody, oceanic-watery, spicy clove 0.44%   α-Bisabolol Fruity, nutty, coconut
0.31%   Limonene Citrus, orange, sweet 0.29%   Valenence Sweet, citrus, grapefruit, woody, orange

Value in parenthesis indicates percentage of terpene present in the total sample (weight percentage, wt/wt%).
Value in doughnut slice indicates individual terpene abundance with respect to the total terpenes detected.

This sample has not been tested according to OAR 333-007. These results should therefore be used for research and development or quality control purposes only.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.
Joseph Rutowski Iron laboratories Joseph Rutowski

Tested by Iron Laboratories Oregon, 71 Centennial Loop Suite D Eugene, OR 97401

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