IRON Laboratories     PJLA

ISO/IEC 17025:2017 Accredited

Marihuana Potency Analysis by
High Performance Liquid Chromatography
Testing Accreditation #: 77802 *Test Certificate #: 122021-002
Client Name, Sample Details

David Cole
, MI
Sample: TEST 2/25
License: 1234567890ABCDEFG
Type: Flower
Method: FE04U12 HPLC-UV
Metrc Test Pkg#: DFBDFDFGDFG
Metrc Source Pkg#: 3544574576567845675
***Water Activity: 0.5
***Moisture: 30%
Test Conditions

Prepsheet ID#: DAVE TEST
Scale: XS205-MI1
Temp: 21.9 °C
Baro Pressure: 979.2 hPa
Analyst: MEH
Technician: MEH
Sample ID#: 122021

Lot #: ASDSDGRWREGWRE
Batch #: 123456
Batch Weight (g): 2
Harvest/Process Date: 03/10/2020
Serving Size (g): 10
Package Weight (g):4
Date Received: 03/10/2020
Test Date: 03/27/2020
Valid Through: 03/27/2021
Report Issued: 03/27/2020
Sample #122021
Test
Compounds		 Δ9-THC THCA Δ8-THC CBD CBDA CBG CBGA CBN CBC CBL THCV CBDV Total
Cannabinoids*		 Total THC Total CBD Calc Max Total
Cannabinoids*
Amount (%) 0.10 0.30 0.50 0.70 1.10 1.30 1.70 1.90 2.30 2.90 3.10 3.70 19.60 0.86 1.67 19.22
Amount (mg/g) 1.00 3.00 5.00 7.00 11.00 13.00 17 19.00 23.00 29.00 31.00 37.00 196 8.63 16.65 192.20
Amount per Serving (mg) 10 30 50 70 110 130 170 190 230 290 310 370 1,960.00 Serving Size~ (g): 10.00
LOQ (mg/g) 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1 0.1   %Decarb. THC CBD
±%RPD 32.56% 116.67% 37.84% 37.62% 9.52% 12.77% 46.15% 136.45% 135.48% 33.33% 141.46% 82.35% 25 39

test

LOQ = Limit of Quantitation; %RPD = Relative Percent Deviation; %RSD = Relative Standard Deviation; N/D = Not Detected

*Designates values that are not currently included in the accredited scope of Iron Laboratories.

*** Designates tests that use the method FE-45. FE-45 is performed using AOAC 966.02 and 32.004-32.009.

FE-45 has relative expanded (k=2) uncertainties of 1.098% for moisture, 1.754% for water activity for unprocessed plant materials, and 13.102% for water activity for infused products.

Vitamin E acetate analysis has a relative expanded (k=2) uncertainty of 18.614%.

Total THC and CBD is the calculated sum of Δ9-THC and Δ8-THC or CBD plus the amount of THC or CBD derived from THCA or CBDA, respectively.

These values are calculated by applying a molar correction factor of 0.877 to the THCA or the CBDA value.

Calc Max Total Cannabinoids is the sum of Total THC, Total CBD, CBN, Total CBG, CBC, THCV, CBDV, and CBL.

Total CBG is calculated as CBG plus CBGA*0.878 (the molar correction factor for CBGA to CBG conversion).

%Decarb. THC and CBD refer to the percentage of Δ9-THC or CBD relative to THCA or CBDA, respectively.

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Test Certificate No. 122021-002 supersedes Test Certificate No. 122021-001
MEH QM Iron laboratories MEH QM

Iron Laboratories, LLC is an ISO/IEC 17025:2017 Testing Laboratory laboratory accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

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IRON Laboratories     PJLA

ISO/IEC 17025:2017 Accredited

QC Report
Testing Accreditation #: 77802 *Test Certificate #: 122021-002
Client Name, Sample Details

David Cole
, MI
Sample: TEST 2/25
License: 1234567890ABCDEFG
Type: Flower
Method: FE04U12 HPLC-UV
Metrc Test Pkg#: DFBDFDFGDFG
Metrc Source Pkg#: 3544574576567845675
***Water Activity: 0.5
***Moisture: 30%
Test Conditions

Prepsheet ID#: DAVE TEST
Scale: XS205-MI1
Temp: 21.9 °C
Baro Pressure: 979.2 hPa
Analyst: MEH
Technician: MEH
Sample ID#: 122021

Lot #: ASDSDGRWREGWRE
Batch #: 123456
Batch Weight (g): 2
Harvest/Process Date: 03/10/2020
Serving Size (g): 10
Package Weight (g):4
Date Received: 03/10/2020
Test Date: 03/27/2020
Valid Through: 03/27/2021
Report Issued: 03/27/2020
Sample #122021
Target Compound Name Method Blank (μg/g) LCS Spike (μg/g) LCS Amount (μg/g) Percent Recovery (%) LCS LCS Duplicate Amount (μg/g) Percent Recovery (%) LCSD Relative Percent Difference (%) QC Flag
Δ9-THC 5 5 5 100.00 3.6 72.00 32.56% A
THCA 1 1 1 100.00 3.8 380.00 116.67% A
Δ8-THC 3 3 3 100.00 4.4 146.67 37.84% A
CBD 6 6 6 100.00 4.1 68.33 37.62% A
CBDA 3 3 3 100.00 3.3 110.00 9.52% A
CBG 5 5 5 100.00 4.4 88.00 12.77% A
CBGA 4 4 4 100.00 2.5 62.50 46.15% A
CBN 9 9 9 100.00 1.7 18.89 136.45% A
CBC 1 1 1 100.00 5.2 520.00 135.48% A
CBCA 1 1 1 100.00 4.5 450.00 127.27% A
CBL 2 2 2 100.00 2.8 140.00 33.33% A
THCV 7 7 7 100.00 1.2 17.14 141.46% A
CBDV 2.3 4 1.2 30.00 0.5 12.50 82.35% A

N.D. = Not Detected

LR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) Low recovery should be scrutinized for possible fail as it could indicate more compound present than is detected.

I = indicates that an amount of an interfering compound greater than the methods limit of detection was detected in the method blank sample. May indicate contamination of analytical system or consumables.

Q = indicates that the relative percent diference of two identicly prepared Matrix Spike samples for a target analyte was greater than 20%

HR = indicates compound recovery of matrix spike was outside the methods acceptable limits. (70-130%) high recoveries should be scrutinized for passing as more compound may be detected than is actually present in the sample.

Sample was sampled and tested in accordance with the Safety Compliance Facility Sampling and Testing Information.

This certificate shall not be reproduced except in full, without written approval of Iron Laboratories, LLC.

Test Certificate No. 122021-002 supersedes Test Certificate No. 122021-001
MEH QM Iron laboratories MEH QM

Iron Laboratories, LLC is an ISO/IEC 17025:2017 Testing Laboratory laboratory accredited by (PJLA) Perry Johnson Laboratory Accreditation, Certificate No. 77802

Tested by Iron Laboratories Michigan, 1825 E. West Maple Walled Lake, MI 48390

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